CN106720468A - A kind of spicy fresh fragrant Zanthoxylum essential oil preparation method - Google Patents
A kind of spicy fresh fragrant Zanthoxylum essential oil preparation method Download PDFInfo
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- CN106720468A CN106720468A CN201611025337.3A CN201611025337A CN106720468A CN 106720468 A CN106720468 A CN 106720468A CN 201611025337 A CN201611025337 A CN 201611025337A CN 106720468 A CN106720468 A CN 106720468A
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- oil
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- zanthoxylum essential
- capsicum
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
Abstract
The present invention provides a kind of preparation method of spicy fresh wild citron oil, is obtained by the raw material comprising 10~30% dry pericarpium zanthoxyli schinifoliis, 10~30% extra dry red wine Chinese prickly ashes, 10~30% dry big capsicums, 10~30% dry capsicums；By in the complete manufacture craft for incorporating Zanthoxylum essential oil of the scarlet and pungent of capsicum, by specific filter plant, obtained final Zanthoxylum essential oil need not stand and can be achieved with transparent glow, and retain numb, peppery, fragrant three kinds of characteristics simultaneously, the limitation of existing Zanthoxylum essential oil single varieties is broken, more demands are provided to consumer, it is deep to be liked by consumer.Extraction process step of the present invention is simple, the Zanthoxylum essential oil red, transparent of preparation, glossy, free from admixture bright in colour, and without precipitation, pectin, oily value, acid value, peroxide content are low and relatively low to equipment, site requirements, are adapted to large-scale promotion application.
Description
Technical field
The present invention relates to Zanthoxylum essential oil, and in particular to a kind of spicy fresh fragrant Zanthoxylum essential oil preparation method.
Background technology
Chinese prickly ash is used as China " one of eight big flavouring ", and vitamin C, copper, zinc, manganese, selenium rich in needed by human body etc. are various
Element, its is widely used, and economic worth is high.Chinese prickly ash on ordinary meaning refers to pericarpium zanthoxyli schinifolii or pericarpium zanthoxyli bungeani, and pericarpium zanthoxyli schinifolii color and luster is blue or green
Green, fragrance overflows people, and numb taste is moderate, but the numb taste of pericarpium zanthoxyli schinifolii is slightly relatively low for the place of the numb tastes of some pursuits and products；
Pericarpium zanthoxyli bungeani fragrance is not enough, and it is strongly lasting in numb taste to win, and is to use most wide kind now.
In recent years, with the improvement of people ' s living standards, market is also increasing to the demand of Chinese prickly ash.But fresh pepper
Greatest problem be it is not easy to maintain, extremely blacking, go mouldy, spread the shelf-life under normal temperature and there was only 3~5 days, stacking the shelf-life is no more than 2
My god；Refrigerator freezing just occurs blacking phenomenon in 7 days.Therefore, domestic Chinese prickly ash is more is deposited with dry product.Complete dried pepper or zanthoxylum powder are given
Culinary art and the edible inconvenience for bringing, recent years Zanthoxylum essential oil not only remain the original spicy hot taste of Chinese prickly ash because of it, also solve Chinese prickly ash
Grain and zanthoxylum powder to culinary art and it is edible bring it is inconvenient the characteristics of and gradually liked by consumer.Existing Zanthoxylum essential oil mouthfeel list
One, otherwise numb taste strong fragrance is not enough, otherwise aromatic flavour fiber crops taste is poor；In order to enrich flavouring species, more hobbies are met
The culinary art demand of spicy family, it is necessary to develop a kind of spicy fresh fragrant Zanthoxylum essential oil.
The content of the invention
In order to solve the problems of the prior art, it is an object of the invention to provide a kind of preparation of spicy fresh wild citron oil
Method, the method by the complete manufacture craft for incorporating Zanthoxylum essential oil of the scarlet and pungent of capsicum, protect simultaneously by the Zanthoxylum essential oil of preparation
Spicy fresh fragrant characteristic is stayed, it is deep to be liked by consumer.
Unless otherwise specified, number of the present invention is weight portion, and the percentage is mass percent.
The object of the present invention is achieved like this：
A kind of preparation method of Zanthoxylum essential oil, by comprising 10~30% dry pericarpium zanthoxyli schinifoliis, 10~30% extra dry red wine Chinese prickly ashes, 10~30% dry big peppery
Green pepper, 10~30% dry capsicums are obtained in interior raw material.
Above-mentioned big capsicum is long red pepper, capsicum long, green pepper or bell pepper, and above-mentioned capsicum is capsicum annum fasciculatum.
Above-mentioned chilli is the ripe capsicum dried, such as dry capsicum can be the ripe capsicum annum fasciculatum dried；It is dry big peppery
Green pepper can be ripe long red pepper, capsicum long, green pepper or the bell pepper dried.
The preparation method of above-mentioned Zanthoxylum essential oil, by Chinese prickly ash and Capsicum crushing after, with oil plant volume ratio in deep fat：10:1~5
Oil immersion, then filter be obtained.
The preparation method of above-mentioned Zanthoxylum essential oil, comprises the following steps：
（1）After 10~30% are mixed with 10~30% without the dry pericarpium zanthoxyli schinifolii of seed without seed extra dry red wine Chinese prickly ash, totally enclosed type pulverizer is used with 5
The sieve of~10 mesh is crushed to form material one；
（2）After 10~30% dry big capsicums are mixed with 10~30% dry capsicums, use totally enclosed type pulverizer with 2500~
4000 turns/h is not added with sieve and crushes, and forms material two；
（3）By step（1）Material one and step（2）Material two well mixed form material three；
（4）Vegetable oil is heated to 120-240 DEG C, stops heating, with vegetable oil and the volume ratio 10 of material three after static 1-3min：
1~5, material three is added, 4~6min is stirred continuously, 25~35min is stood, 25~35min is often stood in 3 hours, it is stirred for 4
~6min；Stop stirring after 3 hours, immersion 2-6h makes oil be fully immersed into Chinese prickly ash and capsicum, and the spicy fragrance of the inside is all complete
Portion is dipped in oil；
（5）The step of by standing（4）Dregs of fat mixture carry out dregs of fat separation, the rotating speed of oil-residue separator is 4500~5500
Turn/h, be then filtrated to get Zanthoxylum essential oil.
In R＆D process, inventor has found, the dregs of fat separate after refined filtration Zanthoxylum essential oil, oil colours it is muddy, it is necessary to stand 10~
20 days could be limpid, this not only adds production cost, extend product export time limit, the also covert guarantor for shortening Zanthoxylum essential oil
The matter phase.
The preparation method of above-mentioned Zanthoxylum essential oil, by step（5）The isolated Zanthoxylum essential oil crude product Zanthoxylum essential oil filtering of the dregs of fat sets
Standby filtering is obtained final product；The step（5）Filter plant include be arrangeding in parallel filtering tank and oil storage tank, at the top of the filtering tank
Oil inlet is provided with, the bottom of the oil storage tank is provided with oil-out, transparent observation is provided with the top of the oil storage tank
Window, the bottom of the filtering tank is connected with the top of the oil storage tank by pipeline, and top and the vavuum pump of the oil storage tank connect
Connect；Wherein, the filtering tapered A of pot bottom, and the pipeline and the taper A bottoms UNICOM, the oil storage pot bottom is in
Taper B, slag notch is provided with the taper B bottoms, and the oil-out is arranged on the side wall of the taper B, and described
Valve is provided with oil-out, base is provided with the filtering tank and the oil storage pot bottom, the base has can
Wrap up the inner chamber of the taper A and/or taper B；Also include filter house, the filter house is to be arranged in the filtering tank inner chamber
Three layer filtration layer, wherein, each layer of filter layer all includes stainless steel stratum reticulare and the mistake being arranged on the stainless steel stratum reticulare
Filter cloth, the stainless steel stratum reticulare is from top to bottom followed successively by 120 mesh, 140 mesh and 160 mesh, and the thickness of the filter cloth is from top to bottom
It is followed successively by 2mm, 3mm and 4mm, and retractable clean-up port is provided with tank skin above each layer of filter layer.
A kind of preparation method of Zanthoxylum essential oil, comprises the following steps：
（1）After 25% is mixed with 25% without the dry pericarpium zanthoxyli schinifolii of seed without seed extra dry red wine Chinese prickly ash, totally enclosed type pulverizer is used with 5~10 purposes
Sieve is crushed to form material one；
（2）After 25% dry big capsicum is mixed with 25% dry capsicum, use totally enclosed type pulverizer with 2500~4000 turns/h not
Plus sieve is crushed, material two is formed；
（3）By step（1）Material one and step（2）Material two well mixed form material three；
（4）Vegetable oil is heated to 120-240 DEG C, stops heating, with vegetable oil and the volume ratio 10 of material three after static 1-3min：
1~5, material three is added, 4~6min is stirred continuously, 25~35min is stood, 25~35min is often stood in 3 hours, it is stirred for 4
~6min；Stop stirring after 3 hours, immersion 2-6h makes oil be fully immersed into Chinese prickly ash and capsicum, and the spicy fragrance of the inside is all complete
Portion is dipped in oil；
（5）The step of by standing（4）Dregs of fat mixture carry out dregs of fat separation, the rotating speed of oil-residue separator is 4500~5500
Turn/h；
（6）The isolated Zanthoxylum essential oil crude product Zanthoxylum essential oil filter plant filtering of the dregs of fat is obtained final product；The step（5）Filtering set
It is standby to include be arranged in parallel filtering tank and oil storage tank, oil inlet is provided with the top of the filtering tank, under the oil storage tank
Portion is provided with oil-out, and transparent observation window, the bottom of the filtering tank and the oil storage are provided with the top of the oil storage tank
The top of tank is connected by pipeline, and the top of the oil storage tank is connected with vavuum pump；Wherein, the filtering tapered A of pot bottom,
And the pipeline and the taper A bottoms UNICOM, the tapered B of oil storage pot bottom, it is provided with the taper B bottoms and is slagged tap
Mouthful, the oil-out is arranged on the side wall of the taper B, and is provided with valve on the oil-out, in the filtering tank
Base is provided with the oil storage pot bottom, the base has the inner chamber that can wrap up the taper A and/or taper B；Also
Including filter house, the filter house is the three layer filtration layer being arranged in the filtering tank inner chamber, wherein, each layer of filter layer is all
Stainless steel stratum reticulare and the filter cloth being arranged on the stainless steel stratum reticulare are included, the stainless steel stratum reticulare is from top to bottom followed successively by
120 mesh, 140 mesh and 160 mesh, the thickness of the filter cloth are from top to bottom followed successively by 2mm, 3mm and 4mm, and in each layer of mistake
Retractable clean-up port is provided with tank skin above filtering layer.
Beneficial effect：
The present invention provides a kind of preparation method of spicy fresh wild citron oil, by the scarlet and pungent of capsicum it is complete incorporate Zanthoxylum essential oil
Manufacture craft in, the Zanthoxylum essential oil of preparation retains numb, peppery, fragrant three kinds of characteristics simultaneously, has broken existing Zanthoxylum essential oil single varieties
Limitation, more demands are provided to consumer, deep to be liked by consumer.The present invention using totally enclosed type crush Chinese prickly ash with it is peppery
Green pepper, can reduce the loss of material in crushing process, and dust pollution can be reduced again, effectively the operating environment of protection workman.This hair
Bright by specific filter plant, obtained final Zanthoxylum essential oil need not stand and can be achieved with transparent glow, save operation step
Suddenly, time and fund cost are saved.Preparation process of the present invention is not used organic solvent, and product does not exist organic solvent residual,
Product Safety is high.Chinese prickly ash spunyarn taste of the present invention is full, and strongly fragrant, free from extraneous odour is more steady to high temperature, high humidity and illumination condition
It is fixed.Extraction process step of the present invention is simple, the Zanthoxylum essential oil outward appearance red, transparent of preparation, glossy, free from admixture bright in colour, without heavy
Form sediment, pectin, oily value, acid value, peroxide content are low and relatively low to equipment, site requirements, are adapted to large-scale promotion application.
Brief description of the drawings
Fig. 1 is the Zanthoxylum essential oil filter plant of embodiment 1.
Specific embodiment
The present invention is specifically described below by specific embodiment, it is pointed out here that following examples are served only for this hair
It is bright to be further described, it is impossible to be interpreted as limiting the scope of the invention, the person skilled in the art of this area can be with root
Some nonessential modifications and adaptations are made to the present invention according to foregoing invention content.The all raw materials of the present invention and reagent are commercially available
Product.
Embodiment 1
As shown in figure 1, a kind of Zanthoxylum essential oil filter plant, including tank body, oil inlet 3, oil-out 5 and filter house, the tank body is
Horizontally disposed two and respectively filtering tank 1 and oil storage tank 2, the bottom of the filtering tank 1 lead to the top of the oil storage tank 2
Piping 4 is connected, and the top of the oil storage tank 2 is connected with vavuum pump 5；The oil inlet 3 is arranged on the top of the filtering tank 1,
The oil-out 6 is arranged on the bottom of the oil storage tank 2, and the filter house is set in the filtering tank inner chamber.Wherein, it is described true
Empty pump can be also connected by pipeline with the top of the oil storage tank.
Wherein, it is provided with three layer filtration layer 7 from top to bottom in the inner chamber of the filtering tank 1, is followed successively by 120 mesh stainless (steel) wires
Layer, 140 mesh stainless steel stratum reticulares, 160 mesh stainless steel stratum reticulares.The filter layer 7 is connected by welding with the inwall of the filtering tank 1,
In addition, being placed with filter cloth on each layer of filter layer 7, the thickness of the filter cloth is followed successively by 2mm, 3mm and 4mm.Also
It is to say to place the thick filter cloths of 2mm on 120 mesh stainless steel stratum reticulares, the thick filterings of 3mm is placed on 140 mesh stainless steel stratum reticulares
Cloth, the filter cloth after placing 4mm on 160 mesh stainless steel stratum reticulares.
And, it is provided with retractable clean-up port 8 on each layer of tank skin of the top of filter layer 7.The clean-up port 8 is can
For the size that people enters, workman can be allowed to enter into filtering tank filter layer 7 is cleared up.
In addition, the tapered A in the bottom of the filtering tank 1, and the entrance of the pipeline 4 and the taper A bottoms UNICOM, the pipe
The outlet of road 4 is connected with the top of oil storage tank 2.The bottom of the oil storage tank 2 is provided with out to be also taper B in the taper B bottoms
Cinder notch 9, is provided with the oil-out 6 on the side wall of the taper B, and valve 10 is provided with the oil-out 6.And
And, base 12 is provided with the filtering tank 1 and the bottom of the oil storage tank 2, the base 12 has can wrap up the cone
The inner chamber of shape A and/or taper B.The top of the base 12 welding or mode connects for screw by way of with the filtering tank 1 or
The outer wall connection of oil storage tank 2.Enable that what the oil storage tank 2 and filtering tank 1 consolidated is placed on bottom surface.
In addition, being provided with transparent observation window 11 at the top of the oil storage tank 2.
Using the Zanthoxylum essential oil filter plant of the present embodiment, the Zanthoxylum essential oil that need to be filtered is poured into tank from the oil inlet 3 of filtering tank 1
Interior, by almost having filtered out the granule foreign in oil after three layer filtration, the oil after filtering is in the filtering tank 1 for the Zanthoxylum essential oil
Congregate precipitation, having after then the vavuum pump 5 is by way of vacuumizing by filtering be drawn into storage from filtering tank 1
In oil tank 2, and precipitated again in oil storage tank 2, the impurity for precipitating is removed by slag notch 9, limpid Chinese prickly ash
Oil is just flowed out by oil-out 6.Be additionally provided on the top of the oil storage tank 2 observation window 11 can real-time monitored to oil storage tank 2
Interior oily depth, need to ensure entrance of the oily height no more than the pipeline being connected with the vavuum pump 5 in oil storage tank 2
Place.In the present embodiment, as long as the Zanthoxylum essential oil in oil storage tank 2 is discontented with, being capable of normal work.
Embodiment 2
The preparation method of Zanthoxylum essential oil, comprises the following steps：
（1）After 25% is mixed with 25% without the dry pericarpium zanthoxyli schinifolii of seed without seed extra dry red wine Chinese prickly ash, totally enclosed type pulverizer is used with the sieve of 10 mesh
Son is crushed and forms material one；
（2）After 25% dry big capsicum is mixed with 25% dry capsicum, totally enclosed type pulverizer is used to be not added with sieve with 3000 turns/h broken
Powder, forms material two；
（3）By step（1）Material one and step（2）Material two well mixed form material three；
（4）Vegetable oil is heated to 240 DEG C, stops heating, static 2min, after after the peculiar smell volatilization completely in vegetable oil, to plant
Thing oil and the volume ratio 10 of material three：3, material three is added, 5min is stirred continuously, 30min is stood, 5min is stirred for, then stand
30min；30min is often stood in 3 hours, 5min is stirred for；5h is soaked after 3 hours, oil is fully immersed into Chinese prickly ash and capsicum,
The spicy fragrance of the inside is all totally immersed into oil；
（5）Dregs of fat separation is carried out by what is stood, the rotating speed of oil-residue separator is 5000 turns/h.
（6）The Zanthoxylum essential oil that the dregs of fat are separate is filtered with the filter of embodiment 1, obtains the transparent Chinese prickly ash of color glow
Oil.
Embodiment 3
The preparation method of Zanthoxylum essential oil, comprises the following steps：
（1）After 15% is mixed with 30% without the dry pericarpium zanthoxyli schinifolii of seed without seed extra dry red wine Chinese prickly ash, totally enclosed type pulverizer is used with the sieve of 10 mesh
Son is crushed and forms material one；
（2）After 25% dry big capsicum is mixed with 30% dry capsicum, totally enclosed type pulverizer is used to be not added with sieve with 4000 turns/h broken
Powder, forms material two；
（3）By step（1）Material one and step（2）Material two well mixed form material three；
（4）Vegetable oil is heated to 120 DEG C, stops heating, static 1min, after after the peculiar smell volatilization completely in vegetable oil, to plant
Thing oil and the volume ratio 10 of material three：5, material three is added, 6min is stirred continuously, 25min is stood, 6min is stirred for, then stand
25min；25min is often stood in 3 hours, 6min is stirred for；6h is soaked after 3 hours, oil is fully immersed into Chinese prickly ash and capsicum,
The spicy fragrance of the inside is all totally immersed into oil；
（5）Dregs of fat separation is carried out by what is stood, the rotating speed of oil-residue separator is 4500 turns/h.
（6）The Zanthoxylum essential oil that the dregs of fat are separate is filtered with the filter of embodiment 1, obtains the transparent Chinese prickly ash of color glow
Oil.
Embodiment 4
The preparation method of Zanthoxylum essential oil, comprises the following steps：
（1）After 30% is mixed with 30% without the dry pericarpium zanthoxyli schinifolii of seed without seed extra dry red wine Chinese prickly ash, totally enclosed type pulverizer is used with the sieve of 10 mesh
Son is crushed and forms material one；
（2）After 25% dry big capsicum is mixed with 15% dry capsicum, totally enclosed type pulverizer is used to be not added with sieve with 2500 turns/h broken
Powder, forms material two；
（3）By step（1）Material one and step（2）Material two well mixed form material three；
（4）Vegetable oil is heated to 180 DEG C, stops heating, static 3min, after after the peculiar smell volatilization completely in vegetable oil, to plant
Thing oil and the volume ratio 10 of material three：1, material three is added, 4min is stirred continuously, 30min is stood, 4min is stirred for, then stand
30min；30min is often stood in 3 hours, 4min is stirred for；2h is soaked after 3 hours, oil is fully immersed into Chinese prickly ash and capsicum,
The spicy fragrance of the inside is all totally immersed into oil；
（5）Dregs of fat separation is carried out by what is stood, the rotating speed of oil-residue separator is 5500 turns/h.
（6）The Zanthoxylum essential oil that the dregs of fat are separate is filtered with the filter of embodiment 1, obtains the transparent Chinese prickly ash of color glow
Oil.
Embodiment 5（Comparative example 1）
The preparation method of Zanthoxylum essential oil, comprises the following steps：
（1）After 25% is mixed with 25% without the dry pericarpium zanthoxyli schinifolii of seed without seed extra dry red wine Chinese prickly ash, totally enclosed type pulverizer is used with the sieve of 10 mesh
Son is crushed and forms material one；
（2）After 25% dry big capsicum is mixed with 25% dry capsicum, totally enclosed type pulverizer is used to be not added with sieve with 3000 turns/h broken
Powder, forms material two；
（3）By step（1）Material one and step（2）Material two well mixed form material three；
（4）Vegetable oil is heated to 300 DEG C, stops heating, static 2min, after after the peculiar smell volatilization completely in vegetable oil, to plant
Thing oil and the volume ratio 10 of material three：3, material three is added, 5min is stirred continuously, 30min is stood, 5min is stirred for, then stand
30min；30min is often stood in 3 hours, 5min is stirred for；5h is soaked after 3 hours, oil is fully immersed into Chinese prickly ash and capsicum,
The spicy fragrance of the inside is all totally immersed into oil；
（5）Dregs of fat separation is carried out by what is stood, the rotating speed of oil-residue separator is 5000 turns/h.
（6）The Zanthoxylum essential oil that the dregs of fat are separate is filtered with the filter of embodiment 1, obtains the transparent Chinese prickly ash of color glow
Oil.
Embodiment 6（Comparative example 2）
The preparation method of Zanthoxylum essential oil, comprises the following steps：
（1）After 25% is mixed with 25% without the dry pericarpium zanthoxyli schinifolii of seed without seed extra dry red wine Chinese prickly ash, totally enclosed type pulverizer is used with the sieve of 10 mesh
Son is crushed and forms material one；
（2）After 25% dry big capsicum is mixed with 25% dry capsicum, totally enclosed type pulverizer is used to be not added with sieve with 3000 turns/h broken
Powder, forms material two；
（3）By step（1）Material one and step（2）Material two well mixed form material three；
（4）Vegetable oil is heated to 240 DEG C, stops heating, static 2min, after after the peculiar smell volatilization completely in vegetable oil, to plant
Thing oil and the volume ratio 10 of material three：3, material three is added, 5min is stirred continuously, 30min is stood, 5min is stirred for, then stand
30min；30min is often stood in 3 hours, 5min is stirred for；5h is soaked after 3 hours, oil is fully immersed into Chinese prickly ash and capsicum,
The spicy fragrance of the inside is all totally immersed into oil；
（5）Dregs of fat separation is carried out by what is stood, the rotating speed of oil-residue separator is 5000 turns/h.
（6）The Zanthoxylum essential oil that the dregs of fat are separate is filtered with conventional refined filtration equipment, obtains Zanthoxylum essential oil.
Embodiment 7
Zanthoxylum essential oil performance measurement prepared by embodiment 2-6
The measure of acid value
Measure according to the animal and plant fat acid values of GB/T 5530-1998 is operated；
The measure of peroxide value
Measure according to the animal and plant fat peroxide values of GB/T 5538-2005 is operated；
Color and luster, numb taste and aroma test
10g Chinese prickly ashes flavored oils are placed in beaker, 50 DEG C or so are heated in water-bath.After glass holds in both hands stirring, 10 persons of commenting are asked to enter
Row evaluation color and luster, numb taste and aroma test.
The evaluation of Chinese prickly ash flavored oils fragrance, using the quantitative description of flavour of food products：Aroma strength does not exist（0 point）,
Aroma strength is just recognized（30 points）, aroma strength is light（45 points）, in aroma strength（60 points）, aroma strength is dense（80 points）, it is fragrant
Gas intensity is dense（100 points）.
The evaluation of Chinese prickly ash seasoning spunyarn taste, using the quantitative description of flavour of food products, the evaluation of Chinese prickly ash flavored oils fragrance,
Using the quantitative description of flavour of food products：Numb taste intensity does not exist（0 point）, numb taste intensity just recognizes（30 points）, numb taste is strong
Maintain normal supply during the slack season（45 points）, in numb taste intensity（60 points）, numb taste intensity is dense（80 points）, numb taste intensity is dense（100 points）
The evaluation of Chinese prickly ash flavored oils pungent, using the quantitative description of flavour of food products, the evaluation of Chinese prickly ash flavored oils pungent is used
The quantitative description of flavour of food products：Pungent intensity does not exist（0 point）, pungent intensity just recognizes（30 points）, pungent intensity is light
（45 points）, in pungent intensity（60 points）, pungent intensity is dense（80 points）, pungent intensity is dense（100 points）
The evaluation of Chinese prickly ash color and luster and transparency
Chinese prickly ash flavored oils 50mL to colorimetric cylinder is measured, 1h is stood at room temperature, then moved to white background wall and visually observe.
And investigate the stability of Zanthoxylum essential oil.
Each embodiment sample is taken respectively appropriate, simulation listing packaging is 75% ± 5% in 40 DEG C ± 2 DEG C of temperature, relative humidity
Under the conditions of place 6 months, respectively at the 0th, 1,2,3,6 the end of month it is separately sampled, to color and luster and transparency, numb taste, pungent, fragrance,
Acid value（MgKOH/g oil）, peroxide（g/100g）Equistability inspection target is measured, and measurement result is shown in Table 1.
Performance prepared by the embodiment 2-7 of table 1
Zanthoxylum essential oil simulation listing packaging prepared by embodiment of the present invention 2-4, is 75% ± 5% in 40 DEG C ± 2 DEG C of temperature, relative humidity
Under the conditions of place 6 months, numb taste, pungent and fragrance are very strong（Higher than 80 points）, and acid value（MgKOH/g oil）Less than 0.5,
Peroxide（g/100g）Less than 0.25.In Chinese prickly ash oil making technology, oil temperature can cause the Zanthoxylum essential oil peroxide for preparing more than 300 DEG C
Change value significantly increases（Such as embodiment 5）, oil temperature it is too low and can in residual plant in the peculiar smell such as the pea green taste, the dark greyish green taste that carry, and
Seize the fragrance of Chinese prickly ash.Meanwhile, the dregs of fat use the Zanthoxylum essential oil of conventional equipment refined filtration after separating（Embodiment 6）, oil colours it is muddy, it is necessary to
Standing 10~20 days could be limpid, this not only adds production cost, extends the product export time limit, and also covert shortens flower
The shelf-life of green pepper oil.The present invention by the complete manufacture craft for incorporating Zanthoxylum essential oil of the scarlet and pungent of capsicum, the Chinese prickly ash of preparation
Oil retains numb, peppery, fragrant three kinds of characteristics simultaneously, and the Zanthoxylum essential oil red, transparent of preparation is spicy full, gives off a strong fragrance, Chinese prickly ash oil quality
It is superior, it is deep to be liked by consumer.
Claims (5)
1. a kind of preparation method of Zanthoxylum essential oil, by comprising 10~30% dry pericarpium zanthoxyli schinifoliis, 10~30% extra dry red wine Chinese prickly ashes, 10~30% dry big
Capsicum, 10~30% dry capsicums are obtained in interior raw material；The big capsicum is long red pepper, capsicum long, green pepper or bell pepper；Institute
Capsicum is stated for capsicum annum fasciculatum.
2. the method for claim 1, it is characterised in that：After by Chinese prickly ash and Capsicum crushing, with oil plant volume in deep fat
Than：10:1~5 oil immersion, then filters and is obtained.
3. the method for claim 1, it is characterised in that comprise the following steps,
Step 1：After 10~30% are mixed with 10~30% without the dry pericarpium zanthoxyli schinifolii of seed without seed extra dry red wine Chinese prickly ash, using totally enclosed type pulverizer
Crush to form material one with the sieve of 5~10 mesh；
Step 2：After 10~30% dry big capsicums are mixed with 10~30% dry capsicums, use totally enclosed type pulverizer with 2500~
4000 turns/h is not added with sieve and crushes, and forms material two；
Step 3：Material one is well mixed to form material three with material two；
Step 4：Vegetable oil is heated to 120-240 DEG C, stops heating, with vegetable oil and the volume ratio of material three after static 1-3min
10：1~5, material three is added, 4~6min is stirred continuously, 25~35min is stood, 25~35min is often stood in 3 hours, then stir
Mix 4~6min；Stop stirring after 3 hours, immersion 2-6h makes oil be fully immersed into Chinese prickly ash and capsicum, the spicy fragrance of the inside all
It is totally immersed into oil；
Step 5：The dregs of fat mixture that will be stood carries out dregs of fat separation, and the rotating speed of oil-residue separator is 4500~5500 turns/h,
Then it is filtrated to get Zanthoxylum essential oil.
4. method as claimed in claim 3, it is characterised in that：The isolated Zanthoxylum essential oil crude product of the dregs of fat is filtered with Zanthoxylum essential oil
Equipment filtering is obtained final product；The filter plant includes the filtering tank that be arranged in parallel（1）And oil storage tank（2）, at the top of the filtering tank
Oil inlet is provided with, the bottom of the oil storage tank is provided with oil-out, in the oil storage tank（2）Top is provided with transparent sight
Examine window（11）, the filtering tank（1）Bottom and the oil storage tank（2）Top pass through pipeline（4）Connection, the oil storage tank
（2）Top and vavuum pump（5）Connection；Wherein, the filtering tank（1）The tapered A in bottom, and the pipeline（4）With the cone
Shape A bottoms UNICOM, the oil storage tank（2）The tapered B in bottom, slag notch is provided with the taper B bottoms（9）, it is described fuel-displaced
Mouth is arranged on the side wall of the taper B, and in the oil-out（6）On be provided with valve（10）, in the filtering tank（1）With
The oil storage tank（2）Bottom is provided with base（12）, the base（12）With the taper A and/or taper B can be wrapped up
Inner chamber；Also include filter house, the filter house is the three layer filtration layer being arranged in the filtering tank inner chamber, wherein, it is each
Layer filter layer all includes stainless steel stratum reticulare and the filter cloth being arranged on the stainless steel stratum reticulare, and the stainless steel stratum reticulare is by upper
120 mesh, 140 mesh and 160 mesh are followed successively by under, the thickness of the filter cloth is from top to bottom followed successively by 2mm, 3mm and 4mm, and
Retractable clean-up port is provided with tank skin above each layer of filter layer.
5. a kind of preparation method of Zanthoxylum essential oil, comprises the following steps,
Step 1：After 25% is mixed with 25% without the dry pericarpium zanthoxyli schinifolii of seed without seed extra dry red wine Chinese prickly ash, totally enclosed type pulverizer is used with 5~10
Purpose sieve is crushed to form material one；
Step 2：After 25% dry big capsicum is mixed with 25% dry capsicum, totally enclosed type pulverizer is used with 2500~4000 turns/h
It is not added with sieve to crush, forms material two；
Step 3：Material one is well mixed to form material three with material two；
Step 4：Vegetable oil is heated to 120-240 DEG C, stops heating, with vegetable oil and the volume ratio of material three after static 1-3min
10：1~5, material three is added, 4~6min is stirred continuously, 25~35min is stood, 25~35min is often stood in 3 hours, then stir
Mix 4~6min；Stop stirring after 3 hours, immersion 2-6h makes oil be fully immersed into Chinese prickly ash and capsicum, the spicy fragrance of the inside all
It is totally immersed into oil；
Step 5：The dregs of fat mixture that will be stood carries out dregs of fat separation, and the rotating speed of oil-residue separator is 4500~5500 turns/h；
Step 6：The isolated Zanthoxylum essential oil crude product Zanthoxylum essential oil filter plant filtering of the dregs of fat is obtained final product；The filter plant includes
Be arranged in parallel filtering tank（1）And oil storage tank（2）, oil inlet is provided with the top of the filtering tank, under the oil storage tank
Portion is provided with oil-out, in the oil storage tank（2）Top is provided with transparent observation window（11）, the filtering tank（1）Bottom
With the oil storage tank（2）Top pass through pipeline（4）Connection, the oil storage tank（2）Top and vavuum pump（5）Connection；Wherein,
The filtering tank（1）The tapered A in bottom, and the pipeline（4）With the taper A bottoms UNICOM, the oil storage tank（2）Bottom is in
Taper B, slag notch is provided with the taper B bottoms（9）, the oil-out is arranged on the side wall of the taper B, and in institute
State oil-out（6）On be provided with valve（10）, in the filtering tank（1）With the oil storage tank（2）Bottom is provided with base
（12）, the base（12）With the inner chamber that can wrap up the taper A and/or taper B；Also include filter house, the filtering
Portion is the three layer filtration layer being arranged in the filtering tank inner chamber, wherein, each layer of filter layer all include stainless steel stratum reticulare and
The filter cloth on the stainless steel stratum reticulare is arranged on, the stainless steel stratum reticulare is from top to bottom followed successively by 120 mesh, 140 mesh and 160
Mesh, the thickness of the filter cloth is from top to bottom followed successively by 2mm, 3mm and 4mm, and on tank skin above each layer of filter layer
It is provided with retractable clean-up port.
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