CN106739752A - A kind of preparation method of rose immortality flower - Google Patents
A kind of preparation method of rose immortality flower Download PDFInfo
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- CN106739752A CN106739752A CN201611203740.0A CN201611203740A CN106739752A CN 106739752 A CN106739752 A CN 106739752A CN 201611203740 A CN201611203740 A CN 201611203740A CN 106739752 A CN106739752 A CN 106739752A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C5/00—Processes for producing special ornamental bodies
- B44C5/06—Natural ornaments; Imitations thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N3/00—Preservation of plants or parts thereof, e.g. inhibiting evaporation, improvement of the appearance of leaves or protection against physical influences such as UV radiation using chemical compositions; Grafting wax
- A01N3/02—Keeping cut flowers fresh chemically
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Abstract
The invention discloses a kind of preparation method of rose immortality flower, by fixation, rinsing, dehydration, decolouring, dye and shield shape, the series of process such as drying, making obtains rose immortality flower, with method is easy, shield shape effect substantially, uniform in color, not fugitive color, effect advantage true to nature.
Description
Technical field
The invention belongs to immortality flower processing technique field, and in particular to a kind of preparation method of rose immortality flower.
Background technology
Immortality flower, also known as preserved flower, ecological flower, forever amaranthine fresh flower, it is with rose, carnation, iris, silk ball
Etc. the Fresh Cutting flower of category, using high-tech means, processed by a series of complex operations such as dehydration, decolouring, drying, dyeing
Dried flower, be generally possible to the year of preservation 2~3, or even 5 years.Immortality flower changes conventional cut flower vase short life, views and admires
Phase short shortcoming, substantially prolongs flowers views and admires the life-span.Because immortality spends novelty, ornamental value is high, it is adaptable to indoor dress
Repair, household is displayed, wedding is live, the friend that escorts the bride to the groom's home or the wedding hall expresses friendship etc. with lover, liked by consumer deeply.
At present, if the published patent about immortality flower preparation method of State Intellectual Property Office of the People's Republic of China has
Dry, corresponding flowers have Chinese rose (publication number CN105660610A), lotus flower (publication number CN105191911A), lotus respectively
(publication number CN105211055A), laurustinus (publication number CN105052898A), camellia (publication number CN105145976A) etc., forever
Raw flower patent numbers and flowers species used are few, it is difficult to meet huge demand and personalized system of the consumer to all kinds of flowers examination material
Provisioning request, is more missing from simultaneously for the deep rose immortality flower preparation method liked by China traditional consumer.Further, since
All kinds of flowers corolla biological natures (shape, size, color, lobed, quality etc.) come in every shape, and vary, a kind of immortality flower
Manufacture craft, physico-chemical process are dfficult to apply to all of flowers examination material, therefore, exploring the preparation method of rose immortality flower is
One is highly desirable to, and problem in the urgent need to address.
The content of the invention
It is an object of the invention to overcome the deficiencies in the prior art part, there is provided a kind of making side of rose immortality flower
Method, by fixation, rinsing, dehydration, decolouring, dye and shield shape, the series of process such as drying, makes a kind of rose immortality flower, has
Method is easy, shield shape effect is obvious, uniform in color, non-fading advantage.
The technical solution adopted for the present invention to solve the technical problems is：
A kind of preparation method of rose immortality flower, including：
1) it is fixed：Rose Fresh Cut Flowers are taken, is cut at least 1cm under calyx, be immersed in FAA fixers, it is quiet
Put 22~26h of immersion；Fixed main purpose is to preserve rose tissue inner cell form, structure and its composition, is bordering on it
Animation, while having anti-corrosion and the effect for preserving concurrently.
2) rinse：Take step 1) rose that obtains, with 45~55% ethanol rinse 2~5 times；The purpose of rinsing is removal
Fixer, meanwhile, it is subsequently to be prepared using moisture in ethanol removing rose tissue.
3) it is dehydrated：Take step 2) rose that obtains, it is immersed in 45~55% ethanol, it is standing and soak for 10~14h；Then
10~14h is standing and soak for successively with 55~65%, 65~75%, 75~85%, 85~95% ethanol successively；Finally use anhydrous second
Alcohol is standing and soak for 45~50h；The ethanol of high concentration is used for also causing phytoprotein to be denatured while removing moisture, increased
Plant tissue continues the difficulty being dehydrated；And be dehydrated using the ethanol of increasing concen-trations, water separation capability progressively strengthens, and can overcome
The increased influence of dehydration difficulty that protein denaturation is brought, so as to ensure that dehydration is complete；
4) decolourize：Take step 3) rose that obtains, it is immersed in volume ratio 0.8~1.2:0.8~1.2 EtOH-MeOH
In mixed liquor, while adding acetic acid according to the amount of 12~18ml/, 22~26h is standing and soak for；Decolouring is to make use of polar molecule
Readily soluble principle, methyl alcohol in EtOH-MeOH mixed liquor is easily combined as a whole and separates out plant with the main component of pigment,
It is dissolved into mixed liquor；And acetic acid is acid, for softening rose tissue, increase cell permeability, so that intracellular
Pigment is easier to separate out；
The present invention first removes the moisture in rose, then in ethanol-first using dehydration and the method for successively carrying out of decolourizing
Decolourized in alcohol mixed liquor, now the pigment in rose cell can fully be combined with methyl alcohol and molten be integrated and fully analyse
Go out, it is ensured that decolourize complete.If dehydration and decolouring are carried out, due to the presence of moisture simultaneously, it will reduce methyl alcohol and pigment is combined
Speed, cause to decolourize incomplete.
5) dye and shield shape：Take step 4) rose that obtains, it is immersed in volume ratio 0.8~1.2:0.8~1.2 second
In alcohol-methyl alcohol mixed liquor, while acetic acid and polyethylene glycol are separately added into according to the amount of 25~35ml/ and 45~55ml/, and
Fresh flower special stain therefor is added, 20~50h is standing and soak for；Polyethylene glycol can fix rose cell wall and membrane structure,
It is allowed to keep excellent in shape；Liquid macrogol PEG400, mean molecule quantity 380-420, concentration are used in this method
50%.
The coloring agent used in this method, one is commercially available dyeing powder；Two is watercolor board pen ink, and brand has more imperial, Deli/ to obtain
Power etc., above-mentioned two class is used alone, and works well.
6) dry：Take step 5) rose that obtains, rose is gently wrapped up using the food fresh-keeping film of uniform punching
One circle, in then putting the container equipped with silica-gel desiccant into, sealing dries 20~50h, takes out, be placed in 1 at shady and cool ventilation~
4d, obtains final product rose immortality flower.In drying process, there is speed difference in roseleaf, easily cause flower due to inside and outside liquid evaporation
Valve deforms, and the purpose of punching preservative film parcel had not only kept flower pattern but also do not influenceed moisture evaporation.
In one embodiment：The step 1) in, FAA fixers are volume ratio 85~95:4~6:4~6 45~55% second
Alcohol, glacial acetic acid, 35~45% formaldehyde mixed liquors.
In one embodiment：The step 1) in, rose is immersed in FAA fixers and is standing and soak for 24h.
In one embodiment：The step 3) in, successively using 50%, 60%, 70%, 80%, 90% ethanol by rose
It is standing and soak for 12h；Finally 48h is standing and soak for absolute ethyl alcohol.
In one embodiment：The step 4) in, rose is immersed in volume ratio 1:In 1 EtOH-MeOH mixed liquor, together
When according to 15ml/ amount add acetic acid, be standing and soak for 24h.
In one embodiment：The step 5) in, rose is immersed in volume ratio 1:In 1 EtOH-MeOH mixed liquor, together
When be separately added into acetic acid and polyethylene glycol according to the amount of 30ml/ and 50ml/, and add coloring agent, be standing and soak for 24~
48h。
In one embodiment：The step 5) in, coloring agent is soaking at least 24h using preposition in ethanol, makes coloring agent
Fully dissolve and be uniformly dispersed
The solution proportion being related in the present invention, unless otherwise indicated, is volume ratio or volume fraction.
Compared with background technology, it has the following advantages that the technical program：
The present invention is raw material using cutting flower, by fixation, rinsing, dehydration, decolouring, contaminate and protect shape, drying etc.
Series of processes, making reaches rose immortality and spends, and shape is complete, and flower state is graceful, and color uniform nature, not fugitive color, petal are carried
Natural colour and fine texture, neither too hard, nor too soft, pucker-free, its configuration are exactly alike with fresh flower, and effect is true to nature；And flow letter
It is clean, easy to operate quick, the prospect with the popularization and application in immortal peanut product.
Brief description of the drawings
The invention will be further described with reference to the accompanying drawings and examples.
Fig. 1 is through the rose single flower valve and rose corolla design sketch after dehydration, desolventing technology.
Fig. 2 is the rose design sketch after dyeing.
Fig. 3 is the rose immortality flower design sketch for obtaining.
Specific embodiment
Present disclosure is illustrated below by embodiment：
A kind of preparation method of rose immortality flower, including：
1) it is fixed：Rose Fresh Cut Flowers one are taken, is cut less than at 1cm under calyx using the scissors after sterilization, by flower
Hat is placed in beaker, adds the FAA fixer (configuration proportions of FAA fixers：50% ethanol 90ml, glacial acetic acid 5ml, 40% first
Aldehyde 5ml) to corolla is flooded, it is standing and soak for 24h；
2) rinse：Take step 1) rose that obtains, with 50% ethanol rinse 3~4 times；
3) it is dehydrated：Take step 2) rose that obtains, 50% ethanol of addition is standing and soak for 12h, to corolla is flooded
Fall solution；Then treatment 12h is standing and soak for successively with 60%, 70%, 80%, 90% ethanol successively；Finally absolute ethyl alcohol with (i.e.
100% ethanol) it is standing and soak for processing 48h；
4) decolourize：Take step 3) rose that obtains, it is immersed in volume ratio 1:In 1 EtOH-MeOH mixed liquor, while plus
Enter 15ml acetic acid, be standing and soak for processing 24h；Through dehydration, the rose single flower valve after desolventing technology and rose corolla as shown in figure 1,
It can be seen that rose single flower valve and rose corolla are in colourless, near-transparent shape, color is more uniform, without original color residual；And petal shape
Completely, corolla form is intact；
5) dye and shield shape：Take step 4) rose that obtains, it is immersed in volume ratio 1:In 1 EtOH-MeOH mixed liquor,
30ml acetic acid and 50ml polyethylene glycol are added simultaneously, and (fresh flower special stain therefor makes to add commercially available fresh flower special stain therefor
Need to be placed in before and 24h is soaked in ethanol), 24~48h is standing and soak for, dyeed；Because rose is white in class after desolventing technology
Color, therefore the color of specific dye can be selected as needed herein；Fig. 2 is the rose design sketch after dyeing, and it is red that Fig. 2 is left
Color, it is green Color that Fig. 2 is right, it is seen that the rose form after dyeing is basically identical with fresh flower, and shield shape effect is good
It is good, and color is uniform；
6) dry：Take step 5) rose that obtains, using the food fresh-keeping film of uniform punching, gently wrap up outside rose
Make a circle, should be noted that dynamics is advisable not damage rose form during parcel；Then in putting the container equipped with silica-gel desiccant into,
Sealing, dries 24~48h, takes out, and is placed in 2~3d at shady and cool ventilation, obtains final product rose immortality flower.Fig. 3 is the rose immortality for obtaining
Flower effect diagram, it is white that Fig. 3 is left, and it is pink that Fig. 3 is right, it is seen that rose immortality flower-shape shape is complete, and flower state is graceful, color
Uniform nature, not fugitive color, petal carry natural colour and fine texture, neither too hard, nor too soft, pucker-free, its configuration and fresh flower
Exactly alike, effect is true to nature.
Skilled person will appreciate that, when technical parameter of the invention changes in following scope, it is contemplated that obtain
Technique effect same as the previously described embodiments or close：
A kind of preparation method of rose immortality flower, including：
1) it is fixed：Rose Fresh Cut Flowers are taken, is cut at least 1cm under calyx, be immersed in FAA fixers, it is quiet
Put 22~26h of immersion；The FAA fixers are volume ratio 85~95:4~6:4~6 45~55% ethanol, glacial acetic acid, 35~
45% formaldehyde mixed liquor；
2) rinse：Take step 1) rose that obtains, with 45~55% ethanol rinse 2~5 times；
3) it is dehydrated：Take step 2) rose that obtains, it is immersed in 45~55% ethanol, it is standing and soak for 10~14h；Then
10~14h is standing and soak for successively with 55~65%, 65~75%, 75~85%, 85~95% ethanol successively；Finally use anhydrous second
Alcohol is standing and soak for 45~50h；
4) decolourize：Take step 3) rose that obtains, it is immersed in volume ratio 0.8~1.2:0.8~1.2 EtOH-MeOH
In mixed liquor, while adding acetic acid according to the amount of 12~18ml/, 22~26h is standing and soak for；
5) dye and shield shape：Take step 4) rose that obtains, it is immersed in volume ratio 0.8~1.2:0.8~1.2 second
In alcohol-methyl alcohol mixed liquor, while acetic acid and polyethylene glycol are separately added into according to the amount of 25~35ml/ and 45~55ml/, and
Add coloring agent, coloring agent that at least 24h is being soaked in ethanol using preposition；It is standing and soak for 20~50h；
6) dry：Take step 5) rose that obtains, rose is gently wrapped up using the food fresh-keeping film of uniform punching
One circle, in then putting the container equipped with silica-gel desiccant into, sealing dries 20~50h, takes out, be placed in 1 at shady and cool ventilation~
4d, obtains final product rose immortality flower.
The above, only present pre-ferred embodiments, therefore can not according to this limit the scope of present invention implementation, i.e., according to
Equivalence changes that the scope of the claims of the present invention and description are made and modification, all should still belong in the range of the present invention covers.
Claims (7)
1. the preparation method that a kind of rose immortality is spent, it is characterised in that：Including：
1) it is fixed：Rose Fresh Cut Flowers are taken, is cut at least 1cm under calyx, be immersed in FAA fixers, stand leaching
22~26h of bubble；
2) rinse：Take step 1) rose that obtains, with 45~55% ethanol rinse 2~5 times；
3) it is dehydrated：Take step 2) rose that obtains, it is immersed in 45~55% ethanol, it is standing and soak for 10~14h；Then successively
10~14h is standing and soak for successively with 55~65%, 65~75%, 75~85%, 85~95% ethanol；It is finally quiet with absolute ethyl alcohol
Put 45~50h of immersion；
4) decolourize：Take step 3) rose that obtains, it is immersed in volume ratio 0.8~1.2:0.8~1.2 EtOH-MeOH mixing
In liquid, while adding acetic acid according to the amount of 12~18ml/, 22~26h is standing and soak for；
5) dye and shield shape：Take step 4) rose that obtains, it is immersed in volume ratio 0.8~1.2:0.8~1.2 ethanol-first
In alcohol mixed liquor, while being separately added into acetic acid and polyethylene glycol according to the amount of 25~35ml/ and 45~55ml/, and add
Coloring agent, is standing and soak for 20~50h；
6) dry：Take step 5) rose that obtains, rose is gently wrapped up using the food fresh-keeping film of uniform punching for a circle,
Then put into the container equipped with silica-gel desiccant, sealing dries 20~50h, takes out, and is placed in 1~4d at shady and cool ventilation, obtains final product
Rose immortality flower.
2. the preparation method that rose immortality according to claim 1 is spent, it is characterised in that：The step 1) in, FAA is fixed
Liquid is volume ratio 85~95:4~6:4~6 45~55% ethanol, glacial acetic acid, 35~45% formaldehyde mixed liquors.
3. the preparation method that rose immortality according to claim 1 is spent, it is characterised in that：The step 1) in, by rose
Flower is standing and soak for 24h in being immersed in FAA fixers.
4. the preparation method that rose immortality according to claim 1 is spent, it is characterised in that：The step 3) in, adopt successively
Rose is standing and soak for 12h with 50%, 60%, 70%, 80%, 90% ethanol；Finally 48h is standing and soak for absolute ethyl alcohol.
5. the preparation method that rose immortality according to claim 1 is spent, it is characterised in that：The step 4) in, by rose
Flower is immersed in volume ratio 1:In 1 EtOH-MeOH mixed liquor, while adding acetic acid according to the amount of 15ml/, 24h is standing and soak for.
6. the preparation method that rose immortality according to claim 1 is spent, it is characterised in that：The step 5) in, by rose
Flower is immersed in volume ratio 1:In 1 EtOH-MeOH mixed liquor, while being separately added into acetic acid according to the amount of 30ml/ and 50ml/
And polyethylene glycol, and coloring agent is added, it is standing and soak for 24~48h.
7. the preparation method that rose immortality according to claim 1 is spent, it is characterised in that：The step 5) in, coloring agent
At least 24h is being soaked in ethanol using preposition.
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108189613A (en) * | 2018-03-08 | 2018-06-22 | 河南科技大学 | A kind of immortality flower and preparation method thereof |
| CN108372749A (en) * | 2018-02-28 | 2018-08-07 | 温州莲情水生花卉专业合作社 | A kind of production method of immortality flower |
| CN108407530A (en) * | 2018-04-09 | 2018-08-17 | 河南科技大学 | A kind of phonophoresis prepares the method for immortality flower, immortality flower |
| CN109050142A (en) * | 2018-08-16 | 2018-12-21 | 寻花郎（福建）农业开发有限公司 | A kind of fresh flower intensive processing method |
| CN109380215A (en) * | 2018-08-24 | 2019-02-26 | 昆明统生物科技有限公司 | A kind of production method of primary colors immortality flower |
| CN110271354A (en) * | 2019-07-08 | 2019-09-24 | 西双版纳宝翠香莲生物科技有限公司 | A kind of production method of immortality lotus flower |
| CN110481979A (en) * | 2019-09-12 | 2019-11-22 | 石林华莱永生花卉有限公司 | The processing technology of immortality flower is processed using absorption process and inhales color bucket |
| CN110774818A (en) * | 2019-11-06 | 2020-02-11 | 石林华莱永生花卉有限公司 | Method for decoloring, soaking, dyeing and preserving permanent flower |
| CN110949052A (en) * | 2019-12-16 | 2020-04-03 | 北京园霖昌顺农业种植专业合作社 | Preparation method of immortal lily |
| CN110999654A (en) * | 2019-12-25 | 2020-04-14 | 中国药科大学 | Method for making perpetual multi-color Chinese rose |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108372749A (en) * | 2018-02-28 | 2018-08-07 | 温州莲情水生花卉专业合作社 | A kind of production method of immortality flower |
| CN108189613A (en) * | 2018-03-08 | 2018-06-22 | 河南科技大学 | A kind of immortality flower and preparation method thereof |
| CN108407530A (en) * | 2018-04-09 | 2018-08-17 | 河南科技大学 | A kind of phonophoresis prepares the method for immortality flower, immortality flower |
| CN108407530B (en) * | 2018-04-09 | 2019-12-31 | 河南科技大学 | Method for preparing perpetual flower by ultrasonic permeation promotion and perpetual flower |
| CN109050142A (en) * | 2018-08-16 | 2018-12-21 | 寻花郎（福建）农业开发有限公司 | A kind of fresh flower intensive processing method |
| CN109380215A (en) * | 2018-08-24 | 2019-02-26 | 昆明统生物科技有限公司 | A kind of production method of primary colors immortality flower |
| CN110271354A (en) * | 2019-07-08 | 2019-09-24 | 西双版纳宝翠香莲生物科技有限公司 | A kind of production method of immortality lotus flower |
| CN110481979A (en) * | 2019-09-12 | 2019-11-22 | 石林华莱永生花卉有限公司 | The processing technology of immortality flower is processed using absorption process and inhales color bucket |
| CN110774818A (en) * | 2019-11-06 | 2020-02-11 | 石林华莱永生花卉有限公司 | Method for decoloring, soaking, dyeing and preserving permanent flower |
| CN110949052A (en) * | 2019-12-16 | 2020-04-03 | 北京园霖昌顺农业种植专业合作社 | Preparation method of immortal lily |
| CN110999654A (en) * | 2019-12-25 | 2020-04-14 | 中国药科大学 | Method for making perpetual multi-color Chinese rose |
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Application publication date: 20170531 |