CN106881058A - A kind of full-automatic solid-liquid separation system and preparation method thereof - Google Patents
A kind of full-automatic solid-liquid separation system and preparation method thereof Download PDFInfo
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- CN106881058A CN106881058A CN201710221838.7A CN201710221838A CN106881058A CN 106881058 A CN106881058 A CN 106881058A CN 201710221838 A CN201710221838 A CN 201710221838A CN 106881058 A CN106881058 A CN 106881058A
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- retort
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- storage tank
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
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- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
The present invention relates to a kind of full-automatic separation of solid and liquid filtration system and its cleaning method,Clean pressure air system is connected by pipeline with the top of retort,Material/cleaning fluid carrys out liquid pipeline and extends to retort bottom,Retort bypass is provided with retort cleaning feed liquor stop valve,The branch road of coupled reaction tank rotating wash bowl is provided with retort liquid feed valve,The branch road of coupled reaction tank respirator is provided with retort upper end,Branch road is connected with retort interior room,Retort is connected with temporary storage tank,Retort bypass is connected at the A of position,Branch road is additionally provided with the A of position,The branch road of connection temporary storage tank rotating wash bowl is provided with temporary storage tank liquid feed valve,Retort bottom is provided with sieve plate,Retort and temporary pot bottom are equipped with bearing,Weight sensor is equipped with inside bearing,Temporary storage tank is connected by temporary storage tank liquid valve with membrane pump,Membrane pump is connected with filter.The present invention improves the efficiency of separation of solid and liquid, reduces labour intensity, it is to avoid pollution and cross pollution.
Description
Technical field
The present invention relates to a kind of full-automatic separation of solid and liquid filtration system and its cleaning method, belong to solid-liquid separation technique neck
Domain.
Background technology
Most domestic pharmaceutical production industry separation of solid and liquid is simple filter plant, it is impossible to realize that procedure is operated,
Separation of solid and liquid process are time-consuming more long after batch expands, and manual intervention operation stirring tapping or pressure filtration, automaticity are low,
Filter efficiency is low, pollution risk is big.Conventional separation of solid and liquid filter type can cause the blocking of retort sieve plate, it is difficult to process,
And extend activity time, influence the efficiency of whole production technology.
The content of the invention
Based on above-mentioned technical problem, the present invention provides a kind of full-automatic separation of solid and liquid filtration system and its cleaning method.This
Invention improves the efficiency of separation of solid and liquid, reduce labour intensity, it is to avoid pollution and cross pollution.Technical scheme
It is as follows：
A kind of full-automatic separation of solid and liquid filtration system, including retort, temporary storage tank, membrane pump and filter, clean compressed air
System is connected by pipeline with the top of retort, and pipeline is provided with retort clean compressed air intake valve, material/cleaning fluid
Come on liquid pipeline to be sequentially provided with dereaction pot valve, retort cleaning feed liquor stop valve and retort liquid feed valve, material/cleaning fluid comes
Liquid pipeline is extended to inside retort, is opened on retort bottom, is provided with by retort at retort cleaning feed liquor stop valve
Road, the original position of retort bypass is provided with bypass valve in retort, and the cleaning of coupled reaction tank is provided with retort liquid feed valve
The branch road of ball, the branch road of coupled reaction tank rotating wash bowl is provided with retort purge valve, and coupled reaction tank is provided with retort upper end
The branch road of respirator, branch road is connected with retort interior room, and the branch road of coupled reaction tank respirator is provided with retort pressure sensing
Device, the bottom of retort is provided with coupled reaction tank tank bottom liquid valve in the middle of retort sieve plate, sieve plate, and reaction pot bottom is provided with reaction
Tank bearing, is provided with weight sensor in retort bearing, the bottom of retort is connected by pipeline with temporary storage tank, coupled reaction tank
With retort tank bottom liquid valve is sequentially provided with the pipeline of temporary storage tank, temporary pot valve and temporary storage tank liquid feed valve, retort bypass is removed
By at the position A that bypass valve under retort is connected to retort tank bottom liquid valve and goes between temporary pot valve, being gone back at the A of position
The branch road that liquid/tapping valve is returned with retort CIP is provided with, the branch of connection temporary storage tank rotating wash bowl is provided with temporary storage tank liquid feed valve
Road, connection branch road is provided with temporary storage tank purge valve, and temporary pot bottom is provided with temporary storage tank bearing, weight is provided with inside temporary storage tank bearing
Sensor, temporary storage tank is connected by temporary storage tank liquid valve with membrane pump, and membrane pump is connected with filter, the drain pipe road of filter
It is provided with flow sensor.
On the basis of above-mentioned technical proposal, agitator is provided with the top of retort, agitator extends to retort sieve plate
Top；The agitator is helical form.
On the basis of above-mentioned technical proposal, the retort tank bottom liquid valve is the special dual-purpose tank bottom of Germany and Britain's separation of solid and liquid
Valve.
On the basis of above-mentioned technical proposal, reaction pot sidewall is provided with chuck, and water pipe is provided with chuck, anti-for controlling
Answer the temperature in tank；Chuck also is provided with temporary pot sidewall, for being incubated to temporary storage tank.
On the basis of above-mentioned technical proposal, the membrane pump is wildenP2 plastic corrosion-resisting pneumatic diaphragm pumps, described
Filter is Milllipore10 inches of 316L stainless steel filter.
On the basis of above-mentioned technical proposal, all valves are pneumatic diaphragm valve, and pneumatic diaphragm valve is by pneumatic diaphragm valve
Source of the gas control, the source of the gas of pneumatic diaphragm valve by central controller controls solenoid valve control；The weight sensor is by leading
Line is connected with central processing unit.
On the basis of above-mentioned technical proposal, shown filter is detachable filter.
The cleaning method of separation of solid and liquid filtration system of the present invention is as follows：
Detachable filter Manual-cleaning, the cleaning method of other systems structure is as follows：
Cleaning process point four-stage：
First stage opens dereaction pot valve, and retort cleaning feed liquor stop valve, retort liquid feed valve, retort tank bottom goes out liquid
Valve, retort CIP returns liquid/tapping valve, and retort input duct is cleaned according to setting time；
Second stage：After first stage terminates, other valves keep in situ and open retort purge valve, close retort feed liquor
Valve, according to setting time cleaning reaction tank；
Phase III：After second stage terminates, other valves keep in situ, close retort purge valve, retort cleaning feed liquor
Stop valve, retort tank bottom liquid valve and retort CIP return liquid/tapping valve, open bypass valve in retort, are bypassed under retort
Valve, removes temporary pot valve, temporary storage tank liquid feed valve and temporary storage tank liquid valve, according to setting time cleaning retort bypass and temporary storage tank
Water influent pipeline；
Fourth stage：After phase III terminates, other valves keep in situ, close temporary storage tank liquid feed valve, open temporary storage tank cleaning
Valve, according to setting time cleaning temporary tank and membrane pump, cleaning terminates.
The present invention has advantages below compared with prior art：
（1）The present invention is reacted by retort and terminates rear supernatant by retort bypass siphon to temporary storage tank, and remaining feed liquid is led to
Cross sieve plate to filter to temporary storage tank, rationally supernatant branch mode effectively increases the efficiency of separation of solid and liquid after control separation of solid and liquid,
Process time 40%-50% can effectively be shortened, the risk of pollution and cross pollution is reduced, personnel labor intensity and work work is reduced
When；
（2）The present invention coordinates membrane pump and temporary storage tank liquid feed valve, liquid valve, Comprehensive Control filter filtering behaviour by flow sensor
Make, reduce filter air inlet, the risk of filter core blocking, effectively shorten the process time；
（3）Present invention, avoiding the human error caused during clean operation, pollution and cross pollution are avoided, reduce behaviour
Make personnel labor intensity and man hour of labour；
（4）The present invention reduces the operation difficulty of technique, the differences between batches of feed liquid transfer time are reduced, it is ensured that downstream is expecting
Liquid is the normalization of the production technology of raw material, and improves the reliability of system checking, is met《GMP
（Revised edition in 2010）》Requirement.
Brief description of the drawings
Fig. 1 is schematic structural view of the invention.
Symbol description：
1- retort, 2- temporary storage tanks, 3- membrane pumps, 4- filters, 101- clean pressure air systems, 102 materials/cleaning fluid comes
Liquid pipeline, 103 retort bypass, bypass valve in 103-1- retort, bypass valve under 103-2- retort, 104- retort is clear
Wash ball, 105- retort feed liquors opening, 105-1 retort liquid feed valves, 106- retort respirators, 107- retort pressure sensings
Device, 108- retort sieve plates, 109- retort tank bottom liquid valves, 110- retort CIP returns liquid/tapping valve, and 111- retort is clear
Feed liquor stop valve is washed, 112- retort purge valves, 113- dereaction pot valves, 114- removes temporary pot valve, the clean pressure of 115- retort
Contracting air inlet valve, 116- agitators, 117- retort bearings, 118- positions A, 119- retort chuck, 120- water pipes, 201-
Temporary storage tank liquid feed valve, 202- temporary storage tank rotating wash bowls, 203- temporary storage tank respirators, 204- temporary storage tank liquid valves, 205- temporary storage tanks are clear
Wash valve, 206- temporary storage tank bearings, 207- temporary storage tank chucks, 401- flow sensors.
Specific embodiment
Further describe the present invention with reference to specific embodiment, advantages of the present invention and feature will be with description and
It is apparent.But embodiment is only exemplary, does not constitute any limitation to the scope of the present invention.Those skilled in the art should
It should be appreciated that, the details of technical solution of the present invention and form can be repaiied without departing from the spirit and scope of the invention
Change or replace, but these modifications and replacement are each fallen within protection scope of the present invention.
Embodiment 1
A kind of full-automatic separation of solid and liquid filtration system, as shown in figure 1, separating and filtering system includes retort 1, temporary storage tank 2, barrier film
Pump 3 and filter 4, clean pressure air system 101 are connected by pipeline with the top of retort 1, and pipeline is provided with retort
Clean compressed air intake valve 115, it is clear that material/cleaning fluid carrys out on liquid pipeline 102 to be sequentially provided with dereaction pot valve 113, retort
Feed liquor stop valve 111 and retort liquid feed valve 105-1 are washed, material/cleaning fluid carrys out liquid pipeline 102 and extends to inside retort 1, opens
Mouth 105 is provided with retort bypass 103, retort bypass 103 in the bottom of retort 1 at retort cleaning feed liquor stop valve 111
Original position be provided with bypass valve 103-1 in retort, coupled reaction tank rotating wash bowl is provided with retort liquid feed valve 105-1
104 branch road, the branch road of coupled reaction tank rotating wash bowl 104 is provided with retort purge valve 112, and company is provided with the upper end of retort 1
The branch road of retort respirator 106 is connect, branch road is connected with the interior room of retort 1, and the branch road of coupled reaction tank respirator 106 is provided with
Retort pressure sensor 107, the bottom of retort 1 is provided with retort sieve plate 108, the middle coupled reaction tank tank bottom of sieve plate 108
Liquid valve 109, the bottom of retort 1 is provided with retort bearing 117, retort bearing 117 and is provided with weight sensor, retort 1
Bottom be connected with temporary storage tank 2 by pipeline, retort tank bottom is sequentially provided with the pipeline of coupled reaction tank 1 and temporary storage tank 2 and is gone out
Liquid valve 109, temporary pot valve 114 and temporary storage tank liquid feed valve 201 are removed, retort bypass 103 is connected by bypass valve 103-2 under retort
At position A 118 between being connected on retort tank bottom liquid valve 109 and going to keep in pot valve 113, band is additionally provided with position A 118
There is retort CIP to return the branch road of liquid/tapping valve 110, connection temporary storage tank rotating wash bowl 202 is provided with temporary storage tank liquid feed valve 201
Branch road, connection branch road is provided with temporary storage tank purge valve 205, and the bottom of temporary storage tank 2 is provided with temporary storage tank bearing 206, temporary storage tank bearing 206
Inside is provided with weight sensor, and temporary storage tank 2 is connected by temporary storage tank liquid valve 204 with membrane pump 3, membrane pump 3 and detachable mistake
Filter 4 is connected, and the drain pipe road of detachable filter 4 is provided with flow sensor 401.
Embodiment 2
On the basis of embodiment 1, as shown in figure 1, the top of retort 1 is provided with helical stirrer 116, agitator 116 to
The top of retort sieve plate 108；The retort tank bottom liquid valve 109 is the special dual-purpose bottom valve of Germany and Britain's separation of solid and liquid；Reaction
Tank 1 is provided with chuck 119, chuck 119 and is provided with water pipe 120, and the side wall of temporary storage tank 2 is provided with chuck 207；The membrane pump is
WildenP2 plastic corrosion-resisting pneumatic diaphragm pumps, the filter is Milllipore10 inches of 316L stainless steel filter；Institute
There is valve to be pneumatic diaphragm valve, pneumatic diaphragm valve is controlled by the source of the gas of pneumatic diaphragm valve, and the source of the gas of pneumatic diaphragm valve is by center
The solenoid valve control of controller control；The weight sensor is connected by wire with central processing unit.
Embodiment 3
The cleaning procedure of solid-liquid separation system of the present invention：
Detachable filter Manual-cleaning, the cleaning procedure that other equipment is carried out：
Cleaning process point four-stage：
First stage opens dereaction pot valve 113, retort cleaning feed liquor stop valve 111, retort liquid feed valve 105-1, reaction
Tank tank bottom liquid valve 109 and retort CIP return liquid/tapping valve 110, and retort input duct is cleaned according to setting time；
Second stage：After first stage terminates, other valves keep in situ and open retort purge valve 112, close retort and enter
Liquid valve 105-1, according to setting time cleaning reaction tank；
Phase III：After second stage terminates, other valves keep in situ, close retort purge valve 112, retort clean into
Liquid stop valve 111, retort tank bottom liquid valve 109 and retort CIP return liquid/tapping valve 110, open bypass valve in retort
Bypass valve 103-2 under 103-1, retort, temporary pot valve 114, temporary storage tank liquid feed valve 201 and temporary storage tank liquid valve 204 are removed, according to
Setting time cleaning retort bypass and temporary storage tank water influent pipeline；
Fourth stage：After phase III terminates, other valves keep in situ, close temporary storage tank liquid feed valve 201, open temporary storage tank clear
Valve 205 is washed, according to setting time cleaning temporary tank and membrane pump 3.
Cleaning terminates.
Operation principle of the invention is as follows：
Open dereaction pot valve, retort cleaning feed liquor stop valve and retort liquid feed valve so that material is by material/cleaning fluid
Carry out liquid pipeline and enter retort, after solid-liquid two-phase is separated, two stages are divided into separation of solid and liquid process:
First stage bypasses out liquid：Open other on retort liquid feed valve 105-1, retort cleaning feed liquor stop valve 111, retort
Bypass valve 103-2 under road valve 103-1, retort, go temporary pot valve 114, temporary storage tank liquid feed valve 201 and the clean compression of retort empty
Gas intake valve 115, bypasses 103 and upper liquid is pressed into temporary storage tank 2 by Stress control by the reacted tank of feed liquid, is closed after stabilization anti-
Tank clean compressed air intake valve 115 is answered, upper liquid bypasses 103 and enters temporary storage tank 2, temporary storage tank 2 by siphon by retort
Temporary storage tank liquid valve 204 is opened after weight reaches setting value, and membrane pump 3 is opened, and feed liquid is transferred to next procedure through filter 4,
Temporary storage tank 2 is received after weight exceedes upper limit setting weight and closes temporary storage tank liquid feed valve 201, and rainbow cannot be continued when retort 1 is reached
The setting weight of suction；Valve Close All, membrane pump are closed, into the next step stage；
Second stage tank bottom goes out liquid：Open retort tank bottom liquid valve 109, remove temporary pot valve 114, temporary storage tank liquid feed valve 201, material
Liquid is by after the filtering of retort sieve plate 108, into temporary storage tank 2, the weight of temporary storage tank 2 reaches temporary storage tank liquid valve 204 after setting value
Open, membrane pump 3 is opened, feed liquid is transferred to next procedure through filter 4, temporary storage tank 2 receives weight and exceedes upper limit setting weight
Temporary storage tank liquid feed valve 201 is closed afterwards；
Separation of solid and liquid terminates after the completion of second stage.
The application of the invention of test example 1
Empirical tests, the production for being applied to Human Factor Ⅸ Complex of the invention can effectively improve the recycling number of times of gel,
Access times can be doubled, and be calculated according to annual 160 tons of feed liquids of absorption, and every 16 tons are changed once, are often inhaled after equipment optimization
Gel of attached 32 tons of replacings, can save the nearly 35000g of A-50, cost-effective about 900,000 yuan every year.
Claims (10)
1. a kind of full-automatic separation of solid and liquid filtration system, it is characterised in that separation of solid and liquid filtration system includes retort, temporary
Tank, membrane pump and filter, clean pressure air system are connected by pipeline with the top of retort, and pipeline is provided with retort
Clean compressed air intake valve, material/cleaning fluid comes on liquid pipeline to be sequentially provided with dereaction pot valve, retort cleaning feed liquor cut-off
Valve and retort liquid feed valve, material/cleaning fluid carry out liquid pipeline and extend to inside retort, are opened on retort bottom, in reaction
Retort bypass is provided with tank cleaning feed liquor stop valve, the original position of retort bypass is provided with bypass valve in retort, anti-
The branch road of the branch road that coupled reaction tank rotating wash bowl is provided with tank liquid feed valve, coupled reaction tank rotating wash bowl is answered to be provided with retort cleaning
Valve, the branch road of coupled reaction tank respirator is provided with retort upper end, and branch road is connected with retort interior room, the breathing of coupled reaction tank
The branch road of device is provided with retort pressure sensor, and the bottom of retort is provided with coupled reaction tank in the middle of retort sieve plate, sieve plate
Tank bottom liquid valve, reaction pot bottom is provided with retort bearing, and weight sensor is provided with retort bearing, and the bottom of retort leads to
Cross pipeline to be connected with temporary storage tank, retort tank bottom liquid valve is sequentially provided with the pipeline of coupled reaction tank and temporary storage tank, goes to keep in
Pot valve and temporary storage tank liquid feed valve, retort bypass are connected to retort tank bottom liquid valve and go to keep in by bypass valve under retort
At position A between pot valve, the branch road that liquid/tapping valve is returned with retort CIP is additionally provided with the A of position, in temporary storage tank feed liquor
The branch road of connection temporary storage tank rotating wash bowl is provided with valve, connection branch road is provided with temporary storage tank purge valve, and temporary pot bottom is provided with temporary
Tank bearing, is provided with weight sensor inside temporary storage tank bearing, temporary storage tank is connected by temporary storage tank liquid valve with membrane pump, membrane pump
It is connected with filter, the drain pipe road of filter is provided with flow sensor.
2. separation of solid and liquid filtration system according to claim 1, it is characterised in that agitator is provided with the top of retort,
Agitator extends to the top of retort sieve plate.
3. separation of solid and liquid filtration system according to claim 2, it is characterised in that the agitator is helical form.
4. separation of solid and liquid filtration system according to claim 1, it is characterised in that the retort tank bottom liquid valve is English
The special dual-purpose bottom valve of moral separation of solid and liquid.
5. separation of solid and liquid filtration system according to claim 1, it is characterised in that the reaction pot sidewall is provided with folder
Set, is provided with water pipe in chuck.
6. separation of solid and liquid filtration system according to claim 1, it is characterised in that folder also is provided with the temporary pot sidewall
Set.
7. separation of solid and liquid filtration system according to claim 1, it is characterised in that the membrane pump is wildenP2 plastics
Corrosion-resistant pneumatic diaphragm pump, the filter is Milllipore10 inches of 316L stainless steel filter.
8. separation of solid and liquid filtration system according to claim 1, it is characterised in that all valves are pneumatic diaphragm valve,
Pneumatic diaphragm valve is controlled by the source of the gas of pneumatic diaphragm valve, the source of the gas of pneumatic diaphragm valve by central controller controls magnetic valve control
System；The weight sensor is connected by wire with central processing unit.
9. separation of solid and liquid filtration system according to claim 1, it is characterised in that shown filter is detachable filtering
Device.
10. as described in claim any one of 1-9 separation of solid and liquid filtration system cleaning method, comprise the following steps that：
Detachable filter Manual-cleaning, the cleaning process point four-stage of other systems structure：
First stage opens dereaction pot valve, retort cleaning feed liquor stop valve, retort liquid feed valve, retort tank bottom liquid valve
Liquid/tapping valve is returned with retort CIP, retort input duct is cleaned according to setting time；
Second stage：After first stage terminates, other valves keep in situ and open retort purge valve, close retort feed liquor
Valve, according to setting time cleaning reaction tank；
Phase III：After second stage terminates, other valves keep in situ, close retort purge valve, retort cleaning feed liquor
Stop valve, retort tank bottom liquid valve and retort CIP return liquid/tapping valve, open and bypassed under bypass valve, retort in retort
Valve, temporary pot valve, temporary storage tank liquid feed valve and temporary storage tank liquid valve are removed, according to setting time cleaning retort bypass and temporary storage tank
Water influent pipeline；
Fourth stage：After phase III terminates, other valves keep in situ, close temporary storage tank liquid feed valve, open temporary storage tank cleaning
Valve, according to setting time cleaning temporary tank and membrane pump, cleaning terminates.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710221838.7A CN106881058B (en) | 2017-04-06 | 2017-04-06 | Full-automatic solid-liquid separation and filtration system and cleaning method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710221838.7A CN106881058B (en) | 2017-04-06 | 2017-04-06 | Full-automatic solid-liquid separation and filtration system and cleaning method thereof |
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| CN106881058B CN106881058B (en) | 2023-02-03 |
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| CN111093793A (en) * | 2017-08-03 | 2020-05-01 | 瑞普利金公司 | Method for actuating an alternating tangential flow diaphragm pump |
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