CN106748702B - 一种升华法生产对苯醌的设备 - Google Patents
一种升华法生产对苯醌的设备 Download PDFInfo
- Publication number
- CN106748702B CN106748702B CN201710031191.1A CN201710031191A CN106748702B CN 106748702 B CN106748702 B CN 106748702B CN 201710031191 A CN201710031191 A CN 201710031191A CN 106748702 B CN106748702 B CN 106748702B
- Authority
- CN
- China
- Prior art keywords
- sublimator
- pipe
- benzoquinone
- tube
- communicated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 title claims abstract description 112
- 238000005092 sublimation method Methods 0.000 title claims abstract description 10
- 239000000428 dust Substances 0.000 claims abstract description 26
- 238000003756 stirring Methods 0.000 claims abstract description 24
- 238000010438 heat treatment Methods 0.000 claims abstract description 22
- 230000005540 biological transmission Effects 0.000 claims abstract description 4
- 238000007599 discharging Methods 0.000 claims description 26
- 239000002994 raw material Substances 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 229910052751 metal Inorganic materials 0.000 claims description 13
- 239000002184 metal Substances 0.000 claims description 13
- 239000013078 crystal Substances 0.000 claims description 12
- 238000004519 manufacturing process Methods 0.000 claims description 10
- 238000000859 sublimation Methods 0.000 claims description 9
- 230000008022 sublimation Effects 0.000 claims description 9
- 238000005245 sintering Methods 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 7
- 239000012530 fluid Substances 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 4
- 239000007921 spray Substances 0.000 claims description 4
- 238000005485 electric heating Methods 0.000 claims description 3
- 239000010410 layer Substances 0.000 description 45
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 7
- 229910052748 manganese Inorganic materials 0.000 description 7
- 239000011572 manganese Substances 0.000 description 7
- 239000012065 filter cake Substances 0.000 description 6
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 4
- 239000002699 waste material Substances 0.000 description 4
- 239000006096 absorbing agent Substances 0.000 description 3
- 238000004891 communication Methods 0.000 description 3
- 239000005457 ice water Substances 0.000 description 3
- 230000035939 shock Effects 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 239000002356 single layer Substances 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C46/00—Preparation of quinones
- C07C46/10—Separation; Purification; Stabilisation; Use of additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0003—Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D7/00—Sublimation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710031191.1A CN106748702B (zh) | 2017-01-17 | 2017-01-17 | 一种升华法生产对苯醌的设备 |
Applications Claiming Priority (1)
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---|---|---|---|
CN201710031191.1A CN106748702B (zh) | 2017-01-17 | 2017-01-17 | 一种升华法生产对苯醌的设备 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106748702A CN106748702A (zh) | 2017-05-31 |
CN106748702B true CN106748702B (zh) | 2023-09-01 |
Family
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Family Applications (1)
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CN201710031191.1A Active CN106748702B (zh) | 2017-01-17 | 2017-01-17 | 一种升华法生产对苯醌的设备 |
Country Status (1)
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CN (1) | CN106748702B (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107596720B (zh) * | 2017-09-18 | 2020-05-05 | 福建南平青松化工有限公司 | 一种用于合成樟脑连续升华、凝华的成套设备及其控制工艺 |
Citations (16)
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US2743168A (en) * | 1944-09-09 | 1956-04-24 | Krohn Roy | Sublimation apparatus |
GB1172165A (en) * | 1966-02-09 | 1969-11-26 | Commissariat Energie Atomique | Apparatus for the Continuous Purification of Sublimable Substances |
GB1275232A (en) * | 1969-04-16 | 1972-05-24 | Diamond Shamrock Corp | Improvements in or relating to sublimation processes |
SU574478A1 (ru) * | 1971-10-18 | 1977-09-30 | Предприятие П/Я Г-4911 | Установка дл комплексной переработки полиметаллического сырь |
CN1388127A (zh) * | 2001-05-29 | 2003-01-01 | 张国瑞 | 一种均苯四甲酸二酐的捕集工艺方法及设备 |
DE10345841A1 (de) * | 2003-09-30 | 2005-04-14 | Umwelt- und Gebäudetechnik 2000 GmbH | Verfahren zur Entfernung von Tetramethylsuccinodinitril aus Abluft |
CN101721835A (zh) * | 2008-10-21 | 2010-06-09 | 沈善明 | 连续真空动态升华凝华机 |
CN102070519A (zh) * | 2010-12-06 | 2011-05-25 | 横店集团东阳英洛华绿色电化学有限公司 | 一种3,4,5,6-四氯-2-氰基吡啶凝华捕集提纯的方法、捕集器及其装置系统 |
CN102085422A (zh) * | 2009-12-08 | 2011-06-08 | 沈善明 | 连续真空动态升华凝华机 |
CN102596804A (zh) * | 2009-09-15 | 2012-07-18 | Ii-Vi有限公司 | SiC单晶的升华生长 |
CN202398139U (zh) * | 2011-08-31 | 2012-08-29 | 华南理工大学 | 一种卧式螺旋推进式超声冷却结晶机 |
CN203513537U (zh) * | 2013-08-27 | 2014-04-02 | 仙桃市康化科技有限公司 | 对苯醌循环结晶装置 |
CN204582599U (zh) * | 2015-02-06 | 2015-08-26 | 赵雪林 | 高效升华重结晶分离精制装置 |
CN104926635A (zh) * | 2015-06-19 | 2015-09-23 | 湖北开元化工科技股份有限公司 | 一种从苯胺氧化料中升华得到对苯醌的方法 |
CN205373435U (zh) * | 2015-12-24 | 2016-07-06 | 天津市布加迪环保科技发展有限公司 | 冷凝水汽化换热系统 |
CN206396084U (zh) * | 2017-01-17 | 2017-08-11 | 湖北开元化工科技股份有限公司 | 一种升华法生产对苯醌的设备 |
-
2017
- 2017-01-17 CN CN201710031191.1A patent/CN106748702B/zh active Active
Patent Citations (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2743168A (en) * | 1944-09-09 | 1956-04-24 | Krohn Roy | Sublimation apparatus |
GB1172165A (en) * | 1966-02-09 | 1969-11-26 | Commissariat Energie Atomique | Apparatus for the Continuous Purification of Sublimable Substances |
GB1275232A (en) * | 1969-04-16 | 1972-05-24 | Diamond Shamrock Corp | Improvements in or relating to sublimation processes |
SU574478A1 (ru) * | 1971-10-18 | 1977-09-30 | Предприятие П/Я Г-4911 | Установка дл комплексной переработки полиметаллического сырь |
CN1388127A (zh) * | 2001-05-29 | 2003-01-01 | 张国瑞 | 一种均苯四甲酸二酐的捕集工艺方法及设备 |
DE10345841A1 (de) * | 2003-09-30 | 2005-04-14 | Umwelt- und Gebäudetechnik 2000 GmbH | Verfahren zur Entfernung von Tetramethylsuccinodinitril aus Abluft |
CN101721835A (zh) * | 2008-10-21 | 2010-06-09 | 沈善明 | 连续真空动态升华凝华机 |
CN102596804A (zh) * | 2009-09-15 | 2012-07-18 | Ii-Vi有限公司 | SiC单晶的升华生长 |
CN102085422A (zh) * | 2009-12-08 | 2011-06-08 | 沈善明 | 连续真空动态升华凝华机 |
CN102070519A (zh) * | 2010-12-06 | 2011-05-25 | 横店集团东阳英洛华绿色电化学有限公司 | 一种3,4,5,6-四氯-2-氰基吡啶凝华捕集提纯的方法、捕集器及其装置系统 |
CN202398139U (zh) * | 2011-08-31 | 2012-08-29 | 华南理工大学 | 一种卧式螺旋推进式超声冷却结晶机 |
CN203513537U (zh) * | 2013-08-27 | 2014-04-02 | 仙桃市康化科技有限公司 | 对苯醌循环结晶装置 |
CN204582599U (zh) * | 2015-02-06 | 2015-08-26 | 赵雪林 | 高效升华重结晶分离精制装置 |
CN104926635A (zh) * | 2015-06-19 | 2015-09-23 | 湖北开元化工科技股份有限公司 | 一种从苯胺氧化料中升华得到对苯醌的方法 |
CN205373435U (zh) * | 2015-12-24 | 2016-07-06 | 天津市布加迪环保科技发展有限公司 | 冷凝水汽化换热系统 |
CN206396084U (zh) * | 2017-01-17 | 2017-08-11 | 湖北开元化工科技股份有限公司 | 一种升华法生产对苯醌的设备 |
Non-Patent Citations (1)
Title |
---|
沈善明.一种新型连续升华凝华机的介绍.《医药工程设计》.2010,第31卷(第3期),第1-3页. * |
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Legal Events
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PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20231008 Address after: Intersection of Gaoshigang Road and Majiachong Road, Yaojiagang Chemical Park, Zhijiang City, Yichang City, Hubei Province 443200 Patentee after: Hubei Preti Chemical Technology Co.,Ltd. Address before: 443200 Intersection of Shibeishan Road and Shuangshouqiao Road in Majiadian, Zhijiang City, Yichang City, Hubei Province Patentee before: HUBEI KAIYUAN CHEMICALS & TECHNOLOGY Co.,Ltd. |
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TR01 | Transfer of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A sublimation method for producing p-benzoquinone equipment Granted publication date: 20230901 Pledgee: Bank of China Limited by Share Ltd. Three Gorges Branch Pledgor: Hubei Preti Chemical Technology Co.,Ltd. Registration number: Y2024980004557 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |