CN106723371A - A kind of self-heating cigarette substitute and preparation method thereof - Google Patents
A kind of self-heating cigarette substitute and preparation method thereof Download PDFInfo
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- CN106723371A CN106723371A CN201611147507.5A CN201611147507A CN106723371A CN 106723371 A CN106723371 A CN 106723371A CN 201611147507 A CN201611147507 A CN 201611147507A CN 106723371 A CN106723371 A CN 106723371A
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- self
- heating
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- A24F47/002—
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Packaging Of Annular Or Rod-Shaped Articles, Wearing Apparel, Cassettes, Or The Like (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention belongs to cigarette substitute technical field, and in particular to a kind of self-heating cigarette substitute and preparation method thereof.The substitute structure from top to bottom, including set gradually air-permeable layer, spontaneous heating bag, be combined material bed and polyurethane overlay film；The air-permeable layer, using the ventilative membrane materials of PE；Spontaneous heating material composition composition is in spontaneous heating bag：Reduced iron powder 50~65%, activated carbon powder 3~5%, vermiculite 12~20%；Sodium chloride 1~3%, water 15~20%；It is described compound material bed, it is made up of the compound material, cutaneous permeable agent and the class component of skeleton adhesive three that are well mixed；When using, product is taken out from hermetic bag, remove polyurethane overlay film, the compound material bed part with viscose glue is directly adhered to body surface；Now, the air-permeable layer of self-heating bag touches air, begins to warm up, heat by the nonwoven interlining bed of material to it is compound it is material bed heat, be passed to Transdermal absorption and enter human body, meet human body and suck demand.
Description
Technical field
The invention belongs to cigarette substitute technical field, and in particular to a kind of self-heating cigarette substitute and its preparation side
Method.
Background technology
It is a kind of relatively common common recognition that Smoking is harmful to your health, but specific physiology and psychology need due to smoking population
Ask, more serious tobacco dependence is faced with again, thus a substitute for growing tobacco is provided, be allowed to meeting smoking population
Simultaneously, the dependence for alleviating tobacco is a kind of more feasible measure for physiology, psychological needs.
In the prior art, for substitute of tobacco on common meaning, a kind of main substitute is new electronic cigarette, buccal cigarette etc.
Although type tobacco product, wherein electronics smoke product disclosure satisfy that the physiology of part smoking population, psychological needs, but electronic cigarette has
Price is higher and the drawbacks such as mains power are depended on when using, and other kinds of buccal cigarette acceptance at home is not high, because
And the popularization and application of this kind of novel tobacco product are limited to a certain extent.Thus, develop and be with Chinese characteristics, can be by compatriots
The new cigarette substitute of receiving still has highly important application and meaning.
The content of the invention
Present invention aim at a kind of new self-heating cigarette substitute is provided, produced a kind of new cigarette substitute is provided
While product, for the exploitation of new cigarette substitute provides new reference and reference.
The detailed technology scheme that the present invention is taken is as described below.
A kind of self-heating cigarette substitute, its structure from top to bottom, including the air-permeable layer, spontaneous heating bag, multiple for setting gradually
The compound bed of material and polyurethane overlay film；
The air-permeable layer, using the ventilative membrane materials of PE, Air permenbility is arranged on 550 L/（m2·s）To 1500L/（m2·s）Between, this
When spontaneous heating bag maximum heating temperature can occur between 55 DEG C to 75 DEG C correspondence change；
The spontaneous heating bag, to be enclosed with the non-woven fabrics bag of spontaneous heating material composition；In terms of mass fraction, the spontaneous heating thing
Feed composition is constituted：50~65 parts of the reduced iron powder of 100 ~ 150 mesh, 3~5 parts of activated carbon powder, 12~20 parts of vermiculite；Sodium chloride
1~3 part, 15~20 parts of water；The non-woven fabrics, is, for example, specifically SMS non-woven fabrics；
It is described compound material bed, it is made up of the compound material, cutaneous permeable agent and the class component of skeleton adhesive three that are well mixed；Respectively
Material concrete composition and proportioning are：
Compound material：0.2 ~ 0.5g tobacco extracts, 0.02 ~ 0.05g vitamin Es, 0.1 ~ 0.2 g gelatin, 1.0 ~ 2.0g the third two
Alcohol；
Cutaneous permeable agent：0.02 ~ 0.05g caryophyllus oils, 0.02 ~ 0.05g menthols, 0.1 ~ 0.2g glycerine；
Skeleton adhesive：0.5g vinyl alcohols, 2.0g organosilicons；
The polyurethane overlay film, located at compound material bed surface, it is to avoid the volatilization of active ingredient.
The self-heating cigarette substitute, spontaneous heating material composition composition is in spontaneous heating bag：100 mesh reduced iron powders
60%th, 200 mesh activated carbon powders 5%, vermiculite 18%, sodium chloride 2%, water 15%.
The self-heating cigarette substitute, The concrete specification is designed as：It is the rectangle paster of 4cm × 5cm, spontaneous heating bag
Specification is 5g, and it is 3g to be combined material bed.
The self-heating cigarette substitute, be combined it is material bed in, each material concrete composition and optimum ratio are：
Compound material：0.5g tobacco extracts, 0.02g vitamin Es, 0.1g gelatin, 1.0g propane diols,
Cutaneous permeable agent：0.02g caryophyllus oils, 0.02g menthols, 0.1g glycerine,
Skeleton adhesive is：0.5g vinyl alcohols, 2.0g organosilicons.
It should be noted that the self-heating cigarette substitute, when being not used, should be placed in vacuum packaging bag and preserve standby
With.
The preparation method of the self-heating cigarette substitute, specifically includes following steps：
（1）Spontaneous heating bag is prepared, and pastes air-permeable layer, specially：
Material in spontaneous heating material composition is well mixed under the conditions of protective atmosphere in proportion, is fitted into system in non-woven bag
Into spontaneous heating bag；
Under the conditions of protective atmosphere, by the shaping of spontaneous heating bag concora crush（Platypelloid type）, the ventilative membrane materials of PE are sticked in non-woven bag one side
It is standby as air-permeable layer；
The protective atmosphere is nitrogen or inert gas conditions；
（2）Preparation is compound material bed, specially：
First, tobacco extract, vitamin E, gelatin are dissolved in propane diols in proportion, are then sequentially placed into colloid mill and homogeneous
In machine, emulsion dispersion is into emulsion colloid；
Secondly, caryophyllus oil, menthol and glycerine are proportionally added into above-mentioned emulsion colloid, are placed in nano-dispersed machine uniform
It is compound material gel；
Finally, by the pre-configured skeleton adhesive of above-mentioned compound material gel addition, it is well mixed；The skeleton gluing
The viscosity that agent is formed by vinyl alcohol mixes with organosilicon is the rubber cement of 5000mpas；
（3）Self-heating cigarette substitute finished product is prepared, specially：
Using coating machine, by step（2）In prepared compound material bed be uniformly coated on step（1）Middle non-woven fabrics it is another
Face, then pastes polyurethane overlay film, after punching shaping, is placed in packaging bag and vacuumizes preservation.
The self-heating cigarette substitute substitutes the application of articles for use as cigarette, and its application method is after opening packaging, to tear
Remove polyurethane overlay film, will it is compound it is material bed be pasted near the Lieque point of human body lung meridian or Renzhong acupoint position, then tear off
Air-permeable layer, after after spontaneous heating bag and air contact, material is heated volatilization in compound material bag, and the percutaneous skin top layer of the material that volatilizees is entered
Enter human body, so that human body obtains the satisfaction of tobacco sucking.
Self-heating cigarette substitute provided herein, use time suggestion is 30min, after 30min in self-heating bag
Material reaction terminates substantially, and heating effect disappears, and compound material bed interior material has also volatilized totally, thus can consider certainly
Hot type cigarette substitute is using finishing.
During using self-heating cigarette substitute of the present invention, after tearing air-permeable layer, air is by micro- in air-permeable layer
Hole enters spontaneous heating bag, and due to there is air to enter in spontaneous heating bag, spontaneous heating material composition starts to aoxidize and produce heat,
Produced heat be combined it is material bed, make be combined material bed middle each component start to be heated, volatilize.According to the channels and collaterals in the traditional Chinese medical science
Theory, the material that compound material bed middle component is volatilized is conducted so as to stimulate human oral cavity by the acupuncture point of Lieque point or Renzhong acupoint
Interior sense organ, and then meet the physiology and psychological needs of user.
When specific production prepares herein described self-heating cigarette substitute, to realize fitting for heating-up temperature in spontaneous heating bag
Work as control, can be by the selection of the ventilative membrane materials of different pore size PE, so that the Air permenbility of suitable control air-permeable layer；In other words, pass through
The speed that control air enters in spontaneous heating bag, so as to adjust the speed that spontaneous heating material composition produces heat, and then is adjusted
Compound material bed material heating-up temperature and evaporation rate, are suitably adjusted with to sucking experience.
In general, self-heating cigarette substitute provided by the present invention, easy to use, is produced without pyrotechnics, also without substantially
Flue gas is produced, and is that one kind can be applied to various occasions while physiology and the psychological goal of tobacco sucking crowd can preferably be met
Ideal cigarette substitute, with preferably application value.
Brief description of the drawings
Fig. 1 is self-heating cigarette substitute structural representation provided by the present invention；
Fig. 2 is the preparation flow schematic diagram of self-heating cigarette substitute provided by the present invention；
Fig. 3 is heat condition comparison diagram of the self-heating cigarette substitute of different air permeabilities in 30 minutes.
Specific embodiment
With reference to embodiment the present invention will be further explained explanation, before specific embodiment is introduced, to following realities
Material used is briefly discussed below in applying example.
Tobacco extract described herein can use commercialization tobacco extract or prepare as follows：Weigh
During 2.0 g offals samples dry tool plug vial in one, 20mL, 10% ammonia spirit, the min of ultrasonic extraction 2 are added；Add 50
The mixed liquor of mL dichloromethane and methyl alcohol（V/V=3:1）Extracted, oscillation extraction 30min, it is left that last low-press thick is condensed to 0.5g
The right side, as tobacco extract；
Employed in embodiment vitamin E be natural type vitamin E, purity is 96.0%, can also use purity for 100.0% conjunction
Shaping；
The materials such as gelatin, polyvinyl alcohol, caryophyllus oil, menthol, glycerine, propane diols, polyvinyl alcohol and organosilicon are using medicinal
Auxiliary material level.
Embodiment 1
As shown in Fig. 2 herein described self-heating cigarette substitute, is made by the steps and forms：
（1）Spontaneous heating bag is prepared, and pastes air-permeable layer, specially：
Material in spontaneous heating material composition is well mixed under the conditions of protective atmosphere in proportion, is fitted into system in non-woven bag
Into spontaneous heating bag；
Under the conditions of protective atmosphere, by the shaping of spontaneous heating bag concora crush（Platypelloid type）, the ventilative membrane materials of PE are sticked in non-woven bag one side
It is standby as air-permeable layer；
The protective atmosphere is nitrogen or inert gas conditions；
（2）Preparation is compound material bed, specially：
First, tobacco extract, vitamin E, gelatin are dissolved in propane diols in proportion, are subsequently placed in colloid mill and homogenizer
In, emulsion dispersion is into emulsion colloid；
Secondly, caryophyllus oil, menthol and glycerine are proportionally added into above-mentioned emulsion colloid, are placed in nano-dispersed machine uniform
It is compound material gel；
Finally, by the pre-configured skeleton adhesive of above-mentioned compound material gel addition, it is well mixed；The skeleton adhesive
It is the rubber cement of 5000mpas by vinyl alcohol mixes the viscosity for being formed with organosilicon；
（3）Self-heating cigarette substitute finished product is prepared, specially：
Using coating machine, by step（2）In prepared compound material bed be uniformly coated on step（1）Middle non-woven fabrics it is another
Face, then pastes polyurethane overlay film, after punching shaping, is placed in packaging bag and vacuumizes preservation.
Using the above method, prepared self-heating cigarette substitute, its structure as shown in figure 1, including from bottom to up according to
The polyurethane overlay film 5 of secondary setting, compound material bed 4, spontaneous heating bag 2 and air-permeable layer 1；Wherein be combined material bed 4 coat it is spontaneous
On non-woven fabrics 3 outside heat bag 2（In practical application, spontaneous heating bag 2 is wrapped to form by non-woven fabrics 3, for expression understands this Shen in figure
Please structure, be provided without the form and represent）.
Self-heating cigarette substitute prepared by the present embodiment, concrete form and specification are：The rectangle patch of 4cm × 5cm
Piece, spontaneous heating bag specification is 5g, and it is 3g to be combined material bed：
Spontaneous heating material composition composition is in spontaneous heating bag：100 mesh reduced iron powders 60%, 200 mesh activated carbon powders 5%, vermiculite
18%th, sodium chloride 2%, water 15%；
Specifically proportioning is to be combined material bed each material：
Compound material：0.5g tobacco extracts, 0.02g vitamin Es, 0.1g gelatin, 1.0g propane diols,
Cutaneous permeable agent：0.02g caryophyllus oils, 0.02g menthols, 0.1g glycerine,
Skeleton adhesive is：0.5g vinyl alcohols, 2.0g organosilicons.
It should be noted that when being that the ventilative membrane materials of detection different size PE are used, heating-up temperature change feelings in spontaneous heating bag
Condition, and the difference of material bed material release conditions is combined, inventor has selected different Air permenbility specifications respectively（Air permenbility is distinguished
It is 550 L/（m2.s）、1000 L/（m2.s）With 1500 L/（m2.s））The ventilative membrane materials of PE as air-permeable layer, and according to above-mentioned
Formula and method are prepared for self-heating cigarette substitute.To spontaneous heating temperature and compound in 30min after air-permeable layer is torn off
The release conditions of nicotine are detected in the bed of material, and related experiment situation is briefly discussed below.
（One）When Air permenbility is different, heating-up temperature situation of change
Heating-up temperature situation of change is detected using thermocouple.Result is as shown in Figure 3.
From figure 3, it can be seen that being respectively 550 L/ in Air permenbility（m2.s）、1000 L/（m2.s）With 1500 L/
（m2.s）When, maximum heating temperature can respectively reach 55 DEG C, 68 DEG C and 75 DEG C in 30min；Heating effect accordingly, can be according to compound
Material bed interior material composition situation（I.e. required heating-up temperature）Air permenbility is suitably adjusted.
（Two）Nicotine burst size
For tobacco sucking experience, one of its most important influence factor is nicotine burst size, therefore main to prepared
The nicotine burst size of self-heating cigarette substitute is detected.During detection, more than 99% cigarette can be retained due to cambridge filter
Alkali, thus this experiment traps nicotine using cambridge filter, and then represent the present invention by determining on cambridge filter nicotine content
Nicotine burst size when the self-heating cigarette substitute for being provided is used.
Checkout procedure is：Cambridge filter is soaked with clear water first, then by the compound material of self-heating cigarette substitute
Bag is pasted thereon, is surrounded by air in spontaneous heating and enters fashionable beginning timing, and spontaneous heating material composition starts to aoxidize and produce heat,
The compound material bag of produced heat, makes compound material bed interior each component start volatilization of being heated, and nicotine is then filtered by Cambridge
Piece retention trapping, collects volatile quantity in 30 minutes.
After 30min, the nicotine to being trapped on cambridge filter is measured.
Assay method is：By cambridge filter be dissolved in 50mL containing target isopropyl alcohol extraction agent in heptadecane in,
Oscillation extraction 1 hour, makes trapping thing（That is nicotine）It is completely dissolved in isopropanol, through 0.45 μm of membrane filtration, Ran Houyong after shaking up
Gas chromatograph（GC-FID）Determine nicotine content.
Specific measurement result is as shown in the table：
。
Upper table is analyzed as can be seen that the nicotine burst size of self-heating cigarette substitute provided by the present invention is
Between 0.6 mg ~ 0.9mg, and this is close with nicotine content in a conventional cigarette main flume.I.e.：Only nicotine aspect is examined
Amount, self-heating cigarette substitute provided by the present invention is close with the satisfaction that a cigarette gives.
Claims (9)
1. kind of self-heating cigarette substitute, it is characterised in that its structure from top to bottom, including the air-permeable layer, spontaneous for setting gradually
Heat bag, compound material bed and polyurethane overlay film；
The air-permeable layer, using the ventilative membrane materials of PE；
The spontaneous heating bag, to be enclosed with the non-woven fabrics bag of spontaneous heating material composition；In terms of mass fraction, the spontaneous heating thing
Feed composition is constituted：50~65 parts of the reduced iron powder of 100 ~ 150 mesh, 3~5 parts of activated carbon powder, 12~20 parts of vermiculite；Sodium chloride
1~3 part, 15~20 parts of water；
It is described compound material bed, it is made up of the compound material, cutaneous permeable agent and the class component of skeleton adhesive three that are well mixed；Respectively
Material concrete composition and proportioning are：
Compound material：0.2 ~ 0.5g tobacco extracts, 0.02 ~ 0.05g vitamin Es, 0.1 ~ 0.2g gelatin, 1.0 ~ 2.0g the third two
Alcohol；
Cutaneous permeable agent：0.02 ~ 0.05g caryophyllus oils, 0.02 ~ 0.05g menthols, 0.1 ~ 0.2g glycerine；
Skeleton adhesive：0.5g vinyl alcohols, 2.0g organosilicons.
2. self-heating cigarette substitute as claimed in claim 1, it is characterised in that the Air permenbility of air-permeable layer is arranged on 550 L/
（m2·s）To 1500L/（m2·s）Between.
3. self-heating cigarette substitute as claimed in claim 1, it is characterised in that spontaneous heating material composition group in spontaneous heating bag
Turn into：100 mesh reduced iron powders 60%, 200 mesh activated carbon powders 5%, vermiculite 18%, sodium chloride 2%, water 15%.
4. self-heating cigarette substitute as claimed in claim 1, it is characterised in that it is compound it is material bed in, each material concrete composition
And proportioning is：
Compound material：0.5g tobacco extracts, 0.02g vitamin Es, 0.1g gelatin, 1.0g propane diols,
Cutaneous permeable agent：0.02g caryophyllus oils, 0.02g menthols, 0.1g glycerine
Skeleton adhesive is：0.5g vinyl alcohols, 2.0g organosilicons.
5. self-heating cigarette substitute as claimed in claim 1, it is characterised in that The concrete specification is designed as：It is 4cm × 5cm
Rectangle paster, spontaneous heating bag specification be 5g, be combined it is material bed be 3g.
6. the preparation method of self-heating cigarette substitute described in any one of claim 1 ~ 5, it is characterised in that specifically include as follows
Step：
（1）Spontaneous heating bag is prepared, and pastes air-permeable layer, specially：
Material in spontaneous heating material composition is well mixed under the conditions of protective atmosphere in proportion, is fitted into system in non-woven bag
Into spontaneous heating bag；
Under the conditions of protective atmosphere, by the shaping of spontaneous heating bag concora crush, the ventilative membrane materials of PE are sticked as ventilative in non-woven bag one side
Layer is standby；
（2）Preparation is compound material bed, specially：
First, tobacco extract, vitamin E, gelatin are dissolved in propane diols in proportion, are subsequently placed in colloid mill and homogenizer
In, emulsion dispersion is into emulsion colloid；
Secondly, caryophyllus oil, menthol and glycerine are proportionally added into above-mentioned emulsion colloid, are placed in nano-dispersed machine uniform
It is compound material gel；
Finally, by the pre-configured skeleton adhesive of above-mentioned compound material gel addition, it is well mixed；
（3）Self-heating cigarette substitute finished product is prepared, specially：
Using coating machine, by step（2）In prepared compound material bed be uniformly coated on step（1）Middle non-woven fabrics it is another
Face, then pastes polyurethane overlay film, after punching shaping, is placed in packaging bag and vacuumizes preservation.
7. the preparation method of self-heating cigarette substitute as claimed in claim 6, it is characterised in that step（1）In, the protection
Property atmosphere be nitrogen or inert gas conditions.
8. the preparation method of self-heating cigarette substitute as claimed in claim 6, it is characterised in that step（2）In, the skeleton
The viscosity that adhesive is formed by vinyl alcohol mixes with organosilicon is the rubber cement of 5000mpas.
9. self-heating cigarette substitute described in any one of claim 1 ~ 5 substitutes the application of articles for use as cigarette, it is characterised in that
By the compound material bed Lieque point for being pasted on human body lung meridian or Renzhong acupoint position.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611147507.5A CN106723371B (en) | 2016-12-13 | 2016-12-13 | A kind of self-heating cigarette substitute and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611147507.5A CN106723371B (en) | 2016-12-13 | 2016-12-13 | A kind of self-heating cigarette substitute and preparation method thereof |
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| Publication Number | Publication Date |
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| CN106723371A true CN106723371A (en) | 2017-05-31 |
| CN106723371B CN106723371B (en) | 2019-07-23 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1144088A (en) * | 1996-03-11 | 1997-03-05 | 北京克莱斯瑞控释药业有限公司 | Colading sticking sheet and nicotine sticking sheet compound smoking stopping method |
| CN1186659A (en) * | 1998-01-09 | 1998-07-08 | 重庆医科大学 | Compound smoking-refraining adhesive sheet absorbed through skin |
| CN1605294A (en) * | 2003-10-09 | 2005-04-13 | 天津市中宝科技有限公司 | Compound tobacco addict controlling plaster and its preparation method |
| CN104983070A (en) * | 2015-05-26 | 2015-10-21 | 湖北中烟工业有限责任公司 | Non-combustible type cigarette having spontaneous heating material arranged at external of cut tobacco |
| CN105011377A (en) * | 2015-07-29 | 2015-11-04 | 中国烟草总公司郑州烟草研究院 | Self-heating non-combustible wrapping material for tobacco and application of self-heating non-combustible wrapping material in tobacco products |
-
2016
- 2016-12-13 CN CN201611147507.5A patent/CN106723371B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1144088A (en) * | 1996-03-11 | 1997-03-05 | 北京克莱斯瑞控释药业有限公司 | Colading sticking sheet and nicotine sticking sheet compound smoking stopping method |
| CN1186659A (en) * | 1998-01-09 | 1998-07-08 | 重庆医科大学 | Compound smoking-refraining adhesive sheet absorbed through skin |
| CN1605294A (en) * | 2003-10-09 | 2005-04-13 | 天津市中宝科技有限公司 | Compound tobacco addict controlling plaster and its preparation method |
| CN104983070A (en) * | 2015-05-26 | 2015-10-21 | 湖北中烟工业有限责任公司 | Non-combustible type cigarette having spontaneous heating material arranged at external of cut tobacco |
| CN105011377A (en) * | 2015-07-29 | 2015-11-04 | 中国烟草总公司郑州烟草研究院 | Self-heating non-combustible wrapping material for tobacco and application of self-heating non-combustible wrapping material in tobacco products |
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| CN106723371B (en) | 2019-07-23 |
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