CN106753085A - A kind of preparation method of dampproof protection against insects mounting of calligraphy and painting paste - Google Patents
A kind of preparation method of dampproof protection against insects mounting of calligraphy and painting paste Download PDFInfo
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- CN106753085A CN106753085A CN201611030935.XA CN201611030935A CN106753085A CN 106753085 A CN106753085 A CN 106753085A CN 201611030935 A CN201611030935 A CN 201611030935A CN 106753085 A CN106753085 A CN 106753085A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J151/00—Adhesives based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Adhesives based on derivatives of such polymers
- C09J151/02—Adhesives based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Adhesives based on derivatives of such polymers grafted on to polysaccharides
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F251/00—Macromolecular compounds obtained by polymerising monomers on to polysaccharides or derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F289/00—Macromolecular compounds obtained by polymerising monomers on to macromolecular compounds not provided for in groups C08F251/00 - C08F287/00
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J151/00—Adhesives based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Adhesives based on derivatives of such polymers
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Abstract
The present invention relates to a kind of preparation method of dampproof protection against insects mounting of calligraphy and painting paste, belong to paste preparing technical field.The present invention with absolute ether and n-butanol first by pigskin by carrying out degreasing respectively after freezing, defrosting and the treatment of alkali bubble, acid bubble dissolving is carried out after degreasing again, filtering, obtain liquid of vicidity, then thing will must be gelatinized after the heating of the material mixings such as cornstarch and pyrolkigneous liquid, it is ultrasonically treated after mixing with liquid of vicidity, obtain modified gelatinization thing, finally by it with vinyl acetate etc. substance reaction, obtain dampproof protection against insects mounting of calligraphy and painting paste.The dampproof protection against insects mounting of calligraphy and painting paste prepared using the present invention has superior moistureproof and Anti-moth-eating ability, does not occur damaging by worms within 2~3 years, mildew does not occur within 7~10 months, extends its holding time.
Description
Technical field
The present invention relates to a kind of preparation method of dampproof protection against insects mounting of calligraphy and painting paste, belong to paste preparing technical field.
Background technology
Needed in the mounting of calligraphy and painting and repair using paste as the bonding between paper and paper, paper and mounting fabric
Agent is used.Mounting of calligraphy and painting paste has vital influence for the preservation of painting and calligraphy with reparation, and the quality of mounting paste is direct
It is related to the time that the good and bad and works of works are preserved.The mounting of calligraphy and painting with repair in the paste that uses should have and preferably soak
Property, adhesiveness, film forming and invertibity, should modest viscosity, it is clean again, mothproof.Paste quality good or not directly affects mounting
With the quality repaired, paste is a key material in whole mounting process, be also influence mount one of part quality it is important
Factor.Wheat starch Paste is used as the Chinese tradition mounting of calligraphy and painting（Antiquated painting and calligraphy, rare book reparation）Adhesive, had long
History.And because it has stable chemical property and good bond properties and superior dissolubility, receive always for a long time
To the favor of mounting teacher and books repair person.And the slurrying process of wheaten starch, also without the progress because of natural science,
The mankind go deep into material world understanding, and have innovated and changed.
The painting and calligraphy pieces that one width mounting is finished must be subject to factor of natural environment during suspension, appreciation, collection,
Such as：The erosion of malaria, mould, fly worm, light radiation etc., influence.And traditional mounting（Antiquated painting and calligraphy, rare book reparation）Work
Skill, so far to this still without effective solution.Still continue ancient method, add white in wheaten starch slurrying process
The additives such as alum, Chinese prickly ash, the bletilla striata, the tuber of stemona, cloves, and it is unsatisfactory in practical effect, or even there is the effect run counter to desire
Really.For example disclosed in Chinese invention patent a kind of ancient book draws mounting paste and preparation method thereof, and alum is exactly added in flour
The anti-mildew that mounting paste is improved with pericarpium zanthoxyli becomes ability, but it cannot solve the problem of damaging by worms.
Japanese mounting painting and calligraphy（Antiquated painting and calligraphy, rare book reparation）With Wheat starch Paste, " new paste " and " old paste " are generally divided into
Two kinds." new paste " manufacture craft and additive duplicate with the used technique of China, there is also go mouldy, damage by worms, anti-aging problem.
And use " the old paste " of special process, although the problem of going mouldy is effectively controlled, but the paste producing cycle is long（It is not less than 1 year, in addition it is long
Up to more than 10 years）, high cost, be the biggest obstacle of " old paste " Technique Popularizing.The mounting of current China in the industry, loses use " old
Paste ", its reason is also because the cycle is long, high cost.Secondly, " old paste " is also only merely that effective control is gone mouldy, and still can not
Solve the problems, such as to damage by worms, it is anti-aging.
The content of the invention
The technical problems to be solved by the invention：For traditional mounting of calligraphy and painting paste is used, it is obtained by starch gelatinization, it is long
Phase can shorten the holding time of painting and calligraphy so that the phenomenon gone mouldy and damage by worms occur in painting and calligraphy pieces after using, and have impact on its preservation
The problem of quality, there is provided the starch after a kind of glue extracted from pigskin and gelatinization is reacted, and improves the viscosity of gelatinization thing
And film forming, the method for mounting of calligraphy and painting paste will be prepared into after modified gelatinization thing and methyl acrylate, vinyl acetate reaction, this
Pigskin is carried out degreasing by invention with absolute ether and n-butanol respectively after freezing, defrosting and alkali bubble are processed first, after degreasing
Acid bubble dissolving is carried out again, and filtering obtains liquid of vicidity, must be pasted after then the material mixings such as cornstarch and pyrolkigneous liquid are heated
Compound, it is ultrasonically treated after mixing with liquid of vicidity, modified gelatinization thing is obtained, finally by it, material is anti-with vinyl acetate etc.
Should, obtain dampproof protection against insects mounting of calligraphy and painting paste.Dampproof protection against insects mounting of calligraphy and painting paste prepared by the present invention has moisture protection and prevents
Damage by worms ability, the painting and calligraphy after mounting are less prone to the ability of going mouldy, extend the holding time of painting and calligraphy.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
（1）800~1000g pigskins are weighed, is put into refrigerator, 8~10h is freezed at -30~-20 DEG C, taken out after freezing, in room
Lower 8~the 10h that thaws of temperature, by the pigskin stripping and slicing after defrosting, in mass ratio 1:Pigskin after stripping and slicing is put into the hydrogen of mass fraction 10% by 10
20~30h is soaked in sodium hydroxide solution, sodium hydroxide solution is changed once every 6~8h, immersion is filtered after terminating, and obtains filter residue
Afterwards, filter residue is washed with deionized to cleaning solution in neutrality, is put into baking oven after washing, 4~5h is dried at 70~80 DEG C, obtain
Dried object；
（2）By above-mentioned dried object in mass ratio 1:In 5 addition absolute ethers, filtered after 5~10h of immersion, collect filter residue, then pressed
Mass ratio 1:5, the filter residue of collection is added in n-butanol and soaks 10~12h, the filter residue after immersion is taken out, and use deionized water
3~5 times, in mass ratio 1 are washed to it:20, will after washing filter residue add the acetum of mass fraction 10% in, immersion 25~
30h, is constantly stirred while immersion, dissolves the filter residue after washing, filters, and collects filtrate, obtains final product liquid of vicidity；
（3）Weigh 800~1000g cornstarch, 1500~2000g deionized waters, 20~30g pyrolkigneous liquid and 5~7g diacetic acids
Sodium, 3~5g ammonium persulfates are added after stirring mixing, are heated to 90~95 DEG C, and thing must be gelatinized after 30~40min of insulated and stirred, will
Gelatinization thing and above-mentioned liquid of vicidity in mass ratio 2:1 mixing, is placed in ultrasonic emulsator, in 180~200W work(after mixing
Ultrasonically treated 5~10min is carried out under rate, must be modified gelatinization thing after treatment；
（4）Weigh 500~700g it is above-mentioned it is modified be gelatinized in reactor, and to added in reactor 50~60g methyl acrylates,
50~60g vinyl acetates and 2~4g ammonium persulfates, are heated to 70~80 DEG C after stirring mixing, insulated and stirred reacts 3~5h,
Reaction terminates rear cooling discharging, you can obtain dampproof protection against insects mounting of calligraphy and painting paste.
Application process of the invention：In mass ratio 10:1~5:1, dampproof protection against insects mounting of calligraphy and painting paste prepared by the present invention
Mixed with water, and it is stirred uniformly, obtain being watered paste, rice paper is cut into 15mm~300mm rectangular papers
Bar, is uniformly coated with being watered paste in the one side of rice paper, and coating thickness is 0.6~1.1mm, after end to be coated, uses another Zhang Xuan
Paper covering is pasted together, and 45~65h is dried under normal temperature, and after testing, the dampproof protection against insects mounting of calligraphy and painting prepared using the present invention is starched
Paste does not occur damaging by worms for 2~3 years with superior moistureproof and Anti-moth-eating ability, mildew does not occur within 7~10 months, extends its guarantor
Deposit the time.
Compared with other method, Advantageous Effects are the present invention：
（1）The dampproof protection against insects mounting of calligraphy and painting paste prepared using the present invention has superior moistureproof and Anti-moth-eating ability, 2~3 years
Do not occur damaging by worms, mildew do not occur within 7~10 months, extend its holding time；
（2）Dampproof protection against insects mounting of calligraphy and painting paste preparation process prepared by the present invention is simple, required with low cost, should with wide
Use prospect.
Specific embodiment
800~1000g pigskins are weighed first, is put into refrigerator, 8~10h is freezed at -30~-20 DEG C, taken after freezing
Go out, thaw 8~10h at room temperature, by the pigskin stripping and slicing after defrosting, in mass ratio 1:Pigskin after stripping and slicing is put into quality point by 10
20~30h is soaked in several 10% sodium hydroxide solutions, sodium hydroxide solution is changed once every 6~8h, immersion is filtered after terminating,
After obtaining filter residue, filter residue is washed with deionized to cleaning solution in neutrality, is put into baking oven after washing, 4 are dried at 70~80 DEG C
~5h, obtains dried object；By above-mentioned dried object in mass ratio 1:In 5 addition absolute ethers, filtered after 5~10h of immersion, collect filter
Slag, then in mass ratio 1:5, the filter residue of collection is added in n-butanol and soaks 10~12h, the filter residue after immersion is taken out, and
3~5 times, in mass ratio 1 are washed to it with deionized water:20, by after washing filter residue add the acetum of mass fraction 10% in,
25~30h of immersion, is constantly stirred while immersion, dissolves the filter residue after washing, filters, and collects filtrate, obtains final product viscous
Consistence liquid；Weigh the double second of 800~1000g cornstarch, 1500~2000g deionized waters, 20~30g pyrolkigneous liquid and 5~7g
Sour sodium, 3~5g ammonium persulfates are added after stirring mixing, are heated to 90~95 DEG C, and thing must be gelatinized after 30~40min of insulated and stirred,
Thing and above-mentioned liquid of vicidity in mass ratio 2 will be gelatinized:1 mixing, is placed in ultrasonic emulsator, in 180~200W after mixing
Ultrasonically treated 5~10min is carried out under power, must be modified gelatinization thing after treatment；Finally weigh 500~700g it is above-mentioned it is modified be gelatinized in
In reactor, and to 50~60g of addition methyl acrylates, 50~60g vinyl acetates and 2~4g ammonium persulfates in reactor,
70~80 DEG C are heated to after stirring mixing, insulated and stirred reacts 3~5h, reaction terminates rear cooling discharging, you can obtain moistureproof anti-
Worm mounting of calligraphy and painting paste.
Example 1
1000g pigskins being weighed first, being put into refrigerator, 10h is freezed at -20 DEG C, taken out after freezing, thaw 10h at room temperature,
By the pigskin stripping and slicing after defrosting, in mass ratio 1:Pigskin after stripping and slicing is put into the sodium hydroxide solution of mass fraction 10% and soaks by 10
Bubble 30h, sodium hydroxide solution is changed once every 8h, and immersion is filtered after terminating, and after obtaining filter residue, filter residue is washed with deionized extremely
Cleaning solution is put into baking oven in neutrality after washing, and 5h is dried at 80 DEG C, obtains dried object；By above-mentioned dried object in mass ratio 1:5
Add in absolute ether, filtered after immersion 10h, collect filter residue, then in mass ratio 1:5, the filter residue of collection is added to positive fourth
12h is soaked in alcohol, the filter residue after immersion is taken out, and 5 times, in mass ratio 1 are washed to it with deionized water:20, will be filtered after washing
Slag is added in the acetum of mass fraction 10%, soaks 30h, is constantly stirred while immersion, makes the filter residue after washing molten
Filtrate is collected in solution, filtering, obtains final product liquid of vicidity；Weigh 1000g cornstarch, 2000g deionized waters, 30g pyrolkigneous liquid and 7g
Sodium Diacetate, 5g ammonium persulfates are added after stirring mixing, are heated to 95 DEG C, and thing must be gelatinized after insulated and stirred 40min, will be gelatinized thing
With above-mentioned liquid of vicidity in mass ratio 2:1 mixing, is placed in ultrasonic emulsator after mixing, and ultrasound is carried out under 200W power
Treatment 5min, must be modified gelatinization thing after treatment；Finally weigh 700g it is above-mentioned it is modified be gelatinized in reactor, and in reactor plus
Enter 60g methyl acrylates, 60g vinyl acetates and 4g ammonium persulfates, 80 DEG C, insulated and stirred reaction are heated to after stirring mixing
5h, reaction terminates rear cooling discharging, you can obtain dampproof protection against insects mounting of calligraphy and painting paste.
In mass ratio 5:1, dampproof protection against insects mounting of calligraphy and painting paste prepared by the present invention is mixed with water, and it is carried out
Stir, obtain being watered paste, rice paper is cut into rectangle paper slip, be uniformly coated with being watered paste in the one side of rice paper, apply
Thickness is covered for 1.1mm, after end to be coated, is covered with another rice paper and is pasted together, 65h is dried under normal temperature, after testing, make
The dampproof protection against insects mounting of calligraphy and painting paste prepared with the present invention has superior moistureproof and Anti-moth-eating ability, does not occur damaging by worms within 3 years, and 10
There is not mildew within individual month, extend its holding time.
Example 2
800g pigskins being weighed first, being put into refrigerator, 8h is freezed at -30 DEG C, taken out after freezing, thaw 8h at room temperature, will
Pigskin stripping and slicing after defrosting, in mass ratio 1:Pigskin after stripping and slicing is put into the sodium hydroxide solution of mass fraction 10% and soaks by 10
20h, sodium hydroxide solution is changed once every 6h, and immersion is filtered after terminating, and after obtaining filter residue, filter residue is washed with deionized to washing
Liquid is washed in neutrality, is put into baking oven after washing, 4h is dried at 70 DEG C, obtain dried object；By above-mentioned dried object in mass ratio 1:5 add
In entering absolute ether, filtered after immersion 5h, collect filter residue, then in mass ratio 1:5, the filter residue of collection is added in n-butanol
Immersion 10h, takes out the filter residue after immersion, and 3 times, in mass ratio 1 are washed to it with deionized water:20, filter residue after washing is added
Enter in the acetum of mass fraction 10%, soak 25h, be constantly stirred while immersion, dissolve the filter residue after washing,
Filtering, collects filtrate, obtains final product liquid of vicidity；Weigh the double second of 800g cornstarch, 1500g deionized waters, 20g pyrolkigneous liquid and 5g
Sour sodium, 3g ammonium persulfates are added after stirring mixing, are heated to 90 DEG C, and thing must be gelatinized after insulated and stirred 30min, will gelatinization thing and upper
State liquid of vicidity in mass ratio 2:1 mixing, is placed in ultrasonic emulsator after mixing, is carried out under 180W power ultrasonically treated
5min, must be modified gelatinization thing after treatment；Finally weigh 500g it is above-mentioned it is modified be gelatinized in reactor, and in reactor add
50g methyl acrylates, 50g vinyl acetates and 2g ammonium persulfates, are heated to 70 DEG C after stirring mixing, insulated and stirred reacts 3h,
Reaction terminates rear cooling discharging, you can obtain dampproof protection against insects mounting of calligraphy and painting paste.
In mass ratio 10:1, dampproof protection against insects mounting of calligraphy and painting paste prepared by the present invention is mixed with water, and it is entered
Row is stirred, and obtains being watered paste, and rice paper is cut into rectangle paper slip, is uniformly coated with being watered paste in the one side of rice paper,
Coating thickness is 0.6mm, after end to be coated, is covered with another rice paper and is pasted together, and 45h is dried under normal temperature, after testing,
The dampproof protection against insects mounting of calligraphy and painting paste prepared using the present invention has superior moistureproof and Anti-moth-eating ability, does not occur damaging by worms within 2 years,
There is not mildew within 7 months, extend its holding time.
Example 3
900g pigskins being weighed first, being put into refrigerator, 9h is freezed at -25 DEG C, taken out after freezing, thaw 9h at room temperature, will
Pigskin stripping and slicing after defrosting, in mass ratio 1:Pigskin after stripping and slicing is put into the sodium hydroxide solution of mass fraction 10% and soaks by 10
25h, sodium hydroxide solution is changed once every 7h, and immersion is filtered after terminating, and after obtaining filter residue, filter residue is washed with deionized to washing
Liquid is washed in neutrality, is put into baking oven after washing, 4h is dried at 75 DEG C, obtain dried object；By above-mentioned dried object in mass ratio 1:5 add
In entering absolute ether, filtered after immersion 7h, collect filter residue, then in mass ratio 1:5, the filter residue of collection is added in n-butanol
Immersion 11h, takes out the filter residue after immersion, and 4 times, in mass ratio 1 are washed to it with deionized water:20, filter residue after washing is added
Enter in the acetum of mass fraction 10%, soak 27h, be constantly stirred while immersion, dissolve the filter residue after washing,
Filtering, collects filtrate, obtains final product liquid of vicidity；Weigh the double second of 900g cornstarch, 1700g deionized waters, 25g pyrolkigneous liquid and 6g
Sour sodium, 4g ammonium persulfates are added after stirring mixing, are heated to 92 DEG C, and thing must be gelatinized after insulated and stirred 35min, will gelatinization thing and upper
State liquid of vicidity in mass ratio 2:1 mixing, is placed in ultrasonic emulsator after mixing, is carried out under 190W power ultrasonically treated
7min, must be modified gelatinization thing after treatment；Finally weigh 600g it is above-mentioned it is modified be gelatinized in reactor, and in reactor add
55g methyl acrylates, 55g vinyl acetates and 3g ammonium persulfates, are heated to 75 DEG C after stirring mixing, insulated and stirred reacts 4h,
Reaction terminates rear cooling discharging, you can obtain dampproof protection against insects mounting of calligraphy and painting paste.
In mass ratio 7:1, dampproof protection against insects mounting of calligraphy and painting paste prepared by the present invention is mixed with water, and it is carried out
Stir, obtain being watered paste, rice paper is cut into rectangle paper slip, be uniformly coated with being watered paste in the one side of rice paper, apply
Thickness is covered for 0.8mm, after end to be coated, is covered with another rice paper and is pasted together, 60h is dried under normal temperature, after testing, make
The dampproof protection against insects mounting of calligraphy and painting paste prepared with the present invention has superior moistureproof and Anti-moth-eating ability, does not occur damaging by worms within 2 years, and 8
There is not mildew within individual month, extend its holding time.
Claims (1)
1. a kind of preparation method of dampproof protection against insects mounting of calligraphy and painting paste, it is characterised in that specific preparation process is：
（1）800~1000g pigskins are weighed, is put into refrigerator, 8~10h is freezed at -30~-20 DEG C, taken out after freezing, in room
Lower 8~the 10h that thaws of temperature, by the pigskin stripping and slicing after defrosting, in mass ratio 1:Pigskin after stripping and slicing is put into the hydrogen of mass fraction 10% by 10
20~30h is soaked in sodium hydroxide solution, sodium hydroxide solution is changed once every 6~8h, immersion is filtered after terminating, and obtains filter residue
Afterwards, filter residue is washed with deionized to cleaning solution in neutrality, is put into baking oven after washing, 4~5h is dried at 70~80 DEG C, obtain
Dried object；
（2）By above-mentioned dried object in mass ratio 1:In 5 addition absolute ethers, filtered after 5~10h of immersion, collect filter residue, then pressed
Mass ratio 1:5, the filter residue of collection is added in n-butanol and soaks 10~12h, the filter residue after immersion is taken out, and use deionized water
3~5 times, in mass ratio 1 are washed to it:20, will after washing filter residue add the acetum of mass fraction 10% in, immersion 25~
30h, is constantly stirred while immersion, dissolves the filter residue after washing, filters, and collects filtrate, obtains final product liquid of vicidity；
（3）Weigh 800~1000g cornstarch, 1500~2000g deionized waters, 20~30g pyrolkigneous liquid and 5~7g diacetic acids
Sodium, 3~5g ammonium persulfates are added after stirring mixing, are heated to 90~95 DEG C, and thing must be gelatinized after 30~40min of insulated and stirred, will
Gelatinization thing and above-mentioned liquid of vicidity in mass ratio 2:1 mixing, is placed in ultrasonic emulsator, in 180~200W work(after mixing
Ultrasonically treated 5~10min is carried out under rate, must be modified gelatinization thing after treatment；
（4）Weigh 500~700g it is above-mentioned it is modified be gelatinized in reactor, and to added in reactor 50~60g methyl acrylates,
50~60g vinyl acetates and 2~4g ammonium persulfates, are heated to 70~80 DEG C after stirring mixing, insulated and stirred reacts 3~5h,
Reaction terminates rear cooling discharging, you can obtain dampproof protection against insects mounting of calligraphy and painting paste.
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| CN109207089A (en) * | 2018-08-08 | 2019-01-15 | 芜湖职业技术学院 | A kind of mounting of calligraphy and painting paste and its preparation method and application |
| CN115627125A (en) * | 2022-11-02 | 2023-01-20 | 南通亿川复合材料科技有限公司 | Preparation method of fragile self-adhesive paper |
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|---|---|---|---|---|
| CN109207089A (en) * | 2018-08-08 | 2019-01-15 | 芜湖职业技术学院 | A kind of mounting of calligraphy and painting paste and its preparation method and application |
| CN115627125A (en) * | 2022-11-02 | 2023-01-20 | 南通亿川复合材料科技有限公司 | Preparation method of fragile self-adhesive paper |
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| CN106753085B (en) | 2018-09-14 |
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