CN106666634A - Preparation method of natural compound sweetener - Google Patents
Preparation method of natural compound sweetener Download PDFInfo
- Publication number
- CN106666634A CN106666634A CN201611135173.XA CN201611135173A CN106666634A CN 106666634 A CN106666634 A CN 106666634A CN 201611135173 A CN201611135173 A CN 201611135173A CN 106666634 A CN106666634 A CN 106666634A
- Authority
- CN
- China
- Prior art keywords
- sweetener
- powder
- supernatant
- fitted
- obtains
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000003599 food sweetener Nutrition 0.000 title claims abstract description 29
- 239000003765 sweetening agent Substances 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 229930014626 natural product Natural products 0.000 title abstract 5
- 239000000843 powder Substances 0.000 claims abstract description 44
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 28
- 235000014360 Punica granatum Nutrition 0.000 claims abstract description 19
- 238000000605 extraction Methods 0.000 claims abstract description 17
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 claims abstract description 14
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229940013618 stevioside Drugs 0.000 claims abstract description 14
- 235000019202 steviosides Nutrition 0.000 claims abstract description 14
- 241000219991 Lythraceae Species 0.000 claims abstract description 13
- 239000006228 supernatant Substances 0.000 claims description 36
- 239000002131 composite material Substances 0.000 claims description 18
- 239000003643 water by type Substances 0.000 claims description 18
- 235000009815 Momordica Nutrition 0.000 claims description 12
- 241000218984 Momordica Species 0.000 claims description 12
- 238000010009 beating Methods 0.000 claims description 12
- 238000005119 centrifugation Methods 0.000 claims description 12
- 238000001556 precipitation Methods 0.000 claims description 12
- 239000000284 extract Substances 0.000 claims description 10
- 241000628997 Flos Species 0.000 claims description 7
- 244000294611 Punica granatum Species 0.000 claims description 6
- 238000004140 cleaning Methods 0.000 claims description 6
- 230000007159 enucleation Effects 0.000 claims description 6
- 210000002615 epidermis Anatomy 0.000 claims description 6
- 239000004570 mortar (masonry) Substances 0.000 claims description 6
- 239000007921 spray Substances 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 238000002390 rotary evaporation Methods 0.000 claims description 2
- 208000008589 Obesity Diseases 0.000 abstract description 9
- 235000020824 obesity Nutrition 0.000 abstract description 9
- 238000000034 method Methods 0.000 abstract description 8
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 abstract description 5
- 231100000252 nontoxic Toxicity 0.000 abstract description 5
- 230000003000 nontoxic effect Effects 0.000 abstract description 5
- 229910052711 selenium Inorganic materials 0.000 abstract description 5
- 239000011669 selenium Substances 0.000 abstract description 5
- 229930003231 vitamin Natural products 0.000 abstract description 5
- 235000013343 vitamin Nutrition 0.000 abstract description 5
- 239000011782 vitamin Substances 0.000 abstract description 5
- 229940088594 vitamin Drugs 0.000 abstract description 5
- 239000000287 crude extract Substances 0.000 abstract description 4
- 229930006000 Sucrose Natural products 0.000 abstract description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 abstract description 3
- 206010012601 diabetes mellitus Diseases 0.000 abstract description 3
- 235000013305 food Nutrition 0.000 abstract description 3
- 235000013373 food additive Nutrition 0.000 abstract description 3
- 239000002778 food additive Substances 0.000 abstract description 3
- 238000000227 grinding Methods 0.000 abstract description 3
- 239000005720 sucrose Substances 0.000 abstract description 3
- 239000002253 acid Substances 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 244000228451 Stevia rebaudiana Species 0.000 abstract 2
- 238000013329 compounding Methods 0.000 abstract 2
- HELXLJCILKEWJH-NCGAPWICSA-N rebaudioside A Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HELXLJCILKEWJH-NCGAPWICSA-N 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 1
- 235000015203 fruit juice Nutrition 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 229930189775 mogroside Natural products 0.000 abstract 1
- 235000015816 nutrient absorption Nutrition 0.000 abstract 1
- 230000001737 promoting effect Effects 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 4
- 239000008280 blood Substances 0.000 description 4
- 210000004369 blood Anatomy 0.000 description 4
- 239000008103 glucose Substances 0.000 description 4
- 108010011485 Aspartame Proteins 0.000 description 3
- 239000000605 aspartame Substances 0.000 description 3
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 description 3
- 229960003438 aspartame Drugs 0.000 description 3
- 235000010357 aspartame Nutrition 0.000 description 3
- 230000029087 digestion Effects 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 235000021096 natural sweeteners Nutrition 0.000 description 3
- 230000001175 peptic effect Effects 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- 150000003722 vitamin derivatives Chemical class 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 235000019605 sweet taste sensations Nutrition 0.000 description 2
- 208000017667 Chronic Disease Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000508269 Psidium Species 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 230000000675 anti-caries Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000037406 food intake Effects 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- 210000003491 skin Anatomy 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention relates to a preparation method of a natural compound sweetener, and belongs to the technical filed of food additives. The preparation method of the natural compound sweetener comprises the following steps: adopting fructus momordicae and stevia as the raw materials; carrying out crude extraction by using an ethanol method so as to obtain mogroside and stevioside; compounding the selenium in the crude extract of the fructus momordicae with the vitamins and the like in the crude extract of the stevia; and then, carrying out compounding with pomegranate fruit juice powder, and carrying out grinding and mixing, so that the natural compound sweetener is prepared. The natural compound sweetener prepared by the preparation method has the characteristics that the sweetener is non-toxic, low in calorie, and high in sweetness; moreover, the sweetener is rich in selenium and vitamins, capable of promoting nutrient absorption, and refreshing in taste. The prepared sweetener is relatively stable to acid and alkali, so that the sweetener can be widely used in various kinds of foods instead of sucrose; and the sweetener can be used as substitute sugar for the patients with obesity and diabetes. The sweetener is low in cost, and has wide application prospects.
Description
Technical field
The present invention relates to a kind of preparation method of natural type composite sweetener, belongs to technical field of food additives.
Background technology
It is the main cause for causing the chronic diseases such as diabetes that phitosite is particularly the excess ingestion of glucide.Mesh
Just there is the nearly 1/3 edible low calories food of people in the Qian Jin U.S..According to estimates, the total demand of sweeting agent is very big, and about equivalence is in 3000
The sucrose of ten thousand t.The weak point such as the side effect existed due to artificial synthesis edulcorant and flavor taste, so many countries, special
It is not that developed country has put into effect corresponding control measures in succession.Thus novel low amount（Or empty calory）Natural sweetener is especially
The exploitation of sweeting agent increasingly draws attention with research.
Natural sweetener has the characteristics such as nontoxic, low in calories, high sugariness, anti-caries, safety, and tool is found from plant resourceses
There are several functions, high sugariness, safety non-toxic, the pure natural sweetener of sweet taste has become the heat of current food additive research
Point.
Sweeting agent contributes to alleviating pressure, makes people feel happy, but scientific research indicates sweeting agent at present on the market
Excessive intake can cause obesity, and produce various diseases, even shorten the life-span.Therefore, a kind of sweet taste of pure natural is studied
Agent is used as obesity and the aspartame of diabeticss, it appears particularly important.
The content of the invention
The technical problem to be solved：Can cause obesity for the excessive intake of sweeting agent at present on the market,
And various diseases are produced, even contract short-life problem, the invention provides a kind of preparation side of natural type composite sweetener
Method, the present invention is adopted with Fructus Momordicae, and Folium Stevlae Rebaudianae is raw material, and by Ethanol Method Momordica-Glycosides and stevioside are slightly carried, and is combined
Vitamin in selenium and Folium Stevlae Rebaudianae crude extract in Fructus Momordicae crude extract etc., finally compounds, ground and mixed with guava juice powder,
Prepared natural type composite sweetener.The characteristics of composite sweetener prepared by the present invention has nontoxic, low in calories, high sugariness, also richness
Containing selenium and vitamin, alimentation can be effectively facilitated, and mouthfeel is pure and fresh, it is relatively stable to soda acid, sucrose can be replaced and extensively should
In for varieties of food items, can be low as obesity and the aspartame of diabeticss, use cost.
To solve above-mentioned technical problem, the technical solution used in the present invention is：
（1）500~600g Fructus Momordicaes are weighed, is washed and cut open after epidermis enucleation, then added with 200~300mL deionized waters
10~15min of crushing and beating in refiner, obtains Fructus Momordicae serosity, measures 200~300mL Fructus Momordicaes serosity and adds 2~3L mass
Fraction is in 70% ethanol solution, under 70~75 DEG C of waters bath with thermostatic control, and with 60W ultrasonic echography 50~60min of assisted extraction,
Obtain Fructus Momordicae extracting solution；
（2）Above-mentioned Fructus Momordicae extracting solution is fitted in centrifuge, with 4000~6000/min, 10~15min of centrifugation, is collected
Supernatant, and precipitation is extracted again 1~2 time by aforesaid operations, merge supernatant, the supernatant after merging is loaded into rotary evaporation
In instrument, at 60~65 DEG C, it is evaporated to dryness under reduced pressure, is subsequently filled in pulverizer and crushes, cross 60 mesh sieves, obtains rich Momordica-Glycosides powder
End, it is standby；
（3）The fresh Folium Chrysanthemi of 200~300g is weighed, is added in refiner with 100~150mL deionized waters after washing and is crushed
10~12min of beating, obtains Folium Chrysanthemi serosity, and it is 70% ethanol to measure 100~150mL Folium Chrysanthemi serosity and add 2~3L mass fractions
In solution, under 65~68 DEG C of waters bath with thermostatic control, and with 80W ultrasonic echography 30~36min of assisted extraction, Folium Chrysanthemi extraction is obtained
Liquid；
（4）Above-mentioned Flos Chrysanthemi leaf extract is fitted in centrifuge, with 5000~6000/min, 10~12min of centrifugation, is collected
Supernatant, and precipitation is extracted again 1~2 time, merge supernatant, the supernatant after merging is fitted in Rotary Evaporators, 60
At~65 DEG C, it is evaporated to dryness under reduced pressure, is subsequently filled in pulverizer and crushes, cross 60 mesh sieves, obtains rich stevioside powder；
（5）1~2kg Punica granatum L.s are weighed, is removed the peel after cleaning up, and be fitted into homogenate in homogenizing refiner, Sucus Granati is obtained, by Sucus Granati
In adding spray dryer, powder is dried at 160~170 DEG C, obtains pomegranate powder, by weight 2：1：4, by step（2）Prepare
Rich Momordica-Glycosides powder, above-mentioned rich stevioside powder, pomegranate powder be fitted in mortar grind, cross 100 mesh sieves, obtain natural type
Composite sweetener.
The present invention application process be：It is 1 ~ 3% by addition, natural type composite sweetener prepared by the present invention is added
To tea-drinking, obesity patient or diabeticss drink daily 100 ~ 200mL, it is possible to decrease blood glucose 11 ~ 18%, and can promote diabetes involving middle-JIAO
Change.
The method have the benefit that：
（1）Natural type composite sweetener prepared by the present invention, nontoxic, low in calories, high sugariness, and mouthfeel is excellent, to ph stability
Property is good；
（2）Natural type composite sweetener prepared by the present invention can effectively facilitate alimentation rich in selenium and vitamin, can be used as fertilizer
The aspartame of fat disease and diabeticss.
Specific embodiment
500~600g Fructus Momordicaes are weighed, is washed and cut open after epidermis enucleation, then added with 200~300mL deionized waters
10~15min of crushing and beating in refiner, obtains Fructus Momordicae serosity, measures 200~300mL Fructus Momordicaes serosity and adds 2~3L mass
Fraction is in 70% ethanol solution, under 70~75 DEG C of waters bath with thermostatic control, and with 60W ultrasonic echography 50~60min of assisted extraction,
Obtain Fructus Momordicae extracting solution；Above-mentioned Fructus Momordicae extracting solution is fitted in centrifuge, with 4000~6000/min centrifugations 10~
15min, collects supernatant, and precipitation is extracted again 1~2 time by aforesaid operations, merges supernatant, and the supernatant after merging is filled
In entering Rotary Evaporators, at 60~65 DEG C, it is evaporated to dryness under reduced pressure, is subsequently filled in pulverizer and crushes, crosses 60 mesh sieves, get Fu Luo
The sweet glycoside powder of Chinese fruit；The fresh Folium Chrysanthemi of 200~300g is weighed, refiner is added with 100~150mL deionized waters after washing
Middle 10~12min of crushing and beating, obtains Folium Chrysanthemi serosity, measures 100~150mL Folium Chrysanthemi serosity addition 2~3L mass fractions and is
In 70% ethanol solution, under 65~68 DEG C of waters bath with thermostatic control, and with 80W ultrasonic echography 30~36min of assisted extraction, Flos Chrysanthemi is obtained
Leaf extract；Above-mentioned Flos Chrysanthemi leaf extract is fitted in centrifuge, with 5000~6000/min, 10~12min of centrifugation, is received
Collection supernatant, and precipitation is extracted again 1~2 time, merge supernatant, the supernatant after merging is fitted in Rotary Evaporators,
At 60~65 DEG C, it is evaporated to dryness under reduced pressure, is subsequently filled in pulverizer and crushes, cross 60 mesh sieves, obtains rich stevioside powder；Weigh 1
~2kg Punica granatum L.s, remove the peel after cleaning up, and are fitted into homogenate in homogenizing refiner, obtain Sucus Granati, Sucus Granati is added and is spray-dried
In device, powder is dried at 160~170 DEG C, obtains pomegranate powder, by weight 2：1：4, by above-mentioned rich Momordica-Glycosides powder, on
Rich stevioside powder is stated, pomegranate powder is fitted in mortar grinds, and crosses 100 mesh sieves, obtains natural type composite sweetener.
Example 1
500g Fructus Momordicaes are weighed, is washed and cut open after epidermis enucleation, then broken in refiner beating is added with 200mL deionized waters
Slurry 10min, obtains Fructus Momordicae serosity, and it is in 70% ethanol solution, at 70 DEG C to measure 200mL Fructus Momordicaes serosity and add 2L mass fractions
Under water bath with thermostatic control, and with 60W ultrasonic echography assisted extraction 50min, obtain Fructus Momordicae extracting solution；By above-mentioned Fructus Momordicae extracting solution dress
In entering centrifuge, with 4000/min centrifugation 10min, supernatant is collected, and precipitation is extracted again 1 time by aforesaid operations, closed
And supernatant, the supernatant after merging is fitted in Rotary Evaporators, at 60 DEG C, it is evaporated to dryness under reduced pressure, it is subsequently filled into crushing
Crush in machine, cross 60 mesh sieves, obtain rich Momordica-Glycosides powder；Weigh the fresh Folium Chrysanthemi of 200g, wash after and 100mL go from
Sub- water adds crushing and beating 10min in refiner, obtains Folium Chrysanthemi serosity, measures 100mL Folium Chrysanthemi serosity and adds 2L mass fractions
In for 70% ethanol solution, under 65 DEG C of waters bath with thermostatic control, and with 80W ultrasonic echography assisted extraction 30min, Folium Chrysanthemi extraction is obtained
Liquid；Above-mentioned Flos Chrysanthemi leaf extract is fitted in centrifuge, with 5000/min centrifugation 10min, supernatant is collected, and will precipitation
Extract again 1 time, merge supernatant, the supernatant after merging is fitted in Rotary Evaporators, at 60 DEG C, be evaporated to dryness under reduced pressure,
It is subsequently filled in pulverizer and crushes, cross 60 mesh sieves, obtains rich stevioside powder；1kg Punica granatum L.s are weighed, is removed the peel after cleaning up, and
It is fitted in homogenizing refiner and is homogenized, obtain Sucus Granati, Sucus Granati is added in spray dryer, at 160 DEG C powder is dried to, obtains stone
Pomegranate powder, by weight 2：1：4, by above-mentioned rich Momordica-Glycosides powder, above-mentioned rich stevioside powder, pomegranate powder is fitted in mortar
Grinding, crosses 100 mesh sieves, obtains natural type composite sweetener.
The present invention application process be：By addition be 1%, by the present invention prepare natural type composite sweetener add to
Tea-drinking, obesity patient or diabeticss drink daily 100 ~ 200mL, it is possible to decrease blood glucose 11%, and can promote peptic digestion.
Example 2
550g Fructus Momordicaes are weighed, is washed and cut open after epidermis enucleation, then broken in refiner beating is added with 250mL deionized waters
Slurry 12min, obtains Fructus Momordicae serosity, and it is in 70% ethanol solution, 72 to measure 250mL Fructus Momordicaes serosity and add 2.5L mass fractions
Under DEG C water bath with thermostatic control, and with 60W ultrasonic echography assisted extraction 55min, obtain Fructus Momordicae extracting solution；By above-mentioned Fructus Momordicae extracting solution
In being fitted into centrifuge, with 5000/min centrifugation 12min, supernatant is collected, and precipitation is extracted again 1 time by aforesaid operations,
Merge supernatant, the supernatant after merging is fitted in Rotary Evaporators, at 62 DEG C, be evaporated to dryness under reduced pressure, be subsequently filled into powder
Crush in broken machine, cross 60 mesh sieves, obtain rich Momordica-Glycosides powder；The fresh Folium Chrysanthemi of 250g is weighed, is gone with 120mL after washing
Ionized water adds crushing and beating 11min in refiner, obtains Folium Chrysanthemi serosity, measures 120mL Folium Chrysanthemi serosity and adds 2.5L mass
Fraction is in 70% ethanol solution, under 66 DEG C of waters bath with thermostatic control, and with 80W ultrasonic echography assisted extraction 32min, to obtain Folium Chrysanthemi
Extracting solution；Above-mentioned Flos Chrysanthemi leaf extract is fitted in centrifuge, with 5500/min centrifugation 11min, supernatant is collected, and will
Precipitation extract again 1 time, merge supernatant, the supernatant after merging is fitted in Rotary Evaporators, at 62 DEG C, be evaporated under reduced pressure to
It is dry, it is subsequently filled in pulverizer and crushes, 60 mesh sieves are crossed, obtain rich stevioside powder；1.5kg Punica granatum L.s are weighed, is gone after cleaning up
Skin, and it is fitted into homogenate in homogenizing refiner, Sucus Granati is obtained, Sucus Granati is added in spray dryer, it is dried at 165 DEG C
Powder, obtains pomegranate powder, by weight 2：1：4, by above-mentioned rich Momordica-Glycosides powder, above-mentioned rich stevioside powder, pomegranate powder dress
Enter in mortar and grind, cross 100 mesh sieves, obtain natural type composite sweetener.
The present invention application process be：By addition be 2%, by the present invention prepare natural type composite sweetener add to
Tea-drinking, obesity patient or diabeticss drink daily 150mL, it is possible to decrease blood glucose 13%, and can promote peptic digestion.
Example 3
600g Fructus Momordicaes are weighed, is washed and cut open after epidermis enucleation, then broken in refiner beating is added with 300mL deionized waters
Slurry 15min, obtains Fructus Momordicae serosity, and it is in 70% ethanol solution, at 75 DEG C to measure 300mL Fructus Momordicaes serosity and add 3L mass fractions
Under water bath with thermostatic control, and with 60W ultrasonic echography assisted extraction 60min, obtain Fructus Momordicae extracting solution；By above-mentioned Fructus Momordicae extracting solution dress
In entering centrifuge, with 6000/min centrifugation 15min, supernatant is collected, and precipitation is extracted again 2 times by aforesaid operations, closed
And supernatant, the supernatant after merging is fitted in Rotary Evaporators, at 65 DEG C, it is evaporated to dryness under reduced pressure, it is subsequently filled into crushing
Crush in machine, cross 60 mesh sieves, obtain rich Momordica-Glycosides powder；Weigh the fresh Folium Chrysanthemi of 300g, wash after and 150mL go from
Sub- water adds crushing and beating 12min in refiner, obtains Folium Chrysanthemi serosity, measures 150mL Folium Chrysanthemi serosity and adds 3L mass fractions
In for 70% ethanol solution, under 68 DEG C of waters bath with thermostatic control, and with 80W ultrasonic echography assisted extraction 36min, Folium Chrysanthemi extraction is obtained
Liquid；Above-mentioned Flos Chrysanthemi leaf extract is fitted in centrifuge, with 6000/min centrifugation 12min, supernatant is collected, and will precipitation
Extract again 2 times, merge supernatant, the supernatant after merging is fitted in Rotary Evaporators, at 65 DEG C, be evaporated to dryness under reduced pressure,
It is subsequently filled in pulverizer and crushes, cross 60 mesh sieves, obtains rich stevioside powder；2kg Punica granatum L.s are weighed, is removed the peel after cleaning up, and
It is fitted in homogenizing refiner and is homogenized, obtain Sucus Granati, Sucus Granati is added in spray dryer, at 170 DEG C powder is dried to, obtains stone
Pomegranate powder, by weight 2：1：4, by above-mentioned rich Momordica-Glycosides powder, above-mentioned rich stevioside powder, pomegranate powder is fitted in mortar
Grinding, crosses 100 mesh sieves, obtains natural type composite sweetener.
The present invention application process be：By addition be 3%, by the present invention prepare natural type composite sweetener add to
Tea-drinking, obesity patient or diabeticss drink daily 100 ~ 200mL, it is possible to decrease blood glucose 18%, and can promote peptic digestion.
Claims (1)
1. a kind of preparation method of natural type composite sweetener, it is characterised in that concrete preparation process is：
（1）500~600g Fructus Momordicaes are weighed, is washed and cut open after epidermis enucleation, then added with 200~300mL deionized waters
10~15min of crushing and beating in refiner, obtains Fructus Momordicae serosity, measures 200~300mL Fructus Momordicaes serosity and adds 2~3L mass
Fraction is in 70% ethanol solution, under 70~75 DEG C of waters bath with thermostatic control, and with 60W ultrasonic echography 50~60min of assisted extraction,
Obtain Fructus Momordicae extracting solution；
（2）Above-mentioned Fructus Momordicae extracting solution is fitted in centrifuge, with 4000~6000/min, 10~15min of centrifugation, is collected
Supernatant, and precipitation is extracted again 1~2 time by aforesaid operations, merge supernatant, the supernatant after merging is loaded into rotary evaporation
In instrument, at 60~65 DEG C, it is evaporated to dryness under reduced pressure, is subsequently filled in pulverizer and crushes, cross 60 mesh sieves, obtains rich Momordica-Glycosides powder
End, it is standby；
（3）The fresh Folium Chrysanthemi of 200~300g is weighed, is added in refiner with 100~150mL deionized waters after washing and is crushed
10~12min of beating, obtains Folium Chrysanthemi serosity, and it is 70% ethanol to measure 100~150mL Folium Chrysanthemi serosity and add 2~3L mass fractions
In solution, under 65~68 DEG C of waters bath with thermostatic control, and with 80W ultrasonic echography 30~36min of assisted extraction, Folium Chrysanthemi extraction is obtained
Liquid；
（4）Above-mentioned Flos Chrysanthemi leaf extract is fitted in centrifuge, with 5000~6000/min, 10~12min of centrifugation, is collected
Supernatant, and precipitation is extracted again 1~2 time, merge supernatant, the supernatant after merging is fitted in Rotary Evaporators, 60
At~65 DEG C, it is evaporated to dryness under reduced pressure, is subsequently filled in pulverizer and crushes, cross 60 mesh sieves, obtains rich stevioside powder；
（5）1~2kg Punica granatum L.s are weighed, is removed the peel after cleaning up, and be fitted into homogenate in homogenizing refiner, Sucus Granati is obtained, by Sucus Granati
In adding spray dryer, powder is dried at 160~170 DEG C, obtains pomegranate powder, by weight 2：1：4, by step（2）Prepare
Rich Momordica-Glycosides powder, above-mentioned rich stevioside powder, pomegranate powder be fitted in mortar grind, cross 100 mesh sieves, obtain natural type
Composite sweetener.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611135173.XA CN106666634A (en) | 2016-12-11 | 2016-12-11 | Preparation method of natural compound sweetener |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611135173.XA CN106666634A (en) | 2016-12-11 | 2016-12-11 | Preparation method of natural compound sweetener |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106666634A true CN106666634A (en) | 2017-05-17 |
Family
ID=58868523
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611135173.XA Pending CN106666634A (en) | 2016-12-11 | 2016-12-11 | Preparation method of natural compound sweetener |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106666634A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108606297A (en) * | 2018-04-24 | 2018-10-02 | 晨光生物科技集团股份有限公司 | A kind of industrial production process of composite sweetener |
| CN109043469A (en) * | 2018-08-03 | 2018-12-21 | 湖北艾中艾本草科技有限公司 | A kind of composite sweetener and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101854814A (en) * | 2007-11-12 | 2010-10-06 | 三荣源有限公司 | Method of improving sweetness qualities of stevia extract |
| CN102084982A (en) * | 2009-12-02 | 2011-06-08 | 桂林莱茵生物科技股份有限公司 | Sweetening agent composition |
-
2016
- 2016-12-11 CN CN201611135173.XA patent/CN106666634A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101854814A (en) * | 2007-11-12 | 2010-10-06 | 三荣源有限公司 | Method of improving sweetness qualities of stevia extract |
| CN102084982A (en) * | 2009-12-02 | 2011-06-08 | 桂林莱茵生物科技股份有限公司 | Sweetening agent composition |
Non-Patent Citations (2)
| Title |
|---|
| 史一鸣等: "亲水色谱法测定甜叶菊叶片中糖苷含量", 《食品研究与开发》 * |
| 马少妹等: "超声波强化乙醇提取罗汉果甜苷", 《沈阳药科大学学报》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108606297A (en) * | 2018-04-24 | 2018-10-02 | 晨光生物科技集团股份有限公司 | A kind of industrial production process of composite sweetener |
| CN109043469A (en) * | 2018-08-03 | 2018-12-21 | 湖北艾中艾本草科技有限公司 | A kind of composite sweetener and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104432084B (en) | A kind of conditioning powder and its production and use | |
| CN102669671B (en) | Preparation method for ultrafine nutrient powder of yams, seeds of Job's tears, and red jujubes | |
| CN1871932A (en) | Method for preparing climbing fig seed glue and gel powder of climbing fig seed glue | |
| CN103393183B (en) | Traditional Chinese medicine health-care beverage having effects of clearing heat and moisturizing dryness and preparation method thereof | |
| CN103494292A (en) | Oily peony seed meal cake plant protein beverage and preparation method thereof | |
| CN106071627B (en) | A kind of preparation method of purple sweet potato mulberries instant powder | |
| CN106578077A (en) | Milk tea containing kelp dietary fibers and preparation method thereof | |
| CN111685214A (en) | A health candy containing natural plant edible gum and its preparation method | |
| CN106666634A (en) | Preparation method of natural compound sweetener | |
| CN101554242A (en) | Honeysuckle drink and processing technique thereof | |
| CN105266149A (en) | Herba dendrodii officinalis compound health-care capsule and preparation method thereof | |
| CN104472746A (en) | Processing method of camellia nitidissima chi health tea | |
| CN108887624A (en) | A kind of high-quality berry pomace meal replacement powder and its processing method | |
| CN106136116A (en) | A kind of wheat seedling lung moistening intestine moistening meal replacement powder and preparation method thereof | |
| CN101248892B (en) | Sea-tangle sesame paste | |
| CN113925172A (en) | Giant salamander peptide nutritional composition suitable for children | |
| CN106578186A (en) | Electuary of Stevia rebaudiana health-care tea | |
| CN109043469B (en) | Compound sweetener and preparation method thereof | |
| CN101862375A (en) | Compound jellyfish soluble granules for reducing blood pressure and preparation method thereof | |
| KR101316090B1 (en) | Health assistance food using abalone shell and manufacturing method thereof | |
| CN106035869A (en) | Preparation method of siraitia grosvenorii and isatis root extract compound tea | |
| CN105166902A (en) | Preparation method of quick-dissolving type okra submicron powder and quick-dissolving type okra submicron powder prepared through preparation method | |
| CN108968041A (en) | A kind of big bean seedlings appetizing ease constipation meal replacement powder and preparation method thereof | |
| CN104721622B (en) | A kind of preparation for being used to prevent and treat liver fibrosis | |
| CN108851054A (en) | A kind of eucommia Bark male flower chewable tablets and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170517 |