CN106758198A - Synthetic fibers mellowing method and fiber softening treatment compositions - Google Patents
Synthetic fibers mellowing method and fiber softening treatment compositions Download PDFInfo
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- CN106758198A CN106758198A CN201611108983.6A CN201611108983A CN106758198A CN 106758198 A CN106758198 A CN 106758198A CN 201611108983 A CN201611108983 A CN 201611108983A CN 106758198 A CN106758198 A CN 106758198A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Abstract
The present invention relates to a kind of synthetic fibers mellowing method and fiber softening treatment compositions, processing method includes（1）In pressure vessel, to sprinkling fiber softening treatment fluid on pending synthetic fibers；（2）To being passed through vapor in pressure vessel, it is exhausted simultaneously, is drained the cold air in pressure vessel using the water vapour being passed through, after cold air is drained, close exhaust outlet, continue to be passed through vapor simultaneously, until reservoir pressure is 0.1 ~ 0.2MPa, temperature is 110 ~ 115 DEG C, stop logical steam, 20 ~ 30 minutes are stood, pressure vessel is opened and is taken out synthetic fibers, drying.Composition includes fibroin enzyme, acetic acid, antistatic additive, silicone emulsifier, dodecyl benzyl dimethyl ammonium chloride and water.Mellowing method of the present invention, process time is short, and without discharging of waste liquid and process problem, environmental protection, economical and efficient is easy to operate, safety；And the inventive method has splendid soft effect to fiber.
Description
Technical field
The present invention relates to a kind of method that soft treatment is carried out to fiber and soft treatment composition used.
Background technology
New fiber materials are the emerging services expanded energetically by China, put forth effort to develop high-performance using technical advantage, newly
Type environmental protection is renewable, high in technological content, big fibrous material of new generation -- the soft compound of added value, while being devoted to existing
Generation science and technology, promotes Industrial Technical Progress and industrial upgrading, the development for leading fiber to modernize.
Research of technique is carried out domestic new fiber materials process engineering superior resources are actively integrated, is made great efforts in tencel
Material, there is breakthrough in technology, forge into the fiber such as tencel such as polyester, polyimide fiber function fibre in differentiation
China is largest, and technology is most advanced, horizontal highest new fiber materials -- and cannot be with the woven structure of synthetic fibers
Silk, cotton, natural fiber compare, and the weakness of the tencel of synthesis is hard, it is impossible to be made into silk like, Silk industry,
And the product of wool class good hand touch.
In the prior art, the soft finish being often mentioned is the important finishing process in dyeing and printing process.Textile is adding
During work, feel can become coarse after repeatedly treatment, and general synthetic fabrics is worse, and especially superfine fibre is knitted
Thing.In order that fabric has soft, smooth, comfortable feel, it is necessary to which it is arranged, widely used is with softness
Agent is arranged.In addition in chemical fibre spinning, softening agent is largely used during spinning, weaving of various fibers etc.,
Because as a large amount of of textile processing high speed and short liquor ratio mode use, between fabric and fabric and equipment it
Between phase mutual friction increase, be also easy to produce the phenomenons such as scratch, bar defect.Using softening agent can make fiber in itself have and processing conditions phase
The flexible smooth of adaptation is avoiding damage to.
But existing softening agent can only to a certain extent improve the flexibility of fabric, it is impossible to reach the flexibility of fabric
Silk level, is entirely capable of realizing so far Silk in the world, the crepe de Chine class Artificial Silk of superfine denier fiber Artificial Silk,
World-class class true silk products, including wool product, only there was only two countries at present, but the corresponding technology for using is not public
Open.Additionally, existing soft finish method is all using dip finishing method, in order to fiber impregnation wherein be needed using a large amount of
Water（The consumption of water is about 30 times of softening agent or so）, so as to generate substantial amounts of waste liquid accordingly（3 tons of maceration extracts accordingly will
Produce the waste liquid more than 2 tons）, the treatment of these waste liquids is also a problem, is processed, and increases cost, is not processed and then can
Severe contamination environment.And, existing process cycle was more long, it usually needs up to 24 hours, operated for temperature for a long time
Control it is inconvenient, and substantially increase cost.
The content of the invention
Problem to be solved by this invention is to overcome the deficiencies in the prior art to provide a kind of improved fiber softening treatment side
Method.
Present invention simultaneously provides a kind of fiber softening group for being used cooperatively with methods described and can obtaining notable soft effect
Compound.
To solve above technical problem, the present invention takes following technical scheme：
A kind of synthetic fibers mellowing method, the processing method uses special processor, and special processor is including having
The pressure vessel of air inlet and exhaust outlet, for the steam providing apparatus that vapor is passed through in pressure vessel, methods described bag
Include following steps：
（1）Pending synthetic fibers are positioned in pressure vessel, to spraying thereon by fiber softening treatment fluid；Or, first
To fiber softening treatment fluid is sprayed on synthetic fibers, then it is positioned in pressure vessel again；
（2）Steam providing apparatus are opened, to vapor is passed through in pressure vessel, while opening the exhaust outlet of pressure vessel, is utilized
The water vapour being passed through drains the cold air in pressure vessel, after cold air is drained, exhaust outlet is closed, while continuing to be passed through water
Steam, until reservoir pressure is 0.1 ~ 0.2MPa, temperature is 110 ~ 115 DEG C, stops logical steam, stands 20 ~ 30 minutes,
Open pressure vessel and take out synthetic fibers, drying.
Preferably, step（1）In, synthetic fibers are wrapped with cloth before sprinkling fiber softening treatment fluid, it is then placed in pressure
In force container, closing presure container, and fiber softening treatment fluid is sprayed into, and until synthetic fibers are submerged, 8-15min is kept, will
Fiber softening treatment fluid is discharged, until synthetic fibers No drip type.
Preferably, step（2）In, it is 0.15 ~ 0.2MPa to be passed through water vapour to reservoir pressure.
According to the present invention, described fiber softening treatment fluid is general by being made after fiber softening composition dilute with water.
Fiber softening composition can using it is known in the art those.It is preferred to use particular design of the present invention is soft
Soft-combine thing, with reference to processing method of the present invention and soft compound, the soft effect to fiber is best.If pending synthesis
Fiber is emulation silk fiber, then the rear effect that can reach complete simulation silk processed by the invention.
According to an aspect of the present invention, the preferred soft compound its include fibroin enzyme, acetic acid, antistatic
Agent, silicone emulsifier, dodecyl benzyl dimethyl ammonium chloride and water, and fibroin enzyme, acetic acid, antistatic additive, silicone breast
Agent, the mass ratio of dodecyl benzyl dimethyl ammonium chloride are 6 ~ 8：8~12：1：0.3~0.8：0.3~0.8.
It is further preferred that the fiber softening composition is emulsified by useless silk-extract, wooden vinegar, antistatic additive, silicone
Agent and water are mixed, wherein containing acetic acid 20% ~ 50% in wooden vinegar.
Preferably, acetic acid 30% ~ 45% is contained in wooden vinegar.
Preferably, the wooden vinegar is lemon vinegar.
Preferably, the useless silk-extract carries out refluxing extraction acquisition by with ether to discarded silk, wherein containing
35 ~ 40% fibroin enzyme.
A specific aspect of the invention, fiber softening composition by useless silk-extract, wooden vinegar, antistatic additive,
Silicone emulsifier and water are mixed, and useless silk-extract carries out refluxing extraction acquisition by with ether to discarded silk, its
In containing 35 ~ 40% fibroin enzyme, wooden vinegar be lemon vinegar, wherein containing acetic acid 30% ~ 45%；Antistatic additive is that PK is antistatic
Agent（Potassium alkyl phosphate）, silicone emulsifier is in silicone emulsion OP-4, silicone emulsion OP-10, silicone emulsion OP-20
Plant or various combinations.
The inventive method is particularly suitable for carrying out soft treatment to emulation silk fiber, therefore, synthetic fibers are preferably Silk
Fiber.The species of fiber can be polyester, polyimide fiber or composite fibre etc., wherein it is preferred that polyester fiber.
According to another aspect of the invention, fiber softening composition includes following composition：SN series softening agent, peregal,
1 part of stearic acid diisopropanolamine (DIPA), PK antistatic additive, butyl cellosolve and water, SN series softening agent, peregal 25 ~ 35, stearic acid
The mass ratio of diisopropanolamine (DIPA) 6 ~ 9,1 part of PK antistatic additive and butyl cellosolve is 1 ~ 1.5：25~35：6~9：1：1~3.
The invention further relates to a kind of fiber softening composition, it includes fibroin enzyme, acetic acid, antistatic additive, silicone breast
Agent, dodecyl benzyl dimethyl ammonium chloride and water, the fibroin enzyme, acetic acid, antistatic additive, silicone emulsifier, ten
The mass ratio of dialkyl dimethyl benzyl ammonium chloride is 6 ~ 8：8~12：1：0.3~0.8：0.3~0.8.
Preferably, the fiber softening composition by useless silk-extract, wooden vinegar, antistatic additive, silicone emulsifier and
Water is mixed, and the useless silk-extract carries out refluxing extraction acquisition by with ether to discarded silk, wherein containing 35 ~
40% fibroin enzyme, the wooden vinegar is lemon vinegar, wherein containing acetic acid 20% ~ 50%；The antistatic additive is that PK is antistatic
Agent, one or more in the silicone emulsion OP-4, silicone emulsion OP-10, silicone emulsion OP-20 of combination.
More than, although mellowing method of the present invention and composition for processing fiber, the inventive method
It is equally applicable for the soft treatment of fabric with composition.Particularly soft compound may be adapted to the fabrics such as wool, silk, polyester.
Because above-mentioned technical proposal is used, the present invention has following advantages compared with prior art：
Mellowing method of the present invention, process time is short, without discharging of waste liquid and process problem, environmental protection, economical and efficient, operation
It is convenient, safety；And the inventive method has splendid soft effect to fiber, the Silk processed using the method is soft easypro
Suitable, smell is pure and fresh, smooth docile, will not deform, and the elegant effect same with the textile that silk is made is reached, with wide
Application prospect.
Specific embodiment
Fiber softening composition of the invention and mellowing method, break-through skill tackling key problem, be expected to free from environmental pollution and
The real production for realizing Artificial Silk on the premise of reduces cost.The present invention is done further below in conjunction with specific embodiment
Detailed description, but the invention is not restricted to following examples.
In the present invention when not clearly stating, represent that " % " or " percentage " of content is weight percentage content.Below
In embodiment, unreceipted experiment condition is conventional experiment condition.Used raw material is by commercially available.
Embodiment 1
The present invention provides a kind of fiber softening composition, and it is resisted quiet by useless silk-extract 19.27kg, lemon vinegar 26.04kg, PK
Electric agent 2.8kg, silicone emulsion OP-4 1.4kg, distilled water（Steam again）160kg and dodecyl benzyl dimethyl ammonium chloride
0.5kg is mixed, wherein useless silk-extract extracts gained by the silk discarded by aether backflow, wherein containing 38.4%
Fibroin enzyme；Lemon vinegar is the vinegar being made up of lemon, wherein containing acetic acid 40%；Active ingredient contains in PK antistatic additive
It is 35.7% to measure, and the content of active ingredient is 35.7% in silicone emulsifier.
Embodiment 2
The present invention provides a kind of fiber softening composition, and it is different by SN series softening agents 1.2kg, peregal 28kg, stearic acid two
Propanolamine 7.7kg, PK antistatic additive 1kg, butyl cellosolve 2kg and distilled water 160kg are mixed.
Embodiment 3
A kind of Silk polyester fiber（50D/96F fine denier filaments high）Mellowing method, the device that it is used include can bear
Vapour pressure 0.3MPa（3kg）Pressure vessel, steam providing apparatus and two pressure gauges of more than 5kg, pressure vessel have into
Gas port and exhaust outlet, and safety valve is installed.Steam providing apparatus supply water vapour by air inlet, the supply of water vapour and disconnected
Valve was opened to control.
This example processing method comprises the following steps：
（1）The packing of Silk polyester fiber is divided into required metering, and after being wrapped up with cloth, is added in pressure vessel, will had
The fiber softening composition being made up of the formula of embodiment 1 is diluted preparation and obtains fiber by the concentration that composition levels are 10%
Soft treatment liquid, and fiber softening treatment fluid is sprayed onto fiber surface, pending liquid submerges fiber, stops sprinkling treatment
Liquid, and 10min is soaked, treatment fluid is then discharged out, until No drip type on fiber, carries out next step operation；
（2）Debugging apparatus, after all going well, open valve to water vapour is passed through in pressure vessel, while opening on exhaust outlet
Drain tap, cold air is bled off, and after cold air bleeds off, closes drain tap, continues to be passed through water vapour, about 30min or so
Reservoir pressure rises to about 1.5kg, and temperature is for about 110 DEG C, now closes valve, and stopping is passed through water vapour, stands 20
Door can be opened after minute to take out, normal drying can be used.
Untreated Silk is compared on fabric hand after treatment substantially soft, comfortably, smooth, outward appearance is smooth, feel
It is as good as with silk, surveys cohesive force between fiber（cN）It is 200 or so.
Embodiment 4
The present embodiment provides a kind of mellowing method of Silk polyester fiber, and it is substantially with embodiment 3, the difference is that control
Step（2）When middle pressure is to 2kg, temperature closes valve when being 115 DEG C.
Untreated Silk is compared on fabric hand after treatment substantially soft, comfortably, smooth, outward appearance is smooth, feel
It is as good as with silk, surveys cohesive force between fiber（cN）It is 200 or so.
Embodiment 5-6
Embodiment 5 and 6 provides the mellowing method of Silk polyester fiber respectively, and it is basic with embodiment 3 and 4 respectively, no
Same is the soft compound that used soft compound is embodiment 2.
Untreated Silk is compared on fabric hand after treatment more soft, comfortably, smooth, outward appearance is smooth, but feel
It is slightly more inferior than silk, difference can be felt, survey cohesive force between fiber（cN）It is 160 or so.
In sum, the present invention is innovated to the mellowing method and soft compound of fiber, on the one hand, the fibre after treatment
The unusual soft comfortable of dimension, smell is pure and fresh, removes electrostatic, as bright as new, will not modification, it is smooth docile；On the other hand, process time
Short, efficiency high produces without waste liquid or waste liquid is greatly decreased, cost reduction.Therefore, the present invention has important for Silk industry
Meaning.
It is worth noting that, installing special processor of the present invention first and using the inventive method, Ying Xianxue
Practise operation to require and associated safety knowledge, possessing can be on duty after respective capabilities, to ensure absolute security.
The above embodiments merely illustrate the technical concept and features of the present invention, its object is to allow person skilled in the art
Scholar will appreciate that present disclosure and implement according to this that it is not intended to limit the scope of the present invention, all according to the present invention
The equivalent change or modification that Spirit Essence is made, should all be included within the scope of the present invention.
Claims (10)
1. a kind of synthetic fibers mellowing method, it is characterised in that the processing method uses special processor, it is described specially
With processing unit including the pressure vessel with air inlet and exhaust outlet, for the steaming that vapor is passed through in the pressure vessel
Vapour feeding mechanism, the described method comprises the following steps：
（1）Pending synthetic fibers are positioned in pressure vessel, to spraying thereon by fiber softening treatment fluid；Or, first
To fiber softening treatment fluid is sprayed on synthetic fibers, then it is positioned in pressure vessel again；
（2）The steam providing apparatus are opened, to vapor is passed through in the pressure vessel, while opening the pressure vessel
Exhaust outlet, is drained the cold air in pressure vessel using the water vapour being passed through, and after cold air is drained, closes exhaust outlet, together
Shi Jixu is passed through vapor, until reservoir pressure is 0.1 ~ 0.2MPa, temperature is 110 ~ 115 DEG C, stops logical steam, quiet
Put 20 ~ 30 minutes, open pressure vessel and take out synthetic fibers, drying.
2. synthetic fibers mellowing method according to claim 1, it is characterised in that：Step（1）In, sprinkling fiber is soft
Synthetic fibers are wrapped with cloth before supple-settlement liquid, is then placed in pressure vessel, closing presure container, and spray into fiber softening
Treatment fluid, until synthetic fibers are submerged, keeps 8-15min, by the discharge of fiber softening treatment fluid, until synthetic fibers do not drip
Liquid.
3. synthetic fibers mellowing method according to claim 1, it is characterised in that：Step（2）In, it is passed through water vapour
It is 0.15 ~ 0.2MPa to reservoir pressure.
4. synthetic fibers mellowing method according to claim 1, it is characterised in that：Described fiber softening treatment fluid
By being made after fiber softening composition dilute with water, the fiber softening composition includes fibroin enzyme, acetic acid, antistatic
Agent, silicone emulsifier, dodecyl benzyl dimethyl ammonium chloride and water, and the fibroin enzyme, acetic acid, antistatic additive, silicon
Ketone emulsifying agent, the mass ratio of dodecyl benzyl dimethyl ammonium chloride are 6 ~ 8：8~12：1：0.3~0.8：0.3~0.8.
5. synthetic fibers mellowing method according to claim 4, it is characterised in that：The fiber softening composition by
Useless silk-extract, wooden vinegar, antistatic additive, silicone emulsifier and water are mixed, in the wooden vinegar containing acetic acid 20% ~
50%。
6. synthetic fibers mellowing method according to claim 5, it is characterised in that：The useless silk-extract passes through
Refluxing extraction acquisition is carried out to discarded silk with ether, wherein containing 35 ~ 40% fibroin enzyme.
7. synthetic fibers mellowing method according to claim 5, it is characterised in that：The wooden vinegar is lemon vinegar.
8. synthetic fibers mellowing method according to claim 1, it is characterised in that：The synthetic fibers are Silk
Fiber.
9. a kind of fiber softening composition, it is characterised in that：The composition includes fibroin enzyme, acetic acid, antistatic additive, silicon
Ketone emulsifying agent, dodecyl benzyl dimethyl ammonium chloride and water, the fibroin enzyme, acetic acid, antistatic additive, silicone breast
Agent, the mass ratio of dodecyl benzyl dimethyl ammonium chloride are 6 ~ 8：8~12：1：0.3~0.8：0.3~0.8.
10. fiber softening composition according to claim 9, it is characterised in that：The fiber softening composition is by silkworm of giving up
Silk extract, wooden vinegar, antistatic additive, silicone emulsifier and water are mixed, and the useless silk-extract is by with ether pair
Discarded silk carries out refluxing extraction acquisition, wherein containing 35 ~ 40% fibroin enzyme, the wooden vinegar is lemon vinegar, wherein containing
Acetic acid 20% ~ 50%；The antistatic additive is PK antistatic additive, and the silicone emulsifier is silicone emulsion OP-4, silicone emulsion OP-
10th, the combination of one or more in silicone emulsion OP-20.
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| CN201611108983.6A CN106758198B (en) | 2016-12-06 | 2016-12-06 | Synthetic fibers mellowing method and fiber softening treatment compositions |
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| CN201611108983.6A CN106758198B (en) | 2016-12-06 | 2016-12-06 | Synthetic fibers mellowing method and fiber softening treatment compositions |
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| CN106758198B CN106758198B (en) | 2019-08-06 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111172784A (en) * | 2020-03-03 | 2020-05-19 | 南通思聪家居有限公司 | Printing process of magic velvet fabric |
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| CN102808231A (en) * | 2012-08-27 | 2012-12-05 | 嘉兴市普利莱新材料有限公司 | Preparation method of polylactic acid fiber filament imitated silk material |
| CN103103676A (en) * | 2012-12-14 | 2013-05-15 | 常熟市同昌服装有限公司 | Processing craft of cloth |
| CN203668698U (en) * | 2013-12-23 | 2014-06-25 | 江苏华超纺织实业有限公司 | Soft finishing machine |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111172784A (en) * | 2020-03-03 | 2020-05-19 | 南通思聪家居有限公司 | Printing process of magic velvet fabric |
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