CN106900748A - A kind of plant vaccine of phosphorous worm prestige and nicotinic insecticide and preparation method thereof - Google Patents
A kind of plant vaccine of phosphorous worm prestige and nicotinic insecticide and preparation method thereof Download PDFInfo
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- CN106900748A CN106900748A CN201710150859.4A CN201710150859A CN106900748A CN 106900748 A CN106900748 A CN 106900748A CN 201710150859 A CN201710150859 A CN 201710150859A CN 106900748 A CN106900748 A CN 106900748A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing within the same carbon skeleton a carboxylic group or a thio analogue, or a derivative thereof, and a carbon atom having only two bonds to hetero atoms with at the most one bond to halogen, e.g. keto-carboxylic acids
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
- A01N41/04—Sulfonic acids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N51/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds having the sequences of atoms O—N—S, X—O—S, N—N—S, O—N—N or O-halogen, regardless of the number of bonds each atom has and with no atom of these sequences forming part of a heterocyclic ring
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
- A01N57/14—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing aromatic radicals
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Abstract
The invention discloses a kind of phosphorous worm prestige and the plant vaccine of nicotinic insecticide, including 1 ~ 10 part of phosphorus worm prestige, 1 ~ 10 part of nicotinic insecticide, 1 ~ 2 part of sodium lignin sulfonate, 0.2 ~ 1 part of galacturonic acid, 5 ~ 10 parts of sodium alginate, 1 ~ 2 part of wood oligose, 100 ~ 110 parts of 1 ~ 3 part of abscisic acid, 0.1 ~ 0.5 part of xanthans and water；Described nicotinic insecticide is imidacloprid, Acetamiprid, Diacloden, thiacloprid, MTI-446, Nitenpyram, clothianidin, paichongding or imidaclothiz；The plant vaccine of phosphorous worm prestige of the invention and sandworm toxin insecticide, can improve the immune system of crop, balance the nutrition of each side, make robust plant vibrant, so as to resist the attack and harm of pathogen and insect to crop, the quality and quality of crop are improved, reach the effect of increase harvest；The plant vaccine of phosphorous worm prestige of the invention and sandworm toxin insecticide, especially causing the pathogen of crop powdery mildew has stronger bactericidal effect, can well prevent and treat the powdery mildew of various crops.
Description
Technical field
The present invention relates to plant vaccine technical field, the plant epidemic disease of specifically a kind of phosphorous worm prestige and nicotinic insecticide
Seedling and preparation method thereof.
Background technology
Powdery mildew occurs at positions such as the leaf of crop, tender stem, anthocaulus, bud and petals, and the initial stage is that yellow green is irregularly small
Spot, edge is not obvious, and subsequent scab constantly expands, and white powder spot is born on surface, finally grows countless stains.Affected part becomes ash
Color, covers its surface in flakes, and blur margin is clear, in dirty white or light canescence.Leaf-shrinkage diminishes when aggrieved serious, and tender tip is turned round
Bent deformity, bud is not opened, and has a strong impact on the yield of crop, and conventional prevention and treatment method generally has selection disease-resistant variety, buying seedling
It is strict except strain of catching an illness when wooden, prevent pathogeny, or using with non-host flowers and trees crop rotation 2 to 3 years, reduce cause of disease, or to farmland, big
Canopy carries out strict sterilization, and above method operability is smaller, and simply the passive possibility for reducing viral communication, is not positive treatment
Disease, therefore effect on driving birds is not good, in order to reach the purpose of agricultural production and income, are badly in need of a kind of exploitativeness by force, and prevention effect is good, from
Improve the plant vaccine that crop immunity aspect is prevented and treated to powdery mildew.
The content of the invention
To solve the above problems, it is an object of the invention to provide a kind of phosphorous worm prestige and the plant vaccine of nicotinic insecticide
And preparation method thereof.
The present invention to achieve the above object, is achieved through the following technical solutions：
A kind of plant vaccine of phosphorous worm prestige and nicotinic insecticide, in parts by weight, including 1 ~ 10 part of phosphorus worm prestige, nicotinoids are killed
1 ~ 10 part of worm agent, 1 ~ 2 part of sodium lignin sulfonate, 0.2 ~ 1 part of galacturonic acid, 5 ~ 10 parts of sodium alginate, 1 ~ 2 part of wood oligose takes off
Fall 100 ~ 110 parts of 1 ~ 3 part of acid, 0.1 ~ 0.5 part of xanthans and water；Described nicotinic insecticide is imidacloprid, Acetamiprid, thiophene worm
Piperazine, thiacloprid, MTI-446, Nitenpyram, clothianidin, paichongding or imidaclothiz.
Preferred plant vaccine, also including 2 ~ 5 parts of 5 ~ 10 parts of lentinan and polyglutamic acid.
Preferred plant vaccine, in parts by weight, including 5 parts of phosphorus worm prestige, 5 parts of nicotinic insecticide, sodium lignin sulfonate
1.5 parts, 0.6 part of galacturonic acid, 8 parts of sodium alginate, 1.5 parts of wood oligose, 2 parts of abscisic acid, 0.4 part of xanthans, lentinan 8
105 parts of part, 4 parts of polyglutamic acid and water；Described nicotinic insecticide is imidacloprid.
Present invention additionally comprises phosphorous worm prestige and the preparation method of the plant vaccine of nicotinic insecticide, comprise the following steps：
1. in parts by weight, by 5 ~ 10 parts of sodium alginates, 1 ~ 10 part of phosphorus worm prestige and 1 ~ 10 part of nicotinic insecticide be added to 100 ~
In 110 parts of water, stirred 2 ~ 3 hours with the speed of 500r/min, stand 2 ~ 3 hours, then stir 1 ~ 2 with the speed of 300r/min
Hour obtains mixed liquor；Described nicotinic insecticide is imidacloprid, Acetamiprid, Diacloden, thiacloprid, MTI-446, alkene pyridine worm
Amine, clothianidin, paichongding or imidaclothiz；
2. by step, 1. gained mixed liquor is added dropwise in calcium chloride solution, step 1. gained mixing after instilling 30 ~ 45 minutes
Liquid forms Spherical pellets in calcium chloride solution, gained Spherical pellets clear water is rinsed well and obtains sphere matrix；The chlorine
The mass fraction for changing calcium solution is 20 ~ 25%；
3. in parts by weight, by 1 ~ 2 part of sodium lignin sulfonate, 0.2 ~ 1 part of galacturonic acid, 1 ~ 2 part of wood oligose, 1 ~ 3 part comes off
Acid and the mixing of 0.1 ~ 0.5 part of xanthans, are stirring evenly and then adding into step 2. in gained sphere matrix, obtain phosphorous worm prestige and cigarette
The plant vaccine of bases insecticide.
Preferred preparation method, comprises the following steps：(1) in parts by weight, by 5 ~ 10 parts of sodium alginates, 1 ~ 10 part of phosphorus worm
Prestige and 1 ~ 10 part of nicotinic insecticide are added in 100 ~ 110 parts of water, are stirred 2 ~ 3 hours with the speed of 500r/min, stand 2 ~ 3
Hour, mixed liquor is then obtained in 1 ~ 2 hour with the speed stirring of 300r/min；Described nicotinic insecticide is imidacloprid, pyridine
Worm amidine, Diacloden, thiacloprid, MTI-446, Nitenpyram, clothianidin, paichongding or imidaclothiz；
(2) by step, (1) gained mixed liquor is added dropwise in calcium chloride solution, step 1. gained mixing after instilling 30 ~ 45 minutes
Liquid forms Spherical pellets in calcium chloride solution, gained Spherical pellets clear water is rinsed well and obtains sphere matrix；The chlorine
The mass fraction for changing calcium solution is 20 ~ 25%；
(3) in parts by weight, by 1 ~ 2 part of sodium lignin sulfonate, 0.2 ~ 1 part of galacturonic acid, 1 ~ 2 part of wood oligose, 1 ~ 3 part comes off
Acid, 0.1 ~ 0.5 part of xanthans, 5 ~ 10 parts of lentinans and 2 ~ 5 parts of polyglutamic acid mixing, are stirring evenly and then adding into step (2) institute
Obtain in sphere matrix, obtain the plant vaccine of phosphorous worm prestige and nicotinic insecticide.
Further preferred preparation method, comprises the following steps：
(1), in parts by weight, by 8 parts of sodium alginates, 5 parts of phosphorus worm prestige and 5 parts of nicotinic insecticides are added in 105 parts of water, with
The speed of 500r/min is stirred 2.5 hours, stands 2.5 hours, is then mixed within 1.5 hours with the speed stirring of 300r/min
Liquid；Described nicotinic insecticide is imidacloprid；
(2) by step, (1) gained mixed liquor is added dropwise in calcium chloride solution, and 1. gained mixed liquor exists step after instilling 40 minutes
Spherical pellets are formed in calcium chloride solution, gained Spherical pellets clear water is rinsed well and is obtained sphere matrix；The calcium chloride
The mass fraction of solution is 20%；
(3) in parts by weight, by 1.5 parts of sodium lignin sulfonates, 0.6 part of galacturonic acid, 1.5 parts of wood oligoses, 2 parts of abscisic acids,
0.4 part of xanthans, 8 parts of lentinans and 4 parts of polyglutamic acid mixing, are stirring evenly and then adding into step (2) gained sphere matrix
In, obtain the plant vaccine of phosphorous worm prestige and nicotinic insecticide.
The present invention has advantages below compared to existing technology：
The plant vaccine of phosphorous worm prestige of the invention and sandworm toxin insecticide, can improve the immune system of crop, and balance is each
The nutrition of aspect, makes robust plant vibrant, so as to resist the attack and harm of pathogen and insect to crop, improves crop
Quality and quality, reach the effect of increase harvest；The plant vaccine of phosphorous worm prestige of the invention and sandworm toxin insecticide, especially
It causes the pathogen of crop powdery mildew to have stronger bactericidal effect, can well prevent and treat the powdery mildew of various crops.
The plant vaccine of phosphorous worm prestige of the invention and nicotinic insecticide, containing various natural polymerses, can
Directly for plant growth provides nutrition, promote crop root flourishing, strengthen crop leaf photosynthesis and crop disease-resistant, degeneration-resistant energy
Power, strong sprout, healthy tree increase yield, improving quality；Galacturonic acid, wood oligose and abscisic acid in plant vaccine of the invention
Deng produce the disease-resistant factors such as substantial amounts of biology enzyme, organic acid, alkaloid with the use of can activate, induce plant, stimulate crop
Growth, reaches the effect of increasing both production and income；
The active ingredient of the plant vaccine of phosphorous worm prestige of the invention and nicotinic insecticide, can by flora conduit transport to
All parts of a plant, has good prevention and treatment effect to fractilinea oryzae；Each component of the invention is used cooperatively,
Content is moderate, scientific and reasonable, can play a part of plant vaccine, it is adaptable to various crops and fruits and vegetables, can stimulate and make produce
The biological resistant factor of raw similar protective plant protecting agent, promotes its root growth, promotes cell elongation and division, increases yield, improves
Fruit development, improves the metabolism of plant, increases the anti-adversity of disease-resistant, insect-prevention；
Phosphorus worm prestige, nicotinic insecticide composition and marine alga in the plant vaccine of phosphorous worm prestige of the invention and nicotinic insecticide
Sour sodium is prepared into sphere matrix, it is ensured that phosphorus worm prestige and nicotinic insecticide can be well mixed with other compositions, without additionally making
Disperseed with other auxiliary agents, solubility is minimum in water and in organic solvent to solve phosphorus worm prestige and nicotinic insecticide,
It is difficult to be prepared into the problem of the formulations such as conventional missible oil, aqua and soluble concentrate；And after being sprayed on crop using the method
Medicine can be sustained on blade, long action time, good absorbing, and can persistently play drug effect plant growth is interim, play
Preferably prevent or treat the effect of powdery mildew.
Specific embodiment
Plant vaccine it is an object of the invention to provide a kind of phosphorous worm prestige and nicotinic insecticide and preparation method thereof, leads to
Cross following technical scheme realization：
A kind of plant vaccine of phosphorous worm prestige and nicotinic insecticide, in parts by weight, including 1 ~ 10 part of phosphorus worm prestige, nicotinoids are killed
1 ~ 10 part of worm agent, 1 ~ 2 part of sodium lignin sulfonate, 0.2 ~ 1 part of galacturonic acid, 5 ~ 10 parts of sodium alginate, 1 ~ 2 part of wood oligose takes off
Fall 100 ~ 110 parts of 1 ~ 3 part of acid, 0.1 ~ 0.5 part of xanthans and water；Described nicotinic insecticide is imidacloprid, Acetamiprid, thiophene worm
Piperazine, thiacloprid, MTI-446, Nitenpyram, clothianidin, paichongding or imidaclothiz.
Preferred plant vaccine, also including 2 ~ 5 parts of 5 ~ 10 parts of lentinan and polyglutamic acid.
Preferred plant vaccine, in parts by weight, including 5 parts of phosphorus worm prestige, 5 parts of nicotinic insecticide, sodium lignin sulfonate
1.5 parts, 0.6 part of galacturonic acid, 8 parts of sodium alginate, 1.5 parts of wood oligose, 2 parts of abscisic acid, 0.4 part of xanthans, lentinan 8
105 parts of part, 4 parts of polyglutamic acid and water；Described nicotinic insecticide is imidacloprid.
Present invention additionally comprises phosphorous worm prestige and the preparation method of the plant vaccine of nicotinic insecticide, comprise the following steps：
1. in parts by weight, by 5 ~ 10 parts of sodium alginates, 1 ~ 10 part of phosphorus worm prestige and 1 ~ 10 part of nicotinic insecticide be added to 100 ~
In 110 parts of water, stirred 2 ~ 3 hours with the speed of 500r/min, stand 2 ~ 3 hours, then stir 1 ~ 2 with the speed of 300r/min
Hour obtains mixed liquor；Described nicotinic insecticide is imidacloprid, Acetamiprid, Diacloden, thiacloprid, MTI-446, alkene pyridine worm
Amine, clothianidin, paichongding or imidaclothiz；
2. by step, 1. gained mixed liquor is added dropwise in calcium chloride solution, step 1. gained mixing after instilling 30 ~ 45 minutes
Liquid forms Spherical pellets in calcium chloride solution, gained Spherical pellets clear water is rinsed well and obtains sphere matrix；The chlorine
The mass fraction for changing calcium solution is 20 ~ 25%；
3. in parts by weight, by 1 ~ 2 part of sodium lignin sulfonate, 0.2 ~ 1 part of galacturonic acid, 1 ~ 2 part of wood oligose, 1 ~ 3 part comes off
Acid and the mixing of 0.1 ~ 0.5 part of xanthans, are stirring evenly and then adding into step 2. in gained sphere matrix, obtain phosphorous worm prestige and cigarette
The plant vaccine of bases insecticide.
Preferred preparation method, comprises the following steps：(1) in parts by weight, by 5 ~ 10 parts of sodium alginates, 1 ~ 10 part of phosphorus worm
Prestige and 1 ~ 10 part of nicotinic insecticide are added in 100 ~ 110 parts of water, are stirred 2 ~ 3 hours with the speed of 500r/min, stand 2 ~ 3
Hour, mixed liquor is then obtained in 1 ~ 2 hour with the speed stirring of 300r/min；Described nicotinic insecticide is imidacloprid, pyridine
Worm amidine, Diacloden, thiacloprid, MTI-446, Nitenpyram, clothianidin, paichongding or imidaclothiz；
(2) by step, (1) gained mixed liquor is added dropwise in calcium chloride solution, step 1. gained mixing after instilling 30 ~ 45 minutes
Liquid forms Spherical pellets in calcium chloride solution, gained Spherical pellets clear water is rinsed well and obtains sphere matrix；The chlorine
The mass fraction for changing calcium solution is 20 ~ 25%；
(3) in parts by weight, by 1 ~ 2 part of sodium lignin sulfonate, 0.2 ~ 1 part of galacturonic acid, 1 ~ 2 part of wood oligose, 1 ~ 3 part comes off
Acid, 0.1 ~ 0.5 part of xanthans, 5 ~ 10 parts of lentinans and 2 ~ 5 parts of polyglutamic acid mixing, are stirring evenly and then adding into step (2) institute
Obtain in sphere matrix, obtain the plant vaccine of phosphorous worm prestige and nicotinic insecticide.
Further preferred preparation method, comprises the following steps：
(1), in parts by weight, by 8 parts of sodium alginates, 5 parts of phosphorus worm prestige and 5 parts of nicotinic insecticides are added in 105 parts of water, with
The speed of 500r/min is stirred 2.5 hours, stands 2.5 hours, is then mixed within 1.5 hours with the speed stirring of 300r/min
Liquid；Described nicotinic insecticide is imidacloprid；
(2) by step, (1) gained mixed liquor is added dropwise in calcium chloride solution, and 1. gained mixed liquor exists step after instilling 40 minutes
Spherical pellets are formed in calcium chloride solution, gained Spherical pellets clear water is rinsed well and is obtained sphere matrix；The calcium chloride
The mass fraction of solution is 20%；
(3) in parts by weight, by 1.5 parts of sodium lignin sulfonates, 0.6 part of galacturonic acid, 1.5 parts of wood oligoses, 2 parts of abscisic acids,
0.4 part of xanthans, 8 parts of lentinans and 4 parts of polyglutamic acid mixing, are stirring evenly and then adding into step (2) gained sphere matrix
In, obtain the plant vaccine of phosphorous worm prestige and nicotinic insecticide.
Below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1
The plant vaccine of a kind of phosphorous worm prestige and nicotinic insecticide, including phosphorus worm prestige 1kg, Acetamiprid 1kg, sodium lignin sulfonate
1kg, galacturonic acid 0.2kg, sodium alginate 5kg, wood oligose 1kg, abscisic acid 1kg, xanthans 0.1kg and water 100kg.
Embodiment 2
The plant vaccine of a kind of phosphorous worm prestige and nicotinic insecticide, including phosphorus worm prestige 10kg, Diacloden 10kg, lignin sulfonic acid
Sodium 2kg, galacturonic acid 1kg, sodium alginate 10kg, wood oligose 2kg, abscisic acid 3kg, xanthans 0.5kg and water 110kg.
Embodiment 3
The plant vaccine of a kind of phosphorous worm prestige and nicotinic insecticide, including phosphorus worm prestige 7kg, thiacloprid 4kg, sodium lignin sulfonate
1.5kg, galacturonic acid 0.4kg, sodium alginate 6kg, wood oligose 1.4kg, abscisic acid 2.5kg, xanthans 0.2kg and water
102kg。
Embodiment 4
The plant vaccine of a kind of phosphorous worm prestige and nicotinic insecticide, including phosphorus worm prestige 1kg, MTI-446 10kg, lignin sulfonic acid
Sodium 2kg, galacturonic acid 0.2kg, sodium alginate 5kg, wood oligose 2kg, abscisic acid 1kg, xanthans 0.5kg, lentinan
10kg, polyglutamic acid 2kg and water 110kg.
Embodiment 5
The plant vaccine of a kind of phosphorous worm prestige and nicotinic insecticide, including phosphorus worm prestige 10kg, Nitenpyram 1kg, sulfomethylated lignin
Sour sodium 1kg, galacturonic acid 1kg, sodium alginate 10kg, wood oligose 1kg, abscisic acid 3kg, xanthans 0.1kg, water 100kg are fragrant
Mushroom polysaccharide 5kg and polyglutamic acid 5kg.
Embodiment 6
The plant vaccine of a kind of phosphorous worm prestige and nicotinic insecticide, including phosphorus worm prestige 5kg, imidacloprid 5kg, sodium lignin sulfonate
1.5kg, galacturonic acid 0.6kg, sodium alginate 8kg, wood oligose 1.5kg, abscisic acid 2kg, xanthans 0.4kg, lentinan
8kg, polyglutamic acid 4kg and water 105kg.
Embodiment 7
The preparation method of the plant vaccine of phosphorous worm prestige and nicotinic insecticide described in embodiment 1, comprises the following steps：
1. by 5kg sodium alginates, 1kg phosphorus worm prestige and 1kg Acetamiprids are added in 100kg water, and 2 are stirred with the speed of 500r/min
Hour, 2 hours are stood, mixed liquor is then obtained in 1 hour with the speed stirring of 300r/min；
2. by step, 1. gained mixed liquor is added dropwise in calcium chloride solution, and 1. gained mixed liquor exists step after instilling 30 minutes
Spherical pellets are formed in calcium chloride solution, gained Spherical pellets clear water is rinsed well and is obtained sphere matrix；The calcium chloride
The mass fraction of solution is 20%；Tested through particle diameter, the average grain diameter of sphere matrix is 315 μm；
3. by 1kg sodium lignin sulfonates, 0.2kg galacturonic acids, 1kg wood oligoses, 1kg abscisic acids and 0.1kg xanthans mix,
Be stirring evenly and then adding into step 2. gained sphere matrix in, obtain the plant vaccine of phosphorous worm prestige and nicotinic insecticide.
Equally, after the quality of each component in embodiment 2 ~ 3 is replaced, phosphorous worm prestige and nicotinic insecticide be can obtain
Plant vaccine.
Embodiment 8
The preparation method of the plant vaccine of the phosphorous worm prestige and nicotinic insecticide of embodiment 4, comprises the following steps：
(1) by 5kg sodium alginates, 1kg phosphorus worm prestige and 10kg MTI-446s are added in 110 parts of water, are stirred with the speed of 500r/min
3 hours, 3 hours are stood, mixed liquor is then obtained in 2 hours with the speed stirring of 300r/min；
(2) by step, (1) gained mixed liquor is added dropwise in calcium chloride solution, and 1. gained mixed liquor exists step after instilling 45 minutes
Spherical pellets are formed in calcium chloride solution, gained Spherical pellets clear water is rinsed well and is obtained sphere matrix；The calcium chloride
The mass fraction of solution is 25%；Tested through particle diameter, the average grain diameter of sphere matrix is 308 μm；
(3) by 2kg sodium lignin sulfonates, 0.2kg galacturonic acids, 2kg wood oligoses, 1kg abscisic acids, 0.5kg xanthans, 10kg
Lentinan and 2kg polyglutamic acids mix, and are stirring evenly and then adding into step (2) in gained sphere matrix, obtain phosphorous worm prestige and
The plant vaccine of nicotinic insecticide.
Equally, after the quality of each component in embodiment 5 is replaced, phosphorous worm prestige and nicotinic insecticide be can obtain
Plant vaccine.
Embodiment 9
The preparation method of the plant vaccine of the phosphorous worm prestige and nicotinic insecticide of embodiment 6, comprises the following steps：
(1) by 8kg sodium alginates, 5kg phosphorus worm prestige and 5kg imidacloprids are added in 105kg water, are stirred with the speed of 500r/min
2.5 hours, 2.5 hours are stood, mixed liquor is then obtained in 1.5 hours with the speed stirring of 300r/min；
(2) by step, (1) gained mixed liquor is added dropwise in calcium chloride solution, and 1. gained mixed liquor exists step after instilling 40 minutes
Spherical pellets are formed in calcium chloride solution, gained Spherical pellets clear water is rinsed well and is obtained sphere matrix；The calcium chloride
The mass fraction of solution is 20%；Tested through particle diameter, the average grain diameter of sphere matrix is 302 μm；
(3) by 1.5kg sodium lignin sulfonates, 0.6kg galacturonic acids, 1.5kg wood oligoses, 2kg abscisic acids, 0.4kg xanthans,
8kg lentinans and 4kg polyglutamic acids mix, and are stirring evenly and then adding into step (2) in gained sphere matrix, obtain phosphorous worm
The plant vaccine of prestige and nicotinic insecticide.
Treatment to muskmelon
Take and plant muskmelon in two pieces of adjacent farmland a plot and b plot, be managed collectively, wherein the muskmelon of a plot plantation
Carry out following treatment：The phosphorous worm prestige of the gained of 10g embodiments 1 and the plant vaccine of nicotinic insecticide are taken, plus 1kg water soaks sweet
Melon kind 12 hours, then carries out seeding and seedling raising, and sprayed once every 20 days after muskmelon enters bud stage, the dosage for using
For 10g converts 50kg water, other drugs are not used；B plot then conventionally carries out nursery plantation muskmelon, uses in the market
Foliar fertilizer and insecticide kill the insect on muskmelon, as a result as follows：
The muskmelon that b plot is cultivated, melon seedling height is uneven, and branches and leaves are sparse, and blade is small and thin, and cane and holder fine hair are sparse and irregular
Uneven, every rice shoot is beared fruit 2 ~ 3,3700 kilograms of per mu yield；And the muskmelon that a plot is planted using plant vaccine of the invention, it is whole
Individual growth period disease-free spot and insect pest；Robust plant is neat, and melon seedling is dense, vigorous, and blade is big and abundant, and cane and holder are fine and soft
Hair is uniform neat closely knit, and it is glossy that fruit is very large, and the later stage bears fruit also without lopsided muskmelon, and 5300 kilograms of per mu yield increases than conventional method
Produce 43.24%.
There is the plant of powdery mildew using the muskmelon that conventional method is planted in the later stage yielded positive results in b plot, although in time
Sprinkling medicine is treated, but its normal metabolism also receives interference, causes early ageing, and yield incurs loss, specifically
It is as follows using medicine and dosage：80% sulphur 400 extraordinarily 72% benzene thiophene cymoxanil, 600 times of sprayings even spray 2-3 times, 3-5 days 1 time.
Preventing and treating to powdery mildew of cucumber
Cucumber first grows small circular white powder shape mildew in later stage planting process in lower blade front or the back side, gradually expands,
It is thick close, join together soon, the whole blade of indivedual plant is covered with white powder, is diagnosed as powdery mildew of cucumber, uses the plant of embodiment 4
Thing vaccine is treated, and method is as follows：100g is watered 50 jin of sprayings, sprays within 3 days 1 time, and even spray 3 times, are found out by treatment results, disease
Feelings are substantially contained that the state of an illness of ill blade is not deepened, and the new blade for having powdery mildew do not occur, on cucumber yield influence not
Greatly.
Phosphorus worm prestige and nicotinic insecticide composition compounding use, can be directly used for preventing and treating the purposes of insect on crops,
The crops multiple kinds of crops such as including rice, corn, vegetables, cotton, tea tree, sugarcane, fruit tree；The insect includes same wing
The various pests of mesh, Lepidoptera, Diptera, Thysanoptera, Semiptera and coleoptera；
The synergy shown by two mixture of active principles can make the administration in one or both of these active components
While amount declines, it is ensured that good prevention effect.There is certain lasting effect more than expected effect after application, so that favorably
Insect is killed in quick, the death rate is improved.The reduction of active component amount of application, reduces the cost of agricultural producer, and drops
Low chemically reactive substance residual in the environment, mitigates environmental pressure, improves foodsafety.
The presence of cooperative effect between two kinds of active components is can determine that by means of Colby publicities：
P=A+B-AB/100；
Using Colby methods, by being primarily based on be administered alone two kinds of activity of component, the prediction activity P of mixture is calculated,
The presence of mutual zuhewu effects is cooperateed between to determine two kinds of active components.
In above-mentioned formula, A is that a kind of component being administered alone with amount of application x is lived with the biology that degree of preventing and treating percentage is represented
Property.B is the bioactivity that the second component applied with amount of application y is represented with degree of preventing and treating percentage.If their effect is strict
On see it is adduction, and in the absence of interaction, then the A that the formula is applied with amount of application x is with the B's applied with amount of application y
The expected bioactivity of mixture calculates P.If the effect of the mixture set up in experiment exists more than expected activity, P
Synergistic function.In order to the active component for applying Colby formula, mixture is administered alone and is administered in combination in testing.
It is below biology test example, the content displaying tested composition of the invention is prevented specific insect
Control effect.Prevention effect represents the suppression to pest development, including dead, the described suppression of insect, including causes insect to ingest
That measures substantially reduces.It will be understood by those skilled in the art that being not limited to these by the control of insect protection that the compound is provided
Species.
To evaluate the prevention effect to diamondback moth (Plutella xylostella), test unit has 12-14 days ages by interior
The small open container of radish plants is constituted.Using the inoculator with auger conveyor, test sheet is dispersed in via corn cob grits
About 50 newborn larvaes in unit infect it in advance.After being distributed in test unit, the larva moves on test plant
It is dynamic.
Test-compound and composition are prepared using the solution comprising nonionic surfactant.The compound of preparation and
Composition is by sprayer in each test unit applied on top 1mL liquid.To test in triplicate.Will prepare number testedization
After compound or composition spray, each test unit is dried 1 hour, black square is then placed on top.Make test sheet
Unit holding 6 days in the growth room of 25 DEG C and 70% relative humidity.Ingested leaf visual assessment plant is then based on to ingest damage
Evil.
Calculate the average value of result in triplicate and will calculate that the results are shown in Table 1.Phosphorus worm prestige is dense with 5.0mg/L
Degree is applied.Nicotine compound is applied with the dosage being shown in Table 1.
The prevention effect table of the phosphorus worm prestige of table 1 and nicotinic insecticide composition to diamondback moth
* desired value using Colby formula based on being calculated.
From the results shown in Table 1, the prevention effect of composition is more than desired value, may infer that composition has collaboration
Synergistic effect.
To evaluate the prevention effect to cabbage aphid (Brevicoryne brassicae), test unit has 12-14 by interior
The small open container of its age radish plants is constituted.Using the inoculator with auger conveyor, examination is dispersed in via corn cob grits
About 50 newborn larvaes in verification certificate unit infect it in advance.After being distributed in test unit, the larva is in test plant
Upper movement.
Test-compound and composition are prepared using the solution comprising nonionic surfactant.The compound of preparation and
Composition is by sprayer in each test unit applied on top 1mL liquid.To test in triplicate.Will prepare number testedization
After compound or composition spray, each test unit is dried 1 hour, black square is then placed on top.Make test sheet
Unit holding 6 days in the growth room of 25 DEG C and 70% relative humidity.Ingested leaf visual assessment plant is then based on to ingest damage
Evil.
Calculate the average value of result in triplicate and will calculate that the results are shown in Table 2.Phosphorus worm prestige is dense with 5.0mg/L
Degree is applied.Nicotine compound is applied with the dosage being shown in Table 2.
The prevention effect table of the phosphorus worm prestige of table 2 and nicotinic insecticide composition to cabbage aphid
* desired value using Colby formula based on being calculated.
From the results shown in Table 2, the prevention effect of composition is more than desired value, may infer that composition has collaboration
Synergistic effect.
Field test
To evaluate the prevention effect of phosphorus worm prestige and nicotine compound to cabbage aphid (Brevicoryne brassicae),
Cabbage aphid early period of origination, suspending agent is configured to by phosphorus worm prestige and nicotine compound, and liquid point is converted into by different dosages
Cell is uniformly sprayed on cabbage plant, drug effect is observed on time and is counted.Test of pesticide effectiveness result is as shown in table 3 below ~ 11.
The prevention effect table of the phosphorus worm prestige of table 3 and imidacloprid to cabbage aphid
| Treatment | Phosphorus worm prestige dosage | Imidacloprid dosage | Average disease refers to | Average preventive effect % |
| 1 | 1.0 grams/acre | 1.5 grams/acre | 1.65 | 78.32 |
| 2 | 1.5 grams/acre | 2.0 grams/acre | 1.71 | 80.65 |
| 3 | 2.0 grams/acre | 2.5 grams/acre | 1.52 | 85.69 |
| Phosphorus worm prestige suspending agent | 5.0 grams/acre | — | 5.69 | 52.03 |
| Imidacloprid suspending agent | — | 5.0 grams/acre | 7.05 | 48.69 |
| Blank | — | — | 9.58 | — |
The prevention effect table of the phosphorus worm prestige of table 4 and Acetamiprid to cabbage aphid
| Treatment | Phosphorus worm prestige dosage | Acetamiprid dosage | Average disease refers to | Average preventive effect % |
| 1 | 1.0 grams/acre | 1.5 grams/acre | 1.15 | 69.58 |
| 2 | 1.5 grams/acre | 2.0 grams/acre | 1.03 | 70.59 |
| 3 | 2.0 grams/acre | 2.5 grams/acre | 1.07 | 86.99 |
| Phosphorus worm prestige suspending agent | 5.0 grams/acre | — | 5.76 | 40.32 |
| Acetamiprid suspending agent | — | 5.0 grams/acre | 6.98 | 35.29 |
| Blank | — | — | 8.86 | - |
The prevention effect table of the phosphorus worm prestige of table 5 and Diacloden to cabbage aphid
| Treatment | Phosphorus worm prestige dosage | Diacloden dosage | Average disease refers to | Average preventive effect % |
| 1 | 1.0 grams/acre | 1.5 grams/acre | 1.08 | 83.21 |
| 2 | 1.5 grams/acre | 2.0 grams/acre | 1.15 | 86.71 |
| 3 | 2.0 grams/acre | 2.5 grams/acre | 1.03 | 88.53 |
| Phosphorus worm prestige suspending agent | 5.0 grams/acre | — | 6.77 | 50.25 |
| Diacloden suspending agent | — | 5.0 grams/acre | 5.69 | 48.69 |
| Blank | — | — | 9.81 | — |
The prevention effect table of the phosphorus worm prestige of table 6 and thiacloprid to cabbage aphid
| Treatment | Phosphorus worm prestige dosage | Thiacloprid dosage | Average disease refers to | Average preventive effect % |
| 1 | 1.0 grams/acre | 1.5 grams/acre | 1.02 | 86.74 |
| 2 | 1.5 grams/acre | 2.0 grams/acre | 1.14 | 88.53 |
| 3 | 2.0 grams/acre | 2.5 grams/acre | 1.03 | 87.69 |
| Phosphorus worm prestige suspending agent | 5.0 grams/acre | — | 6.07 | 46.25 |
| Thiacloprid suspending agent | — | 5.0 grams/acre | 7.21 | 38.28 |
| Blank | — | — | 9.59 | — |
The prevention effect table of the phosphorus worm prestige of table 7 and MTI-446 to cabbage aphid
| Treatment | Phosphorus worm prestige dosage | MTI-446 dosage | Average disease refers to | Average preventive effect % |
| 1 | 1.0 grams/acre | 1.5 grams/acre | 1.35 | 75.49 |
| 2 | 1.5 grams/acre | 2.0 grams/acre | 2.01 | 80.23 |
| 3 | 2.0 grams/acre | 2.5 grams/acre | 1.57 | 88.67 |
| Phosphorus worm prestige suspending agent | 5.0 grams/acre | — | 6.11 | 42.65 |
| MTI-446 suspending agent | — | 5.0 grams/acre | 6.97 | 30.21 |
| Blank | — | — | 9.65 | — |
The prevention effect table of the phosphorus worm prestige of table 8 and alkene pyridine worm to cabbage aphid
| Treatment | Phosphorus worm prestige dosage | Nitenpyram dosage | Average disease refers to | Average preventive effect % |
| 1 | 1.0 grams/acre | 1.5 grams/acre | 1.32 | 78.23 |
| 2 | 1.5 grams/acre | 2.0 grams/acre | 1.15 | 80.31 |
| 3 | 2.0 grams/acre | 2.5 grams/acre | 1.08 | 87.28 |
| Phosphorus worm prestige suspending agent | 5.0 grams/acre | — | 5.87 | 46.31 |
| Nitenpyram suspending agent | — | 5.0 grams/acre | 6.18 | 40.27 |
| Blank | — | — | 9.79 | — |
The prevention effect table of the phosphorus worm prestige of table 9 and clothianidin to cabbage aphid
| Treatment | Phosphorus worm prestige dosage | Clothianidin dosage | Average disease refers to | Average preventive effect % |
| 1 | 1.0 grams/acre | 1.5 grams/acre | 1.17 | 80.03 |
| 2 | 1.5 grams/acre | 2.0 grams/acre | 1.05 | 82.36 |
| 3 | 2.0 grams/acre | 2.5 grams/acre | 1.01 | 85.67 |
| Phosphorus worm prestige suspending agent | 5.0 grams/acre | — | 6.01 | 30.29 |
| Clothianidin suspending agent | — | 5.0 grams/acre | 7.16 | 35.78 |
| Blank | — | — | 8.97 | — |
The prevention effect table of the phosphorus worm prestige of table 10 and paichongding to cabbage aphid
| Treatment | Phosphorus worm prestige dosage | Paichongding dosage | Average disease refers to | Average preventive effect % |
| 1 | 1.0 grams/acre | 1.5 grams/acre | 1.31 | 79.67 |
| 2 | 1.5 grams/acre | 2.0 grams/acre | 1.07 | 83.31 |
| 3 | 2.0 grams/acre | 2.5 grams/acre | 1.03 | 86.21 |
| Phosphorus worm prestige suspending agent | 5.0 grams/acre | — | 6.52 | 35.77 |
| Paichongding suspending agent | — | 5.0 grams/acre | 7.14 | 25.87 |
| Blank | — | — | 9.31 | — |
The prevention effect table of the phosphorus worm prestige of table 11 and imidaclothiz to cabbage aphid
| Treatment | Phosphorus worm prestige dosage | Imidaclothiz dosage | Average disease refers to | Average preventive effect % |
| 1 | 1.0 grams/acre | 1.5 grams/acre | 1.15 | 70.69 |
| 2 | 1.5 grams/acre | 2.0 grams/acre | 1.07 | 78.97 |
| 3 | 2.0 grams/acre | 2.5 grams/acre | 1.13 | 85.63 |
| Phosphorus worm prestige suspending agent | 5.0 grams/acre | — | 6.07 | 40.21 |
| Imidaclothiz suspending agent | — | 5.0 grams/acre | 5.99 | 35.17 |
| Blank | — | — | 8.59 | — |
Phosphorus worm prestige and nicotinic insecticide are can be seen that from the data of field test, dosage is big when being administered alone, to wild cabbage
The preventive effect of aphid is also unsatisfactory, and after the two compounding, dosage declines at least 50%, but preventive effect is greatly improved.
Claims (6)
1. the plant vaccine of a kind of phosphorous worm prestige and nicotinic insecticide, it is characterised in that：In parts by weight, including phosphorus worm prestige 1 ~
10 parts, 1 ~ 10 part of nicotinic insecticide, 1 ~ 2 part of sodium lignin sulfonate, 0.2 ~ 1 part of galacturonic acid, 5 ~ 10 parts of sodium alginate, wood
100 ~ 110 parts of 1 ~ 2 part of oligosaccharides, 1 ~ 3 part of abscisic acid, 0.1 ~ 0.5 part of xanthans and water；Described nicotinic insecticide is pyrrole worm
Quinoline, Acetamiprid, Diacloden, thiacloprid, MTI-446, Nitenpyram, clothianidin, paichongding or imidaclothiz.
2. the plant vaccine of phosphorous worm prestige according to claim 1 and nicotinic insecticide, it is characterised in that：Also include perfume
2 ~ 5 parts of 5 ~ 10 parts of mushroom polysaccharide and polyglutamic acid.
3. the plant vaccine of phosphorous worm prestige according to claim 2 and nicotinic insecticide, it is characterised in that：With weight portion
Meter, including 5 parts of phosphorus worm prestige, 5 parts of nicotinic insecticide, 1.5 parts of sodium lignin sulfonate, 0.6 part of galacturonic acid, sodium alginate 8
105 parts of part, 1.5 parts of wood oligose, 2 parts of abscisic acid, 0.4 part of xanthans, 8 parts of lentinan, 4 parts of polyglutamic acid and water；Described
Nicotinic insecticide is imidacloprid.
4. phosphorous worm prestige and the preparation method of the plant vaccine of nicotinic insecticide described in claim 1, it is characterised in that：Bag
Include following steps：
1. in parts by weight, by 5 ~ 10 parts of sodium alginates, 1 ~ 10 part of phosphorus worm prestige and 1 ~ 10 part of nicotinic insecticide be added to 100 ~
In 110 parts of water, stirred 2 ~ 3 hours with the speed of 500r/min, stand 2 ~ 3 hours, then stir 1 ~ 2 with the speed of 300r/min
Hour obtains mixed liquor；Described nicotinic insecticide is imidacloprid, Acetamiprid, Diacloden, thiacloprid, MTI-446, alkene pyridine worm
Amine, clothianidin, paichongding or imidaclothiz；
2. by step, 1. gained mixed liquor is added dropwise in calcium chloride solution, step 1. gained mixing after instilling 30 ~ 45 minutes
Liquid forms Spherical pellets in calcium chloride solution, gained Spherical pellets clear water is rinsed well and obtains sphere matrix；The chlorine
The mass fraction for changing calcium solution is 20 ~ 25%；
3. in parts by weight, by 1 ~ 2 part of sodium lignin sulfonate, 0.2 ~ 1 part of galacturonic acid, 1 ~ 2 part of wood oligose, 1 ~ 3 part comes off
Acid and the mixing of 0.1 ~ 0.5 part of xanthans, are stirring evenly and then adding into step 2. in gained sphere matrix, obtain phosphorous worm prestige and cigarette
The plant vaccine of bases insecticide.
5. phosphorous worm prestige and the preparation method of the plant vaccine of nicotinic insecticide described in claim 2, it is characterised in that：Bag
Include following steps：
(1) in parts by weight, by 5 ~ 10 parts of sodium alginates, 1 ~ 10 part of phosphorus worm prestige and 1 ~ 10 part of nicotinic insecticide be added to 100 ~
In 110 parts of water, stirred 2 ~ 3 hours with the speed of 500r/min, stand 2 ~ 3 hours, then stir 1 ~ 2 with the speed of 300r/min
Hour obtains mixed liquor；Described nicotinic insecticide is imidacloprid, Acetamiprid, Diacloden, thiacloprid, MTI-446, alkene pyridine worm
Amine, clothianidin, paichongding or imidaclothiz；
(2) by step, (1) gained mixed liquor is added dropwise in calcium chloride solution, step 1. gained mixing after instilling 30 ~ 45 minutes
Liquid forms Spherical pellets in calcium chloride solution, gained Spherical pellets clear water is rinsed well and obtains sphere matrix；The chlorine
The mass fraction for changing calcium solution is 20 ~ 25%；
(3) in parts by weight, by 1 ~ 2 part of sodium lignin sulfonate, 0.2 ~ 1 part of galacturonic acid, 1 ~ 2 part of wood oligose, 1 ~ 3 part comes off
Acid, 0.1 ~ 0.5 part of xanthans, 5 ~ 10 parts of lentinans and 2 ~ 5 parts of polyglutamic acid mixing, are stirring evenly and then adding into step (2) institute
Obtain in sphere matrix, obtain the plant vaccine of phosphorous worm prestige and nicotinic insecticide.
6. the preparation method of the plant vaccine of phosphorous worm prestige according to claim 5 and nicotinic insecticide, its feature exists
In：Comprise the following steps：
(1), in parts by weight, by 8 parts of sodium alginates, 5 parts of phosphorus worm prestige and 5 parts of nicotinic insecticides are added in 105 parts of water, with
The speed of 500r/min is stirred 2.5 hours, stands 2.5 hours, is then mixed within 1.5 hours with the speed stirring of 300r/min
Liquid；Described nicotinic insecticide is imidacloprid；
(2) by step, (1) gained mixed liquor is added dropwise in calcium chloride solution, and 1. gained mixed liquor exists step after instilling 40 minutes
Spherical pellets are formed in calcium chloride solution, gained Spherical pellets clear water is rinsed well and is obtained sphere matrix；The calcium chloride
The mass fraction of solution is 20%；
(3) in parts by weight, by 1.5 parts of sodium lignin sulfonates, 0.6 part of galacturonic acid, 1.5 parts of wood oligoses, 2 parts of abscisic acids,
0.4 part of xanthans, 8 parts of lentinans and 4 parts of polyglutamic acid mixing, are stirring evenly and then adding into step (2) gained sphere matrix
In, obtain the plant vaccine of phosphorous worm prestige and nicotinic insecticide.
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Application publication date: 20170630 |