CN106359660A - Functional peony seed seasoning oil - Google Patents
Functional peony seed seasoning oil Download PDFInfo
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- CN106359660A CN106359660A CN201611049219.6A CN201611049219A CN106359660A CN 106359660 A CN106359660 A CN 106359660A CN 201611049219 A CN201611049219 A CN 201611049219A CN 106359660 A CN106359660 A CN 106359660A
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- oil
- seed
- flos moutan
- peony
- stabilizer
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
Abstract
The invention belongs to the technical field of oil-fat processing, particularly relates to a functional peony seed seasoning oil, and further relates to a preparation method for the seasoning oil. The functional peony seed seasoning oil comprises, by weight, 20-80 parts of peony seed oil and 10-80 parts of sesame oil, and further comprises stabilizer, wherein the consumption of the stabilizer is 20-200 ppm. The preparation method comprises the steps of preprocessing oil plants, wherein low temperature freezing combined with extrusion and swelling is conducted, so that the cell walls of the oil plants are broken thoroughly and are loosened and lacunose, a subcritical solvent enters very easily the inner of the oil plants to make contact with micro-elaioplasts, so as to make the micro-elaioplasts dissolved and collected; the number of times of extraction is reduced from common 3-5 times to 2-3 times, and the process is simplified; the time of extraction every time is reduced from common 40-60 minutes to 30-40 minutes, and the time, energy consumption and cost are saved.
Description
Technical field
The invention belongs to grease processing technology field, and in particular to a kind of seed of Flos Moutan feature flavored oils, further relates to this tune
The preparation method of taste oil.
Background technology
Currently, the edible oil great majority of domestic and international resident are the oils and fatss from animal or plant, and its basis is
The triglyceride of various fatty acids.The essential fatty acid that nutrition educational circles generally acknowledges has two kinds, and one kind is n-6 series linoleic acid (18
Carbon dienoic acid), another kind is the n-3 series fatty acid with alpha linolenic acid (jeceric acid) as representative.According to committee of the Chinese government
Support Chinese Soclety of Nutrition formulate " DRIs (dris) " standard, linoleic for each person every day
Intake should be 2.5-9.0%e；The intake of alpha linolenic acid should be 0.5-2.5%e；Reduced mass numerical value linoleic acid intake should
For 7.2-25.9 gram, linolenic acid intake should be 1.4-7.2 gram.China issue survey data be, linoleic acid intake per capita
Met or exceeded suitable intake standard, and alpha linolenic acid per capita intake be 0.4 gram, only reach suitable intake mark
The 5.7%-28% of quasi- numerical value.Its reason is oils and fatss such as Adeps Sus domestica, Adeps Caprae seu ovis, butter, soybean oil, the flower of China's resident's daily consumption
, all rich in linoleic acid, linolenic acid content is little for oil generation, Oleum Brassicae campestriss, olive oil, Camellia oil.It is considered that at the most of resident of China
Take in wretched insufficiency state in linolenic acid.This situation has important bad shadow for the cardiovascular health of resident and brain health
Ring, so it is significant to supplement linolenic acid in terms of diet nutritional.
The raw material peony seed oil that product of the present invention adopts is a kind of rich in linolenic edible vegetable oil, its linolenic acid content
More than 38%.Experiments verify that peony seed oil has reduction hyperlipidemia, hypercholesterolemia, the function of hyperglycemia aspect.This product
The preparation technology of seed of Flos Moutan crude oil neither adopts milling process, does not also adopt normal hexane solvent extraction method, because the general spiral of milling process
The extruding of its discharging opening terminal of squeezer heats up up to 130 DEG C, can make the protein in seed of Flos Moutan and other active component high temperature
Degeneration, is unfavorable for the preparation of the products such as follow-up Paeonia suffruticosa albumen and biological phenol；Although and normal hexane solvent extraction method is long-term in liquefaction field
Continue to use, but, normal hexane really belongs to hazardous solvent, there is environmental issue and dissolvent residual threatens food-safety problem.This technology is adopted
Butane subcritical abstraction, experiment proves that, is to avoid aforementioned two ways, a kind of low temperature liquefaction separately selecting
Method.
At present China found successively a limited number of with regard to the subcritical report preparing edible vegetable oil of butane, but,
The more effect being only possible to reach compared with high oil recovery of generally existing extraction times, this can produce for the industrial efficiency of large-scale production
Raw adverse effect.For example: Northeast Forestry University Yao Huan joyous " oil seed of Paeonia suffruticosa oil extract and residue comprehensive utilization " is related to make
Oily method compares it is believed that butane subcritical abstraction 3 times, and oil yield only up to 23.92% is hence it is evident that be less than normal hexane ultrasonic extracting method
29.00%；
Jiangsu University Zhou Shilong " the subcritical butane extracted character research of soybean embryo fat/oil " display, butane extraction 3 times, often
Secondary extraction time 30min, extraction yield 9.3%." the subcritical butane extraction preparation Semen sojae atricolor that Wuhan Polytechnic University Zhang Yanpeng discloses
The research of germ oil " report, subcritical butane extraction optimum process condition is: raw material particle size 40 mesh, 50 DEG C of extraction temperature, every time
Extraction time 40min, extracts 5 times.
Gansu light industry academy discloses and extracts shinyleaf yellowhorn oil side from Lignum Xanthoceratiss seed using subcritical tetrafluoroethane fluid
Method.A kind of method extracting shinyleaf yellowhorn oil seed from Lignum Xanthoceratiss, Lignum Xanthoceratiss seed raw material is crushed to 40～60 mesh, subcritical tetrafluoro second
The extraction temperature of alkane fluid is 30～40 DEG C, and extracting pressure is 1.0～1.2mpa, and each extraction time is 30～40min, repeats
Extraction 3 times；Separation temperature is 45～55 DEG C, takes out negative pressure with diaphragm type compressor and is gradually depressured to 5 × 10<sup>- 2</sup>pa,
Disengaging time is 20～30min every time, repeated isolation 3 times；Finally merge shinyleaf yellowhorn oil crude oil and pass through High speed refrigerated centrifuge again
Centrifugation, filtration, obtain shinyleaf yellowhorn oil product.Experiments verify that, under the conditions of process above, shinyleaf yellowhorn oil yield is
31.8%, product quality is good.
Cn 103815053.a discloses a kind of preparation method with seed of Flos Moutan mixed oil for puerpera, specifically, its pretreatment
Soak 5-10h, -20 DEG C to -10 DEG C freezing 8-10h including water, then vacuum microwave drying, heat-pump dehumidification are dried.Next step 20-
60mpa squeezing (static) 8-10h obtains peony seed oil.Above-mentioned method energy consumption higher thus leading to relatively costly.
In cn 103815058.a patent, oil-producing technique be not normal refinery activities for the connection after subcritical abstraction and
It is by molecular distillation twice, collecting its heavy phase composition is peony seed oil it is characterised in that by peony seed oil, rice embryo oil, Fructus Lycopersici esculenti
Extract and catechin composition, the percentage ratio that each raw material addition quality accounts for edible oil gross mass is: peony seed oil 42-65%, rice
Germ oil 33-52%, Fructus Lycopersici esculenti extract 1-4% and catechin 1-2%.In the above mentioned patent applications in file, for oils and fatss
Antioxidative stabilizer, with the addition of polyglycerol monooleate, and this composition can belong to polyglyceryl fatty acid ester additive, but state
Mark gb2760-2014 specifies that this product, when for fat emulsification, must not be used for vegetable oil；As reduced consumption for vegetable oil
When it is stipulated that being only limitted to frying oil.The content of the invention Section 1 of this document is that application catechin makees antioxidant, in order to solve catechu
Element difficult problems of dissolution in edible oil, adds polyglycerol monooleate and ethanol, then increases not clear problem.Above-mentioned
File in the effect of antioxidant is only had " improve the freshness date shelf-life of edible oil " and is in short described, without tool
Body data.
Defect for above-mentioned patent or patent application or document it would be highly desirable to invent a kind of low cost, add plant-derived
Antioxidant with extend oils and fatss holding the time limit seed of Flos Moutan mixed oil.
Content of the invention
In order to solve above-mentioned technical problem, the invention provides one kind combines extruding puffing by freezing pretreatment
The method preparing feature peony seed oil with subcritical abstraction.
The feature seed of Flos Moutan flavored oils of the present invention are to solve above technical problem by following technical schemes:
A kind of feature seed of Flos Moutan flavored oils, including following components:
Peony seed oil, Oleum sesami；The parts by weight of peony seed oil are 20-80, the parts by weight of Oleum sesami are 10-80；
Also include stabilizer, the amount of stabilizer is 20-200ppm.
Above-mentioned stabilizer includes stabilizer a, and stabilizer a includes fresh peony flower quintessence oil.
Stabilizer also includes stabilizer b, and stabilizer b includes lycopene, at least one in capsorubin.
Stabilizer a also includes fat-soluble polyphenol, at least one in Herba Rosmarini Officinalis extract, and fat-soluble polyphenol is fat-soluble tea
At least one in polyphenol or carnosol.
Stabilizer is 10ppm lycopene, the fat-soluble polyphenol of 40ppm, 20ppm fresh peony flower quintessence oil.
Stabilizer also includes astaxanthin.
Seed of Flos Moutan flavored oils include the peony seed oil of 70 weight portions, the Oleum sesami of 20 weight portions, complex stabilizer: tomato red
Element is 10ppm, fat-soluble polyphenol: 50ppm, fresh peony flower quintessence oil are 20ppm.
Seed of Flos Moutan flavored oils include the dha algae of the peony seed oil of 70 weight portions, the Oleum sesami of 20 weight portions, 1-5 weight portion
Oil, complex stabilizer: lycopene is 10ppm, tea polyphenols fatty acid ester: 50ppm, fresh peony flower quintessence oil are 20ppm.
In complex stabilizer, tea polyphenol-palmitate 10ppm, fresh peony flower quintessence oil 20ppm, Herba Rosmarini Officinalis extract 40ppm.
A kind of preparation method of the feature seed of Flos Moutan flavored oils of the present invention, including following steps:
The seed of Flos Moutan choosing is freezed, peels off, expanded, subcritical butane extracts, and obtains seed of Flos Moutan crude oil；
In freezing step, seed of Flos Moutan is placed at a temperature of-9-4 DEG C, freezes 10-24 hour, peel off after taking-up, obtain male
Dan Ziren；
Peony seeds benevolence is rolled embryo and must expect embryo, be dosed to extruder, expect embryo aqueous 10～12%；Roll flake thickness degree 0.35～
0.45mm；Enter bulking machine material embryo moisture 10～11%；Go out bulking machine material embryo moisture 12～13%；105～110 DEG C of drop temperature；
Enter bulking machine steam pressure 0.65～0.75mpa；Vapor (steam) temperature: 174.5 DEG C；Hydraulic system working pressure 10.00
19.00mpa, obtains expanded peony seeds benevolence raw material；
Expanded peony seeds benevolence raw material is put into the extractor of subcritical equipment, raw material with the mass volume ratio of butane solvent is
1:1-1:3, extraction temperature 30-50 DEG C；Extracting pressure is 0.35-0.6mpa, continuously extracts 2-3 time, each time 30-40 divides
Clock；
Using conventional fat degumming decoloring method to seed of Flos Moutan crude oil refine；
Peony seed oil later for refine is mixed by weight proportion with Oleum sesami or dha algae oil；The weight portion of peony seed oil
Number is 20-80 part, and the parts by weight of Oleum sesami are 10-80 part；The amount of complex stabilizer is 20-100ppm；
Complex stabilizer is added in above-mentioned compound lard, obtains feature seed of Flos Moutan flavored oils, described is compound steady
Determine agent include fresh peony flower quintessence oil, fat-soluble polyphenol, Herba Rosmarini Officinalis extract, astaxanthin, lycopene, in capsorubin at least
A kind of.
Flavored oils in the present invention use the stabilizer of plant origin, and this stabilizer makes shelf life of products ratio use this area
Interior conventional tbhq (tert-butylhydroquinone) improves 40%.This product can fill according to the requirement of Chinese residents dietary guidelines
Point supplement China resident general lack of important nutrient linolenic acid, docosahexenoic acid, thus have safeguard brain health and
The function of cardiovascular health；It is respectively provided with significance in terms of economic benefit and social benefit.
In the formula of the present invention, using fresh peony flower quintessence oil as stabilizer, not only improve the abnormal smells from the patient of flavored oils, and
Enhance the non-oxidizability of flavored oils.
The another improvement of the present invention is, in the production technology of flavored oils, peony seeds benevolence is placed in storage in-9-Cool Room 4 DEG C
Deposit, not only preservation by low temperature can guarantee the quality but also be beneficial to subsequent technique.The present inventor through many experiments it was therefore concluded that, inside peony seeds benevolence
Cellularity is the stage that material internal moisture forms ice crystal in -4 DEG C or -5 DEG C, and the expansion of ice crystal can make oil plant cell wall
Rupture.But because seed of Flos Moutan raw aqueous rate is not high, the cell proportion being broken is not high.The present inventor is through test of many times
Prove, profound hypothermia quick-freezing has significant difference with freeze slow compared with low temperature: the ice crystal that quick-freezing produces is less, and the raw ice crystal of slow delivery in cold weather is larger；
Larger ice crystal is larger for the structural change of plant cell, thus is conducive to follow-up smudge cellses to extract oils and fatss.Additionally,
Result of the test shows further, the subsequent product obtained by Different hypothermia handling process, and the clarity within the shelf-life has a difference:
Profound hypothermia handicraft product, in first 2 months of shelf-life, occurs leading to the underproof probability of clarity high because of floccule, and relatively
, never floccule problem in the product of low temperature process.
After freezing, then carry out oil plant extruding puffing process, the extraction ratio for oil product is greatly improved, and right
Quality in oil product also has significant impact.
The present invention is first freezed seed of Flos Moutan so as to internal moisture forms ice crystal by the way of freezing, causes cell rupture,
Be conducive to follow-up extraction；In conjunction with extruding-puffing technique, in the state of the cell wall of oil plant cell has crushed, knot of tissue
Structure internal voids increase, and intracellular micro- elaioleucite is easier to be separated by the external force fusion power of solvent (mechanical force).
Oil plant, in the destruction of expanded middle cell and infiltrative improvement, makes leaching solvent than reducing, solvent is than by raw embryo
0.8:1 is reduced to 0.6:1, it is thus apparent that improve miscella concentration, make miscella concentration improve to 28 from 20% about～
30%.Therefore, the load of miscella evaporation system and the load of solvent recovery are alleviated.Save the steaming of miscella evaporation operation
Vapour consumes.
And processed using extruding puffing, so that the enzyme in oil plant is passivated, improve the quality of Extractive crudeoil.
Enzyme in oil plant in extrusion pressing puffing process and antinutritional factor are passivated, it is to avoid lipoxidase and phospholipid
The impact to phospholipid in oil plant for the enzyme, decreases the content of non-hydratable phospholipid in Extractive crudeoil, increased total phospholipidses in Extractive crudeoil
Content, can effectively improve oil and fat refining efficiency, improve oil and fat product quality, and improve phospholipid by-product in aquation scouring processes
The yield of product and the quality of phospholipid prod.
With respect to cn 103815058.a in background technology, the method for the present invention is that fat-soluble tea polyphenol is added, and does not deposit
Described in the background " application catechin makees antioxidant, in order to solve catechin difficult problems of dissolution in edible oil,
Add polyglycerol monooleate and ethanol, then increase not clear problem " problem of this respect.
With respect to the method disclosed by cn 103815058.a in background technology, the invention provides a kind of low energy consumption, height
Efficiency, meet the peony seed oil production process of laws and regulations requirement: after raw material freezing+extruding puffing, subcritical abstraction obtains final product male
Red seed oil, product meets country and defends the prescription that planning commission's No. 9 bulletin adnexa in 2011 is write exactly.
With respect to cn 103815053.a, method of the present invention energy consumption is relatively low, and low cost.
The beneficial effects of the present invention is, after the present invention is to the pretreatment of oil plant, extruding is combined using fast low temperature freezing
Expanded, so that the cell wall of oil plant is thoroughly ruptured and loose many spaces, subcritical solvent is very easy to enter inside and micro- elaioleucite
Contact, is dissolved and collects out, extraction times are reduced to 2-3 time from 3-5 time common extraction, simplify technique, every time
The time of extraction, from common 40-60min, is reduced to 30-40min, saves time, energy consumption and cost, in large-scale production
In have and important mention production efficiency, energy-saving meaning.
Specific embodiment
The present invention is further described with reference to specific embodiment, so that those skilled in the art is more
Understand the present invention, but the present invention is not limited with this.
Embodiment 1
The seed of Flos Moutan choosing is freezed, peels off, expanded, subcritical butane extracts, and obtains seed of Flos Moutan crude oil；
In freezing step, seed of Flos Moutan is placed at a temperature of -5 DEG C, freezes 16 hours, peel off after taking-up, obtain peony seeds benevolence；
Peony seeds benevolence is rolled embryo and must expect embryo, be dosed to extruder, expect embryo aqueous 11%；Roll flake thickness degree 0.4mm；Enter swollen
Change machine material embryo moisture 10%；Go out bulking machine material embryo moisture 12%；108 DEG C of drop temperature；Enter bulking machine steam pressure 0.7mpa；Steam
Stripping temperature: 174.5 DEG C；Hydraulic system working pressure 15mpa, obtains expanded peony seeds benevolence raw material；
Expanded peony seeds benevolence raw material is put into the extractor of subcritical equipment, raw material with the mass volume ratio of butane solvent is
1:2,40 DEG C of extraction temperature；Extracting pressure is 0.5mpa, continuously extracts 2 times, each 40 minutes time, after solvent evaporation is reclaimed
Obtain seed of Flos Moutan crude oil；
Using conventional fat degumming decoloring method to seed of Flos Moutan crude oil refine；
Peony seed oil later for refine and Oleum sesami are mixed in proportion；The parts by weight of peony seed oil are 80, Oleum sesami
Parts by weight be 20 parts；
Complex stabilizer is added in above-mentioned compound lard, obtains feature seed of Flos Moutan flavored oils.
Complex stabilizer is: 10ppm lycopene, 50ppm fat-soluble tea polyphenol, 20ppm fresh peony flower quintessence oil；
After placing 30 days in above-mentioned oil product photoenvironment at normal temperatures, same, compare its non-oxidizability, instrument:
Edible oil oxidation stability analyzer is led in racimat743 Switzerland ten thousand
Assay method condition: according to US corn chemist association aacc-58-52 standard；120 DEG C, ventilation 20l/h.
Sample quality: 3g about.
Antioxidant is originated: import fat-soluble tea polyphenol egcg oil acts on behalf of japanese product from Beijing Jie Sen source；Domestic
Fat-soluble tea polyphenol is derived from the grand Products of Yuyao curry favour moral.Tbhq is derived from Guangdong Guang Yi food additive company limited.
Oil source: the product of commercially available domestic execution national standard.
Tea polyphenols are derived from a kind of functional components being beneficial to health of Folium Camelliae sinensis, are also a kind of good food
Antioxidant.But, it has good water solublity, and can not dissolve in oils and fatss, thus limiting answering in edible oil
With.Fat-soluble tea polyphenol is equally the antioxidant extracting processing with green tea for raw material, and main component is also catechins,
Important feature be have fat-soluble.
Shown using active oxygen method (aom method) specialty oil oxidative stability analyser test result, its antioxygenic property
Better than capable dibenzylatiooluene (bht) commonly used in the trade, tert-butylhydroquinone (tbhq).Oil can be kept after adding in proportion
The original quality of product, can increase oil product transparency and brightness, increase the fresh peony flower fragrance of product；In terms of the shelf-life, at present I
The commonly used interpolation in state's edible oil field antioxidant tbhq100-200ppm, the shelf-life reaches 18 months, and the present invention adopts
Composite antioxidant is substantially better than the effect of tbhq100-200ppm.Calculate by experience in industry and about can reach 24 months.Checking
Result see table:
The impact of 5 kinds of antioxidants oxidation stability to 7 kinds of oils and fatss
Embodiment 2
The preparation method of feature seed of Flos Moutan flavored oils is as follows:
The seed of Flos Moutan choosing is freezed, peels off, expanded, subcritical butane extracts, and obtains seed of Flos Moutan crude oil；
In freezing step, seed of Flos Moutan is placed at a temperature of -7 DEG C, freezes 15 hours, peel off after taking-up, obtain peony seeds benevolence；
Peony seeds benevolence is rolled embryo and must expect embryo, be dosed to extruder, expect embryo aqueous 10%；Roll flake thickness degree 0.35mm；Enter
Bulking machine material embryo moisture 10%；Go out bulking machine material embryo moisture 12%；105 DEG C of drop temperature；Enter bulking machine steam pressure
0.65mpa；Vapor (steam) temperature: 174.5 DEG C；Hydraulic system working pressure 10.00mpa, obtains expanded peony seeds benevolence raw material；
Expanded peony seeds benevolence raw material is put into the extractor of subcritical equipment, raw material with the mass volume ratio of butane solvent is
1:2,30 DEG C of extraction temperature；Extracting pressure is 0.35mpa, continuously extracts 2 times, each 30 minutes time, after solvent evaporation is reclaimed
Obtain seed of Flos Moutan crude oil；
Using conventional fat degumming decoloring method to seed of Flos Moutan crude oil refine；
Peony seed oil later for refine and Oleum sesami are mixed in proportion；The parts by weight of peony seed oil are 80 parts, Semen Sesami
The parts by weight of oil are 20 parts；
Complex stabilizer is added in above-mentioned compound lard, complex stabilizer is: lycopene 10ppm, fat-soluble
Polyphenol 60ppm, fresh peony flower quintessence oil 10ppm, obtain feature seed of Flos Moutan flavored oils.
Embodiment 3
The preparation method of feature seed of Flos Moutan flavored oils is as follows:
The seed of Flos Moutan choosing is freezed, peels off, expanded, subcritical butane extracts, and obtains seed of Flos Moutan crude oil；
In freezing step, seed of Flos Moutan is placed at a temperature of -4 DEG C, freezes 24 hours, peel off after taking-up, obtain peony seeds benevolence；
Peony seeds benevolence is rolled embryo and must expect embryo, be dosed to extruder, expect embryo aqueous 12%；Roll flake thickness degree 0.45mm；Enter
Bulking machine material embryo moisture 11%；Go out bulking machine material embryo moisture 13%；110 DEG C of drop temperature；Enter bulking machine steam pressure
0.75mpa；Vapor (steam) temperature: 174.5 DEG C；Hydraulic system working pressure 19.00mpa, obtains expanded peony seeds benevolence raw material；
Expanded peony seeds benevolence raw material is put into the extractor of subcritical equipment, raw material with the mass volume ratio of butane solvent is
1:3,50 DEG C of extraction temperature；Extracting pressure is 0.6mpa, continuously extracts 3 times, each 40 minutes time；
Using conventional fat degumming decoloring method to seed of Flos Moutan crude oil refine；
By peony seed oil later for refine and Oleum sesami；The parts by weight of peony seed oil are 80 parts, the weight portion of Oleum sesami
Number is 80 parts；
Complex stabilizer is added in above-mentioned compound lard, obtains feature seed of Flos Moutan flavored oils, complex stabilizer has
Body is: lycopene 10ppm, fat-soluble polyphenol 60ppm, fresh peony flower quintessence oil 30ppm.
Embodiment 4
With embodiment 1 except that, peony seed oil later for refine is mixed in proportion with Oleum sesami, dha algae oil；Male
The parts by weight of red seed oil are 80, and the parts by weight of Oleum sesami are 20 parts；Dha algae oil is 2.5 parts；
Complex stabilizer is added in above-mentioned compound lard, obtains feature seed of Flos Moutan flavored oils.
Complex stabilizer is: the fat-soluble polyphenol of 10ppm lycopene, 60ppm, 20ppm fresh peony flower quintessence oil.
Dha algae oil is a kind of edible oil rich in docosahexenoic acid (english abbreviation dha).It threpsology classification with
Linolenic acid belongs to n-3 (i.e. ω -3) series fatty acid.It is the important composition composition of cranial nerve and optic cell.This material
Very rare in natural food, in abyssal fishes, only there are some contents.In normal human, extend enzyme and dehydrogenation in carbochain
Under the participation of enzyme, linolenic acid can be converted into dha, but conversion ratio there is no final conclusion.In China resident linolenic acid intake really not
Under the background of foot, the source of dha is more deficient, and it is necessary for supplementing in right amount therefore in formula.Its quantity supplemented, ginseng
Examine and employ " DRIs (dris) " required standard, the setting of this standard is for each person every day
Intake 0.2-1.6 gram.
Embodiment 5
With embodiment 1 except that, peony seed oil later for refine is mixed in proportion with Oleum sesami, dha algae oil；Male
The parts by weight of red seed oil are 80, and the parts by weight of Oleum sesami are 20 parts；Dha algae oil is 4 parts；
Complex stabilizer is added in above-mentioned compound lard, obtains feature seed of Flos Moutan flavored oils.
Complex stabilizer is: lycopene is 15ppm, tea polyphenols fatty acid ester is 65ppm, fresh peony flower quintessence oil is
20ppm.
Embodiment 6
With embodiment 1 except that, peony seed oil later for refine is mixed in proportion with Oleum sesami, dha algae oil；Male
The parts by weight of red seed oil are 60, and the parts by weight of Oleum sesami are 50 parts；Dha algae oil is 2.2 weight portions；
Complex stabilizer is added in above-mentioned compound lard, obtains feature seed of Flos Moutan flavored oils；
Tea polyphenol-palmitate 40ppm, fresh peony flower quintessence oil 20ppm, Herba Rosmarini Officinalis extract 20ppm.
Embodiment 7
With embodiment 1 except that, peony seed oil later for refine is mixed in proportion with Oleum sesami, dha algae oil；Male
The parts by weight of red seed oil are 60, and the parts by weight of Oleum sesami are 50 parts；Dha algae oil is 4.4 parts；
Complex stabilizer is added in above-mentioned compound lard, obtains feature seed of Flos Moutan flavored oils；
Astaxanthin 20ppm, tea polyphenol-palmitate 40ppm, fresh peony flower quintessence oil 20ppm, Herba Rosmarini Officinalis extract 10ppm.
Embodiment 8
The research to human body hypolipemic function for the flavored oils of embodiments of the invention 1, specific as follows:
1st, material and method
1.1 sample
The flavored oils of embodiments of the invention 1 are as test specimen；It is placebo that soybean salad oil is bought in market.Human body mouth
Taking recommended dose is daily 10g.
1.2 experimenters select
1.2.1 inclusive criteria: experimenter's male or female, 40 65 years old age.Take a blood sample twice in half a year, T-CHOL twice
All >=5.2mmol/l or triglyceride >=1.65mmol/l, simple dyslipidemia, no obvious brain, the heart, liver, lung, kidney, blood disease
Suffer from, no Long-term taking medicine history, voluntarily tested guarantee cooperation.
1.2.2 Subject Exclusion Criteria: gestation or women breast-feeding their children, merge intentionally, liver, the serious disease such as kidney and hemopoietic system
Patient；Take the article relevant with tested function in a short time, have influence on to result judgement person；Do not meet inclusive criteria, do not press
It is impossible to judge effect or data, umbra does not ring effect or safe sex determination person to the edible given the test agent of regulation.
1.3 experimental design and packet
Using itself and between group two kinds of control design.Divide peony seed oil test-meal group and comfort by experimenter's blood lipid level at random
Agent matched group, considers principal element such as age, sex etc. of impact result as far as possible, carries out harmonious inspection, to ensure between group
Comparability.Carry out test-meal test by double-blind method.Every group of tested number 55 people.
1.4 test method
Require experimenter not change original dietary habit, require nothing more than the original edible cooking oil of the daily minimizing of experimenter
10g, and increase 10g given the test agent.
2 observation index
Every observation index in test-meal on-test and at the end of each measure once.
2.1 safety indexes
2.1.1 general physical examination: inquire and understand the spirit of experimenter, sleep, diet, defecation etc. before test in detail
Situation, body weight, blood pressure, changes in heart rate before and after experiment with measuring.
2.1.2 routine blood test: red blood cell count(RBC), numeration of leukocyte and classification, content of hemoglobin mensure etc..
2.1.3 routine urinalysis: ph value, leukocyte, glucose in urine etc..
2.1.4 stool routine examination.
2.1.5 abdominal part b surpass, electrocardiogram, x line fluoroscopy of chest check (measuring once before on-test).
2.1.6 blood biochemistry index inspection: total serum protein (tp) albumin (alb), glutamate pyruvate transaminase (alt), millet straw turn
Ammonia enzyme (ast), uric acid (ua), blood urea nitrogen (bun), flesh liver (gr), blood glucose (glu) etc. measure.
2.1.7 untoward reaction is observed.
2.2 blood lipids index: cholesterol (ghol), triglyceride (tg), HDL-C (hdl c).
4. statistical procedures
Result mean ± standard deviation represents, self pair data adopts paired t-test, between test group and matched group
On the premise of variance is neat, mean compares and adopts independent samples t-test, otherwise carries out variable transfer, meets variance and adopts t to check together afterwards,
If variance is still uneven, using rank test.
5. result
5.1 safety observations
5.1.1 ordinary circumstance: test-meal group 55, matched group 55.After test in 45 days, test group has 4 experimenters
Because interruption is taken by test product or cannot judge that effect is screened out, matched group has 5 experimenters to take because of interruption to be screened out by test product.
Last efficiency test crowd's test-meal group 51, matched group 50.Before and after test-meal, experimenter's spirit, sleep, diet, defecation shape
Condition no abnormality seen；Test-meal group: male/female is 30:21, the age is 55.7 ± 7.05 years old；Matched group: male/female is 30:20, and the age is
54.1 ± 8.28 years old.
5.1.2 abdominal part b surpass, electrocardiogram, x line fluoroscopy of chest detection；All in normal range.
5.1.3 body weight, heart pressure, heart rate, routine urinalysis, stool routine examination, routine blood indexes situation of change.
It is shown in Table the forward and backward test-meal group of 1. test-meal samples and matched group body weight, blood pressure, heart rate, routine urinalysis, stool routine examination and blood are normal
Rule are showed no obvious abnormalities change.
Body weight, blood pressure, heart rate, routine urinalysis, stool routine examination and routine blood test situation of change (x ± s) before and after table 1 test-meal experiment
5.1.4 blood biochemistry index situation of change before and after test-meal experiment
It is shown in Table the forward and backward test-meal group of 2. examination style product and white (alb) glutamate pyruvate transaminase of matched group serum albumin (tp) albumen
(alt)
Glutamic oxaloacetic transaminase, GOT (ast) creatinine (cr), blood glucose (glu), uric acid (ua) blood urea nitrogen (bun) are showed no obvious abnormalities change
Change.
Blood biochemistry index situation of change (x ± s) after table 2 test-meal experiment
5.1.5 have no obvious adverse reaction during test-meal
5.2 blood lipids index:
It is shown in Table in 3.4 half a year and take a blood sample twice.It is respectively before test-meal 2 blood fat data before 1 and test-meal, be subject near taking with the date
Before the test-meal of style product, 2 blood lipid levels are grouped and statistical disposition.Matched group and test-meal group serum chol, tg and examination before experiment
Compare before food and after matched group test-meal, difference all has significance (p < 0.05).Before and after test-meal, hdl c level has no obvious change
(p>0.05).
Serum chol, tg, hdl c level (x ± s) before table 3 test-meal experiment
Serum chol, tg, hdl-c level (x ± s) before and after table 4 test-meal experiment
Note: * compares with before test-meal that < 0.05# compares p < 0.05 with matched group
6. brief summary
Using counter point between own control and group, the volunteer meeting experiment condition is selected to take tested material 45 days
Afterwards.Result shows: after taking peony seed oil, chol, tg significantly reduce with comparing before test-meal, and difference has significance (p < 0.05) to try
Untoward reaction is had no during food.
Embodiment 9
Experiment contrast
Comparative example 1
Identical with embodiment 1, except for the difference that complex stabilizer has adjustment, and complex stabilizer is: 30ppm Herba Rosmarini Officinalis carries
Take thing, 60ppm fat-soluble tea polyphenol；Remaining is identical；
Comparative example 2
Identical with embodiment 1, except for the difference that complex stabilizer has adjustment, and complex stabilizer is: the fat-soluble tea of 60ppm
Polyphenol, 30ppm magnolia extract；Remaining is identical；
Comparative example 3
Identical with embodiment 1, except for the difference that complex stabilizer has adjustment, and stabilizer is: 10ppm lycopene,
80ppm fat-soluble tea polyphenol；
Comparative example 4
Identical with embodiment 1, except for the difference that complex stabilizer has adjustment, and stabilizer is: 10ppm lycopene,
80ppm Herba Rosmarini Officinalis extract；
The flavored oils of the present invention are carried out non-oxidizability experiment, using its peroxide value of iodometric determination.
By the flavored oils of embodiment 1, comparative example 1,2,3,4 place respectively 1d, 3 days, 6 days, 9 days, 15 days, after 21 days, its
Antioxidation value (meq/kg) result is as follows:
Table 5 non-oxidizability is tested
In comparative example 1,2, have adjusted the species of complex stabilizer, result shows, the non-oxidizability of flavored oils also has difference
Not.It can be seen that single antioxidant lycopene or single fat-soluble tea polyphenol or to be lycopene many with fat-soluble tea
The combination of phenol, or the combination of lycopene and magnolia extract, even if its consumption does not change, its effect is not so good as embodiment 1
In complex stabilizer effect: 10ppm lycopene, 60ppm fat-soluble tea polyphenol, the combination of 20ppm fresh peony flower quintessence oil,
In the present invention, after 120 days, its antioxidation value is still preferable, is maintained at 3.06meq/kg；After 120 days in comparative example 1, its antioxygen
Change is worth for 2.23meq/kg.
In embodiment 1, with the change of flavored oils' storage time, in oils and fatss, lipid hydroperoxide and secondary oxidative are produced
Thing changes of contents Trend Stationary, flavored oils have higher non-oxidizability.
Claims (10)
1. a kind of feature seed of Flos Moutan flavored oils, including following components:
Peony seed oil, Oleum sesami；The parts by weight of described peony seed oil are 20-80, the parts by weight of Oleum sesami are 10-80；
Also include stabilizer, the amount of described stabilizer is 20-200ppm.
2. as claimed in claim 1 a kind of feature seed of Flos Moutan flavored oils it is characterised in that described stabilizer include stable
Agent a, described stabilizer a includes fresh peony flower quintessence oil.
3. as claimed in claim 1 a kind of feature seed of Flos Moutan flavored oils it is characterised in that described stabilizer also includes surely
Determine agent b, described stabilizer b includes lycopene, at least one in capsorubin.
4. as claimed in claim 2 a kind of feature seed of Flos Moutan flavored oils it is characterised in that described stabilizer a also includes
At least one in fat-soluble polyphenol, Herba Rosmarini Officinalis extract, described fat-soluble polyphenol is fat-soluble tea polyphenol or carnosol
In at least one.
5. as claimed in claim 2 a kind of feature seed of Flos Moutan flavored oils it is characterised in that described stabilizer is 10ppm
The fat-soluble polyphenol of lycopene, 40ppm, 20ppm fresh peony flower quintessence oil.
6. as claimed in claim 2 a kind of feature seed of Flos Moutan flavored oils it is characterised in that described stabilizer also includes shrimp
Blue or green element.
7. as claimed in claim 2 a kind of feature seed of Flos Moutan flavored oils it is characterised in that described seed of Flos Moutan flavored oils bag
Include the peony seed oil of 70 weight portions, the Oleum sesami of 20 weight portions, complex stabilizer: lycopene is 10ppm, fat-soluble polyphenol:
50ppm, fresh peony flower quintessence oil are 20ppm.
8. as claimed in claim 2 a kind of feature seed of Flos Moutan flavored oils it is characterised in that described seed of Flos Moutan flavored oils bag
Include the peony seed oil of 70 weight portions, the Oleum sesami of 20 weight portions, the dha algae oil of 1-5 weight portion, complex stabilizer: lycopene
It is 20ppm for 10ppm, tea polyphenols fatty acid ester: 50ppm, fresh peony flower quintessence oil.
9. as claimed in claim 8 a kind of feature seed of Flos Moutan flavored oils it is characterised in that in described complex stabilizer,
Tea polyphenol-palmitate 10ppm, fresh peony flower quintessence oil 20ppm, Herba Rosmarini Officinalis extract 40ppm.
10. a kind of preparation method of feature seed of Flos Moutan flavored oils as claimed in claim 8, including following steps:
The seed of Flos Moutan choosing is freezed, peels off, expanded, subcritical butane extracts, and obtains seed of Flos Moutan crude oil；
In described freezing step, seed of Flos Moutan is placed at a temperature of-9-4 DEG C, freezes 10-24 hour, peel off after taking-up, obtain
Peony seeds benevolence；
Peony seeds benevolence is rolled embryo and must expect embryo, be dosed to extruder, expect embryo aqueous 10～12%；Roll flake thickness degree 0.35～
0.45mm；Enter bulking machine material embryo moisture 10～11%；Go out bulking machine material embryo moisture 12～13%；105～110 DEG C of drop temperature；
Enter bulking machine steam pressure 0.65～0.75mpa；Vapor (steam) temperature: 174.5 DEG C；Hydraulic system working pressure 10.00
19.00mpa, obtains expanded peony seeds benevolence raw material；
Expanded peony seeds benevolence raw material is put into the extractor of subcritical equipment, raw material is 1:1- with the mass volume ratio of butane solvent
1:3, extraction temperature 30-50 DEG C；Extracting pressure is 0.35-0.6mpa, continuously extracts 2-3 time, each time 30-40 minute；
Using conventional fat degumming decoloring method to seed of Flos Moutan crude oil refine；
Peony seed oil later for refine is mixed by weight proportion with Oleum sesami or dha algae oil；The parts by weight of peony seed oil are
20-80 part, the parts by weight of Oleum sesami are 10-80 part；The amount of complex stabilizer is 20-100ppm；
Complex stabilizer is added in above-mentioned compound lard, obtains feature seed of Flos Moutan flavored oils, described complex stabilizer
Including at least in fresh peony flower quintessence oil, fat-soluble polyphenol, Herba Rosmarini Officinalis extract, astaxanthin, lycopene, capsorubin
Kind.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111631309A (en) * | 2020-06-29 | 2020-09-08 | 山东银香伟业集团有限公司 | Daily ration for producing dairy cows containing peony linoleic acid milk and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103859065A (en) * | 2014-03-06 | 2014-06-18 | 洛阳春魁农业开发有限公司 | Peony seed blend oil for clearing heat and removing toxicity and preparation method thereof |
| CN104928020A (en) * | 2015-06-12 | 2015-09-23 | 山西鑫中大生物科技有限公司 | Subcritical production method for peony seed oil extraction |
| CN105685260A (en) * | 2016-01-20 | 2016-06-22 | 和县绿源油脂有限公司 | Nutritious health-care peony seed blend oil and preparing process thereof |
| EP3153214A1 (en) * | 2015-10-08 | 2017-04-12 | Laboratoires Chemineau | Natural vegetable oil and lime water-based composition |
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2016
- 2016-11-24 CN CN201611049219.6A patent/CN106359660A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103859065A (en) * | 2014-03-06 | 2014-06-18 | 洛阳春魁农业开发有限公司 | Peony seed blend oil for clearing heat and removing toxicity and preparation method thereof |
| CN104928020A (en) * | 2015-06-12 | 2015-09-23 | 山西鑫中大生物科技有限公司 | Subcritical production method for peony seed oil extraction |
| EP3153214A1 (en) * | 2015-10-08 | 2017-04-12 | Laboratoires Chemineau | Natural vegetable oil and lime water-based composition |
| CN105685260A (en) * | 2016-01-20 | 2016-06-22 | 和县绿源油脂有限公司 | Nutritious health-care peony seed blend oil and preparing process thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111631309A (en) * | 2020-06-29 | 2020-09-08 | 山东银香伟业集团有限公司 | Daily ration for producing dairy cows containing peony linoleic acid milk and preparation method thereof |
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