CN106619891A - Processing method for quick-freezing and refrigeration, enzyme deactivation and drying through electric field combined with ultrasound and microwave of traditional Chinese medicinal material green plum blossom - Google Patents
Processing method for quick-freezing and refrigeration, enzyme deactivation and drying through electric field combined with ultrasound and microwave of traditional Chinese medicinal material green plum blossom Download PDFInfo
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- CN106619891A CN106619891A CN201611246296.0A CN201611246296A CN106619891A CN 106619891 A CN106619891 A CN 106619891A CN 201611246296 A CN201611246296 A CN 201611246296A CN 106619891 A CN106619891 A CN 106619891A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
- A61K36/736—Prunus, e.g. plum, cherry, peach, apricot or almond
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The invention discloses a processing method for quick-freezing and refrigeration, enzyme deactivation and drying through electric field combined with ultrasound and microwave of a traditional Chinese medicinal material green plum blossom. The method comprises the following steps: firstly, quickly freezing and refrigerating the fresh green plum blossom buds, thereby effectively reducing the oxidase activity, preventing from oxidization and supplying sufficient time for the subsequent operation; treating the green plum blossom buds roasted with hot air by an electric field in combination with ultrasound, thereby facilitating the dissolution of the effective constituents; utilizing microwave and a mixed solution to perform short-time high-temperature high-humidity microwave enzyme deactivation, thereby damaging PPO activity, preventing the green plum blossom buds from turning brown stain and reducing the loss of effective constituents; and finally, performing microwave drying, thereby drying the materials within a short time, uniformly heating and promoting the product color and quality. The green plum blossom processed according to the method has excellent appearance, color, luster and quality and is high in chlorogenic acid, hyperin and isoquercitrin content; after the green plum blossom is brewed, the ingredients can be easily dissolved out; the processing efficiency is high; the automatic control is facilitated; the processing method is suitable for large-scale production.
Description
Technical field
The present invention relates to Chinese medicine processes field, more particularly to a kind of Chinese medicine flower bud of Japanese apricot quick freezing and cold preserving, electric field are combined and surpassed
The concocting method of sound, microwave de-enzyming and drying.
Background technology
Flower bud of Japanese apricot is the dry flower of rosaceous plant FLOS MUME, there is out the effect of Yu Hezhong, resolving sputum, removing toxic substances.In green plum
Find after colored main product ground She County, anhuio investigation, flower bud of Japanese apricot is plucked when deep winter and early spring is bloomed, and cultivation is more not on a large scale.Producing
In ground process, air blast oven drying method is mainly adopted；Learnt by visiting flower-grower, local farmers family is usually used a kind of drying
The easy device of machine processing, mainly with timber as the energy, after combustion of wood heating, by the different wind speed fans blowings of control come
Reach drying effect.Specific practice is as follows：Fresh flower bud of Japanese apricot is plucked, in transporting house back, is laid in the bamboo plaque drawer of hollow out and is divulged information
Cool place is placed,（If meeting the rainy day just to dry in the air to surface without the obvious globule,）Dryer is put into, after heating, little wind, drawer after first strong wind
From bottom to top displacement position successively, with micro-judgment degree of drying, lacks unified parameter to control processing technology, and then controls
Flower bud of Japanese apricot quality.From burn wood, pole not environmentally, is again easily caused fire by drying later still to the main heat energy of said method
The time at one day night is needed, is taken time and effort, and the flower bud of Japanese apricot quality ginseng time not processed with other is uneven, unsuitable for factory
The requirement of large-scale production.Therefore for problem present in flower bud of Japanese apricot Habitat producing traditional handicraft, urgent need is developed a kind of complete
New flower bud of Japanese apricot concocting method, to meet the market demand.
The content of the invention
In order to overcoming prior art and not enough, it is an object of the invention to provide a kind of Chinese medicine flower bud of Japanese apricot is quick-frozen cold
Tibetan, electric field combine the concocting method of ultrasound, microwave de-enzyming and drying.Flower bud of Japanese apricot profile, color and luster and product that the inventive method is processed
Matter is good, and its chlorogenic acid, Hyperoside and isoquercitrin content are high, and composition dissolution is beneficial to after brewing, and high in machining efficiency, easily
It is achieving environmental protection and energy saving in Automated condtrol, be adapted to large-scale production, for flower bud of Japanese apricot industrialization production provide certain technology according to
According to.
For achieving the above object, the technical solution used in the present invention is as follows：
A kind of Chinese medicine flower bud of Japanese apricot quick freezing and cold preserving, electric field combine the concocting method of ultrasound, microwave de-enzyming and drying, including following step
Suddenly：
（1）After fresh flower bud of Japanese apricot bud is plucked, divide and hang surface without the globule；
（2）The flower bud of Japanese apricot bud for just hanging is quick-frozen at a temperature of being placed in -50～-40 DEG C, then is placed in -15～-25 DEG C of temperature
Lower refrigeration 24h-48h, then thaws at a temperature of 2-5 DEG C, and 10-15h is toasted under 40-60 DEG C of hot blast after defrosting；
（3）It is 20-30kV/cm by the flower bud of Japanese apricot bud Jing field intensity after air cooking, pulse frequency is the high pressure of 600-700pps
Impulse electric field processes 1-2ms, then Jing power is 300-400W ultrasonications 15-25min；Then electric field is combined at ultrasound
Flower bud of Japanese apricot bud after reason uniformly sprays mixed solution, and mixed solution sprinkling amount is the 1-1.5% of flower bud of Japanese apricot bud quality, divides
24-48h is hung, then the flower bud of Japanese apricot bud for hanging is placed on the pallet of microwave dryer or conveyer belt, according to processing
Amount adjusts microwave power in closed environment, and the microwave de-enzyming 1-10min at a temperature of 80-95 DEG C, period only heats not air draft not
Dehumidifying, is then shut off microwave and hangs 1-30min, then opens microwave microwave drying 10-60min at a temperature of 40-60 DEG C, and period adds
Air draft dehumidifying while hot, drying is placed at shady and cool ventilation after terminating, divides and hang 20-40min.
A kind of Chinese medicine flower bud of Japanese apricot quick freezing and cold preserving, electric field combine the concocting method of ultrasound, microwave de-enzyming and drying, including following step
Suddenly：
（1）After fresh flower bud of Japanese apricot bud is plucked, divide and hang surface without the globule；
（2）The flower bud of Japanese apricot bud for just hanging is quick-frozen at a temperature of being placed in -50～-40 DEG C, then is placed in -15～-25 DEG C of temperature
Lower refrigeration 24h-48h, then thaws at a temperature of 2-5 DEG C, and 10-15h is toasted under 40-60 DEG C of hot blast after defrosting；
（3）It is 20-30kV/cm by the flower bud of Japanese apricot bud Jing field intensity after air cooking, pulse frequency is the high pressure of 600-700pps
Impulse electric field processes 1-2ms, then Jing power is 300-400W ultrasonications 15-25min；Then electric field is combined at ultrasound
Flower bud of Japanese apricot bud after reason uniformly sprays mixed solution, and mixed solution sprinkling amount is the 1-1.5% of flower bud of Japanese apricot bud quality, divides
24-48h is hung, then the flower bud of Japanese apricot bud for hanging is placed on the pallet of microwave dryer or conveyer belt, according to processing
Amount adjusts microwave power in closed environment, and the microwave de-enzyming 1-10min at a temperature of 80-95 DEG C, period only heats not air draft not
Dehumidifying, is then shut off microwave and hangs 1-30min, then opens microwave microwave drying 10-60min at a temperature of 40-60 DEG C, and period adds
Air draft dehumidifying while hot, drying is placed at shady and cool ventilation after terminating, divides and hang 20-40min.
It is quick-frozen at a temperature of -40 DEG C, then 24h-48h is refrigerated at a temperature of being placed in -15～-25 DEG C, then at a temperature of 2-5 DEG C
Thaw, 10-15h is toasted under 40-60 DEG C of hot blast after defrosting；
（3）It is 20-30kV/cm by the flower bud of Japanese apricot bud Jing field intensity after air cooking, pulse frequency is the high pressure of 600-700pps
Impulse electric field processes 1-2ms, then Jing power is 300-400W ultrasonications 15-25min；Then electric field is combined at ultrasound
Flower bud of Japanese apricot bud after reason uniformly sprays mixed solution, and mixed solution sprinkling amount is the 1-1.5% of flower bud of Japanese apricot bud quality, divides
24-48h is hung, then the flower bud of Japanese apricot bud for hanging is placed on the pallet of microwave dryer or conveyer belt, according to processing
Amount adjusts microwave power in closed environment, and the microwave de-enzyming 1-10min at a temperature of 80-95 DEG C, period only heats not air draft not
Dehumidifying, is then shut off microwave and hangs 1-30min, then opens microwave microwave drying 10-60min at a temperature of 40-60 DEG C, and period adds
Air draft dehumidifying while hot, drying is placed at shady and cool ventilation after terminating, divides and hang 20-40min.
The mixed solution is mixed by the composition of following percentage by weight:Citric acid 2-3%, Cys
0.5-1%, sodium carboxymethylcellulose 3-4%, water 93-98%.
According to multiple batches of sampling test data result analysis for many years：
1st, flower bud of Japanese apricot sample moisture data, traditional processing procedure sample between 9.04-11.18, mean value：10.08；The present invention
Processing procedure sample between 6.04-8.61, mean value：7.05.Total ash data tradition processing procedure sample is in 5.99-6.82
Between, mean value：6.48；Processing procedure sample of the present invention between 5.04-6.07, mean value：5.36.Flower bud of Japanese apricot tradition is processed
Process sample reaches 2015 editions with the moisture of processing procedure sample of the present invention with total ash《Chinese Pharmacopoeia》Mark under plum blossom item
It is accurate：Moisture must not cross 13.0%；Total ash must not cross 10.0%.
2nd, extract data, traditional processing procedure sample between 35.20-40.13, mean value：37.67；Big gun of the present invention
Process sample processed between 38.80-43.49, mean value：40.72.Flower bud of Japanese apricot tradition processing procedure sample processes work with the present invention
The extract of skill sample reaches 2015 editions《Chinese Pharmacopoeia》Standard under plum blossom item：No less than 30.0%.
3rd, chlorogenic acid content, traditional processing procedure sample between 5.63-6.20, mean value：5.86；The present invention processes work
Skill sample between 6.63-7.76, mean value：7.25.
4th, Hyperoside and isoquercitrin total amount, traditional processing procedure sample between 0.98-1.32, mean value：1.11；
Processing procedure sample of the present invention between 1.89-2.79, mean value：2.34.
Can be seen that based on the above results, processing procedure of the present invention is compared with traditional processing procedure, and moisture, ash content are relatively low, leaching
Apparent extract, chlorogenic acid content, Hyperoside and isoquercitrin total amount are higher, and the sample of this traditional processing procedure collected
Outward appearance illustrates that traditional processing procedure has unstability, by each in green, the Habitat producing sample collected during better than pilot experiment
Planting affects larger, and this processing procedure sample appearance of the present invention is consistent with early-stage Study in yellow green, illustrates that its technique is more steady
Fixed, its inherent quality is also more excellent, while have universality, therefore the technique can as a kind of new flower bud of Japanese apricot processing procedure,
The flower bud of Japanese apricot profile of processing, color and luster and quality are good, and its chlorogenic acid, Hyperoside and isoquercitrin content are high, profit after brewing
It is in composition dissolution and high in machining efficiency, it is easy to Automated condtrol, it is achieving environmental protection and energy saving, it is adapted to large-scale production, it is flower bud of Japanese apricot product
Industry metaplasia is produced and provides certain technical basis.
Claims (2)
1. a kind of Chinese medicine flower bud of Japanese apricot quick freezing and cold preserving, electric field combine the concocting method of ultrasound, microwave de-enzyming and drying, and its feature exists
In comprising the following steps：
(1) after fresh flower bud of Japanese apricot bud is plucked, divide and hang surface without the globule；
(2) the flower bud of Japanese apricot bud for just hanging is quick-frozen at a temperature of being placed in -50～-40 DEG C, then is placed in -15～-25 DEG C of temperature
Lower refrigeration 24h-48h, then thaws at a temperature of 2-5 DEG C, and 10-15h is toasted under 40-60 DEG C of hot blast after defrosting；
(3) it is 20-30kV/cm by the flower bud of Japanese apricot bud Jing field intensity after air cooking, pulse frequency is the high pressure of 600-700pps
Impulse electric field processes 1-2ms, then Jing power is 300-400W ultrasonications 15-25min；Then electric field is combined at ultrasound
Flower bud of Japanese apricot bud after reason uniformly sprays mixed solution, and mixed solution sprinkling amount is the 1-1.5% of flower bud of Japanese apricot bud quality, divides
24-48h is hung, then the flower bud of Japanese apricot bud for hanging is placed on the pallet of microwave dryer or conveyer belt, according to processing
Amount adjusts microwave power in closed environment, and the microwave de-enzyming 1-10min at a temperature of 80-95 DEG C, period only heats not air draft not
Dehumidifying, is then shut off microwave and hangs 1-30min, then opens microwave microwave drying 10-60min at a temperature of 40-60 DEG C, and period adds
Air draft dehumidifying while hot, drying is placed at shady and cool ventilation after terminating, divides and hang 20-40min.
2. Chinese medicine flower bud of Japanese apricot quick freezing and cold preserving according to claim 1, electric field combine the big gun of ultrasound, microwave de-enzyming and drying
Method processed, it is characterised in that the mixed solution is mixed by the composition of following percentage by weight:Citric acid 2-3%, L-
Cysteine 0.5-1%, sodium carboxymethylcellulose 3-4%, water 93-98%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611246296.0A CN106619891A (en) | 2016-12-29 | 2016-12-29 | Processing method for quick-freezing and refrigeration, enzyme deactivation and drying through electric field combined with ultrasound and microwave of traditional Chinese medicinal material green plum blossom |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611246296.0A CN106619891A (en) | 2016-12-29 | 2016-12-29 | Processing method for quick-freezing and refrigeration, enzyme deactivation and drying through electric field combined with ultrasound and microwave of traditional Chinese medicinal material green plum blossom |
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| CN106619891A true CN106619891A (en) | 2017-05-10 |
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| CN201611246296.0A Pending CN106619891A (en) | 2016-12-29 | 2016-12-29 | Processing method for quick-freezing and refrigeration, enzyme deactivation and drying through electric field combined with ultrasound and microwave of traditional Chinese medicinal material green plum blossom |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11977154B2 (en) | 2016-10-28 | 2024-05-07 | Ppg Industries Ohio, Inc. | Coatings for increasing near-infrared detection distances |
| US12001034B2 (en) | 2019-01-07 | 2024-06-04 | Ppg Industries Ohio, Inc. | Near infrared control coating, articles formed therefrom, and methods of making the same |
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| CN104222339A (en) * | 2014-09-03 | 2014-12-24 | 湖北友花窨茶花艺科技有限公司 | Production method of calyx canthus flower tea |
| CN104784238A (en) * | 2015-04-23 | 2015-07-22 | 合肥伟海讴斯医药科技有限公司 | Processing method for traditional Chinese medicine huangshan tribute chrysanthemum through steam blanching, microwave de-enzyming and vacuum freeze drying manners |
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| CN104222339A (en) * | 2014-09-03 | 2014-12-24 | 湖北友花窨茶花艺科技有限公司 | Production method of calyx canthus flower tea |
| CN104784238A (en) * | 2015-04-23 | 2015-07-22 | 合肥伟海讴斯医药科技有限公司 | Processing method for traditional Chinese medicine huangshan tribute chrysanthemum through steam blanching, microwave de-enzyming and vacuum freeze drying manners |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11977154B2 (en) | 2016-10-28 | 2024-05-07 | Ppg Industries Ohio, Inc. | Coatings for increasing near-infrared detection distances |
| US12001034B2 (en) | 2019-01-07 | 2024-06-04 | Ppg Industries Ohio, Inc. | Near infrared control coating, articles formed therefrom, and methods of making the same |
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Application publication date: 20170510 |