CN106831128A - A kind of medicament at florescence for extending the bletilla striata and preparation method thereof - Google Patents

A kind of medicament at florescence for extending the bletilla striata and preparation method thereof Download PDF

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Publication number
CN106831128A
CN106831128A CN201710059845.1A CN201710059845A CN106831128A CN 106831128 A CN106831128 A CN 106831128A CN 201710059845 A CN201710059845 A CN 201710059845A CN 106831128 A CN106831128 A CN 106831128A
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China
Prior art keywords
parts
medicament
bletilla striata
florescence
tealeaves
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CN201710059845.1A
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Chinese (zh)
Inventor
晏前海
龙娴郦
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Guizhou Province Wuling Yam Plant Bletilla Development Co Ltd
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Guizhou Province Wuling Yam Plant Bletilla Development Co Ltd
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Priority to CN201710059845.1A priority Critical patent/CN106831128A/en
Publication of CN106831128A publication Critical patent/CN106831128A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/36Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
    • A01N43/38Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/647Triazoles; Hydrogenated triazoles
    • A01N43/6531,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/42Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity

Abstract

The invention provides a kind of medicament at florescence for extending the bletilla striata and preparation method thereof, belong to flower cultivation field.The raw material of the medicament includes by weight:35 parts of 30 40 parts of grape pip, 25 35 parts of aloe, 22 30 parts of tealeaves, 10 15 parts of uniconazole P, 10 14 parts of urea, 38 parts of heteroauxin, 35 parts of NaHS, 12 parts of vitamin, 24 parts of edta salt and potassium dihydrogen phosphate.The cooperation that this medicament passes through grape pip and aloe and tealeaves, collaboration antioxidase removes the active oxygen that bletilla striata flowers produce in aging course, can be by the longer blooming period 14 18 days of the bletilla striata, and will not be to the generation poisoning of bletilla striata flowers.The preparation method includes extraction step and reactions steps, and the reaction condition of the method is gentle, and the solvent toxicity of selection is low, environmental protection;The property of medicine of the medicament for preparing simultaneously is good, and stability is strong, can be used in industrialized production.

Description

A kind of medicament at florescence for extending the bletilla striata and preparation method thereof
Technical field
The present invention relates to flower cultivation field, medicament and its preparation in particular to a kind of florescence for extending the bletilla striata Method.
Background technology
The bletilla striata, is a kind of herbaceos perennial of orchid family bletilla striata category, and its rhizome is used as medicine, with extensive medical value. Bletilla striata bitter, sweet, puckery, cold nature enters lung channel, has functions that tonifying lung, hemostasis, detumescence, myogenic, sore, is mainly used to treat Lung hinders the illnesss such as hemoptysis, bleeding from five sense organs or subcutaneous tissue, metal-inflicted wound bleeding, swollen ulcer drug, canker sores, soup fire burn, rhagadia manus et pedis.
Meanwhile, the flower that the flower of the bletilla striata has multiple color, such as the bletilla striata has aubergine, white, blueness, yellow and pink colour etc., Can be potted plant for indoor appreciation, can also intersperse in the flower stand or garden for more covering, with extensive Ornamental value.However, from The florescence of the bletilla striata under right growth conditions only has 1 month.With the raising and the increasing of international contacts of people's level of cultural life Plus, the demand to bletilla striata flowers constantly increases, and so cultivates the bletilla striata with conventional method, and it is much to supply flower by the natural florescence Inadequate.
At present, although also occur in that the medicament at the florescence of some extension flowers on the market, but due to bletilla striata flowers itself Particularity, makes it very sensitive to this kind of medicament on the market, is mainly manifested in using after these medicaments, and the flower fair of the bletilla striata is subject to Poisoning to a certain extent, accelerates withering for flower.
The content of the invention
The first object of the present invention is to provide a kind of medicament at the florescence for extending the bletilla striata, this medicament by grape pip and Aloe and the cooperation of tealeaves, cooperate with antioxidase to remove the active oxygen that the bletilla striata produces in aging course, can be by the flower of the bletilla striata Phase extends 14-18 days, and will not produce poisoning to bletilla striata plant.
The second object of the present invention is to provide a kind of preparation method of above-mentioned medicament, and the reaction condition of the method is gentle, The solvent toxicity of selection is low, environmental protection;The property of medicine of the medicament for preparing simultaneously is good, and stability is strong, can be used in industrialized production.
In order to realize above-mentioned purpose of the invention, spy uses following technical scheme:
A kind of medicament at the florescence for extending the bletilla striata, the raw material of the medicament includes by weight:Grape pip 30-40 parts, reed Luxuriant growth 25-35 parts, tealeaves 22-30 parts, uniconazole P 10-15 parts, urea 10-14 parts, heteroauxin 3-8 parts, NaHS 3-5 parts, Vitamin 1-2 parts, edta salt 2-4 parts and potassium dihydrogen phosphate 3-5 parts.
A kind of preparation method of the medicament at the florescence for extending the bletilla striata, comprises the following steps:
Grape pip, aloe and tealeaves are taken by weight, again with volume fraction for the alcoholic solution of 60-80% is mixed after being well mixed Close, heating and refluxing extraction twice, the extract solution obtained by merging, and crude extract powder will be obtained after extract solution concentrate drying;
Uniconazole P, edta salt, urea and heteroauxin are mixed with water, and it is small in heating stirring 2-3 at 60-70 DEG C When, then mix with crude extract powder, NaHS, vitamin and potassium dihydrogen phosphate again, then be 5- with organic acid for adjusting pH value 6。
Compared with prior art, beneficial effects of the present invention are:
This medicament with grape pip, aloe and tealeaves these three natural plants as primary raw material, wherein, by grape pip and Mutual cooperation between tealeaves, the effect with Synergistic can promote the nutrient accumulation and mineral matter in bletilla striata flowers body Transport.Meanwhile, by grape pip and tealeaves and the cooperation of aloe, free radical can be removed, collaboration antioxidase removes the bletilla striata The active oxygen that flowers produce in aging course, it is to avoid the too early apoptosis of cell of bletilla striata flowers, so as to delay declining for bletilla striata flowers Old process, extends the florescence of the bletilla striata.
Meanwhile, also containing this plant growth regulators of uniconazole P in this medicament, and in this plant of heteroauxin The Endogenous auxin of generally existing, with the cell metabolization rate of the regulation bletilla striata flowers of further concertedness.Using this medicine Agent is applied on the bletilla striata bud that will be bloomed or is directly applied on the petal of the bletilla striata, can be by the longer blooming period of the bletilla striata 14-18 days, and poisoning will not be produced to bletilla striata flowers.
In the preparation method of this medicament, can be by the work in grape pip, aloe and tealeaves using heating and refluxing extraction method Property material extract, and alcoholic solution with volume fraction as 60-80% is as Extraction solvent, improves the dissolution rate of active material. The materials such as uniconazole P, heteroauxin can be complexed with edta salt, and the crude extract powder of medicinal material then is dissolved in into above-mentioned reaction again In liquid, the solution of clear is formed, so as to improve the drug effect and stability of medicament.Additionally, the reaction condition of the method is gentle, The solvent toxicity of selection is low, environmental protection, is conducive to industrialized production.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the present invention.It is unreceipted specific in embodiment Condition person, the condition advised according to normal condition or manufacturer is carried out.Agents useful for same or the unreceipted production firm person of instrument, are The conventional products that can be obtained by commercially available purchase.
Present embodiment provides a kind of medicament at the florescence for extending the bletilla striata, and the raw material of the medicament includes by weight:Portugal 30-40 parts of grape seed, aloe 25-35 parts, tealeaves 22-30 parts, uniconazole P 10-15 parts, urea 10-14 parts, heteroauxin 3-8 parts, NaHS 3-5 parts, vitamin 1-2 parts, edta salt 2-4 parts and potassium dihydrogen phosphate 3-5 parts.
The OPC contained in grape pip is a kind of efficient free radical scavenger, and the oxidative function of its Green Tea Extract is Ascorbic 20 times, be 50 times of vitamin E, can remove free radical poisonous in plant cell, protection bletilla striata tissue exempt from by The oxidative damage of free radical, so as to extend the florescence of the bletilla striata.
Contain various anthraquinone analog compounds, such as aloe-emodin and aloin etc., these anthraquinone analog compounds in aloe Chemical constitution in contain phenolic hydroxyl group, to O2There is very strong Scavenging activity with OH.
Various catechin compounds, caffeine and mineral matter are rich in tealeaves, with efficient anti-oxidation function, can Effectively suppress the activity of free radical, improve the defence capability of plant tissue, and the nutrient accumulation in plant tissue can be promoted.
This medicament with grape pip, aloe and tealeaves these three natural plants as primary raw material, wherein, by grape pip and Mutual cooperation between tealeaves, the effect with Synergistic can promote the nutrient accumulation and mineral matter in bletilla striata flowers body Transport.Meanwhile, by grape pip and tealeaves and the cooperation of aloe, free radical can be removed, collaboration antioxidase removes the bletilla striata The active oxygen that flowers produce in aging course, it is to avoid the too early apoptosis of cell of bletilla striata flowers, so as to delay declining for bletilla striata flowers Old process, extends the florescence of the bletilla striata.
Meanwhile, also containing this plant growth regulators of uniconazole P in this medicament, uniconazole P has sterilized effect, is Gibberellin class synthetic inhibitor, with control cell elongation, promotes the effect of resistance, can promote the bud differentiation of the bletilla striata, It is bloomed more.The Endogenous auxin of generally existing, white with the regulation of further concertedness in this plant of heteroauxin The cell metabolization rate of splendid achnatherum flowers.
Using this pharmacy application on the bletilla striata bud that will be bloomed or being directly applied on the petal of the bletilla striata, can By longer blooming period 14-18 days of the bletilla striata, and poisoning will not be produced to bletilla striata flowers.
In preferred embodiments of the present invention, count by weight, above-mentioned grape pip is 32-38 parts, and aloe is 28-32 Part, tealeaves is 24-28 parts, and uniconazole P is 12-14 parts, and urea is 12-14 parts, and heteroauxin is 4-6 parts, and NaHS is 4-5 Part, vitamin is 1-2 parts, and edta salt is 2-3 parts, and potassium dihydrogen phosphate is 4-5 parts.Further it is optimized for:35 parts of grape pip, reed 30 parts of luxuriant growth, 26 parts of tealeaves, 13 parts of uniconazole P, 13 parts of urea, 5 parts of heteroauxin, 4 parts of NaHS, 1.5 parts of vitamin, EDTA 4 parts of 3 parts of salt and potassium dihydrogen phosphate.
By optimizing the consumption of each raw material, the drug effect of the medicament can be strengthened, make the effect at its extension bletilla striata florescence more Significantly.
In preferred embodiments of the present invention, above-mentioned raw materials also include the fleece-flower root, sealwort, akebi and climbing groundsel.Further Preferably, the above-mentioned fleece-flower root is 10-15 parts, and sealwort is 10-15 parts, akebi 6-10 parts and climbing groundsel is 6-10 parts.
The fleece-flower root and sealwort are respectively provided with anti-oxidant, anti-aging effect, can cooperate with grape pip, aloe in the medicament With effect of tealeaves this three removing free radical.Akebi and climbing groundsel are respectively provided with very strong antibacterial to various bacteria and fungi and make With addition akebi and the climbing groundsel in the medicament, it is possible to increase the antibacterial activity of the medicament.
In preferred embodiments of the present invention, said vitamin is vitamin C and vitamin E.Vitamin C is a kind of generally acknowledged Antioxidant, be the important vitamin of a class in plant, the oxidation of plant tissue can be avoided to be damaged, while can also help plant Thing resistance arid, ozone and uv damage.Vitamin E, i.e. tocopherol, are the important composition composition on cell membrane, are also thin Primary anti-oxidant on after birth.Vitamin E is the antioxidant of polyenoic fatty acid, on cell membrane with the multivalence of membrane phospholipid not Saturated fatty acid is combined into compound and the structure of stabilization film, prevents on biomembrane sulfur-bearing in polyvalent unsaturated fatty acid and cell The enzyme of base is damaged by oxidant.Therefore, when the vitamin in the medicament is vitamin C and vitamin E, antioxidation is more By force, the extension effect to the florescence of the bletilla striata is more notable.
In preferred embodiments of the present invention, above-mentioned edta salt is selected from EDTA-K2, EDTA-K3 and EDTA-Na2 Any one.EDTA-K2 and EDTA-K3 are the sylvite of EDTA, and EDTA-Na2 is the disodium salt of EDTA, and these three salt are all It is conventional complexing agent.The complexing degree of the materials such as preferably EDTA-Na2, EDTA-Na2 and uniconazole P is high, is favorably improved this The stability of medicament.
Present embodiment also provides a kind of preparation method of above-mentioned medicament, comprises the following steps:
(1) extraction step:Take grape pip, aloe and tealeaves by weight, be well mixed after again with volume fraction be 60- 80% alcoholic solution mixing, heating and refluxing extraction twice, the extract solution obtained by merging, and will obtain thick after extract solution concentrate drying Extract powder.
In this preparation method, can be by the active material in grape pip, aloe and tealeaves using heating and refluxing extraction method Extract, and with the alcoholic solution of 60-80% as Extraction solvent, preferably 70% alcoholic solution improves the dissolution of active material Rate.
In preferred embodiments of the present invention, above-mentioned alcoholic solution is ethanol solution, and the volume of alcoholic solution is grape pip, aloe With 3-5 times of tealeaves three's gross mass, preferably 4 times.Using ethanol solution, toxicity is low, and the pollution to environment is small.Alcoholic solution Volume is 3-5 times of grape pip, aloe and tealeaves three's gross mass, it is possible to increase the dissolution rate of effective active composition, so as to carry The content of the active component in crude extract powder high.
In preferred embodiments of the present invention, the temperature of above-mentioned heating and refluxing extraction is 70-80 DEG C, preferably 75 DEG C;Plus The extraction time of circumfluence distillation is 2-3h, preferably 2.5h.These three medicinal materials are carried out under these conditions be heated to reflux carrying Take, be conducive to improving the dissolution rate of effective active composition in medicinal material.
(2) reactions steps:Uniconazole P, edta salt, urea and heteroauxin are mixed with water, and at 60-70 DEG C plus Thermal agitation 2-3 hours, heating stirring 2.5 hours preferably at 65 DEG C;Then given birth to crude extract powder, NaHS, dimension again Element and potassium dihydrogen phosphate mixing, then be 5-6 with organic acid for adjusting pH value.
The materials such as uniconazole P, heteroauxin can be complexed with edta salt, then again be dissolved in the crude extract powder of medicinal material In above-mentioned reaction solution, the solution of clear is formed, so as to improve the drug effect and stability of medicament.
In preferred embodiments of the present invention, above-mentioned organic acid is tartaric acid and/or citric acid.Tartaric acid and citric acid It is acid moderate, the pH value of medicament will not be allowed to produce larger fluctuation, and covalent bond will not occur with the active ingredient in medicament.
Additionally, the reaction condition of the preparation method is gentle, the solvent toxicity of selection is low, environmental protection, is conducive to industrialization Production.
Feature of the invention and performance are described in further detail with reference to embodiments:
Embodiment 1
The present embodiment provides a kind of medicament at the florescence for extending the bletilla striata, and the raw material of this medicament includes by weight:
30 parts of grape pip, 35 parts of aloe, 30 parts of tealeaves, 15 parts of uniconazole P, 10 parts of urea, 8 parts of heteroauxin, NaHS 3 parts of 5 parts, 2 parts of vitamin, 4 parts of EDTA-Na2 and potassium dihydrogen phosphate.
The preparation method of this medicament is comprised the following steps:
(1) grape pip, aloe and tealeaves are taken by weight, are again 60% methanol solution with volume fraction after being well mixed Mixing, wherein, the volume of methanol solution is 5 times of grape pip, aloe and tealeaves three's gross mass.Heating and refluxing extraction twice, Extract solution obtained by merging, and crude extract powder will be obtained after extract solution concentrate drying.
(2) uniconazole P, edta salt, urea and heteroauxin are mixed with water, and in heating stirring 2 hours at 70 DEG C, Then mix with crude extract powder, NaHS, vitamin and potassium dihydrogen phosphate again, then be 5 with winestone acid for adjusting pH value.
Embodiment 2
The present embodiment provides a kind of medicament at the florescence for extending the bletilla striata, and the raw material of this medicament includes by weight:
32 parts of grape pip, 32 parts of aloe, 28 parts of tealeaves, 12 parts of uniconazole P, 12 parts of urea, 4 parts of heteroauxin, NaHS 5 parts of 5 parts, 2 parts of vitamin, 3 parts of EDTA-Na2 and potassium dihydrogen phosphate.
The preparation method of this medicament is comprised the following steps:
(1) grape pip, aloe and tealeaves are taken by weight, are again 80% ethanol solution with volume fraction after being well mixed Mixing, wherein, the volume of ethanol solution is 3 times of grape pip, aloe and tealeaves three's gross mass.Heating and refluxing extraction twice, Extract solution obtained by merging, and crude extract powder will be obtained after extract solution concentrate drying.
(2) uniconazole P, edta salt, urea and heteroauxin are mixed with water, and in heating stirring 3 hours at 60 DEG C, Then mix with crude extract powder, NaHS, vitamin and potassium dihydrogen phosphate again, then be 6 with lemon acid for adjusting pH value.
Embodiment 3
The present embodiment provides a kind of medicament at the florescence for extending the bletilla striata, the raw material of this medicament to be included by weight:
35 parts of grape pip, 30 parts of aloe, 26 parts of tealeaves, 13 parts of uniconazole P, 13 parts of urea, 5 parts of heteroauxin, NaHS 4 parts of 4 parts, 1.5 parts of vitamin, 3 parts of EDTA-Na2 and potassium dihydrogen phosphate.
The preparation method of this medicament is comprised the following steps:
(1) grape pip, aloe and tealeaves are taken by weight, are again 70% ethanol solution with volume fraction after being well mixed Mixing, wherein, the volume of ethanol solution is 4 times of grape pip, aloe and tealeaves three's gross mass.Heating and refluxing extraction twice, Temperature when extracting every time is 75 DEG C, and extraction time is 2.5 hours.Extract solution obtained by merging, and by extract solution concentrate drying After obtain crude extract powder.
(2) uniconazole P, edta salt, urea and heteroauxin are mixed with water, and it is small in heating stirring 2.5 at 65 DEG C When, then mix with crude extract powder, NaHS, vitamin and potassium dihydrogen phosphate again, then be 6 with winestone acid for adjusting pH value.
Embodiment 4
The present embodiment provides a kind of medicament at the florescence for extending the bletilla striata, and the raw material of this medicament includes by weight:
38 parts of grape pip, 28 parts of aloe, 24 parts of tealeaves, 14 parts of uniconazole P, 14 parts of urea, 6 parts of heteroauxin, NaHS 4 parts of 4 parts, 1 part of vitamin, 2 parts of EDTA-Na2 and potassium dihydrogen phosphate.
The preparation method of this medicament is comprised the following steps:
(1) grape pip, aloe and tealeaves are taken by weight, are again 70% ethanol solution with volume fraction after being well mixed Mixing, wherein, the volume of ethanol solution is 4 times of grape pip, aloe and tealeaves three's gross mass.Heating and refluxing extraction twice, Temperature when extracting every time is 70 DEG C, and extraction time is 3 hours.Extract solution obtained by merging, and by after extract solution concentrate drying Obtain crude extract powder.
(2) uniconazole P, edta salt, urea and heteroauxin are mixed with water, and it is small in heating stirring 2.5 at 65 DEG C When, then mix with crude extract powder, NaHS, vitamin and potassium dihydrogen phosphate again, then be 5 with winestone acid for adjusting pH value.
Embodiment 5
The present embodiment provides a kind of medicament at the florescence for extending the bletilla striata, and the raw material of this medicament includes by weight:
30 parts of grape pip, 25 parts of aloe, 22 parts of tealeaves, 10 parts of uniconazole P, 14 parts of urea, 3 parts of heteroauxin, NaHS 5 parts of 3 parts, 1 part of vitamin, 2 parts of EDTA-Na2 and potassium dihydrogen phosphate.
The preparation method of this medicament is consistent with embodiment 3.
The preparation method of this medicament is comprised the following steps:
(1) grape pip, aloe and tealeaves are taken by weight, are again 70% ethanol solution with volume fraction after being well mixed Mixing, wherein, the volume of ethanol solution is 4 times of grape pip, aloe and tealeaves three's gross mass.Heating and refluxing extraction twice, Temperature when extracting every time is 80 DEG C, and extraction time is 2 hours.Extract solution obtained by merging, and by after extract solution concentrate drying Obtain crude extract powder.
(2) uniconazole P, edta salt, urea and heteroauxin are mixed with water, and it is small in heating stirring 2.5 at 65 DEG C When, then mix with crude extract powder, NaHS, vitamin and potassium dihydrogen phosphate again, then be 6 with winestone acid for adjusting pH value.
Embodiment 6
The present embodiment provides a kind of medicament at the florescence for extending the bletilla striata, and the raw material of this medicament includes by weight:
35 parts of grape pip, 30 parts of aloe, 26 parts of tealeaves, 13 parts of uniconazole P, 13 parts of urea, 5 parts of heteroauxin, NaHS 4 parts, 1.5 parts of vitamin, 3 parts of EDTA-Na2,4 parts of potassium dihydrogen phosphate, 13 parts of the fleece-flower root, 12 parts of sealwort, 8 parts of akebi and thousand In 7 parts of light.
The preparation method of this medicament is comprised the following steps:
(1) grape pip, aloe, tealeaves, the fleece-flower root, sealwort, akebi and climbing groundsel are taken by weight, be well mixed after again with Volume fraction is 70% ethanol solution mixing, wherein, the volume of ethanol solution is 4 times of above-mentioned medicinal material gross mass.Heat back Stream is extracted twice, and temperature when extracting every time is 75 DEG C, and extraction time is 2.5 hours.Extract solution obtained by merging, and will extract Crude extract powder is obtained after liquid concentrate drying.
(2) uniconazole P, edta salt, urea and heteroauxin are mixed with water, and it is small in heating stirring 2.5 at 65 DEG C When, then mix with crude extract powder, NaHS, vitamin and potassium dihydrogen phosphate again, then be 6 with winestone acid for adjusting pH value.
Embodiment 7
The present embodiment provides a kind of medicament at the florescence for extending the bletilla striata, and the raw material of this medicament includes by weight:
35 parts of grape pip, 30 parts of aloe, 26 parts of tealeaves, 13 parts of uniconazole P, 13 parts of urea, 5 parts of heteroauxin, NaHS 4 parts, 1.5 parts of vitamin, 3 parts of EDTA-K3,4 parts of potassium dihydrogen phosphate, 10 parts of the fleece-flower root, 15 parts of sealwort, 10 parts of akebi and thousand In 6 parts of light.
The preparation method of this medicament is consistent with embodiment 6.
Embodiment 8
The present embodiment provides a kind of medicament at the florescence for extending the bletilla striata, and the raw material of this medicament includes by weight:
35 parts of grape pip, 30 parts of aloe, 26 parts of tealeaves, 13 parts of uniconazole P, 13 parts of urea, 5 parts of heteroauxin, NaHS 4 parts, 1.5 parts of vitamin, 3 parts of EDTA-K2,4 parts of potassium dihydrogen phosphate, 15 parts of the fleece-flower root, 10 parts of sealwort, 6 parts of akebi and a thousand li 10 parts of light.
The preparation method of this medicament is consistent with embodiment 6.
Comparative example 1
This comparative example provides a kind of medicament, and the raw material of this medicament includes by weight:
13 parts of uniconazole P, 13 parts of urea, 5 parts of heteroauxin, 4 parts of NaHS, 1.5 parts of vitamin, EDTA-Na2 3 4 parts of part and potassium dihydrogen phosphate.
The preparation method of this medicament is:
Uniconazole P, edta salt, urea and heteroauxin are mixed with water, and in heating stirring 2.5 hours at 65 DEG C, Then mix with NaHS, vitamin and potassium dihydrogen phosphate again, then be 6 with winestone acid for adjusting pH value.
Comparative example 2
This comparative example provides a kind of medicament, and the raw material of this medicament includes by weight:
35 parts of grape pip, 30 parts of aloe, 13 parts of uniconazole P, 13 parts of urea, 5 parts of heteroauxin, 4 parts of NaHS, dimension life 1.5 parts of element, 3 parts of EDTA-K2,4 parts of potassium dihydrogen phosphate.
The preparation method of this medicament is comprised the following steps:
(1) grape pip and aloe are taken by weight, are again that 70% ethanol solution mixes with volume fraction after being well mixed, Wherein, the volume of ethanol solution is 4 times of grape pip and aloe gross mass.Heating and refluxing extraction twice, every time extract when temperature It is 75 DEG C to spend, and extraction time is 2.5 hours.Extract solution obtained by merging, and crude extract powder will be obtained after extract solution concentrate drying End.
(2) uniconazole P, edta salt, urea and heteroauxin are mixed with water, and it is small in heating stirring 2.5 at 65 DEG C When, then mix with crude extract powder, NaHS, vitamin and potassium dihydrogen phosphate again, then be 6 with winestone acid for adjusting pH value.
Experimental example
Effect with reference to field control effectiveness test to medicament provided in an embodiment of the present invention in terms of the florescence of the extension bletilla striata Fruit is evaluated.
The growing way identical bletilla striata plantation field of the bletilla striata is chosen, marking off 11 pieces of identical areas from bletilla striata plantation Tanaka enters Row experiment, respectively 8 pieces experimental plots and 3 pieces of control fields, this 11 groups daily management method are consistent.
Medicament in the bud stage of the bletilla striata, the embodiment of the present invention 1-8 for applying equivalent in each experimental plot respectively, respectively Medicament in applying comparative example 1 and 2 at 3 pieces 2 pieces of control Tanaka, any medicament is not applied in remaining one piece of control field, is empty White control.The method of administration is:After medicament is diluted into 200 times, bletilla striata plantation Tanaka is uniformly sprayed on, and spray the bletilla striata emphatically Bud, dosage is 25kg/ mus.Additionally, spraying after the medicament, bletilla striata plant does not receive rain drop erosion in 1 day.
Observe the growing way and flowering time of the bletilla striata.The flowering time of the bletilla striata is defined as the difference of initial bloom stage and whole florescence, its In, initial bloom stage reaches the time of the 20% of bletilla striata plant total amount for the plant bloomed in bletilla striata plant;The whole florescence has bloomed The plant withered in bletilla striata plant reaches the time of the 80% of bletilla striata plant total amount.Result of the test is referring to table 1:
Influence of the different agents of table 1. to the florescence and growing way of the bletilla striata
As shown in Table 1, in the bud stage of bletilla striata plant, using after the medicament that the present invention is provided, the florescence duration of the bletilla striata is ( More than 46 days) extended 14-18 days compared to the florescence duration (32 days) in blank field, provided wherein in embodiment 6 Medicament is best to the prolongation effect at bletilla striata florescence, a length of 50 days during its florescence.Meanwhile, the blade of the bletilla striata plant in experimental plot Also more glossy than blank Tanaka, sight is higher.
And comparative example 1, compared with blank, florescence duration is only extended one day, while many in its petal atrophy, blade There is dead leaf to occur, in the case of illustrating to be added without in a medicament grape pip, aloe and tealeaves these natural plants, medicament can be right The growth of bletilla striata plant produces poisoning, and can influence the aesthetic property of bletilla striata flower.
Compared with blank, florescence duration is extended 5 days comparative example 2, much smaller than the extension at bletilla striata florescence in experimental plot Time (14-18 days), while the glossiness of blade is also good without the bletilla striata plant in experimental plot, illustrate that the tealeaves in medicament can Significantly improve the effect that the medicament extends the bletilla striata florescence.
Although illustrate and described with specific embodiment the present invention but it will be appreciated that, without departing substantially from of the invention Many other changes and modification can be made in the case of spirit and scope.Therefore, this means in the following claims Including belonging to all such changes and modifications in the scope of the invention.

Claims (10)

1. it is a kind of extend the bletilla striata florescence medicament, it is characterised in that the raw material of the medicament includes by weight:Grape pip 30-40 parts, aloe 25-35 parts, tealeaves 22-30 parts, uniconazole P 10-15 parts, urea 10-14 parts, heteroauxin 3-8 parts, sulphur hydrogen Change 3-5 parts, vitamin 1-2 parts, edta salt 2-4 parts and potassium dihydrogen phosphate 3-5 parts of sodium.
2. it is according to claim 1 extension the bletilla striata florescence medicament, it is characterised in that count by weight, the Portugal Grape seed is 32-38 parts, and the aloe is 28-32 parts, and the tealeaves is 24-28 parts, and the uniconazole P is 12-14 parts, the urine Element is 12-14 parts, and the heteroauxin is 4-6 parts, and the NaHS is 4-5 parts, and the vitamin is 1-2 parts, described Edta salt is 2-3 parts, and the potassium dihydrogen phosphate is 4-5 parts.
3. the medicament at the florescence of the extension bletilla striata according to claim 1, it is characterised in that the raw material also includes that what is first Crow, sealwort, akebi and climbing groundsel.
4. it is according to claim 3 extension the bletilla striata florescence medicament, it is characterised in that count by weight, it is described what The tuber of multiflower knotweed is 10-15 parts, and the sealwort is 10-15 parts, described akebi 6-10 parts and the climbing groundsel is 6-10 parts.
5. it is according to claim 1 extension the bletilla striata florescence medicament, it is characterised in that the vitamin be vitamin C And vitamin E.
6. it is according to claim 1 extension the bletilla striata florescence medicament, it is characterised in that the edta salt be selected from EDTA- Any one in K2, EDTA-K3 and EDTA-Na2.
7. it is a kind of according to any one of claim 1-6 extension the bletilla striata florescence medicament preparation method, its feature It is to comprise the following steps:
The grape pip, the aloe and the tealeaves are taken by weight, again with volume fraction for 60-80% after being well mixed Alcoholic solution mixes, heating and refluxing extraction twice, the extract solution obtained by merging, and slightly being carried after the extract solution concentrate drying Thing powder;
The uniconazole P, the edta salt, the urea and the heteroauxin are mixed with water, and at 60-70 DEG C plus Thermal agitation 2-3 hours, then again with the crude extract powder, the NaHS, the vitamin and the potassium dihydrogen phosphate Mixing, then be 5-6 with organic acid for adjusting pH value.
8. preparation method according to claim 7, it is characterised in that the alcoholic solution is ethanol solution, the alcoholic solution Volume be 3-5 times of the grape pip, the aloe and the tealeaves three gross mass.
9. preparation method according to claim 7, it is characterised in that the temperature of the heating and refluxing extraction is 70-80 DEG C, Extraction time is 2-3h.
10. preparation method according to claim 7, it is characterised in that the organic acid is tartaric acid and/or citric acid.
CN201710059845.1A 2017-01-24 2017-01-24 A kind of medicament at florescence for extending the bletilla striata and preparation method thereof Pending CN106831128A (en)

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