CN106753073A - A kind of high tenacity environment-friendly type peelable glue and preparation method thereof - Google Patents
A kind of high tenacity environment-friendly type peelable glue and preparation method thereof Download PDFInfo
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- CN106753073A CN106753073A CN201710030144.5A CN201710030144A CN106753073A CN 106753073 A CN106753073 A CN 106753073A CN 201710030144 A CN201710030144 A CN 201710030144A CN 106753073 A CN106753073 A CN 106753073A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J127/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Adhesives based on derivatives of such polymers
- C09J127/02—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Adhesives based on derivatives of such polymers not modified by chemical after-treatment
- C09J127/04—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Adhesives based on derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
- C09J127/06—Homopolymers or copolymers of vinyl chloride
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J163/00—Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Inorganic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses a kind of high tenacity environment-friendly type peelable glue and preparation method thereof, described peelable glue is made up of a certain proportion of water-soluble resin, water, filler, defoamer, levelling agent, toughener, rheological agent, pigment, and preparation method is comprised the following steps：A. each component is weighed in proportion；B. water-base resin is dissolved in the water of part and adds toughener, stirred 1.5 2.5 hours；C. by filler, the above-mentioned mixed liquor of pigment addition, ground 25 times with three-roll grinder after stirring, the water of surplus is added in material after grinding, stirred 0.5 2 hours under the conditions of 90 110 DEG C, being stirring evenly and then adding into defoamer carries out defoaming treatment, is eventually adding levelling agent and rheological agent.The peelable glue that the present invention is provided has film strength good, high temperature resistant, extension at break is small, the feature of environmental protection the features such as, using scope than wide, be particularly well-suited to the protection of the operation such as cutting, finishing impression, printing, plated film in touch-screen technique.
Description
Technical field
The invention belongs to technical field of high-molecular polymer, and in particular to a kind of high tenacity environment-friendly type peelable glue, further relate to
The preparation method of high tenacity environment-friendly type peelable glue.
Background technology
High tenacity environment-friendly type peelable glue application is very universal, is obtained in fields such as space flight, aviation, machinery, electronics, medical treatment
It is widely applied, but exists that toughness is poor, solidfied material fragility big, impact resistance and vibratility are poor in utilization, easily ftractures
Etc. defect, as sqtructural adhesive, it is necessary to carry out necessary modified toughened, its special technical matters requirement could be met.Mesh
Preceding in the market peelable glue has the following disadvantages：(1) peelable glue on existing market, can be to scraper plate due to containing volatile solvent
Energy, working environment, hardening time length produce influence, complex process, and have corruption to the base material in touch-screen sensor functional blocks
Erosion；(2) can all be remained when peeling off, there is cull, it is necessary to use solvent wiping, this reason mainly due to its poor toughness；(3) may be used
Stripping glue toxicity is larger, and not only solvent has volatilization, cannot be degraded using complete peelable glue discarded object in addition, as pollutant.
The invention of existing some peelable glues domestic at present, such as " peelable glue coating composition, peelable gel coating, peelable glue are applied
The preparation method and application of layer " (application number：201410709409.0), the invention uses acrylate quasi-oligomer, but
It is to employ poisonous dilution monomer, the feature of environmental protection is poor, it is no to use toughening material and pigment, it is not easy to distinguish removal base material
The residual of surface peelable glue.Patent application " peelable glue composition and peelable glue band " (application number：201410161945.1) with " one
Plant UV and solidify peelable gum resin and preparation method thereof " (application number：201510011918.0) acrylic ester combined polymerization, is used
Thing, radiation curing oligomer, radiation curable monomer or its combination and light trigger, the polymer not environmentally, use ultraviolet
There is certain injury to constructor.Patent application " a kind of protection type elastic peelable indigo plant glue and preparation method thereof " (application number：
201510438687.1) product prepared by has used plasticizer, and difficult degradation is not environmentally.
Compared with foregoing invention application, present invention mainly solves peelable glue poor toughness, not environmentally, construct poisonous to human body
The problems such as having radiation, the toughener for being used can effectively improve the toughness of peelable glue, using water-soluble resin, Neng Gou
Degraded in environment, solve environmentally friendly sex chromosome mosaicism, avoid using ultraviolet radioactive in work progress, preferably, easily grasped with security
The advantages of making.
The content of the invention
It is to provide a kind of high tenacity environment-friendly type peelable glue that the purpose of the present invention is, it has good water solubility, film strength
The features such as height, high tenacity, the scope of application is particularly well-suited to cutting, finishing impression, printing, plated film etc. in touch-screen technique than wide
The protection of technique, meets the high request of the combination properties such as some high-tech sector high tenacity environment-friendly types.
It is to provide a kind of preparation method of high tenacity environment-friendly type peelable glue that another object of the present invention is, technique letter
Single, cost is relatively low, asepsis environment-protecting.
To achieve these goals, the present invention uses following technical scheme：
A kind of high tenacity environment-friendly type peelable glue, it is prepared from by the raw material of following mass percent：
A kind of high tenacity environment-friendly type peelable glue, it is prepared from (preferable scope) by the raw material of following mass percent：
A kind of high tenacity environment-friendly type peelable glue, it is prepared from (optimal value) by the raw material of following mass percent：
Described water-soluble resin is aqueous polyacrylamide acid resin, aqueous epoxy resins, waterborne polyurethane resin, aqueous chlorine
Any one in vinegar resin.
Described filler is any one in calcium carbonate, talcum powder, barium sulfate, silica.
Described defoamer is polyether-type class defoamer or organic silicon defoamer.
Described levelling agent is polyacrylic levelling agent.
Described toughener is XNBR or polyvinyl alcohol.
Described pigment is phthalocyanine blue or ultramarine.
A kind of preparation method of high tenacity environment-friendly type peelable glue, it is characterised in that comprise the following steps：
A. water-base resin, water, filler, defoamer, levelling agent, toughener, rheological agent, pigment are weighed in proportion；
B. it is water-base resin is soluble in water and add toughener, stir 1.5-2.5 hour, acquisition mixed liquor；
C. by filler, the above-mentioned mixed liquor of pigment addition, ground 2-5 times with three-roll grinder after stirring, in grinding
The water of surplus is added in material afterwards, is stirred 0.5-2 hours under the conditions of 90-110 DEG C, being stirring evenly and then adding into defoamer is carried out
Defoaming treatment, is eventually adding levelling agent and rheological agent, that is, obtain high tenacity environment-friendly type peelable glue.
Compared with prior art, the present invention has advantages below and beneficial effect：
The present invention has that film strength is good, high temperature resistant, small extension at break the features such as, the scope of application than wide, particularly
The protection of the operation such as cutting, finishing impression, plated film in OGS techniques, meets some high-tech sector heat-resisting quantities and intensity, toughness etc.
The high request of combination property；Process is simple, cost is relatively low, asepsis environment-protecting.
Specific embodiment
Embodiment 1
A kind of high tenacity environment-friendly type peelable glue, it is prepared from (often produce 100kg peelable glues to measure) by following raw material：
| Raw material | Consumption (kg) |
| Aqueous polyacrylamide acid resin | 40 |
| Water | 48.4 |
| Calcium carbonate | 10 |
| Polyether-type class defoamer | 0.3 |
| Polyacrylic levelling agent | 0.1 |
| XNBR | 1 |
| Rheological agent | 0.1 |
| Phthalocyanine blue | 0.1 |
Raw materials used source is as follows：Water-soluble resin is South Korea Han Hua aqueous polyacrylamides acid hard resin, and model is
Soluryl-160；Defoamer is ten thousand one-tenth group's polyether-type defoamers, and model is XWC-753N；Polyacrylic levelling agent is upper
Hai great Pan Chemical Co., Ltd.s product, model is DP-260；XNBR is Sai Kede rubber and plastic Products, and model is
LR-899；Rheological agent is white carbon, Cabot white carbon TS-720.
The preparation method of above-mentioned high tenacity environment-friendly type peelable glue, its step is：
(1) each component is weighed in proportion；
(2) aqueous polyacrylamide acid resin is dissolved in the water of part and adds toughener XNBR, stirring 1.5 is small
When, obtain mixed liquor；
(3) by filler-calcium carbonate, the above-mentioned mixed liquor of pigment addition, ground 4 times with three-roll grinder after stirring,
The water of surplus is added in material after grinding, is stirred 1 hour under the conditions of 90 DEG C, being stirring evenly and then adding into defoamer carries out froth breaking
Treatment, is eventually adding levelling agent and rheological agent, stirs evenly.
Embodiment 2
A kind of high tenacity environment-friendly type peelable glue, it is prepared from (often produce 100kg peelable glues to measure) by following raw material：
Raw materials used source is as follows：Aqueous epoxy resins are Guangzhou Hong Yu trade Co., Ltds product, and model is HY-
100；Organic silicon defoamer is Guangzhou Yu Heng chemical materials Co., Ltd product, and model is Y-698/699；Polyacrylic stream
Flat agent is Shanghai great Pan Chemical Co., Ltd.s product, and model is DP-260；XNBR is Sai Kede rubber and plastic Products,
Model is LR-899；Rheological agent is white carbon, Cabot white carbon TS-720.
The preparation method of above-mentioned high tenacity environment-friendly type peelable glue, its step is：
(1) each component is weighed in proportion,
(2) aqueous epoxy resins are dissolved in the water of part and add toughener XNBR, stirred 2 hours, obtained
Mixed liquor；
(3) by filler talcum powder, the above-mentioned mixed liquor of pigment addition, ground 2 times with three-roll grinder after stirring,
The water of surplus is added in material after grinding, is stirred 0.5 hour under the conditions of 100 DEG C, being stirring evenly and then adding into defoamer is carried out
Defoaming treatment, is eventually adding levelling agent and rheological agent, stirs evenly.
Embodiment 3
A kind of high tenacity environment-friendly type peelable glue, it is prepared from (often produce 100kg peelable glues to measure) by following raw material：
| Raw material | Consumption kg |
| Waterborne polyurethane resin | 55 |
| Water | 7 |
| Barium sulfate | 20 |
| Polyether-type class defoamer | 1 |
| Polyacrylic levelling agent | 1 |
| Polyvinyl alcohol | 10 |
| Rheological agent | 5 |
| Phthalocyanine blue | 1 |
Raw materials used source is as follows：Waterborne polyurethane resin is Dongguan meter Ren Zhan Chemical Co., Ltd.s product, and model is
MR-701；Polyether-type class defoamer is Weifang great Dong Chemical Co., Ltd.s product, and model is DEFOAMER NXZ；Polyacrylic
Levelling agent is Shanghai great Pan Chemical Co., Ltd.s product, and model is DP-260；Polyvinyl alcohol is Beijing Guo Hao chemical companies product,
Model is GH-JY；Rheological agent is white carbon, Cabot white carbon TS-720.
The preparation method of above-mentioned high tenacity environment-friendly type peelable glue, its step is：
(1) each component is weighed in proportion；
(2) waterborne polyurethane resin is dissolved in the water of part and adds toughener polyvinyl alcohol, stirred 2.5 hours, obtained
Mixed liquor；
(3) by filler barium sulfate, the above-mentioned mixed liquor of pigment addition, ground 3 times with three-roll grinder after stirring,
The water of surplus is added in material after grinding, is stirred 1.5 hours under the conditions of 110 DEG C, being stirring evenly and then adding into defoamer is carried out
Defoaming treatment, is eventually adding levelling agent and rheological agent, stirs evenly.
Embodiment 4
A kind of high tenacity environment-friendly type peelable glue, it is prepared from (often produce 100kg peelable glues to measure) by following raw material：
| Raw material | Consumption kg |
| Aqueous vinyl chloride-vinyl acetate resin | 52 |
| Water | 28.4 |
| Silica | 15 |
| Polyether-type class defoamer | 0.1 |
| Polyacrylic levelling agent | 0.2 |
| Polyvinyl alcohol | 3 |
| Rheological agent | 1 |
| Ultramarine | 0.3 |
Raw materials used source is as follows：Water-soluble resin is day to believe aqueous vinyl chloride-vinyl acetate resin, and model is Vinybl a n.
The preparation method of above-mentioned high tenacity environment-friendly type peelable glue, its step is：
(1) each component is weighed in proportion；
(2) aqueous vinyl chloride-vinyl acetate resin is dissolved in the water of part and adds toughener polyvinyl alcohol, stirred 2.5 hours, mixed
Close liquid；
(3) by filler-silicon dioxide, the above-mentioned mixed liquor of pigment addition, ground 5 times with three-roll grinder after stirring,
The water of surplus is added in material after grinding, is stirred 2 hours under the conditions of 90-110 DEG C,
Being stirring evenly and then adding into defoamer carries out defoaming treatment, is eventually adding levelling agent and rheological agent, stirs evenly.
High tenacity environment-friendly type peelable glue described in embodiment 1-4 is detected that testing result is as shown in the table：
When using, by being screen printed onto on PET, ito film and ito glass, after baking film forming, have to object by film
Effect isolation, reaches the effect put dirty, antirust, anti-soda acid, prevent material to be contaminated in subsequent process or scratched.In touch-screen
Before circuit bonding, can be peeled off with simple and easy method, can be once stripped clean, do not had and remain in material surface or pollution material
Material, will not also corrode base material.
Claims (10)
1. a kind of high tenacity environment-friendly type peelable glue, is made up of the raw material of following mass percent：
2. high tenacity environment-friendly type peelable glue according to claim 1, it is characterised in that：
3. high tenacity environment-friendly type peelable glue according to claim 1, it is characterised in that：
4. high tenacity environment-friendly type peelable glue according to claim 1, it is characterised in that described water-soluble resin is aqueous
Polyacrylic resin, aqueous epoxy resins, waterborne polyurethane resin, any one in aqueous vinyl chloride-vinyl acetate resin.
5. high tenacity environment-friendly type peelable glue according to claim 1, it is characterised in that described filler is calcium carbonate, talcum
Any one in powder, barium sulfate, silica.
6. high tenacity environment-friendly type peelable glue according to claim 1, it is characterised in that described defoamer is polyether-type class
Defoamer or organic silicon defoamer.
7. high tenacity environment-friendly type peelable glue according to claim 1, it is characterised in that described levelling agent is polyacrylic acid
Class levelling agent.
8. high tenacity environment-friendly type peelable glue according to claim 1, it is characterised in that described toughener is carboxyl butyronitrile
Rubber or polyvinyl alcohol.
9. high tenacity environment-friendly type peelable glue according to claim 1, it is characterised in that described pigment is phthalocyanine blue or group
It is blue or green.
10. the preparation method of the high tenacity environment-friendly type peelable glue described in claim 1, it is characterised in that comprise the following steps：
A. water-soluble resin, water, filler, defoamer, levelling agent, toughener, rheological agent, pigment are weighed in proportion；
B. it is water-soluble resin is soluble in water and add toughener, stir 1.5-2.5 hour, acquisition mixed liquor；
C. in filler, pigment being added into above-mentioned mixed liquor, 2-5 times is ground with three-roll grinder after stirring, after grinding
The water of surplus is added in material, is stirred 0.5-2 hours under the conditions of 90-110 DEG C, being stirring evenly and then adding into defoamer carries out froth breaking
Treatment, is eventually adding levelling agent and rheological agent, that is, obtain high tenacity environment-friendly type peelable glue.
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| CN201710030144.5A CN106753073B (en) | 2017-01-17 | 2017-01-17 | A kind of high tenacity environment-friendly type peelable glue and preparation method thereof |
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| CN106753073B CN106753073B (en) | 2018-12-11 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110093133A (en) * | 2018-01-29 | 2019-08-06 | 深圳正峰印刷有限公司 | A kind of silk-screen printing aqueous protective glue and preparation method thereof and printing process |
| CN111303724A (en) * | 2020-02-25 | 2020-06-19 | 南京博物院 | Method for removing sludge on surface of wet color-painted pottery after ancient examination |
| CN114106761A (en) * | 2021-11-23 | 2022-03-01 | 广东华鸿科技有限公司 | Sealant composition and preparation method and application thereof |
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| CN102634313A (en) * | 2012-04-23 | 2012-08-15 | 广州市白云化工实业有限公司 | Epoxy conductive resin applicable to binding of LED (light-emitting diode) chips, and preparation method thereof |
| CN106280898A (en) * | 2016-08-29 | 2017-01-04 | 天津美士邦涂料化工有限公司 | A kind of preparation method of high pressure resistant tough epoxy coating |
| CN106318120A (en) * | 2016-08-29 | 2017-01-11 | 天津美士邦涂料化工有限公司 | High-temperature-resistant and tough epoxy coating |
-
2017
- 2017-01-17 CN CN201710030144.5A patent/CN106753073B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102634313A (en) * | 2012-04-23 | 2012-08-15 | 广州市白云化工实业有限公司 | Epoxy conductive resin applicable to binding of LED (light-emitting diode) chips, and preparation method thereof |
| CN106280898A (en) * | 2016-08-29 | 2017-01-04 | 天津美士邦涂料化工有限公司 | A kind of preparation method of high pressure resistant tough epoxy coating |
| CN106318120A (en) * | 2016-08-29 | 2017-01-11 | 天津美士邦涂料化工有限公司 | High-temperature-resistant and tough epoxy coating |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110093133A (en) * | 2018-01-29 | 2019-08-06 | 深圳正峰印刷有限公司 | A kind of silk-screen printing aqueous protective glue and preparation method thereof and printing process |
| CN111303724A (en) * | 2020-02-25 | 2020-06-19 | 南京博物院 | Method for removing sludge on surface of wet color-painted pottery after ancient examination |
| CN111303724B (en) * | 2020-02-25 | 2022-03-18 | 南京博物院 | Method for removing sludge on surface of wet color-painted pottery after ancient examination |
| CN114106761A (en) * | 2021-11-23 | 2022-03-01 | 广东华鸿科技有限公司 | Sealant composition and preparation method and application thereof |
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| CN106753073B (en) | 2018-12-11 |
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Effective date of registration: 20230217 Address after: 448000 Group 7, Xinqiao Village, Ziling Town, Dongbao District, Jingmen City, Hubei Province Patentee after: Jingmen Bochuang Optoelectronics Technology Co.,Ltd. Address before: 448000 No. 33, Xiangshan Avenue, Jingmen, Hubei Patentee before: JINGCHU University OF TECHNOLOGY |