CN106751523A - A kind of high-power LED chip package protection materials - Google Patents

A kind of high-power LED chip package protection materials Download PDF

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Publication number
CN106751523A
CN106751523A CN201611223148.7A CN201611223148A CN106751523A CN 106751523 A CN106751523 A CN 106751523A CN 201611223148 A CN201611223148 A CN 201611223148A CN 106751523 A CN106751523 A CN 106751523A
Authority
CN
China
Prior art keywords
led chip
chip package
power led
protection materials
package protection
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611223148.7A
Other languages
Chinese (zh)
Inventor
王行柱
肖军
吴卫平
肖启振
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Creates A New Mstar Technology Ltd
Original Assignee
Suzhou Creates A New Mstar Technology Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suzhou Creates A New Mstar Technology Ltd filed Critical Suzhou Creates A New Mstar Technology Ltd
Priority to CN201611223148.7A priority Critical patent/CN106751523A/en
Publication of CN106751523A publication Critical patent/CN106751523A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/34Silicon-containing compounds
    • C08K3/36Silica
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/40Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
    • C08G59/50Amines
    • C08G59/5033Amines aromatic

Abstract

The invention discloses a kind of high-power LED chip package protection materials; using bisphenol type liquid epoxies as matrix epoxy resin; aromatic amine with hydrophobicity side chain is used as curing agent; hydrophobic type fused silica is filler, obtains the mono-component liquid epoxy resin protection materials with good water resistance and heat resistance.

Description

A kind of high-power LED chip package protection materials
Technical field
The present invention relates to a kind of high-power LED chip package protection materials.
Background technology
With the progress of LED encapsulation technologies, LED components constantly develop towards miniaturization, slimming, to packaging protection material The heat endurance of material, mechanical strength, electrical insulating property, humidity resistance, thermal coefficient of expansion, internal stress and modulus etc. require constantly to carry It is high.Due to epoxy encapsulation protection materials for non-airtight is encapsulated, its exposure can at leisure absorb moisture, will lead in atmosphere Cause the deterioration of hot property, electrical property and the mechanical property of packaging protection material etc., the service life of final influence product.In addition, The packaging protection material of hydrone is absorbed, weldering can be occurred because of the vaporized expanding of hydrone and be split phenomenon.Therefore, LED encapsulation is protected The wet-hot aging performance of protective material is particularly important to the package reliability of electronic component.
The content of the invention
It is an object of the invention to provide a kind of high-power LED chip package protection materials, with bisphenol type Breakup of Liquid Ring oxygen tree Used as matrix epoxy resin, used as curing agent, hydrophobic type fused silica is filler to the aromatic amine with hydrophobicity side chain to fat, Mono-component liquid epoxy encapsulation protection materials with good water resistance and heat resistance.
To achieve the above object, the technical scheme is that designing a kind of high-power LED chip package protection materials, lead to Cross following steps preparation:
(1), add 130 parts of active fillers to stir 100 parts of bisphenol type liquid epoxies;
(2), above-mentioned material is uniform through high speed dispersor, double planetary mixer, three-roll grinder grinding distribution;
(3), vacuum purify add after bubble 35 parts of curing agent and 4 accelerator are well mixed and vacuum purify be poured into after bubble it is anti- Answer in device;
(4), carry out by 120 DEG C of conditions of cure solidification 30min after the packaging protection material is obtained.
Preferably, described curing agent is modified aromatic amine.
Preferably, described accelerator is modified imidazole.
Preferably, described active filler is melting silicon powder.
The advantages of the present invention are:Using modified melting silicon powder in water resistance and thermal coefficient of expansion side Face, due to crystallization silicon powder and calcium carbonate, is conducive to improving the heat resistance and water resistance of encapsulating material;Bisphenol-A epoxy tree Fat is favorably improved the heat resistance of encapsulating material as matrix epoxy resin.
Specific embodiment
With reference to embodiment, specific embodiment of the invention is further described.Following examples are only used for more Plus technical scheme is clearly demonstrated, and can not be limited the scope of the invention with this.
The present invention specific implementation technical scheme be:
130 parts of active fillers are added to stir 100 parts of bisphenol type liquid epoxies;By above-mentioned material through telling dispersion Machine, double planetary mixer, three-roll grinder grinding distribution are uniform;Vacuum adds 35 parts of curing agent and 4 accelerator after purifying bubble Well mixed and vacuum is poured into reactor after purifying bubble;Institute is obtained after carrying out solidification 30min by 120 DEG C of conditions of cure State packaging protection material.Described curing agent is modified aromatic amine;Described accelerator is modified imidazole;Described active filler It is melting silicon powder.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, on the premise of the technology of the present invention principle is not departed from, some improvements and modifications can also be made, these improvements and modifications Also should be regarded as protection scope of the present invention.

Claims (5)

1. a kind of high-power LED chip package protection materials, it is characterised in that including bisphenol type liquid epoxies, curing agent, Active filler and accelerator are according to 100: 35:130:4 ratio is mixed to prepare.
2. high-power LED chip package protection materials according to claim 1, it is characterised in that make as follows It is standby:
(1), add 130 parts of active fillers to stir 100 parts of bisphenol type liquid epoxies;
(2), by above-mentioned material through telling dispersion machine, double planetary mixer, three-roll grinder grinding distribution uniform;
(3), vacuum purify add after bubble 35 parts of curing agent and 4 accelerator are well mixed and vacuum purify be poured into after bubble it is anti- Answer in device;
(4), carry out by 120 DEG C of conditions of cure solidification 30min after the packaging protection material is obtained.
3. high-power LED chip package protection materials according to claim 2, it is characterised in that described curing agent is Modified aromatic amine.
4. high-power LED chip package protection materials according to claim 2, it is characterised in that described accelerator is Modified imidazole.
5. high-power LED chip package protection materials according to claim 2, it is characterised in that described active filler It is melting silicon powder.
CN201611223148.7A 2016-12-27 2016-12-27 A kind of high-power LED chip package protection materials Pending CN106751523A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611223148.7A CN106751523A (en) 2016-12-27 2016-12-27 A kind of high-power LED chip package protection materials

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611223148.7A CN106751523A (en) 2016-12-27 2016-12-27 A kind of high-power LED chip package protection materials

Publications (1)

Publication Number Publication Date
CN106751523A true CN106751523A (en) 2017-05-31

Family

ID=58925468

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611223148.7A Pending CN106751523A (en) 2016-12-27 2016-12-27 A kind of high-power LED chip package protection materials

Country Status (1)

Country Link
CN (1) CN106751523A (en)

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101864146A (en) * 2010-06-13 2010-10-20 宏昌电子材料股份有限公司 Epoxy resin composition for printed circuit copper-clad plate
CN102031081A (en) * 2010-11-26 2011-04-27 烟台德邦电子材料有限公司 Liquid epoxy encapsulating material and preparation method thereof
CN102086365A (en) * 2010-12-27 2011-06-08 东莞市腾威电子材料技术有限公司 Adhesive, preparation method and application in integrated circuit board embedment thereof
CN102382421A (en) * 2011-09-16 2012-03-21 汕头市骏码凯撒有限公司 Liquid epoxy resin packaging material and preparation method thereof
CN102585440A (en) * 2012-01-16 2012-07-18 广州宏仁电子工业有限公司 High-CTI (comparative tracking index) halogen-free flame retardant resin composition for copper-clad laminate
CN102850724A (en) * 2012-09-27 2013-01-02 江苏中鹏新材料股份有限公司 Green and environment-friendly epoxy resin composition for high-power device packaging
CN104610701A (en) * 2015-01-14 2015-05-13 景旺电子科技(龙川)有限公司 Insulating layer material, stainless steel based copper clad plate, surface treatment method and preparation method
CN105838030A (en) * 2012-07-20 2016-08-10 纳美仕有限公司 Liquid sealing material and electronic component using same

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101864146A (en) * 2010-06-13 2010-10-20 宏昌电子材料股份有限公司 Epoxy resin composition for printed circuit copper-clad plate
CN102031081A (en) * 2010-11-26 2011-04-27 烟台德邦电子材料有限公司 Liquid epoxy encapsulating material and preparation method thereof
CN102086365A (en) * 2010-12-27 2011-06-08 东莞市腾威电子材料技术有限公司 Adhesive, preparation method and application in integrated circuit board embedment thereof
CN102382421A (en) * 2011-09-16 2012-03-21 汕头市骏码凯撒有限公司 Liquid epoxy resin packaging material and preparation method thereof
CN102585440A (en) * 2012-01-16 2012-07-18 广州宏仁电子工业有限公司 High-CTI (comparative tracking index) halogen-free flame retardant resin composition for copper-clad laminate
CN105838030A (en) * 2012-07-20 2016-08-10 纳美仕有限公司 Liquid sealing material and electronic component using same
CN102850724A (en) * 2012-09-27 2013-01-02 江苏中鹏新材料股份有限公司 Green and environment-friendly epoxy resin composition for high-power device packaging
CN104610701A (en) * 2015-01-14 2015-05-13 景旺电子科技(龙川)有限公司 Insulating layer material, stainless steel based copper clad plate, surface treatment method and preparation method

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Application publication date: 20170531