CN106720464A - It is a kind of to be adapted to peony seeds flavored oils designed for old people - Google Patents
It is a kind of to be adapted to peony seeds flavored oils designed for old people Download PDFInfo
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- CN106720464A CN106720464A CN201611050086.4A CN201611050086A CN106720464A CN 106720464 A CN106720464 A CN 106720464A CN 201611050086 A CN201611050086 A CN 201611050086A CN 106720464 A CN106720464 A CN 106720464A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Edible Oils And Fats (AREA)
Abstract
The invention belongs to grease processing technology field, and in particular to a kind of to be adapted to peony seeds flavored oils designed for old people, the preparation method of the flavored oils is further related to.It is a kind of to be adapted to peony seeds flavored oils designed for old people, including following components：Peony seed oil, DHA algal oil, phosphatidylserine, compound stabilizer.The present invention is pre-processed to oil plant：Using cryogenic freezing combination extrusion, the cell membrane of oil plant is set thoroughly to rupture and loose many spaces, subcritical solvent is very easy to be contacted with micro- elaioleucite into internal, is dissolved and collects out；Extraction times are reduced to 23 times from 35 times common extractions, technique is simplified, the time for extracting every time, from 40 common 60min, is reduced to 30 40min, saves time, energy consumption and cost.
Description
Technical field
The invention belongs to grease processing technology field, and in particular to a kind of to be adapted to peony seeds flavored oils designed for old people,
Further relate to the preparation method of the flavored oils.
Background technology
Currently, most of edible oil of domestic and international resident is the grease from animal or plant, and its basis is
The triglycerides of various aliphatic acid.The generally acknowledged essential fatty acid of nutrition educational circles has two kinds, and one kind is n-6 series linoleic acid (18
Carbon dienoic acid), another kind is the n-3 series fatty acids as representative with alpha linolenic acid (octatecatrienoic acid).Entrusted according to the Chinese government
Support Chinese Soclety of Nutrition formulates《DRIs (DRIs)》Standard, it is linoleic for each person every day
Intake should be 2.5-9.0%E；The intake of alpha linolenic acid should be 0.5-2.5%E；Reduced mass numerical value linoleic acid intake should
It it is 7.2-25.9 grams, leukotrienes intake should be 1.4-7.2 grams.The survey data of China's issue is, linoleic acid intake per capita
Met or exceeded suitable intake standard, and alpha linolenic acid intake is 0.4 gram per capita, only reach suitable intake mark
The 5.7%-28% of quasi- numerical value.Its reason is grease such as lard, sheep oil, cream, soybean oil, the flower of China's resident's daily consumption
Oil generation, rapeseed oil, olive oil, camellia oil are rich in linoleic acid, and linolenic acid content is little.It is considered that at the most of residents of China
Wretched insufficiency state is taken in leukotrienes.This situation has important bad shadow for the cardiovascular health and brain health of resident
Ring, so it is significant that leukotrienes is supplemented in terms of diet nutritional.
Current China found successively it is a limited number of on the subcritical report for preparing edible vegetable oil of butane, but,
Generally existing extraction times are more to be only possible to reach the effect compared with high oil recovery, and this can be produced for the industrial efficiency of large-scale production
Raw adverse effect.For example：Northeast Forestry University Yao Huan is joyous《Oil is comprehensively utilized with Paeonia suffruticosa seed oil extract and residue》It is related to system
Oily method compares, it is believed that butane subcritical abstraction 3 times, oil yield only up to 23.92%, hence it is evident that less than n-hexane ultrasonic extracting method
29.00%；
Jiangsu University Zhou Shilong《The subcritical butane extracted character research of soybean embryo fat/oil》It has been shown that, butane extraction 3 times, often
Secondary extraction time 30min, extraction yield 9.3%.What Wuhan Polytechnic University Zhang Yanpeng was disclosed《Subcritical butane extraction prepares soybean
The research of embryo oil》Report, subcritical butane extracts optimum process condition and is：The mesh of raw material particle size 40,50 DEG C of extraction temperature, every time
Extraction time 40min, extracts 5 times.
Gansu light industry research institute discloses and shinyleaf yellowhorn oil side is extracted from shiny-leaved yellowhorn seed using subcritical HFC-134a fluid
Method.A kind of method that shinyleaf yellowhorn oil is extracted in seed from shiny-leaved yellowhorn, shiny-leaved yellowhorn seed raw material is crushed to 40~60 mesh, subcritical tetrafluoro second
The extraction temperature of alkane fluid is 30~40 DEG C, and extracting pressure is 1.0~1.2MPa, and each extraction time is 30~40min, is repeated
Extraction 3 times；Separation temperature is 45~55 DEG C, takes out negative pressure with diaphragm type compressor and is gradually depressured to 5 × 10<sup>-2</sup>Pa,
Each disengaging time is 20~30min, repeated isolation 3 times；Finally merge shinyleaf yellowhorn oil crude oil and pass through high speed freezing centrifuge again
Centrifugation, filtering, obtain shinyleaf yellowhorn oil product.Experiments verify that, shinyleaf yellowhorn oil yield is under the conditions of process above
31.8%, product quality is good.
CN 103815053.A disclose a kind of preparation method of puerpera with peony seeds flavored oils, specifically, its pretreatment
Including water immersion 5-10h, -20 DEG C to -10 DEG C freezing 8-10h, then vacuum microwave drying, heat-pump dehumidification are dried.Next step 20-
60MPa squeezings (static state) 8-10h obtains peony seed oil.Above-mentioned method energy consumption is higher relatively costly so as to cause.
In CN 103815058.A patents, oil-producing technique for the connection after subcritical abstraction be not normal refinery activities and
It is to carry out molecular distillation twice, collects its heavy phase composition i.e. peony seed oil, it is characterised in that by peony seed oil, rice embryo oil, tomato
Extract and catechin are constituted, and the percentage that each raw material addition quality accounts for edible oil gross mass is：Peony seed oil 42-65%, rice
Embryo oil 33-52%, tomato extract 1-4% and catechin 1-2%.In the above mentioned patent applications in file, for grease
Antioxidative stabilizer, with the addition of polyglycerol monooleate, and the composition can belong to polyglyceryl fatty acid ester additive, but GB
GB2760-2014 specifies that the product when for fat emulsification, must not be used for vegetable oil；When such as reducing consumption for vegetable oil,
Regulation is only limitted to frying oil.The content of the invention Section 1 of this document is to make antioxidant using catechin, in order to solve catechin
Difficult problems of dissolution, adds polyglycerol monooleate and ethanol in edible oil, then increases not clear problem.Above-mentioned
Only has the freshness date shelf-life in short description that improve edible oil in file for the effect of antioxidant, without specifically grinding
Study carefully data.
According to Chinese Diet Balance Index (DB1), the Dietary Quality of overall merit the elderly finds edible oil (c7) intake
It is suitable only to account for 20.9%, intake excessively lacked of proper care with fatty acid proportion up to 79.1%.China's many regional the elderly's markization generations
Thank to syndrome illness rate and reach 28,8%, markization central obesity rate 41.2%, markization hypertension rate 50.3%, markization hyperglycaemia
Rate is 39.5%；Logistic regression analyses show that different Dietary Patterns have Different Effects to metabolic syndrome and its component.Knot
By：The elderly's metabolic syndrome and its component abnormal rate are higher than low age groups, and wherein edible oil intake is higher, n-3 is serial
It is important factor in order that aliphatic acid intake is relatively low.It is that senile dementia is outside the old human factor of harm to remove metabolic syndrome
The bigger threat of the elderly.The present invention should focus on the prevention and treatment for senile dementia.For above-mentioned patent or patent Shen
Please or document defect, it would be highly desirable to invent a kind of low cost, plant-derived antioxidant is added to extend the holding phase of grease
The peony seeds flavored oils of limit.
The content of the invention
In order to solve above-mentioned technical problem, extrusion is combined the invention provides a kind of pretreatment by cryogenic freezing
With the method that subcritical abstraction prepares feature peony seed oil.
Suitable peony seeds flavored oils designed for old people of the invention are to solve the above by following technical schemes
Technical problem：
It is a kind of to be adapted to peony seeds flavored oils designed for old people, including following components：
Peony seed oil, DHA algal oil；
The parts by weight of peony seed oil are 20-80, the parts by weight of DHA algal oil are 1-4；
Also include phosphatidylserine；The amount of phosphatidylserine is 40-80ppm；
Also include stabilizer, the amount of stabilizer is 20-100ppm.
Stabilizer includes that stabilizer A, stabilizer A include fresh peony flower essential oil.
Stabilizer also includes that stabilizer B, stabilizer B include at least one in lycopene, capsorubin.
Stabilizer A also includes at least one in fat-soluble polyphenol, Rosmarinus officinalis extract, and fat-soluble polyphenol is fat-soluble tea
At least one in polyphenol or carnosol.
Stabilizer is 10ppm lycopenes, the fat-soluble polyphenol of 70ppm, 20ppm fresh peony flower essential oils.
Stabilizer also includes astaxanthin.
Peony seeds flavored oils include peony seed oil, the DHA algal oil of 2 weight portions, the compound stabilizer of 70 weight portions：Tomato red
Element is 10ppm, fat-soluble polyphenol is 60ppm, fresh peony flower essential oil is 20ppm.
Peony seeds flavored oils include peony seed oil, the DHA algal oil of 2 weight portions, the compound stabilizer of 70 weight portions：Tomato red
Element is 10ppm, Tea Polyphenols fatty acid ester:60ppm, fresh peony flower essential oil are 20ppm.
In compound stabilizer, tea polyphenol-palmitate 40ppm, fresh peony flower essential oil 20ppm, Rosmarinus officinalis extract 10ppm.
A kind of preparation method for being adapted to peony seeds flavored oils designed for old people of the invention, including following steps：
The peony seeds that will be chosen are freezed, peeled off, expanded, subcritical butane extraction, obtain peony seeds crude oil；
In freezing step, peony seeds are placed at a temperature of-9-- 4 DEG C, freezed 10-24 hours, peeled off after taking-up, obtained
Peony seeds benevolence；
Peony seeds benevolence is rolled into embryo must expect embryo, be dosed to extruder, expect embryo aqueous 10~12%；Roll flake thickness degree 0.35~
0.45mm；Enter bulking machine material embryo moisture 10~11%；Go out bulking machine material embryo moisture 12~13%；105~110 DEG C of drop temperature；
Enter 0.65~0.75Mpa of bulking machine steam pressure；Vapor (steam) temperature：174.5℃；Hydraulic system working pressure 10.00-
19.00Mpa, obtains expanded peony seeds benevolence raw material；
Expanded peony seeds benevolence raw material is put into the extractor of subcritical equipment, raw material is with the mass volume ratio of butane solvent
1:1-1:3,30-50 DEG C of extraction temperature；Extracting pressure is 0.35-0.6Mpa, continuous to extract 2-3 times, each time 30-40 points
Clock；
Peony seeds crude oil is refined using conventional fat degumming decoloring method；
The peony seed oil for refining later is mixed by weight proportion with DHA algal oil, phosphatidylserine, emulsifying agent is added
And compound stabilizer, stir, emulsion is obtained, emulsified solution is emulsified to obtain to emulsion high shear, then to emulsified solution
Ultrasonication, obtains suitable peony seeds flavored oils designed for old people；
The parts by weight of peony seed oil are 20-80 parts, and the parts by weight of DHA algal oil are 1-4 parts；The amount of compound stabilizer is
20-160ppm；The amount of phosphatidylserine is 50ppm；
Compound stabilizer includes fresh peony flower essential oil, fat-soluble polyphenol, Rosmarinus officinalis extract, astaxanthin, lycopene, peppery
At least one in green pepper red pigment.
Flavored oils in the present invention using plant origin stabilizer, the stabilizer makes shelf life of products ratio use this area
Interior conventional TBHQ (tert-butylhydroquinone) improves 40%.The product can fill according to the requirement of Chinese residents dietary guidelines
Point supplement China resident general lack of important nutrient leukotrienes, DHA so that have safeguard brain health and
The function of cardiovascular health；Significance is respectively provided with terms of economic benefit and social benefit.
In formula of the invention, using fresh peony flower essential oil as stabilizer, the smell of flavored oils is not only improved, and
And enhance the inoxidizability of flavored oils.
The raw material peony seed oil that product of the present invention is used is a kind of rich in linolenic edible vegetable oil, its linolenic acid content
More than 38%.Experiments verify that peony seed oil has the function of reducing in terms of high fat of blood, high cholesterol, hyperglycaemia.The present invention
Product peony seeds crude oil preparation technology neither use milling process, n-hexane lixiviation process is not used yet, because milling process is general
The extruding of pressafiner its discharging opening terminal heat up up to 130 DEG C, can make protein and other activity in peony seeds into
Divide high-temperature denatured, be unfavorable for the preparation of the products such as follow-up tree peony albumen and biological phenol；Although and n-hexane lixiviation process is led in liquefaction
Domain is continued to use for a long time, but, n-hexane really belongs to hazardous solvent, there is environmental issue and dissolvent residual threatens food-safety problem.This
Invent use butane subcritical abstraction, experiment proves that, be to avoid foregoing two ways, a kind of low temperature system for separately selecting
The method of oil.
Another improvement of the invention is in the production technology of flavored oils, peony seeds benevolence to be placed in-9-- Cool Room 4 DEG C
Storage, not only can preservation by low temperature guarantee the quality again be beneficial to subsequent technique.The present inventor is by many experiments, it was therefore concluded that, in peony seeds benevolence
Portion's eucaryotic cell structure is the stage that material internal moisture forms ice crystal in -4 DEG C or -5 DEG C, and the expansion of ice crystal can make oil plant cell
Wall ruptures.But because peony seeds raw aqueous rate is not high, the cell proportion being broken is not high.The present inventor is by repeatedly examination
Checking is bright, and profound hypothermia is quick-frozen to have significant difference with freezing slowly compared with low temperature：The ice crystal of quick-frozen generation is smaller, it is slow freeze the ice crystal that produces compared with
Greatly；Larger ice crystal is larger for the structural change of plant cell, thus is conducive to follow-up smudge cells to extract grease.This
Outward, result of the test further shows that the subsequent product obtained by Different hypothermia handling process, the clarity within the shelf-life has not
Together：In first 2 months of shelf-life, appearance causes the underproof probability of clarity high to profound hypothermia handicraft product because of floccule,
And compared with the product of low temperature process, never there is floccule problem.
After freezing, then oil plant extrusion treatment is carried out, the recovery rate for oil product is greatly improved, and right
Also there is significant impact in the quality of oil product.
The present invention is first freezed peony seeds by the way of freezing, its internal moisture is formed ice crystal, causes cell to break
Split, be conducive to follow-up extraction；In conjunction with extruding-puffing technique, in the state of the cell membrane of oil plant cell has been crushed, group
The increase of inside configuration space is knitted, intracellular micro- elaioleucite is easier to be separated by external force (mechanical force, the fusion power of solvent).
Oil plant makes leaching solvent than reducing in the destruction and infiltrative improvement of expanded middle cell, and solvent is than by raw embryo
0.8:1 is reduced to 0.6:1, it is thus apparent that improve miscella concentration, make miscella concentration improve to 28 from 20% or so~
30%.Therefore, the load of miscella evaporation system and the load of solvent recovery are alleviated.Save the steaming of miscella evaporation operation
Vapour is consumed.
And using extrusion treatment, it is passivated the enzyme in oil plant, improve the quality of Extractive crudeoil.
Enzyme and ANFs in oil plant in extrusion pressing puffing process be passivated, it is to avoid lipoxidase and phosphatide
Influence of the enzyme to phosphatide in oil plant, reduces the content of non-hydratable phospholipid in Extractive crudeoil, increased total phospholipids in Extractive crudeoil
Content, can effectively improve oil and fat refining efficiency, improve oil and fat product quality, and improve phosphatide by-product in aquation scouring processes
The yield of product and the quality of phospholipid prod.
Relative to CN 103815058.A in background technology, the method for the present invention is that fat-soluble tea polyphenol is added, and is not deposited
Described in the background " make antioxidant using catechin, in order to solve catechin difficult problems of dissolution in edible oil,
Polyglycerol monooleate and ethanol are added, then increase not clear problem " problem of this respect.
Relative to the method disclosed by CN 103815058.A in background technology, the invention provides a kind of low energy consumption, height
Efficiency, the peony seed oil production process for meeting laws and regulations requirement：After raw material freezing+extrusion, subcritical abstraction obtains final product male
Red seed oil, product meets country and defends the quality requirement that No. 9 bulletin annex of planning commission 2011 year is write exactly.
Relative to CN 103815053.A, method of the present invention energy consumption is relatively low, and low cost.
The beneficial effects of the present invention are after the present invention is to the pretreatment of oil plant, using fast low temperature freezing combination extruding
It is expanded, make the cell membrane of oil plant thoroughly rupture and loose many spaces, subcritical solvent is very easy to enter internal with micro- elaioleucite
Contact, is dissolved and collects out, and extraction times are reduced to 2-3 times from 3-5 times common extraction, simplifies technique, every time
The time of extraction, from common 40-60min, is reduced to 30-40min, time, energy consumption and cost is saved, in large-scale production
In have and important mention production efficiency, energy-saving meaning.
Peony seeds flavored oils of the invention, overcome fatty acid proportion imbalance in background technology the elderly's intake edible oil
Problem, improve n-3 aliphatic acid intakes, flavored oils of the invention play the role of good for prevention elderly dementia.
Specific embodiment
The present invention is further described with reference to specific embodiment, so as to those skilled in the art more
Understand the present invention, but the present invention do not limited with this.
Embodiment 1
It is adapted to peony seeds flavored oils designed for old people, its preparation method includes following steps：
The peony seeds that will be chosen are freezed, peeled off, expanded, subcritical butane extraction, obtain peony seeds crude oil；
In freezing step, peony seeds are placed at a temperature of -5 DEG C, freezed 16 hours, peeled off after taking-up, obtain peony seeds benevolence；
Peony seeds benevolence is rolled into embryo must expect embryo, be dosed to extruder, expect embryo aqueous 11%；Roll flake thickness degree 0.4mm；Enter swollen
Change machine material embryo moisture 10%；Go out bulking machine material embryo moisture 12%；108 DEG C of drop temperature；Enter bulking machine steam pressure 0.7Mpa；Steam
Stripping temperature：174.5℃；Hydraulic system working pressure 15Mpa, obtains expanded peony seeds benevolence raw material；
Expanded peony seeds benevolence raw material is put into the extractor of subcritical equipment, raw material is with the mass volume ratio of butane solvent
1:2,40 DEG C of extraction temperature；Extracting pressure is 0.5Mpa, continuous to extract 2 times, 40 minutes each time, after solvent evaporation is reclaimed
Obtain peony seeds crude oil；
Peony seeds crude oil is refined using conventional fat degumming decoloring method；
The peony seed oil for refining later is mixed by weight proportion with DHA algal oil, phosphatidylserine, emulsifying agent is added
Soybean lecithin and compound stabilizer, are stirred, and obtain emulsion, and emulsified solution is emulsified to obtain to emulsion high shear, then right
Emulsified solution ultrasonication, obtains suitable peony seeds flavored oils designed for old people；
The parts by weight of peony seed oil are 60 parts, and the parts by weight of DHA algal oil are 3 parts；The amount of phosphatidylserine is
50ppm；
Compound stabilizer is：The fat-soluble polyphenol of 20ppm lycopenes, 40ppm, 20ppm fresh peony flower essential oils；
The condition of emulsion high shear emulsification is that shearing rotating speed is 12000r/min, and the time is 20min, high-pressure homogeneous
The pressure for the treatment of is divided into two-stage, and the first stage pressure is 40MPa, and the second stage pressure is 150MPa, and homogeneous 1-2 times obtains emulsification molten
Liquid.
After being placed 30 days in above-mentioned oil product photoenvironment at normal temperatures, same, compare its inoxidizability, instrument：
Edible oil oxidation stability analyzer is led in the Switzerland ten thousand of racimat 743
Assay method condition：According to US corn chemist association AACC-58-52 standards；120 DEG C, throughput 20L/h.
Sample quality：3g or so.
Antioxidant is originated：Import fat-soluble tea polyphenol EGCg Oil act on behalf of japanese product from Beijing Jie Sen sources；It is domestic
Fat-soluble tea polyphenol comes from Yuyao grand Products of curry favour moral.TBHQ comes from Guangdong Guang Yi food additives Co., Ltd.
Oil source：The product of commercially available domestic execution national standard.
Tea Polyphenols is derived from a kind of of tealeaves is beneficial to the functional components of health, is also a kind of good food
Antioxidant.But, it has good water solubility, and can not be dissolved in grease, so as to limit answering in edible oil
With.Fat-soluble tea polyphenol is equally the antioxidant for extracting processing as raw material with green tea, and main component is also catechin thing
Matter, important feature is with fat-soluble.
Shown using active oxygen method (AOM methods) specialty oil oxidative stability analyzer test result, its antioxygenic property
Dibutyl hydroxy toluene (BHT), the tert-butylhydroquinone (TBHQ) commonly used in the trade better than row.Oil can be kept after adding in proportion
The original quality of product, can increase oil product transparency and brightness, increase the fresh peony flower fragrance of product；In terms of the shelf-life, at present I
Generally using addition antioxidant TBHQ100-200ppm, the shelf-life reaches 18 months, what the present invention was used in state's edible oil field
Composite antioxidant is substantially better than the effect of TBHQ100-200ppm.Calculated by experience in industry and about can reach 24 months.Checking
Result see the table below：
5 kinds of antioxidants are to 7 kinds of influences of the oxidation stability of grease
Embodiment 2
The preparation method for being adapted to peony seeds flavored oils designed for old people is as follows：
The peony seeds that will be chosen are freezed, peeled off, expanded, subcritical butane extraction, obtain peony seeds crude oil；
In freezing step, peony seeds are placed at a temperature of -7 DEG C, freezed 15 hours, peeled off after taking-up, obtain peony seeds benevolence；
Peony seeds benevolence is rolled into embryo must expect embryo, be dosed to extruder, expect embryo aqueous 10%；Roll flake thickness degree 0.35mm；Enter
Bulking machine material embryo moisture 10%；Go out bulking machine material embryo moisture 12%；105 DEG C of drop temperature；Enter bulking machine steam pressure
0.65Mpa；Vapor (steam) temperature：174.5℃；Hydraulic system working pressure 10.00Mpa, obtains expanded peony seeds benevolence raw material；
Expanded peony seeds benevolence raw material is put into the extractor of subcritical equipment, raw material is with the mass volume ratio of butane solvent
1:2,30 DEG C of extraction temperature；Extracting pressure is 0.35Mpa, continuous to extract 2 times, 30 minutes each time, after solvent evaporation is reclaimed
Obtain peony seeds crude oil；
Peony seeds crude oil is refined using conventional fat degumming decoloring method；
The peony seed oil for refining later is mixed by weight proportion with DHA algal oil, phosphatidylserine, emulsifying agent is added
Soybean lecithin and compound stabilizer, are stirred, and obtain emulsion, and emulsified solution is emulsified to obtain to emulsion high shear, then right
Emulsified solution ultrasonication, obtains suitable peony seeds flavored oils designed for old people；
The parts by weight of peony seed oil are 60 parts, and the parts by weight of DHA algal oil are 1.8 parts, and the amount of phosphatidylserine is
50ppm；
Compound stabilizer is：20ppm lycopenes, 60ppm Tea Polyphenols fatty acid ester, 20ppm fresh peony flower essential oils；
The condition of emulsion high shear emulsification is that shearing rotating speed is 12000r/min, and the time is 20min, high-pressure homogeneous
The pressure for the treatment of is divided into two-stage, and the first stage pressure is 40MPa, and the second stage pressure is 150MPa, and homogeneous 1-2 times obtains emulsification molten
Liquid.
Embodiment 3
The preparation method for being adapted to peony seeds flavored oils designed for old people is as follows：
The peony seeds that will be chosen are freezed, peeled off, expanded, subcritical butane extraction, obtain peony seeds crude oil；
In freezing step, peony seeds are placed at a temperature of -4 DEG C, freezed 24 hours, peeled off after taking-up, obtain peony seeds benevolence；
Peony seeds benevolence is rolled into embryo must expect embryo, be dosed to extruder, expect embryo aqueous 12%；Roll flake thickness degree 0.45mm；Enter
Bulking machine material embryo moisture 11%；Go out bulking machine material embryo moisture 13%；110 DEG C of drop temperature；Enter bulking machine steam pressure
0.75Mpa；Vapor (steam) temperature：174.5℃；Hydraulic system working pressure 19.00Mpa, obtains expanded peony seeds benevolence raw material；
Expanded peony seeds benevolence raw material is put into the extractor of subcritical equipment, raw material is with the mass volume ratio of butane solvent
1:3,50 DEG C of extraction temperature；Extracting pressure is 0.6Mpa, continuous to extract 3 times, 40 minutes each time；
Peony seeds crude oil is refined using conventional fat degumming decoloring method；
The peony seed oil for refining later is mixed by weight proportion with DHA algal oil, phosphatidylserine, emulsifying agent is added
Soybean lecithin and compound stabilizer, are stirred, and obtain emulsion, and emulsified solution is emulsified to obtain to emulsion high shear, then right
Emulsified solution ultrasonication, obtains suitable peony seeds flavored oils designed for old people；
The parts by weight of peony seed oil are 50 parts, and the parts by weight of DHA algal oil are 3 parts；The amount of phosphatidylserine is
50ppm；
Compound stabilizer is：Tea polyphenol-palmitate 60ppm, fresh peony flower essential oil 20ppm, Rosmarinus officinalis extract 20ppm；
The condition of emulsion high shear emulsification is that shearing rotating speed is 12000r/min, and the time is 20min, high-pressure homogeneous
The pressure for the treatment of is divided into two-stage, and the first stage pressure is 40MPa, and the second stage pressure is 150MPa, and homogeneous 1-2 times obtains emulsification molten
Liquid.
Embodiment 4
With embodiment 1 except that, the parts by weight of peony seed oil are 80, and DHA algal oil is 2.5 parts, phosphatidyl silk ammonia
Acid is 45ppm；
Compound stabilizer is added in above-mentioned compound lard, suitable peony seeds flavored oils designed for old people are obtained.
Compound stabilizer is：The fat-soluble polyphenol of 10ppm lycopenes, 40ppm, 30ppm fresh peony flowers essential oil, 5ppm shrimps are blue or green
Element.
DHA algal oil is a kind of edible oil rich in DHA (english abbreviation DHA).It nutrition classification with
Leukotrienes belongs to n-3 (i.e. ω -3) series fatty acid.It is the important composition composition of cranial nerve and optic cell.The material
It is very rare in natural food, only there are some contents in abyssal fishes.In normal human, enzyme and dehydrogenation are extended in carbochain
Under the participation of enzyme, leukotrienes can be converted into DHA, but conversion ratio there is no final conclusion.It is certain not in China resident leukotrienes intake
Under the background of foot, the source of DHA is more deficient, therefore it is necessary to give appropriate supplement in formula.The quantity of its supplement, ginseng
Examine and employ《DRIs (DRIs)》Required standard, the setting of the standard is for for each person every day
0.2-1.6 grams of intake.
Embodiment 5
With embodiment 1 except that, the parts by weight of peony seed oil are 80, and DHA algal oil is 4 parts, phosphatidylserine
It is 60ppm；
Compound stabilizer is added in above-mentioned compound lard, suitable peony seeds flavored oils designed for old people are obtained.
Compound stabilizer is：Lycopene is 50ppm, astaxanthin 5ppm, and Tea Polyphenols fatty acid ester is 40ppm, tree peony is fresh
Flower essential oil is 20ppm.
Embodiment 6
With embodiment 1 except that, the parts by weight of peony seed oil are 70, and DHA algal oil is 2 weight portions, phosphatidyl silk
Propylhomoserin is 50ppm；
Compound stabilizer is added in above-mentioned compound lard, suitable peony seeds flavored oils designed for old people are obtained；
Tea polyphenol-palmitate 80ppm, fresh peony flower essential oil 20ppm, Rosmarinus officinalis extract 10ppm.
Embodiment 7
With embodiment 1 except that, the parts by weight of peony seed oil are 70, and DHA algal oil is 4 parts, phosphatidylserine
It is 55ppm；
Compound stabilizer is added in above-mentioned compound lard, suitable peony seeds flavored oils designed for old people are obtained；
Astaxanthin 20ppm, tea polyphenol-palmitate 80ppm, fresh peony flower essential oil 20ppm, Rosmarinus officinalis extract 10ppm.
Claims (10)
1. it is a kind of to be adapted to peony seeds flavored oils designed for old people, including following components：
Peony seed oil, DHA algal oil；
The parts by weight of described peony seed oil are 20-80, the parts by weight of DHA algal oil are 1-4；
Also include phosphatidylserine；The amount of described phosphatidylserine is 40-80ppm；
Also include stabilizer, the amount of described stabilizer is 20-100ppm.
2. it is a kind of as claimed in claim 1 to be adapted to peony seeds flavored oils designed for old people, it is characterised in that described stabilization
Agent includes that stabilizer A, described stabilizer A include fresh peony flower essential oil.
3. it is a kind of as claimed in claim 1 to be adapted to peony seeds flavored oils designed for old people, it is characterised in that described stabilization
Agent also includes that stabilizer B, described stabilizer B include at least one in lycopene, capsorubin.
4. it is a kind of as claimed in claim 2 to be adapted to peony seeds flavored oils designed for old people, it is characterised in that described stabilization
Agent A also includes at least one in fat-soluble polyphenol, Rosmarinus officinalis extract, described fat-soluble polyphenol for fat-soluble tea polyphenol or
At least one in carnosol.
5. it is a kind of as claimed in claim 2 to be adapted to peony seeds flavored oils designed for old people, it is characterised in that described stabilization
Agent is 10ppm lycopenes, the fat-soluble polyphenol of 50ppm, 20ppm fresh peony flower essential oils.
6. it is a kind of as claimed in claim 2 to be adapted to peony seeds flavored oils designed for old people, it is characterised in that described stabilization
Agent also includes astaxanthin.
7. it is a kind of as claimed in claim 2 to be adapted to peony seeds flavored oils designed for old people, it is characterised in that described tree peony
Seed flavored oils include peony seed oil, the DHA algal oil of 2 weight portions, the compound stabilizer of 70 weight portions：Lycopene is 10ppm, fat
Dissolubility polyphenol is 50ppm, fresh peony flower essential oil is 20ppm.
8. it is a kind of as claimed in claim 2 to be adapted to peony seeds flavored oils designed for old people, it is characterised in that described tree peony
Seed flavored oils include peony seed oil, the DHA algal oil of 2 weight portions, the compound stabilizer of 70 weight portions：Lycopene is 10ppm, tea
Polyphenolic fatty acid ester:60ppm, fresh peony flower essential oil are 20ppm.
9. it is a kind of as claimed in claim 8 to be adapted to peony seeds flavored oils designed for old people, it is characterised in that described is compound
In stabilizer, tea polyphenol-palmitate 40ppm, fresh peony flower essential oil 20ppm, Rosmarinus officinalis extract 10ppm.
10. a kind of preparation method for being adapted to peony seeds flavored oils designed for old people as claimed in claim 8, including it is following
Step：
The peony seeds that will be chosen are freezed, peeled off, expanded, subcritical butane extraction, obtain peony seeds crude oil；
In described freezing step, peony seeds are placed at a temperature of-9-- 4 DEG C, freezed 10-24 hours, peeled off after taking-up, obtained
Peony seeds benevolence；
Peony seeds benevolence is rolled into embryo must expect embryo, be dosed to extruder, expect embryo aqueous 10~12%；Roll flake thickness degree 0.35~
0.45mm；Enter bulking machine material embryo moisture 10~11%；Go out bulking machine material embryo moisture 12~13%；105~110 DEG C of drop temperature；
Enter 0.65~0.75Mpa of bulking machine steam pressure；Vapor (steam) temperature：174.5℃；Hydraulic system working pressure 10.00-
19.00Mpa, obtains expanded peony seeds benevolence raw material；
Expanded peony seeds benevolence raw material is put into the extractor of subcritical equipment, raw material is 1 with the mass volume ratio of butane solvent:1-
1:3,30-50 DEG C of extraction temperature；Extracting pressure is 0.35-0.6Mpa, continuous to extract 2-3 times, each time 30-40 minutes；
Peony seeds crude oil is refined using conventional fat degumming decoloring method；
The peony seed oil for refining later is mixed by weight proportion with DHA algal oil, phosphatidylserine, emulsifying agent is added and is answered
Stabilizer is closed, is stirred, obtain emulsion, emulsified solution is emulsified to obtain to emulsion high shear, then to emulsified solution ultrasound
Ripple treatment, obtains suitable peony seeds flavored oils designed for old people；
The parts by weight of peony seed oil are 20-80 parts, and the parts by weight of DHA algal oil are 1-4 parts；The amount of compound stabilizer is 20-
160ppm；The amount of phosphatidylserine is 50ppm；
Described compound stabilizer include fresh peony flower essential oil, fat-soluble polyphenol, Rosmarinus officinalis extract, astaxanthin, lycopene,
At least one in capsorubin.
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