CN103918802A - Pure natural zanthoxylum oil and industrial production method thereof - Google Patents
Pure natural zanthoxylum oil and industrial production method thereof Download PDFInfo
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- CN103918802A CN103918802A CN201410173303.3A CN201410173303A CN103918802A CN 103918802 A CN103918802 A CN 103918802A CN 201410173303 A CN201410173303 A CN 201410173303A CN 103918802 A CN103918802 A CN 103918802A
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Abstract
The invention discloses pure natural zanthoxylum oil and an industrial production method thereof. The method comprises the following steps: A, removing seeds and stems of high-quality dried zanthoxylum raw materials, and grinding at a low temperature till the granularity of ground raw materials is 40-60 meshes; B, stirring and leaching at room temperature for 1-2 hours by pure natural edible plant oil without any additive, performing reduced pressure suction filtration, and stirring and leaching filter residue for the second time, wherein the volume of the pure natural edible plant oil is 5-10 times that of the ground raw materials or a weight ratio of the ground raw materials to the pure natural edible plant oil 1:(3-6), and the obtained filtrate is used for cycle extraction or mixing; C, centrifugally filtering the filtrate; D, detecting and mixing, namely detecting the obtained zanthoxylum oil, and diluting to a normal spicy degree by vegetable oil; and E, filling to obtain the finished product. The method is simple in process, convenient to operate and low in cost, the edible plant oil which does not contain an additive is adopted, heating is not needed, wastes are not generated, the method has an environment-friendly effect, the squeezed rapeseed oil can be adopted, the requirement that any food additive is not needed is met, the original taste of the zanthoxylum and the rapeseed oil is preserved, precipitate and bitterness are avoided, and the pure natural zanthoxylum oil is full in spicy taste and fragrance of zanthoxylum and is suitable for families, restaurants, hotels, seasoning packets of instant noodles and the like.
Description
Technical field
The invention belongs to food or flavouring manufacture field, relate to particularly a kind of pure natural Zanthoxylum essential oil and industrialized preparing process thereof.
Background technology
At present, Zanthoxylum essential oil has been produced following several method, has very large problem, and 1, solvent extraction method prepares Zanthoxylum essential oil, equipment investment is large, and solvent is inflammable and explosive, has a big risk; Meanwhile, in product, there is dissolvent residual, edible dangerous, add that in production process, solvent evaporates has pollution, not environmental protection.2, supercritical extraction is produced Zanthoxylum essential oil, and equipment investment is large, and output is little, is unfavorable for suitability for industrialized production; In producing, there is very large CO2 emission simultaneously, can produce greenhouse effects.
Above-mentioned two kinds of methods are at present with the most use, allocate, otherwise have a lot of sediments but the xanthoxylum oleoresin extracting all needs to add emulsifying agent after diluting with vegetable oil, do not reach the effect of pure natural.In addition, carry out lixiviate with 80-260 degree oil, this method at high temperature easily produces carcinogen, and the quick-fried squeezing Zanthoxylum essential oil of high temperature produces a large amount of oil smoke, contaminated environment.Aromatic oil in Chinese prickly ash at high temperature volatilizees soon simultaneously, does not utilize to greatest extent the aromatic oil in Chinese prickly ash, thereby causes the fragranced deficiency in product.
Moreover fresh pepper is mixed squeezing and is prepared the method for Zanthoxylum essential oil with rape oil, squeeze insufficiently, extract not thoroughly, to carry out water-oil separating simultaneously, complex process, operating difficulties, human cost is high.
Chinese patent 200810045997.7 discloses " a kind of leaching device of Zanthoxylum essential oil and leach extraction method thereof ", and vegetable oil need be heated to 80-90 ° of C, and this also can bring adverse effect.
Summary of the invention
The object of the present invention is to provide a kind of pure natural Zanthoxylum essential oil and industrialized preparing process thereof, solved the deficiency of said method, the method technique is simple, easy to operate, cost is low, does not produce waste material, environmental protection, without any food additives, keep the original flavor of Chinese prickly ash and rapeseed oil, without precipitation, without bitter taste, Chinese prickly ash fiber crops taste and fragranced foot, be applicable to the aspects such as family, restaurant, hotel and condiment for instant noodles bag and use.
Object of the present invention and solve its technical problem underlying and realize by the following technical solutions: a kind of pure natural Zanthoxylum essential oil, obtains through following industrialized preparing process: A, high-quality dried flower green pepper raw material carry out low-temperature grinding 40-60 order after the past, seed removed handle;
B, by the raw material of steps A at room temperature with 5-10 times of volume or weight ratio be 1:3-6 containing the hatvral food plants oil stirring and leaching 1-2 hour of additive, carry out decompress filter; Filter residue carries out stirring and leaching for the second time, and filtrate being used for of gained circulates and extract or allotment;
C, filtrate are through centrifugal filtration;
D, detection allotment, the Zanthoxylum essential oil of gained detects, and is then diluted to normal numb degree with rape oil;
E, the filling finished product that obtains.
Described high-quality dried flower green pepper is the expensive pericarpium zanthoxyli schinifolii of Guizhou plate.
Described step D, it is 2.5% that rape oil is diluted to numb degree.
The present invention compared with prior art has obvious advantage and beneficial effect.From above technical scheme, technique of the present invention is simple, easy to operate, cost is low, adopts hatvral food plants oil, does not heat, do not produce waste material, environmental protection, can adopt the rapeseed oil oneself squeezing simultaneously, reach the requirement without any food additives, keep the original flavor of Chinese prickly ash and rapeseed oil, without precipitation, without bitter taste, Chinese prickly ash fiber crops taste and fragranced foot, product is applicable to the aspects such as family, restaurant, hotel and condiment for instant noodles bag and uses.
Brief description of the drawings
Fig. 1 is process chart of the present invention.
Detailed description of the invention
Below in conjunction with accompanying drawing and preferred embodiment, to a kind of pure natural Zanthoxylum essential oil and industrialized preparing process detailed description of the invention, feature and effect thereof of proposing according to the present invention, be described in detail as follows.
Referring to Fig. 1, a kind of pure natural Zanthoxylum essential oil, obtains through following industrialized preparing process:
1, high-quality dried flower green pepper raw material carries out low-temperature grinding 40-60 order after the past, seed removed handle; As too thin in pulverized, after lixiviate, suction filtration is very difficult, easily stops up.
2, by the raw material of step 1 at room temperature with 5-10 times of volume or weight ratio be 1:3-6 containing the hatvral food plants oil stirring and leaching 1-2 hour of additive, the time is short, the lixiviate vegetable oil state that do not reach capacity, carries out decompress filter; After lixiviate, in zanthoxylum powder, also contain for the first time part numb-taste component of zanthoxylum and aromatic substance, filter residue carries out stirring and leaching for the second time, and filtrate being used for of gained circulates and extract or allotment.As vegetable oil heating lixiviate easily produces carcinogen, under heated condition, the aromatic substance in Chinese prickly ash is volatile, thereby causes the fragranced deficiency of product simultaneously.
3, filtrate is through centrifugal filtration, and centrifugal filtration can be by a small amount of suspended material and moisture removal in Zanthoxylum essential oil, and it is transparent that product reaches, without precipitation state.
4, detect allotment, the Zanthoxylum essential oil of gained detects, and is then diluted to normal edible numb degree 2%-3% with rape oil.
5, the filling finished product that obtains, in product, the impurity such as polysaccharide and resin is few, and viscosity is low, and without precipitation, without any additive, numb taste, fragrance foot, meet the requirement of natural green food, edible safety.
Described high-quality dried flower green pepper is the expensive pericarpium zanthoxyli schinifolii of Guizhou plate.
Described step 4, it is 2.5% that rape oil is diluted to numb degree.
According to the sense organ requirement of Zanthoxylum essential oil in the provincial standard DB52/493-2005 of Guizhou Province, formulate sensory evaluation scores standard scale 1 of the present invention:
By pure natural Zanthoxylum essential oil sensory evaluation scores of the present invention is drawn to following experimental data.The evaluation group (being professional flavoring researcher) being made up of 7 people, judges chamber according to standard shown in table 1 in specialty product sensory quality is evaluated.Evaluation is carried out under nature light in the time that product temperature and room temperature reach constant: first get appropriate sample in colorimetric cylinder, observe its color and luster and transparency, the judge smell of then unpacking, finally gargles by warm water, trial test product flavour.Product sensory scoring is all averaged and is drawn data, in table 2.
As shown in Table 2, the present invention adequately and reasonably utilizes the pericarpium zanthoxyli schinifolii aboundresources of From Anshun of Guizhou, the feature that numb taste is high, fragranced is sufficient, pericarpium zanthoxyli schinifolii is developed into family expenses Zanthoxylum essential oil, solve the shortcoming that Chinese prickly ash spunyarn taste is not high in the market, fragranced is not enough, temperature production simultaneously, has avoided vegetable oil in high temperature process process to produce carcinogen.Comprehensive sensory evaluation, conclusion: green zanthoxylum oil of the present invention, numb taste and the fragrant of pericarpium zanthoxyli schinifolii are fully used, be that a kind of color and luster is good, fragranced is good, the flavoring of numb taste foot.Technique is simple, easy to operate simultaneously, and cost is low, employing hatvral food plants oil, does not heat, and does not produce waste material, environmental protection, can adopt the rapeseed oil oneself squeezing, reach the requirement without any food additives, keep the original flavor of Chinese prickly ash and rapeseed oil simultaneously, without precipitation, without bitter taste, Chinese prickly ash fiber crops taste and fragranced foot, product is applicable to the aspects such as family, restaurant, hotel and condiment for instant noodles bag and uses.
The above, it is only preferred embodiment of the present invention, not the present invention is done to any pro forma restriction, any technical solution of the present invention content that do not depart from, any simple modification, equivalent variations and the modification above embodiment done according to technical spirit of the present invention, all still belong in the scope of technical solution of the present invention.
Claims (3)
1. a pure natural Zanthoxylum essential oil, is characterized in that: obtain through following industrialized preparing process:
A, high-quality dried flower green pepper raw material carry out low-temperature grinding 40-60 order after the past, seed removed handle;
B, by the raw material of steps A at room temperature with 5-10 times of volume or weight ratio be 1:3-6 containing the hatvral food plants oil stirring and leaching 1-2 hour of additive, carry out decompress filter; Filter residue carries out stirring and leaching for the second time, and filtrate being used for of gained circulates and extract or allotment;
C, filtrate are through centrifugal filtration;
D, detection allotment, the Zanthoxylum essential oil of gained detects, and is then diluted to normal numb degree with rape oil;
E, the filling finished product that obtains.
2. a kind of pure natural Zanthoxylum essential oil as claimed in claim 1, is characterized in that: described high-quality dried flower green pepper is the expensive pericarpium zanthoxyli schinifolii of Guizhou plate.
3. a kind of pure natural Zanthoxylum essential oil as claimed in claim 1, is characterized in that: described step D, it is 2.5% that rape oil is diluted to numb degree.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410173303.3A CN103918802A (en) | 2014-04-28 | 2014-04-28 | Pure natural zanthoxylum oil and industrial production method thereof |
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| CN201410173303.3A CN103918802A (en) | 2014-04-28 | 2014-04-28 | Pure natural zanthoxylum oil and industrial production method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104172067A (en) * | 2014-07-17 | 2014-12-03 | 江苏华桑食品科技有限公司 | Method for preparing green prickleyash extract |
| CN104255955A (en) * | 2014-09-05 | 2015-01-07 | 周顺 | Fresh green pepper edible oil |
| CN105907460A (en) * | 2016-06-12 | 2016-08-31 | 四川厚德医药科技有限公司 | Preparation method of dry pricklyash peel oil |
| CN106720468A (en) * | 2016-11-15 | 2017-05-31 | 重庆凯莱调味食品有限公司 | A kind of spicy fresh fragrant Zanthoxylum essential oil preparation method |
| CN109090266A (en) * | 2018-08-29 | 2018-12-28 | 陕西为康食品科技股份有限公司 | A kind of production method of quick-fried wild citron oil |
| CN110651839A (en) * | 2019-10-31 | 2020-01-07 | 宁夏回春生物科技有限公司 | Preparation method of grape seed nutritional oil |
| CN112552994A (en) * | 2020-12-16 | 2021-03-26 | 四川怡味生物科技有限公司 | Zanthoxylum oil and preparation method thereof |
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| CN101606676A (en) * | 2009-07-13 | 2009-12-23 | 周大甫 | A kind of production technology of fresh zanthoxylum oil |
| CN102757860A (en) * | 2012-07-20 | 2012-10-31 | 王贤成 | Preparation method of pepper oil |
| CN102934705A (en) * | 2012-10-25 | 2013-02-20 | 四川五丰黎红食品有限公司 | Preparation method of olive zanthoxylum oil |
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2014
- 2014-04-28 CN CN201410173303.3A patent/CN103918802A/en active Pending
Patent Citations (3)
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| CN101606676A (en) * | 2009-07-13 | 2009-12-23 | 周大甫 | A kind of production technology of fresh zanthoxylum oil |
| CN102757860A (en) * | 2012-07-20 | 2012-10-31 | 王贤成 | Preparation method of pepper oil |
| CN102934705A (en) * | 2012-10-25 | 2013-02-20 | 四川五丰黎红食品有限公司 | Preparation method of olive zanthoxylum oil |
Non-Patent Citations (1)
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104172067A (en) * | 2014-07-17 | 2014-12-03 | 江苏华桑食品科技有限公司 | Method for preparing green prickleyash extract |
| CN104172067B (en) * | 2014-07-17 | 2015-12-09 | 江苏华桑食品科技有限公司 | A kind of preparation method of pericarpium zanthoxyli schinifolii extract |
| CN104255955A (en) * | 2014-09-05 | 2015-01-07 | 周顺 | Fresh green pepper edible oil |
| CN105907460A (en) * | 2016-06-12 | 2016-08-31 | 四川厚德医药科技有限公司 | Preparation method of dry pricklyash peel oil |
| CN106720468A (en) * | 2016-11-15 | 2017-05-31 | 重庆凯莱调味食品有限公司 | A kind of spicy fresh fragrant Zanthoxylum essential oil preparation method |
| CN109090266A (en) * | 2018-08-29 | 2018-12-28 | 陕西为康食品科技股份有限公司 | A kind of production method of quick-fried wild citron oil |
| CN110651839A (en) * | 2019-10-31 | 2020-01-07 | 宁夏回春生物科技有限公司 | Preparation method of grape seed nutritional oil |
| CN112552994A (en) * | 2020-12-16 | 2021-03-26 | 四川怡味生物科技有限公司 | Zanthoxylum oil and preparation method thereof |
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Application publication date: 20140716 |