CN106727259A - A kind of, perfume that storage stability high low to skin irritation and preparation method thereof - Google Patents

A kind of, perfume that storage stability high low to skin irritation and preparation method thereof Download PDF

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Publication number
CN106727259A
CN106727259A CN201710154888.8A CN201710154888A CN106727259A CN 106727259 A CN106727259 A CN 106727259A CN 201710154888 A CN201710154888 A CN 201710154888A CN 106727259 A CN106727259 A CN 106727259A
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China
Prior art keywords
parts
perfume
storage stability
skin irritation
high low
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Pending
Application number
CN201710154888.8A
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Chinese (zh)
Inventor
徐洪泉
汪虎
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Shanghai Malibu New Materials Co Ltd
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Shanghai Malibu New Materials Co Ltd
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Priority to CN201710154888.8A priority Critical patent/CN106727259A/en
Publication of CN106727259A publication Critical patent/CN106727259A/en
Pending legal-status Critical Current

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/347—Phenols
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35—Ketones, e.g. benzophenone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41—Amines
    • A61K8/416—Quaternary ammonium compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4993—Derivatives containing from 2 to 10 oxyalkylene groups
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/678—Tocopherol, i.e. vitamin E
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86—Polyethers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00—Formulations or additives for perfume preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/70—Biological properties of the composition as a whole
    • A61K2800/72—Hypo-allergenic

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Zoology (AREA)
  • Cosmetics (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention provides the perfume that a kind of skin irritation is low, storage stability is high, the perfume is made up of following parts by weight component：15 20 portions of essence, 30 40 portions of deionized waters, 10 15 portions of solubilizer, 20 30 portions of compound stabilizers, 35 portions of ethanol, 13 parts of antioxidants and 0.5 2 portions of preservatives；The compound stabilizer is made up of following parts by weight component：30 40 parts of polyethylene glycol, 8 15 parts of cationic surfactants, 20 30 part of 1,4 butanediol and 10 15 parts of octadecylamine APEOs.Perfume provided by the present invention, ethanol content is low, and the excitant to skin is small, and Simultaneous Stabilization is high, and storage one-year age does not produce precipitation and lamination.

Description

A kind of, perfume that storage stability high low to skin irritation and preparation method thereof
Technical field
The invention belongs to cosmetic technical field, and in particular to a kind of, perfume (or spice) that storage stability high low to skin irritation Water and preparation method thereof.
Background technology
Perfume, " Perfume " is derived from " Parfumare " in Latin.Globally, perfume is a value 250 Hundred million dollars of industry, the new product for having more than 300 artificial using names every year is listed.Perfume abroad, is one and intervenes already in life The element of various aspects, from the educational supply of children, to various daily necessitiess, there is the intervention of perfumery specialty, in France, Perfume has been an important element of Frenchman's life, indispensable as clothing, food, lodging and transportion -- basic necessities of life.
Effective lasting composition is essence in perfume, typically using ethanol as solvent, adds the system such as deionized water and auxiliary agent Obtain homogeneous, transparent system.Ethanol content in usual perfume is higher, stronger to skin irritation when using, while existing perfume (or spice) Water stability is not high, and storage is also easy to produce sediment or layering after a period of time, has a strong impact on the quality of perfume.
The content of the invention
The invention provides a kind of, perfume that storage stability high low to skin irritation, ethanol content is low, to skin Excitant is small, and Simultaneous Stabilization is high, and storage one-year age does not produce precipitation and lamination.
The technical proposal for solving the technical problem of the invention is：
A kind of, perfume that storage stability high low to skin irritation, the perfume is made up of following parts by weight component： 15-20 parts of essence, 30-40 parts of deionized water, 10-15 parts of solubilizer, 20-30 parts of compound stabilizer, 3-5 parts of ethanol, 1-3 parts resist Oxidant and 0.5-2 portions of preservative；
The compound stabilizer is made up of following parts by weight component：30-40 parts of polyethylene glycol, 8-15 parts of cationic surface Activating agent, 20-30 part of 1,4- butanediol and 10-15 parts of octadecylamine APEO.
Preferably, the perfume is made up of following parts by weight component：15 parts of essence, 35 parts of deionized waters, 15 parts of increasings Solvent, 25 portions of compound stabilizers, 4 portions of ethanol, 2 parts of antioxidants and 1 portion of preservative.
Preferably, described essence is butoxy dibenzoyl methane, ethylhexyl methoxy cinnamate or Moschus 105。
Preferably, the solubilizer is sorbitan fatty ester or polyethenoxy sorbitan list oleic acid Ester.
Essence indissoluble in water, adds solubilizer that its can be made fully emulsified, uniform with molecular conformation in deionized water Distribution, reduces the usage amount of ethanol.Ethanol has volatile feature, and a small amount of ethanol can promote essence compound to volatilize, so that The fragrance being in a cheerful frame of mind is made us in generation.When ethanol usage amount is too low, essence volatile quantity is relatively low, and perfume fragrance is subtle；When When ethanol usage amount is too high, it is irritating to the skin, while essence volatilization is very fast, perfume fragrance remaining time is shorter.
Compound stabilizer can further improve the stability of system, increase dissolubility of the essence in system, so that fragrant Water keeps dedusting stability higher in a long time, and perfume quality is higher.
The antioxidant is tocopherol, tertiary butyl hydroxy-methylbenzene or gallic acid third lipoprotein.
Preferably, the preservative is p-hydroxybenzoate, OIT or imidazolidinyl urea.
Preferably, the cationic surfactant is hexadecyltrimethylammonium chloride or cetyl trimethyl bromine Change ammonium.
It is described invention also provides a kind of method for preparing perfume low to skin irritation, that storage stability is high Preparation method comprises the following steps：
(1) by antioxidant and preservative addition ethanol, after stirring to its all dissolving, sealing is aged 1 at room temperature It is stand-by after individual month；
(2) by essence, deionized water, solubilizer, compound stabilizer and step (1) gained mixed liquor add mulser in, After being stirred 20-30 minutes under 1200-1500r/min, after 7d is aged at -18 DEG C, sediment is filtered to remove, filtrate is through low pressure Deaerate to obtain required perfume；
Step (1) compound stabilizer is made up of following parts by weight component：30-40 parts of polyethylene glycol, 8-15 parts of sun Ionic surface active agent, 20-30 part of 1,4- butanediol and 10-15 parts of octadecylamine APEO.
Beneficial effects of the present invention are：
1st, perfume provided by the present invention, ethanol content is relatively low, and smaller to skin irritatin, fragrance remaining time is long, and effect is good.
2nd, perfume stability provided by the present invention is higher, and the phenomenons such as muddy, layering does not occur in storage after 1 year.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments to the present invention It is further elaborated.It should be appreciated that specific embodiment described herein is only used to explain the present invention, limit is not used to The fixed present invention.
Embodiment 1
(1) by 2g tocopherols and 1g p-hydroxybenzoates addition 4g ethanol, after stirring to its all dissolving, seal, It is stand-by after being aged 1 month at room temperature；
(2) by 15g butoxy dibenzoyl methane, 35g deionized waters, 15g sorbitan fatty esters, 25g Compound stabilizer and step (1) gained mixed liquor are added in mulser, after being stirred 25 minutes under 1300r/min, at -18 DEG C After being aged 7d, sediment is filtered to remove, filtrate deaerates to obtain required perfume through low pressure；
Step (1) compound stabilizer is made up of following parts by weight component：30 parts of polyethylene glycol, 10 parts of cetyls Trimethyl ammonium chloride, 25 parts of 1,4- butanediols and 10 parts of octadecylamine APEOs.
Made perfume does not produce precipitation, lamination after storing 1 year.
Embodiment 2
(1) by 1g tertiary butyls hydroxy-methylbenzene and 2g OITs addition 3g ethanol, stir to its all dissolving, it is close Envelope, it is stand-by after being aged 1 month at room temperature；
(2) by 18g ethylhexyl methoxy cinnamates, 30g deionized waters, 12g polyethenoxy sorbitan list oleic acid Ester, 20g compound stabilizers and step (1) gained mixed liquor are added in mulser, after being stirred 20 minutes under 1200r/min, in- At 18 DEG C after ageing 7d, sediment is filtered to remove, filtrate deaerates to obtain required perfume through low pressure；
Step (1) compound stabilizer is made up of following parts by weight component：35 parts of polyethylene glycol, 8 parts of cetyls Trimethylammonium bromide, 20 parts of 1,4- butanediols and 12 parts of octadecylamine APEOs.
Made perfume does not produce precipitation, lamination after storing 1 year.
Embodiment 3
(1) by 3g gallic acid third lipoproteins and 0.5g imidazolidinyl ureas addition 5g ethanol, stir to its all dissolving, it is close Envelope, it is stand-by after being aged 1 month at room temperature；
(2) by 20g Moschus 105,40g deionized waters, 10g sorbitan fatty esters, 30g compound stabilizers and step Suddenly during (1) gained mixed liquor adds mulser, after being stirred 30 minutes under 1500r/min, after 7d is aged at -18 DEG C, filter Removing sediment, filtrate deaerates to obtain required perfume through low pressure；
Step (1) compound stabilizer is made up of following parts by weight component：40 parts of polyethylene glycol, 15 parts of cetyls Trimethyl ammonium chloride, 30 parts of 1,4- butanediols and 15 parts of octadecylamine APEOs.
Made perfume does not produce precipitation, lamination after storing 1 year.
Comparative example 1
(1) by 2g tocopherols and 1g p-hydroxybenzoates addition 4g ethanol, after stirring to its all dissolving, seal, It is stand-by after being aged 1 month at room temperature；
(2) by 15g butoxy dibenzoyl methane, 35g deionized waters, 15g sorbitan fatty esters and step Suddenly during (1) gained mixed liquor adds mulser, after being stirred 25 minutes under 1300r/min, after 7d is aged at -18 DEG C, filter Removing sediment, filtrate deaerates to obtain required perfume through low pressure.
Made perfume produces precipitation, lamination after storing 1 year.
By comparative example 1 and comparative example 1 it can be found that compound stabilizer provided by the present invention is favorably improved perfume (or spice) The stability of water, improves the quality of perfume.
Presently preferred embodiments of the present invention is the foregoing is only, is not intended to limit the invention, it is all in essence of the invention Any modification, equivalent and improvement made within god and principle etc., should be included within the scope of the present invention.

Claims (8)

1. a kind of, perfume that storage stability high low to skin irritation, it is characterised in that the perfume is by following parts by weight Component is constituted：15-20 parts of essence, 30-40 parts of deionized water, 10-15 parts of solubilizer, 20-30 parts of compound stabilizer, 3-5 parts of second Alcohol, 1-3 part antioxidant and 0.5-2 portions of preservative；
The compound stabilizer is made up of following parts by weight component：30-40 parts of polyethylene glycol, 8-15 parts of cation surface activating Agent, 20-30 parts of 1,4- butanediol and 10-15 parts of octadecylamine APEO.
2., perfume that storage stability high low to skin irritation as claimed in claim 1, it is characterised in that the perfume It is made up of following parts by weight component：15 parts of essence, 35 parts of deionized waters, 15 parts of solubilizer, 25 parts of compound stabilizers, 4 parts of second Alcohol, 2 parts of antioxidants and 1 portion of preservative.
3., perfume that storage stability high low to skin irritation as claimed in claim 1, it is characterised in that described perfume (or spice) Essence is butoxy dibenzoyl methane, ethylhexyl methoxy cinnamate or Moschus 105.
4., perfume that storage stability high low to skin irritation as claimed in claim 1, it is characterised in that the solubilising Agent is sorbitan fatty ester or polyoxyethylene sorbitan monooleate.
5., perfume that storage stability high low to skin irritation as claimed in claim 1, it is characterised in that the antioxygen Agent is tocopherol, tertiary butyl hydroxy-methylbenzene or gallic acid third lipoprotein.
6., perfume that storage stability high low to skin irritation as claimed in claim 1, it is characterised in that the anti-corrosion Agent is p-hydroxybenzoate, OIT or imidazolidinyl urea.
7., perfume that storage stability high low to skin irritation as claimed in claim 1, it is characterised in that the sun from Sub- surfactant is hexadecyltrimethylammonium chloride or cetyl trimethylammonium bromide.
8. the method for preparing the perfume described in claim 1-7 any one, it is characterised in that the preparation method includes as follows Step：
(1) by antioxidant and preservative addition ethanol, after stirring to its all dissolving, seal, at room temperature ageing 1 month Afterwards, it is stand-by；
(2) by essence, deionized water, solubilizer, compound stabilizer and step (1) gained mixed liquor add mulser in, in After being stirred 20-30 minutes under 1200-1500r/min, after 7d is aged at -18 DEG C, sediment is filtered to remove, filtrate is de- through low pressure It is so incensed that required perfume；
Step (1) compound stabilizer is made up of following parts by weight component：30-40 parts of polyethylene glycol, 8-15 parts of cation Surfactant, 20-30 part of 1,4- butanediol and 10-15 parts of octadecylamine APEO.
CN201710154888.8A 2017-03-17 2017-03-17 A kind of, perfume that storage stability high low to skin irritation and preparation method thereof Pending CN106727259A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109199929A (en) * 2018-11-07 2019-01-15 上海芬尚生物科技有限公司 perfume and preparation method thereof
CN111388338A (en) * 2020-03-20 2020-07-10 广州乐宠宠物用品有限公司 Pet perfume with lasting fragrance retaining effect and preparation method thereof
CN112891259A (en) * 2021-02-25 2021-06-04 蔓莎(苏州)工艺制品有限公司 Plant perfume and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101491484A (en) * 2008-12-12 2009-07-29 颜林 Milky perfume and preparation method thereof
CN103637942A (en) * 2013-06-30 2014-03-19 金玛瑙香水（明光）有限公司 Alcohol-free transparent perfume composition

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101491484A (en) * 2008-12-12 2009-07-29 颜林 Milky perfume and preparation method thereof
CN103637942A (en) * 2013-06-30 2014-03-19 金玛瑙香水（明光）有限公司 Alcohol-free transparent perfume composition

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109199929A (en) * 2018-11-07 2019-01-15 上海芬尚生物科技有限公司 perfume and preparation method thereof
CN111388338A (en) * 2020-03-20 2020-07-10 广州乐宠宠物用品有限公司 Pet perfume with lasting fragrance retaining effect and preparation method thereof
CN112891259A (en) * 2021-02-25 2021-06-04 蔓莎(苏州)工艺制品有限公司 Plant perfume and preparation method thereof
CN112891259B (en) * 2021-02-25 2022-09-30 蔓莎(苏州)工艺制品有限公司 Plant perfume and preparation method thereof

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