CN104095082A - Health-care peony seed blend oil and preparation method thereof - Google Patents
Health-care peony seed blend oil and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a health-care peony seed blend oil and a preparation method thereof. The method includes: firstly, preparation of peony seed oil: putting crushed peony seeds into an extraction kettle to undergo extraction by a subcritical CO2 collaborative ultrasonic generator; at the end of extraction, conveying peony seed oil carrying subcritical CO2 into a separation kettle to conduct molecular distillation, thus obtaining the peony seed oil; preparation of garlic essential oil: preparing garlic oil by subcritical CO2 extraction, and then conducting centrifugal separation to obtain the garlic essential oil; and finally, preparation of blend oil: mixing the filtered peony seed oil with the prepared garlic essential oil evenly according to a ratio of 15-50:1, then adding vitamin E according to 19mg/L, with the Ve being obtained by extraction and concentration of soybean oil deodorization distillate. The blend oil prepared by the method has nutrition and health care efficacy, and has strong stability.
Description
Technical field
The present invention relates to edible oil field, relate in particular to a kind of health-care peony seed ready-mixed oil and preparation method thereof.
Background technology
Peony seeds is the elite crystallization of peony plant, has passed on outside all characteristics that tree peony itself has, and it more has own unique medicine and nutritional labeling, and Paeonia suffruticosa seed is the nut that is subject to shell and plants shell double shielding, has natural " longevity " gene.Peony seed oil is plant grease, is light yellow transparent liquid, has light peony fragrance.Peony seed oil unsaturated fatty acid content reaches more than 90%, and especially estimable is that wherein polyunsaturated fatty acid---leukotrienes (belonging to w-3 series) content surpasses 38%, and oleic acid content is that more than 21% linoleic acid content is greater than 25%.Leukotrienes, linoleic acid have good prevention and therapeutic efficiency to people's cardiovascular and cerebrovascular disease; In addition, leukotrienes also has antiallergy, absorbs ultraviolet ray, delaying cell aging, prevents the effects such as dry skin.
Garlic oil is the particular matter in garlic, presents the liquid of bright clear amber in color, it be in garlic, extract and most important material, this essential oil is containing very important active sulfide, it is helpful to general health and cardiovascular health.Meanwhile, garlic oil is also a kind of broad-spectrum antiseptic material, has activating cell, promotes power generation, increases antibacterial and anti-virus ability, the multiple pharmacological function such as quickening metabolism, fatigue-relieving.Therefore, in a lot of fields, be all widely used.Aspect medical, allicin can be used for treating infectious diseases, disease of digestive system, mouth disease, cardiovascular and cerebrovascular disease etc., and has the effects such as anti-aging, anti-metal poisoning, cancer-resisting.
Summary of the invention
The technical problem to be solved in the present invention is: a kind of preparation method of health-care peony seed ready-mixed oil is provided, and ready-mixed oil nutrition, health care, stability that the method makes are strong.
To achieve these goals, the technical solution used in the present invention is: a kind of preparation method of health-care peony seed ready-mixed oil, comprises the following steps:
Step 1, prepare peony seed oil:
(1) dry peony seeds raw material is shelled, is crushed to 10～30 orders, pack subcritical abstraction still into;
(2) by subcritical CO
2inject extraction kettle and mix with peony seeds raw material, keep subcritical CO
2with the volume ratio of raw material be 6～10:1, open ultrasonic generator auxiliary extraction simultaneously;
(3) at stockpile density 0.6～0.8kg/L, under the condition of 35～45 ℃ of extraction temperature, extracting pressure 0.4～0.6MPa, ultrasonic power 750～900W, supersonic frequency 35～48KHz, raw material is extracted, extraction time is 40～70min;
(4) after extraction finishes, the subcritical CO of peony seed oil will be carried
2be transported in separating still and carry out molecular clock, temperature is 150～170 ℃, and vacuum is 1.0～2.0Pa;
Step 2, prepare galic essential oil:
(1) garlic, through peeling and after machinery and supersonic wave synchronism are pulverized, obtains broken garlic;
(2) broken garlic is put into cryogenic refrigerator, controlling temperature is-40 ℃ of precooling 2h, and then carries out vacuum dehydration at-40 ℃, and vacuum is 8Pa;
(3) garlic through vacuum dehydration is inserted in subcritical abstraction still, simultaneously by subcritical CO
2inject extraction kettle, at 70～100 ℃ of extraction temperature, extracting pressure 3～8MPa, CO
2flow is 40～44kg/h, extracts, and extraction time is 35～60min;
(4) after extraction finishes, the subcritical CO of extract will be dissolved with
2fluid is emitted from extraction tank, delivers in separating still, then carries out reduction vaporization, controls temperature 45 C～75 ℃ in evaporation process, finally from separating still bottom, emits extracted garlic oil;
(5) garlic oil, through centrifugation, obtains galic essential oil and paste oleoresin, gets galic essential oil standby;
Step 3, prepare ready-mixed oil:
The peony seed oil filtering clearly and the galic essential oil making are mixed according to 15～50:1 ratio, then according to 15～35mg/L, add vitamin E, this vitamin E extracts concentrated and obtains in soybean oil deodorizer distillate.
In described step 1 (2) step, ultrasonic generator comprises ultrasonic generator and ultrasonic transducer, and ultrasonic generator is positioned at the outside of extraction kettle, and ultrasonic transducer directly passes in extraction kettle by its ultrasonic transformer.
In step 1 (3) step, at stockpile density 0.8kg/L, under the condition of 45 ℃ of extraction temperature, extracting pressure 0.5MPa, ultrasonic power 850W, supersonic frequency 40KHz, raw material is extracted, extraction time is 45min.
In described step 2, mechanical disintegration is that colloid mill or homogenizer carry out fragmentation, and in described ultrasonic wave pulverizing, supersonic frequency is 20～25KHz; Broken garlic granularity is 0.1～0.05mm.
By peony seed oil, galic essential oil and in soybean oil deodorizer distillate extraction concentrated and vitamin E form.
The beneficial effect that the present invention brings is: (1) utilizes subcritical CO
2technology abstracting tree peony seed oil and galic essential oil, can shorten extraction time, improves extraction yield, extraction temperature is lower, can not affect the natural activity of heat-sensitive substance, improve nutritive value and the quality of peony seed oil and galic essential oil, and with short production cycle, safe and reliable, no solvent residue; (2) higher for subcritical peony seed oil acid value, carry out molecular clock depickling, the acid value that makes peony seed oil is 0.21mg/g, declines 70.87%.(3) garlic, before extracting, first carries out precooling, vacuum dehydration processing, occurs white emulsion while avoiding because of the too high extraction causing of garlic water content.(4) equipment investment is low, and product oil yield is high, and without CO
2residual, safe, healthy.(5) soybean natural Ve is more suitable in being added into edible oil and fat than BHA and BHT, adds shelf-life, minimizing Oxidation of Fat and Oils phenomenon that Ve can extend ready-mixed oil.
The specific embodiment
Embodiment mono-
Step 1, prepare peony seed oil:
(1) dry peony seeds is shelled, is crushed to 10 orders, pack subcritical abstraction still into;
(2) by subcritical CO
2inject extraction kettle and mix with peony seeds raw material, keep subcritical CO
2with the volume ratio of raw material be 6:1, open ultrasonic generator auxiliary extraction simultaneously; Ultrasonic generator comprises ultrasonic generator and ultrasonic transducer, and ultrasonic generator is positioned at the outside of extraction kettle, and ultrasonic transducer directly passes in extraction kettle by its ultrasonic transformer.Adopt ultrasonic generator to carry out auxiliary extraction, can shorten extraction time, improve extraction yield.
(3) at stockpile density 0.6kg/L, under the condition of 35 ℃ of extraction temperature, extracting pressure 0.4MPa, ultrasonic power 750W, supersonic frequency 35KHz, raw material is extracted, extraction time is 40min.
Extracting pressure is to change the important parameter of subcritical fluids to grease solvability, by intensified pressure, can increase the solvability of fluid to grease.But in industrial production, extracting pressure but limits the feasibility of its utilization.When extracting pressure is less than 0.4MPa, peony seed oil yield increases with the increase of extracting pressure, and reaches maximum 97.1% when 0.4MPa, and after surpassing 0.4MPa, yield trend is stable.Its former because: subcritical fluids exists with liquid form under the environment of vacuum, anaerobic, and it is little that too much change pressure reaches capacity variation to it.Therefore, extracting pressure is between 0.4 to 0.6MPa.
(4) after extraction finishes, the subcritical CO of peony seed oil will be carried
2be transported in separating still and carry out molecular clock, temperature is 150 ℃, and vacuum is 1.0Pa;
Step 2, prepare galic essential oil:
(1) garlic, through peeling and after machinery and supersonic wave synchronism are pulverized, obtains broken garlic; Mechanical disintegration is that colloid mill or homogenizer carry out fragmentation, and in described ultrasonic wave pulverizing, supersonic frequency is 20KHz; Broken garlic granularity is 0.1mm.
(2) broken garlic is put into cryogenic refrigerator, controlling temperature is-40 ℃ of precooling 2h, and then carries out vacuum dehydration at-40 ℃, and vacuum is 8Pa.
(3) garlic through vacuum dehydration is inserted in subcritical abstraction still, simultaneously by subcritical CO
2inject extraction kettle, at 70 ℃ of extraction temperature, extracting pressure 3MPa, CO
2flow is 40kg/h, extracts, and extraction time is 35min; In carrying out the extraction process of garlic oil, can adopt ultrasonic or microwave to carry out assisted extraction.
At present, the extracting process of garlic oil has three kinds: (1) steam distillation.Its principle is that steam is passed into water insoluble or is insoluble in water but has (garlic oil has certain volatility) in certain volatile organic substance, this organic matter is distilled with steam at the temperature lower than 100 ℃, then through further separated acquisition compared with pure material.The great advantage of this law is that equipment is simple, and cost is low, but because of fermentation and vapo(u)rizing temperature relatively high, the decline of the activity of allinnase, allicin has loss, makes oil yield lower.And the garlic oil of gained has one ripe taste, pure and fresh not.(2) solvent extraction.Garlic oil is slightly soluble in water, is soluble in the organic solvents such as ethanol, benzene, ether, utilizes this character can be with organic solvent by garlic oil lixiviate out.The shortcoming of the method is to have dissolvent residual.(3) supercritical CO
2extraction.This technology is to utilize fluid in a certain region of Near The Critical Point, has the behavior that extremely balances each other to reach a separated technology of solute with transmitting performance and solute solvability being changed and change this characteristic in quite wide scope with pressure and temperature with solute to be separated.
The advantage of subcritical abstraction is, nontoxic, harmless, and environmental protection, pollution-free, non-hot-working, the biologically active prod that retains extract do not destroy, are not oxidized, and production capacity is large, can large-scale industrialization produce, energy-conservation, operating cost is low, is easy to and product separation.
In addition, when carrying out the extraction of garlic oil, garlic is dried or the pretreatment of dewatering is also a committed step.At present, be nearly all to adopt fresh garlic section or direct broken pretreatment, be only suitable in steam extraction or solvent extraction, for subcritical CO
2during extraction garlic oil, a small amount of water can play the effect of guiding and supporting agent, be conducive to extract polar compound, when but moisture content is too high, extract and separate product is white emulsion, must just can obtain pure garlic oil through further separation, if adopt natural drying mode to dewater, the volatile component loss in garlic totally.The present invention adopts the freeze drying pretreatment of dewatering, and can obtain high-quality garlic oil.
(4) after extraction finishes, will be dissolved with the subcritical CO of extract
2fluid is emitted from extraction tank, delivers in separating still, then carries out reduction vaporization, controls temperature 45 C in evaporation process, finally from separating still bottom, emits extracted garlic oil;
(5) garlic oil, through centrifugation, obtains galic essential oil and paste oleoresin;
Step 3, prepare ready-mixed oil:
The peony seed oil filtering clearly and the galic essential oil making are mixed according to 15:1 ratio, then according to 15mg/L, add vitamin E, this vitamin E extracts concentrated and obtains in soybean oil deodorizer distillate.
Embodiment bis-
A preparation method for health-care peony seed ready-mixed oil, comprises the following steps:
Step 1, prepare peony seed oil:
(1) dry peony seeds is shelled, is crushed to 30 orders, pack subcritical abstraction still into; The size of raw material particle size, the contact area of decision extraction process Raw and extractant, feed particles is less, and the contact area of subcritical fluids and material is larger, is conducive to improve extraction yield.But undersized, the bulk density of raw material increases, and has increased resistance to mass tranfer, and raw material easily hardens into piece, but subcritical fluids needs to utilize the granularity of raw material to promote the formation of pressure differential in extraction process.When raw material granularity is 30 order, the yield of peony seed oil is the highest.
(2) by subcritical CO
2inject extraction kettle and mix with peony seeds raw material, keep subcritical CO
2with the volume ratio of raw material be 10:1, open ultrasonic generator auxiliary extraction simultaneously;
(3) at stockpile density 0.8kg/L, under the condition of 45 ℃ of extraction temperature, extracting pressure 0.6MPa, ultrasonic power 900W, supersonic frequency 48KHz, raw material is extracted, extraction time is 70min.
The size of extraction temperature affects the density of subcritical fluids and the vapour pressure of grease, and then affects the solvability of fluid to grease.Before 45 ℃, peony seed oil yield sharply changes with the rising of extraction temperature, in the time of 45 ℃, can reach maximum 97.89%, and on a declining curve after 45 ℃.Temperature rises, and the solubility of grease increases, and yield rises; But temperature rises to a certain degree, fluid is easily gasification in extraction kettle, reaches motive force and reduce in extraction process, and yield reduces.Therefore select 35 ℃ to 45 ℃.
(4) after extraction finishes, the subcritical CO of peony seed oil will be carried
2be transported in separating still and carry out molecular clock, temperature is 170 ℃, and vacuum is 2.0Pa;
Step 2, prepare galic essential oil:
(1) garlic, through peeling and after machinery and supersonic wave synchronism are pulverized, obtains broken garlic; In described step 2, mechanical disintegration is that colloid mill or homogenizer carry out fragmentation, and in described ultrasonic wave pulverizing, supersonic frequency is 25KHz; Broken garlic granularity is 0.05mm.
(2) broken garlic is put into cryogenic refrigerator, controlling temperature is-40 ℃ of precooling 2h, and then carries out vacuum dehydration at-40 ℃, and vacuum is 8Pa;
(3) garlic through vacuum dehydration is inserted in subcritical abstraction still, simultaneously by subcritical CO
2inject extraction kettle, at 100 ℃ of extraction temperature, extracting pressure 8MPa, CO
2flow is 44kg/h, extracts, and extraction time is 60min;
(4) after extraction finishes, will be dissolved with the subcritical CO of extract
2fluid is emitted from extraction tank, delivers in separating still, then carries out reduction vaporization, controls 75 ℃ of temperature in evaporation process, finally from separating still bottom, emits extracted garlic oil;
(5) garlic oil, through centrifugation, obtains galic essential oil and paste oleoresin;
Step 3, prepare ready-mixed oil:
The peony seed oil filtering clearly and the galic essential oil making are mixed according to 50:1 ratio, then according to 35mg/L, add vitamin E, this vitamin E extracts concentrated and obtains in soybean oil deodorizer distillate.
Embodiment tri-
A preparation method for health-care peony seed ready-mixed oil, comprises the following steps:
Step 1, prepare peony seed oil:
(1) dry peony seeds is shelled, is crushed to 15 orders, pack subcritical abstraction still into;
(2) by subcritical CO
2inject extraction kettle and mix with peony seeds raw material, keep subcritical CO
2with the volume ratio of raw material be 8:1, open ultrasonic generator auxiliary extraction simultaneously; Ultrasonic generator comprises ultrasonic generator and ultrasonic transducer, and ultrasonic generator is positioned at the outside of extraction kettle, and ultrasonic transducer directly passes in extraction kettle by its ultrasonic transformer.
(3) at stockpile density 0.8kg/L, under the condition of 45 ℃ of extraction temperature, extracting pressure 0.5MPa, ultrasonic power 850W, supersonic frequency 40KHz, raw material is extracted, extraction time is 45min.
Grease reaches dissolution equilibrium in subcritical fluids needs the regular hour, but long extraction time returns increase energy consumption.The prolongation of extraction time, the yield of peony seed oil can increase, and reaches maximum 75.65% when 70min, and after surpassing 70min, yield trend is stable.The increase of extraction time can cause the increase of energy consumption and the prolongation of activity time, considers, and extraction time is advisable 40 to 70min.
The size of bulk density not only affects the size of production efficiency, also affects the formation of extraction process total pressure head.Bulk density is less, and fluid can not contact with raw material well; Bulk density is excessive, and it is larger that fluid reaches resistance, and grease can not fully be dissolved in fluid.When bulk density is 0.8kg/L, yield is up to 97.94%, and surpasses 0.8kg/L yield slow decreasing later, therefore can select 0.8kg/L as optimum bulk density.
(4) after extraction finishes, the subcritical CO of peony seed oil will be carried
2be transported in separating still and carry out molecular clock, temperature is 160 ℃, and vacuum is 1.5Pa;
Step 2, prepare galic essential oil:
(1) garlic, through peeling and after machinery and supersonic wave synchronism are pulverized, obtains broken garlic; In described step 2, mechanical disintegration is that colloid mill or homogenizer carry out fragmentation, and in described ultrasonic wave pulverizing, supersonic frequency is 22KHz; Broken garlic granularity is 0.08mm left and right.
(2) broken garlic is put into cryogenic refrigerator, controlling temperature is-40 ℃ of precooling 2h, and then carries out vacuum dehydration at-40 ℃, and vacuum is 8Pa;
(3) garlic through vacuum dehydration is inserted in subcritical abstraction still, simultaneously by subcritical CO
2inject extraction kettle, at 85 ℃ of extraction temperature, extracting pressure 5MPa, CO
2flow is 42kg/h, extracts, and extraction time is 50min;
(4) after extraction finishes, will be dissolved with the subcritical CO of extract
2fluid is emitted from extraction tank, delivers in separating still, then carries out reduction vaporization, controls temperature 60 C in evaporation process, finally from separating still bottom, emits extracted garlic oil;
(5) garlic oil, through centrifugation, obtains galic essential oil and paste oleoresin;
Step 3, prepare ready-mixed oil:
The peony seed oil filtering clearly and the galic essential oil making are mixed according to 45:1 ratio, then according to 19mg/L, add vitamin E, this vitamin E extracts concentrated and obtains in soybean oil deodorizer distillate.
Edible oil and fat contain unrighted acid, owing to storing after improper or high temperature fried food, tend to produce a series of lipid peroxide.Lipid peroxide is a kind of harmful substance containing free radical, if accumulation in vivo can destroy eucaryotic cell structure and normal physiological function, impels generation and the development of disease, and therefore the grease of edible oxidation is extremely unfavorable to the health of human body.For avoiding Oxidation of Fat and Oils, generally add BHA and the BHT of chemical synthesis.But BHA and BHT at high temperature easily volatilize and lose its antioxidation, on the contrary, soybean natural V
eit is the good fat-soluble antioxidant of heat endurance.
No matter the peony seed oil of subcritical method extraction is at saponification number, iodine number, refraction coefficient, or on the physical and chemical index such as smoke point, unsaponifiable matter, can reach the standard that one-level leaches product oil.Extraction temperature is 40 ℃ of left and right, can well avoid like this oxidation of the grease that high temperature causes and become sour.
The optimum process condition of subcritical abstraction peony seed oil is: stockpile density 0.8kg/L, under the condition of 45 ℃ of extraction temperature, extracting pressure 0.5MPa, ultrasonic power 850W, supersonic frequency 40KHz, raw material is extracted, and extraction time is 45min; According to this extraction process, carry out demonstration test, recovery rate can reach 99.23%.Higher for subcritical peony seed oil acid value, carry out molecular clock depickling, molecular clock optimum condition is: 160 ℃ of temperature, vacuum is 1.7Pa, refined oil acid value is 0.22mg/g, declines 70.87%.
Main composition in garlic is allicin, is described as plant antimicrobial, and it contributes to: eliminate and anti-bacteria, strengthen body immunity.The whole intestines of stomach invigorating, promote appetite and digestion.Reduce cholesterol and blood fat, strengthen blood vessel elasticity, lower platelet aggregation and facilitate blood circulation, can pre-preventing thrombosis, the angiocardiopathies such as hypertension.Sterilization, antibacterial antiplaque effect are strong, are especially applicable to lung, the infection of stomach.Preventing cold, and be applicable to the cold symptoms such as fever, pain relieving, cough, laryngalgia and nasal obstruction.Can regulate blood sugar, the outbreak of prevention diabetes.Activate gastrointestinal mucosa, the whole intestines of stomach invigorating, promote appetite, accelerate digestion.Containing polythiaether compound and the selenium of tool reproducibility, can, to Green Tea Extract, remove heavy metal of body.
Therefore, galic essential oil and peony seed oil are in harmonious proportion to the immunity that the ready-mixed oil of gained is nutritious, can strengthen human body.
Claims (5)
1. a preparation method for health-care peony seed ready-mixed oil, is characterized in that, comprises the following steps:
Step 1, prepare peony seed oil:
(1) dry peony seeds raw material is shelled, is crushed to 10～30 orders, pack subcritical abstraction still into;
(2) by subcritical CO
2inject extraction kettle and mix with peony seeds raw material, keep subcritical CO
2with the volume ratio of raw material be 6～10:1, open ultrasonic generator auxiliary extraction simultaneously;
(3) at stockpile density 0.6～0.8kg/L, under the condition of 35～45 ℃ of extraction temperature, extracting pressure 0.4～0.6MPa, ultrasonic power 750～900W, supersonic frequency 35～48KHz, raw material is extracted, extraction time is 40～70min;
(4) after extraction finishes, the subcritical CO of peony seed oil will be carried
2be transported in separating still and carry out molecular clock, temperature is 150～170 ℃, and vacuum is 1.0～2.0Pa;
Step 2, prepare galic essential oil:
(1) garlic, through peeling and after machinery and supersonic wave synchronism are pulverized, obtains broken garlic;
(2) broken garlic is put into cryogenic refrigerator, controlling temperature is-40 ℃ of precooling 2h, and then carries out vacuum dehydration at-40 ℃, and vacuum is 8Pa;
(3) garlic through vacuum dehydration is inserted in subcritical abstraction still, simultaneously by subcritical CO
2inject extraction kettle, at 70～100 ℃ of extraction temperature, extracting pressure 3～8MPa, CO
2flow is 40～44kg/h, extracts, and extraction time is 35～60min;
(4) after extraction finishes, the subcritical CO of extract will be dissolved with
2fluid is emitted from extraction tank, delivers in separating still, then carries out reduction vaporization, controls temperature 45 C～75 ℃ in evaporation process, finally from separating still bottom, emits extracted garlic oil;
(5) garlic oil, through centrifugation, obtains galic essential oil and paste oleoresin, gets galic essential oil standby;
Step 3, prepare ready-mixed oil:
The peony seed oil filtering clearly and the galic essential oil making are mixed according to 15～50:1 ratio, then according to 15～35mg/L, add vitamin E, this vitamin E extracts concentrated and obtains in soybean oil deodorizer distillate.
2. the preparation method of a kind of health-care peony seed ready-mixed oil according to claim 1, it is characterized in that: in described step 1 (2) step, ultrasonic generator comprises ultrasonic generator and ultrasonic transducer, ultrasonic generator is positioned at the outside of extraction kettle, and ultrasonic transducer directly passes in extraction kettle by its ultrasonic transformer.
3. the preparation method of a kind of health-care peony seed ready-mixed oil according to claim 1, it is characterized in that: in step 1 (3) step, at stockpile density 0.8kg/L, under the condition of 45 ℃ of extraction temperature, extracting pressure 0.5MPa, ultrasonic power 850W, supersonic frequency 40KHz, raw material is extracted, and extraction time is 45min.
4. the preparation method of a kind of health-care peony seed ready-mixed oil according to claim 1, is characterized in that: in described step 2, mechanical disintegration is that colloid mill or homogenizer carry out fragmentation, and in described ultrasonic wave pulverizing, supersonic frequency is 20～25KHz; Broken garlic granularity is 0.1～0.05mm.
5. a kind of health-care peony seed ready-mixed oil of being prepared by method claimed in claim 1, is characterized in that, by peony seed oil, galic essential oil and in soybean oil deodorizer distillate extraction concentrated and vitamin E form.
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| CN104928020A (en) * | 2015-06-12 | 2015-09-23 | 山西鑫中大生物科技有限公司 | Subcritical production method for peony seed oil extraction |
| CN106467861A (en) * | 2015-08-17 | 2017-03-01 | 洛阳健特生物科技有限公司 | Peony seed oil subcritical fluid extraction technique |
| CN106720464A (en) * | 2016-11-24 | 2017-05-31 | 菏泽尧舜牡丹生物科技有限公司 | It is a kind of to be adapted to peony seeds flavored oils designed for old people |
| CN108060012A (en) * | 2017-12-19 | 2018-05-22 | 贵州航天乌江机电设备有限责任公司 | A kind of extracting method of peony seed oil |
| CN108219959A (en) * | 2018-03-07 | 2018-06-29 | 安徽心缘康生物科技有限公司 | A kind of method that essential oil is extracted from peony petal |
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| CN104920638A (en) * | 2015-06-04 | 2015-09-23 | 北京同仁堂安徽中药材有限公司 | Health-care blend oil and preparation method thereof |
| CN104928020A (en) * | 2015-06-12 | 2015-09-23 | 山西鑫中大生物科技有限公司 | Subcritical production method for peony seed oil extraction |
| CN106467861A (en) * | 2015-08-17 | 2017-03-01 | 洛阳健特生物科技有限公司 | Peony seed oil subcritical fluid extraction technique |
| CN106720464A (en) * | 2016-11-24 | 2017-05-31 | 菏泽尧舜牡丹生物科技有限公司 | It is a kind of to be adapted to peony seeds flavored oils designed for old people |
| CN108060012A (en) * | 2017-12-19 | 2018-05-22 | 贵州航天乌江机电设备有限责任公司 | A kind of extracting method of peony seed oil |
| CN108219959A (en) * | 2018-03-07 | 2018-06-29 | 安徽心缘康生物科技有限公司 | A kind of method that essential oil is extracted from peony petal |
| CN108378140A (en) * | 2018-03-08 | 2018-08-10 | 丽江先锋食品开发有限公司 | A kind of purple perilla seed ready-mixed oil of high unsaturated fatty acid content |
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