CN106747616A - One kind is based on diatomaceous porous ceramic tile and preparation method thereof - Google Patents

One kind is based on diatomaceous porous ceramic tile and preparation method thereof Download PDF

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Publication number
CN106747616A
CN106747616A CN201611013869.5A CN201611013869A CN106747616A CN 106747616 A CN106747616 A CN 106747616A CN 201611013869 A CN201611013869 A CN 201611013869A CN 106747616 A CN106747616 A CN 106747616A
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CN
China
Prior art keywords
ceramic tile
porous ceramic
diatomaceous
diatomite
preparation
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611013869.5A
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Chinese (zh)
Inventor
王福明
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YINGKOU BOHAI TECHNOLOGY Co Ltd
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YINGKOU BOHAI TECHNOLOGY Co Ltd
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Priority to CN201611013869.5A priority Critical patent/CN106747616A/en
Publication of CN106747616A publication Critical patent/CN106747616A/en
Pending legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B28—WORKING CEMENT, CLAY, OR STONE
    • B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B11/00—Apparatus or processes for treating or working the shaped or preshaped articles
    • B28B11/14—Apparatus or processes for treating or working the shaped or preshaped articles for dividing shaped articles by cutting
    • B28B11/16—Apparatus or processes for treating or working the shaped or preshaped articles for dividing shaped articles by cutting for extrusion or for materials supplied in long webs
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B28—WORKING CEMENT, CLAY, OR STONE
    • B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B11/00—Apparatus or processes for treating or working the shaped or preshaped articles
    • B28B11/24—Apparatus or processes for treating or working the shaped or preshaped articles for curing, setting or hardening
    • B28B11/243—Setting, e.g. drying, dehydrating or firing ceramic articles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B28—WORKING CEMENT, CLAY, OR STONE
    • B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B3/00—Producing shaped articles from the material by using presses; Presses specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B28—WORKING CEMENT, CLAY, OR STONE
    • B28C—PREPARING CLAY; PRODUCING MIXTURES CONTAINING CLAY OR CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28C5/00—Apparatus or methods for producing mixtures of cement with other substances, e.g. slurries, mortars, porous or fibrous compositions
    • B28C5/003—Methods for mixing
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/14—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62204—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products using waste materials or refuse
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/06—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances
    • C04B38/063—Preparing or treating the raw materials individually or as batches
    • C04B38/0635—Compounding ingredients
    • C04B38/0645—Burnable, meltable, sublimable materials
    • C04B38/0675—Vegetable refuse; Cellulosic materials, e.g. wood chips, cork, peat, paper
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/08—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by adding porous substances
    • E—FIXED CONSTRUCTIONS
    • E04—BUILDING
    • E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
    • E04F13/00—Coverings or linings, e.g. for walls or ceilings
    • E04F13/07—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor
    • E04F13/072—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor composed of specially adapted, structured or shaped covering or lining elements
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427—Silicates other than clay, e.g. water glass
    • C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
    • C04B2235/3472—Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/349—Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Structural Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Architecture (AREA)
  • Inorganic Chemistry (AREA)
  • Civil Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Press-Shaping Or Shaping Using Conveyers (AREA)
  • Finishing Walls (AREA)

Abstract

The invention discloses one kind based on diatomaceous porous ceramic tile and preparation method thereof, it is described that side (1), hole (2), muscle (3) and groove (4) are included based on diatomaceous porous ceramic tile, porous ceramic tile surrounding is surrounded by side (1), centre is provided with some uniform circular or square holes (2), connected by muscle (3) between some uniform holes (2), if the groove (4) that the side on four sides is provided with cladding mud oar is constituted；The surface of the porous ceramic tile is smooth.The preparation method based on diatomaceous porous ceramic tile, including：After dispensing, mud refining, extrusion molding, blank shaping, it is dried, is burnt till；Wherein, raw material proportioning is：Diatomite 60% 80%；Flyash 20% 30%；Wood chip 5% 10%.The present invention is based on diatomaceous porous ceramic tile, with diatomite as major ingredient, with good environmental-protecting performance.

Description

One kind is based on diatomaceous porous ceramic tile and preparation method thereof
Technical field
It is more particularly to a kind of to be based on diatomaceous porous ceramic tile and its preparation side the present invention relates to architectural decoration material field Method.
Background technology
Diatomite is after ancient times unicellular rudimentary plant diatom remains are piled up, by diagenesis under certain geological conditions It is to deposit what is formed by the dead later remains of diatom and the one kind for being formed has porous biogenic deposit rock, essential mineral Composition is opal and its mutation, and chemical composition is mainly SiO2, and contain a small amount of Al2O3、Fe2O3、CaO、Na2O, MgO etc. With the impurity such as organic matter.Diatomaceous color is white, canescence, grey and terra brown etc..Have multistage, big on diatom wall shell Amount, the microcellular structure of ordered arrangement so that diatomite has many excellent properties：Light weight, surface area are big, porosity High, adsorptive liquid ability is strong, fusing point is high；Chemical stability is high, insoluble in hydrochloric acid, is soluble in alkali；With relative Incoercibility, Matter is soft, sound insulation, many excellent properties such as wear-resisting, heat-resisting, therefore diatomite at home and abroad have been obtained for extensive exploitation with should With market application foreground is infinitely wide.
Traditional ceramic tile is solid ceramic tile, its own weight weight, and is not incubated, and the feature of environmental protection is poor, easily discharges pollutant And indoor air pollutants can not be absorbed.Environment-friendly type indoor hardware fitting with many micropore matter diatomite as raw material, such as diatomite Coating, wallpaper, sheet material and brick material etc., particularly the state such as Japan is increasingly subject to the favor of consumer and likes abroad.But, Diatomite environmental protection decoration materials do not obtain substantial amounts of popularization and application also at home at present, and the technical research of related fields also just just rises Step.
The content of the invention
Asked to solve the poor existing ceramic tile feature of environmental protection, easy release pollutant and the technologies such as indoor air pollutants can not be absorbed Topic, the present invention provides a kind of based on diatomaceous porous ceramic tile and preparation method thereof.
The present invention provides a kind of based on diatomaceous porous ceramic tile, including side (1), hole (2), muscle (3) and groove (4), many Hole ceramic tile surrounding is surrounded by side (1), and centre is provided with some uniform circular or square holes (2), between some uniform holes (2) Connected by muscle (3), if the groove (4) that the side on four sides is provided with cladding mud oar is constituted；The surface of the porous ceramic tile is smooth.
Preferably, the thickness of the porous ceramic tile is 5-20mm.
Corresponding, the present invention also provides a kind of preparation method based on diatomaceous porous ceramic tile, by following raw material by weight Amount per distribution ratio constitutes and is：Diatomite 60%-80%；Flyash 20%-30%；Wood chip 5%-10%；The diatomite porous guarantor The manufacture method of warm brick, (1) dispensing：Flux is fitted into ball grinder with material ball ratio 1: 2,5~6 h are mixed with dry ball milling； The flux that will be well mixed is added in diatomite, flyash, wood chip mixture, and is fitted into ball grinder with material ball ratio 1: 2, is adopted Mix 60 min with dry ball milling and diatomite compound is obtained；(2) mud refining：Dispensing is sent into roller after twisting refining well in tank diameter Machine is crushed, and makes mixing pug, control moisture content ＜ 28%, plasticity of slurry index 8-12；(3) extrusion molding：In mud extruder In squeeze out porous mud bar adobe cut into by blank cutter, control crushing strength (0.8-1.0) MPa；(4) it is right after blank shaping It is dried, burns till.
Preferably, raw material per distribution ratio by weight constitutes its optimum proportioning and is：Diatomite 65%；Flyash 26%；Wood chip 9%.
Preferably, the flux be pyrophillite, spodumene, albite and talcum etc. prepare according to a certain percentage and Into its preferred mass ratio is 2: 3：3:2.
Preferably, flux and diatomaceous mass ratio are 1 during described:20~30.
Beneficial effect：The present invention is based on diatomaceous porous ceramic tile, with diatomite as major ingredient, so with good environmental protection Performance, can adsorb indoor air pollutants, while heat-insulation and heat-preservation, fire protecting performance, high temperature resistant, long service life again, its volume Density is small, and larger alleviates building load.Preparation method process is simple, the technique mistake of diatomaceous porous ceramic tile are based on simultaneously Journey is easily controllable, is conducive to industrialized realization, with wide business and market prospects.
Brief description of the drawings
Fig. 1 is structural representation of the present invention based on diatomaceous porous ceramic tile.
Specific embodiment
With reference to embodiment, the present invention is described in detail.
The embodiment of the present invention provides a kind of based on diatomaceous porous ceramic tile, including side (1), hole (2), muscle (3) and groove (4), porous ceramic tile surrounding is surrounded by side (1), and centre is provided with some uniform circular or square holes (2), some uniform holes (2) connected by muscle (3) between, if the groove (4) that the side on four sides is provided with cladding mud oar is constituted；The surface of the porous ceramic tile It is smooth.The thickness of the porous ceramic tile is 5-20mm.
The embodiment of the present invention also provides a kind of preparation method based on diatomaceous porous ceramic tile, by following raw material by weight Per distribution ratio is constituted：Diatomite 60%-80%；Flyash 20%-30%；Wood chip 5%-10%；The diatomite porous insulation The manufacture method of brick, (1) dispensing：Flux is fitted into ball grinder with material ball ratio 1: 2,5~6 h are mixed with dry ball milling；Will Well mixed flux is added in diatomite, flyash, wood chip mixture, and is fitted into ball grinder with material ball ratio 1: 2, is used Dry ball milling mixes 60 min and diatomite compound is obtained；(2) mud refining：Dispensing sends into twin rollers after twisting refining well in tank diameter Crush, make mixing pug, control moisture content ＜ 28%, plasticity of slurry index 8-12；(3) extrusion molding：In mud extruder Squeeze out porous mud bar and adobe is cut into by blank cutter, control crushing strength (0.8-1.0) MPa；(4) after blank shaping, to it It is dried, burns till.
Wherein, raw material per distribution ratio by weight constitutes its optimum proportioning and is：Diatomite 65%；Flyash 26%；Wood chip 9%.The flux is that pyrophillite, spodumene, albite and talcum etc. are formulated according to a certain percentage, its preferred mass Than being 2: 3：3:2.Flux and diatomaceous mass ratio are 1 during described:20~30.
In addition, the calcining system of the porous ceramic tile is：The min of room temperature~180 DEG C heating-up time 6,180~350 DEG C of intensifications The min of time 12,350~950 DEG C of min of heating-up times 30,950~1050 DEG C of min of heating-up times 8,1050 DEG C of insulations 40 Min, 1050~800 DEG C are lowered the temperature with stove, and 800~300 DEG C of blow-on coolings, 300 DEG C~room temperature is lowered the temperature with stove.
Above content is the further description done to the present invention with reference to optimal technical scheme, it is impossible to assert invention Specific implementation is only limitted to these explanations.For general technical staff of the technical field of the invention, the present invention is not being departed from Design on the premise of, can also make it is simple deduce and replace, should all be considered as protection scope of the present invention.

Claims (6)

1. it is a kind of to be based on diatomaceous porous ceramic tile, including side (1), hole (2), muscle (3) and groove (4), it is characterised in that porous Ceramic tile surrounding is surrounded by side (1), centre be provided with some uniform circular or square holes (2), between some uniform holes (2) by Muscle (3) is connected, if the groove (4) that the side on four sides is provided with cladding mud oar is constituted；The surface of the porous ceramic tile is smooth.
2. it is according to claim 1 based on diatomaceous porous ceramic tile, it is characterised in that the thickness of the porous ceramic tile is 5-20mm。
3. a kind of preparation method based on diatomaceous porous ceramic tile, it is characterised in that by following raw material per distribution ratio by weight Constitute and be：Diatomite 60%-80%；Flyash 20%-30%；Wood chip 5%-10%；The manufacture of the diatomite porous thermal insulation brick Method, (1) dispensing：Flux is fitted into ball grinder with material ball ratio 1: 2,5~6 h are mixed with dry ball milling；Will be well mixed Flux add diatomite, flyash, in wood chip mixture, and be fitted into ball grinder with material ball ratio 1: 2, using dry ball milling Mix 60 min and diatomite compound is obtained；(2) mud refining：Dispensing is sent into twin rollers and is crushed after twisting refining well in tank diameter, is allowed to As mixing pug, control moisture content ＜ 28%, plasticity of slurry index 8-12；(3) extrusion molding：Squeezed out in mud extruder porous Mud bar cuts into adobe by blank cutter, controls crushing strength (0.8-1.0) MPa；(4) after blank shaping, it is dried, is burnt Into.
4. the preparation method based on diatomaceous porous ceramic tile according to claim 3, it is characterised in that raw material is by weight Per distribution ratio constitutes its optimum proportioning：Diatomite 65%；Flyash 26%；Wood chip 9%.
5. the preparation method based on diatomaceous porous ceramic tile according to claim 3, it is characterised in that the flux For pyrophillite, spodumene, albite and talcum etc. are formulated according to a certain percentage, its preferred mass ratio is 2: 3：3:2.
6. the preparation method based on diatomaceous porous ceramic tile according to claim 3 or 5, it is characterised in that the mistake Flux and diatomaceous mass ratio are 1 in journey:20~30.
CN201611013869.5A 2016-11-18 2016-11-18 One kind is based on diatomaceous porous ceramic tile and preparation method thereof Pending CN106747616A (en)

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Application Number Priority Date Filing Date Title
CN201611013869.5A CN106747616A (en) 2016-11-18 2016-11-18 One kind is based on diatomaceous porous ceramic tile and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201611013869.5A CN106747616A (en) 2016-11-18 2016-11-18 One kind is based on diatomaceous porous ceramic tile and preparation method thereof

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108997002A (en) * 2018-08-10 2018-12-14 张家港市沐和新材料技术开发有限公司 A kind of preparation method of Diatomite-based Porous Ceramics material
CN109824350A (en) * 2019-02-25 2019-05-31 高阳 A kind of preparation method of ceramics resistant brick
CN110091426A (en) * 2019-05-23 2019-08-06 佛山市思特四通化工有限公司 A kind of manufacturing equipment and preparation method thereof of honeycomb structure ceramics ceramic tile

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108997002A (en) * 2018-08-10 2018-12-14 张家港市沐和新材料技术开发有限公司 A kind of preparation method of Diatomite-based Porous Ceramics material
CN109824350A (en) * 2019-02-25 2019-05-31 高阳 A kind of preparation method of ceramics resistant brick
CN110091426A (en) * 2019-05-23 2019-08-06 佛山市思特四通化工有限公司 A kind of manufacturing equipment and preparation method thereof of honeycomb structure ceramics ceramic tile

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