CN106619704A - Trace element supplement and preparation method thereof - Google Patents
Trace element supplement and preparation method thereof Download PDFInfo
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- CN106619704A CN106619704A CN201611169567.7A CN201611169567A CN106619704A CN 106619704 A CN106619704 A CN 106619704A CN 201611169567 A CN201611169567 A CN 201611169567A CN 106619704 A CN106619704 A CN 106619704A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/01—Hydrocarbons
- A61K31/015—Hydrocarbons carbocyclic
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/04—Sulfur, selenium or tellurium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/24—Heavy metals; Compounds thereof
- A61K33/30—Zinc; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/232—Angelica
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- Engineering & Computer Science (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a trace element supplement, which is mainly made from the following components, by weight part, maifan stone, micalex and montmorillonite. The invention further provides a preparation method of the trace element supplement. The method mainly comprises the following steps: (1) obtaining original stones; (2) pulverizing the original stones obtained in the step (1); (3) making the pulverized particles obtained in the step (2) into nanometer particles; (4) making the nanometer original stone power obtained in the step (3) into mixed nanometer particles; (5) putting the nanometer original stone powder obtained in the step (4) in a soaking containing for negative-pressure soaking to dissolve mineral elements; (6) performing centrifugation to the mineral element soaking liquid obtained in the step (5) to extract a supernatant; and (7) repeating the step (5) and the step (6),concentrating the obtained supernatant, and putting the concentrated liquid in an oven for drying to remove water to obtain a powder preparation. The preparation method is very simple, easy for industrial production and beneficial for massive popularization and use.
Description
Technical field
The present invention relates to replenishers field, more particularly to a kind of micro element supplement agent and preparation method thereof.
Background technology
Human body is made up of 50 multiple elements.Content according to element in human body is different, can be divided into macroelement
With micro- two big class.Although content of the trace element in human body is few, closely bound up with the existence of people and health, right
The life of people plays vital effect.Their excess intake, deficiency, imbalance or shortage all can to some extent cause people
Body it is physiological abnormal or occur disease.
However, the micro- arbitrary way of people's employing now is more single and effect is bad, a kind of supplement is needed badly
Effect is good and the micro element supplement agent that can be widely popularized.
The content of the invention
The purpose of the present invention aims to provide a kind of micro element supplement agent and preparation method thereof, is asked with solving above-mentioned technology
Topic.
The first object of the present invention is to provide a kind of micro element supplement agent, and above-mentioned purpose is able to by the following technical programs
Realize：A kind of micro element supplement agent, by weight calculating, is extracted by the material including following raw material components and is made：Medical stone 3
~ 20 parts, 2 ~ 2.5 parts of micarex, 4 ~ 10 parts of montmorillonite.
The second object of the present invention is to provide a kind of preparation method of micro element supplement agent, and above-mentioned purpose is by following skill
Art scheme is achieved：A kind of method for preparing micro element supplement agent as claimed in claim 1, mainly including following step
Suddenly：
（1）Obtain former stone：The former stone of medical stone, micarex and montmorillonite；
（2）Crush：By step（1）In former stone to be crushed to grain graininess respectively be less than 300 mesh；
（3）Prepare nanometer original stone powder：By step（2）It is 50 ~ 500nm that the particle that middle crushing is obtained distinguishes high-temperature calcination into granularity
Nanosizing particle；
（4）Mixing nano particle：By step（3）In obtain various nanometers original stone powder make mixing nano particle in proportion；
（5）Soak extraction：By step（4）In nanometer original stone powder is fitted in soaking container, addition soak, in -1000KPa
Soak extraction under the subnormal ambient of ~ -3500KPa, dissolution of minerals element；
（6）Centrifugation：By step（5）In mineral element soak adopt centrifugation, extract supernatant；
（7）Concentrate and be dried：Repeat step（5）And step（6）10-20 time, will be placed in baking oven after the supernatant concentration for obtaining
75 ~ 80 DEG C of dryings, go moisture removal to obtain powder preparation.
Preferably, step（2）Middle employing eccentric vibrating crusher is respectively by the original stone grinding of medical stone, micarex and montmorillonite
Into powder, 300 mesh sieves are then crossed respectively, remove particle of the grain diameter more than 300 mesh, retain grain diameter in 300 ~ 800 mesh
Between particle.
Preferably, step（3）Middle each former stone powder is respectively put in electric arc furnaces is calcined, with the intensification side of 10 DEG C/min
Formula is warming up to 1500 DEG C, calcines 8 h, and cooling after 3 h of insulation obtains nano medical stone powder, nano mica stone powder and nanometer
Montmorillonite powder.
Preferably, the soak adopts electrical conductivity and prepares for the selenium powder of additional 0.1 part of the ultra-pure water of 18.25 M Ω .cm
Form.
Preferably, step（6）The speed of middle centrifugation is 1000 rpm/min, and 3 min are centrifuged.
Preferably, step（7）In add additive in the supernatant that obtains, supernatant is 1 according to weight ratio with additive:
1 proportions；The additive formulations are 1 ~ 2 part of zinc lactate：2 parts of carrotene：1 part of beet：0.5 part of Radix Angelicae Sinensis：Magnesium sulfate
0.2 part, will add water to cook by the load weighted component of above-mentioned formula, remove residue, collecting decoction will be obtained final product.
Preferably, step（7）Middle oven temperature is 75 ~ 80 DEG C.
Preferably, the time of negative pressure soak extraction is 12 ~ 24 h.
Relative to prior art, beneficial effects of the present invention：The present invention is ultrapure by the way that the trace element in ore is dissolved in
In water, and appropriate trace element is with the addition of in ultra-pure water, have selected moderate soak time, by the trace element in ore
Sufficiently be dissolved in water body, additive then with the addition of in lysate, further improve micro element supplement agent into
Point, powdery replenishers are eventually fabricated, rapid and convenient is dissolved when using, supplementary form is various.Additionally, the trace element that this law is provided
The preparation technology of replenishers is very simple, and the cooperative effect between each component is good, cost is relatively low, it is easy to industrialized production, is beneficial to
Promote the use of on a large scale.
Description of the drawings
Fig. 1 is the processing step flow chart of the preparation method of micro element supplement agent.
Specific embodiment
With the following Examples the invention will be further described.
A kind of micro element supplement agent that the present embodiment of embodiment 1 is provided, by weight calculating, by including following raw material group
The material for dividing is extracted and made：3 parts of medical stone, 2.5 parts of micarex, 8 parts of montmorillonite.
Such as Fig. 1, what described micro element supplement agent was prepared as follows, mainly include the following steps that：
（1）Obtain former stone：The former stone of medical stone, micarex and montmorillonite；
（2）Crush：By step（1）In various former stone grind into powder is distinguished using eccentric vibrating crusher, then mistake respectively
300 mesh sieves, remove particle of the grain diameter more than 300 mesh, retain particle of the grain diameter between 300 ~ 800 mesh；
（3）Prepare nanometer original stone powder：By step（2）The various former stone powder that middle crushing is obtained is respectively put in electric arc furnaces to be forged
Burn, with the heating mode of 10 DEG C/min 1500 DEG C are warming up to, calcine 8 h, cool down after 3 h of insulation, respectively obtain granularity for 50 ~
The nano medical stone powder of 500nm, nano mica stone powder and nano montmorillonite powder；
（4）Mixing nano particle：By weight calculating, step is taken（3）In 3 parts of the nanosizing maifanite powder, the nanosizing that obtain
2.5 parts of mica stone powder, 8 parts of nanosizing montmorillonite powder, are mixed uniform；
（5）Soak extraction：Take step（4）The mixing nanometer original stone powder of gained is fitted in soaking container, and adds mixing nanometer
The soak of 2 times of amounts of former stone powder, the soak extraction about 12h under the subnormal ambient of about -1000 KPa makes the ore deposit in former stone powder
Matter-element element is dissolved in soak；
The soak adopts electrical conductivity for the ultra-pure water of 18.25 M Ω .cm；
（6）Centrifugation：By step（5）Middle gained soak is centrifuged 3 min, Ran Houti under conditions of rotating speed is 1000 rpm/min
Take supernatant；
（7）Concentrate and be dried：Repeat step（5）And step（6）10 ~ 20 times, in repeat step（5）When soak extraction, can
Be gradually increased the pressure of negative pressure so as between -1000 KPa of KPa ~ -3500 adjust, the negative pressure impregnation time can 12 ~ 24h it
Between adjustment control；After collecting the supernatant decocting and concentrating obtained by repeatedly extracting, it is placed in baking oven and is dried in 75 ~ 80 DEG C, removes
Moisture, obtains final product mineral matter powder preparation.
A kind of micro element supplement agent that the present embodiment of embodiment 2 is provided, by weight calculating, by including following raw material group
The material for dividing is extracted and made：5 parts of medical stone, 2 parts of micarex, 4 parts of montmorillonite.
The preparation method of the micro element supplement agent of the present embodiment is mainly included the following steps that：
（1）The step of with embodiment 1（1）~ step（3）
（4）Mixing nano particle：By weight calculating, step is taken（3）In 5 parts of the nanosizing maifanite powder, the nanosizing that obtain
2 parts of mica stone powder, 8 parts of nanosizing montmorillonite powder, are mixed uniform；
（5）Soak extraction：Take step（4）The mixing nanometer original stone powder of gained is fitted in soaking container, and adds mixing nanometer
The soak of 3 times of amounts of former stone powder, the soak extraction about 20h under the subnormal ambient of about -2500 KPa makes the ore deposit in former stone powder
Matter-element element is dissolved in soak；
The soak adopts electrical conductivity and is formulated for the selenium powder of additional 0.1 part of the ultra-pure water of 18.25 M Ω .cm；
（6）Centrifugation：By step（5）Middle gained soak is centrifuged 3 min, Ran Houti under conditions of rotating speed is 1000 rpm/min
Take supernatant；
（7）Concentrate and be dried：Repeat step（5）And step（6）10 ~ 20 times；Collect the supernatant obtained by repeatedly extracting, according to
Supernatant weight ratio is 1:1 amount adds additive；After decocting and concentrating, it is placed in baking oven and is dried in 75 ~ 80 DEG C, goes eliminating water
Point, obtain final product mineral matter powder preparation；
Wherein, the formula of additive be 1 ~ 2 part of zinc lactate, 2 parts of carrotene, 1 part of beet, 0.5 part of Radix Angelicae Sinensis, 0.2 part of magnesium sulfate,
To add water to cook by the load weighted component of above-mentioned formula, remove residue, collecting decoction will be obtained final product.
A kind of micro element supplement agent that the present embodiment of embodiment 3 is provided, by weight calculating, by including following raw material group
The material for dividing is extracted and made：20 parts of medical stone, 2.5 parts of micarex, 6 parts of montmorillonite.
The preparation method of the present embodiment, its step is consistent with the step of embodiment 2, and difference is：
The step of the present embodiment（5）The condition of soak extraction is, by the soak of mixing nanometer original 1 times of amount of stone powder, about-
Soak extraction about 20h under the subnormal ambient of 3500 KPa, makes the mineral element in former stone powder be dissolved in soak；
The step of the present embodiment（7）The formula of the additive of middle addition is：Added water to cook by husk, wheat husk, remove residue gained
Additive.
A kind of micro element supplement agent that the present embodiment of embodiment 4 is provided, by weight calculating, by including following raw material group
The material for dividing is extracted and made：8 parts of medical stone, 2 parts of micarex, 10 parts of montmorillonite.
The preparation method of the present embodiment, its step is consistent with the step of embodiment 3, and difference is：
The step of the present embodiment（7）The formula of the additive of middle addition is：Carried by adding water to cook by agriculture waste string
Take, remove additive obtained by residue.
Test example surveys the micro element supplement agent of the gained of 1 ~ embodiment of embodiment 4 by atomic absorption spectrophotometry
It is fixed, as a result can obtain, it is the macroelement that contains in the micro element supplement agent of the gained of 1 ~ embodiment of embodiment 4, micro- and dilute
The species that earth elements are amounted to is more than 38 kinds；Wherein at least includes：K, Na, Ca, Mg, Cu, Mo, Fe, Ti, Sl, Zn, Mn, P, S,
Etc..
The content of K, Na, Ca, Mg, Cu, Mo is more than 3% in 1 ~ embodiment of embodiment 4.
Finally it should be noted that：Preparation process（7）In can according to actual needs be equipped with different types of additive.
Above example is only to illustrate technical scheme, rather than limiting the scope of the invention, although reference is preferably
Embodiment has been made to explain to the present invention, it will be understood by those within the art that, can be to the technology of the present invention
Scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Claims (9)
1. micro element supplement agent, it is characterised in that by weight calculating, system is extracted by the material including following raw material components
Into：3 ~ 20 parts of medical stone, 2 ~ 2.5 parts of micarex, 4 ~ 10 parts of montmorillonite.
2. a kind of method for preparing micro element supplement agent as claimed in claim 1, it is characterised in that mainly including following step
Suddenly：
（1）Obtain former stone：The former stone of medical stone, micarex and montmorillonite；
（2）Crush：By step（1）In former stone to be crushed to grain graininess respectively be less than 300 mesh；
（3）Prepare nanometer original stone powder：By step（2）It is 50 ~ 500nm that the particle that middle crushing is obtained distinguishes high-temperature calcination into granularity
Nanosizing particle；
（4）Mixing nano particle：By step（3）In obtain various nanometers original stone powder make mixing nano particle in proportion；
（5）Soak extraction：By step（4）In nanometer original stone powder is fitted in soaking container, addition soak, in -1000KPa
Soak extraction under the subnormal ambient of ~ -3500KPa, dissolution of minerals element；
（6）Centrifugation：By step（5）In mineral element soak adopt centrifugation, extract supernatant；
（7）Concentrate and be dried：Repeat step（5）And step（6）10-20 time, will be placed in baking oven after the supernatant concentration for obtaining
75 ~ 80 DEG C of dryings, go moisture removal to obtain powder preparation.
3. the preparation method of micro element supplement agent as claimed in claim 2, it is characterised in that step（2）It is middle to adopt eccentric
Vibration crusher by medical stone, micarex and montmorillonite original stone grind into powder, then crosses respectively 300 mesh sieves, removal respectively
Grain particle diameter retains particle of the grain diameter between 300 ~ 800 mesh more than the particle of 300 mesh.
4. the preparation method of micro element supplement agent as claimed in claim 2, it is characterised in that step（3）It is middle by each former stone
Powder is respectively put in electric arc furnaces and calcines, and with the heating mode of 10 DEG C/min 1500 DEG C are warming up to, and 8 h is calcined, after 3 h of insulation
Cooling obtains nano medical stone powder, nano mica stone powder and nano montmorillonite powder.
5. the preparation method of micro element supplement agent as claimed in claim 2, it is characterised in that the soak adopts conductance
Rate is that the selenium powder of additional 0.1 part of the ultra-pure water of 18.25 M Ω .cm is formulated.
6. the preparation method of micro element supplement agent as claimed in claim 2, it is characterised in that step（6）The speed of middle centrifugation
Spend for 1000 rpm/min, 3 min of centrifugation.
7. the preparation method of micro element supplement agent as claimed in claim 2, it is characterised in that step（7）In obtain it is upper
Additive is added in clear liquid, supernatant is 1 according to weight ratio with additive:1 proportions；The additive formulations are lactic acid
1 ~ 2 part of zinc：2 parts of carrotene：1 part of beet：0.5 part of Radix Angelicae Sinensis：0.2 part of magnesium sulfate, will add water by the load weighted component of above-mentioned formula
Decoct, remove residue, collecting decoction is obtained final product.
8. the preparation method of micro element supplement agent as claimed in claim 2, it is characterised in that step（7）Middle oven temperature
For 75 ~ 80 DEG C.
9. the preparation method of micro element supplement agent as claimed in claim 2, it is characterised in that the time of negative pressure soak extraction
For 12 ~ 24 h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611169567.7A CN106619704A (en) | 2016-12-16 | 2016-12-16 | Trace element supplement and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611169567.7A CN106619704A (en) | 2016-12-16 | 2016-12-16 | Trace element supplement and preparation method thereof |
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| CN106619704A true CN106619704A (en) | 2017-05-10 |
Family
ID=58822135
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| CN201611169567.7A Pending CN106619704A (en) | 2016-12-16 | 2016-12-16 | Trace element supplement and preparation method thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1247165A (en) * | 1998-09-10 | 2000-03-15 | 葛筠 | Method for making water-mineralizing medical stone balls |
| WO2007073216A1 (en) * | 2005-12-21 | 2007-06-28 | Kagree Holdings Limited | Bio-processed mineral fertilisers including micro-elements. |
| CN101139128A (en) * | 2006-09-08 | 2008-03-12 | 魏亮 | Medical stone mineralization, degasification activation and galvanomagnetism water preparing method |
| CN101323477A (en) * | 2008-07-25 | 2008-12-17 | 赵文谦 | Preparation of activated immune health preserving water |
| CN101643255A (en) * | 2009-09-07 | 2010-02-10 | 胡建忠 | Micro-electrolysis water-activating material and preparation method thereof |
| CN104787819A (en) * | 2015-03-31 | 2015-07-22 | 宁波方太厨具有限公司 | Method for preparing microelement replenishing agent and replenishing agent prepared by using same |
-
2016
- 2016-12-16 CN CN201611169567.7A patent/CN106619704A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1247165A (en) * | 1998-09-10 | 2000-03-15 | 葛筠 | Method for making water-mineralizing medical stone balls |
| WO2007073216A1 (en) * | 2005-12-21 | 2007-06-28 | Kagree Holdings Limited | Bio-processed mineral fertilisers including micro-elements. |
| CN101139128A (en) * | 2006-09-08 | 2008-03-12 | 魏亮 | Medical stone mineralization, degasification activation and galvanomagnetism water preparing method |
| CN101323477A (en) * | 2008-07-25 | 2008-12-17 | 赵文谦 | Preparation of activated immune health preserving water |
| CN101643255A (en) * | 2009-09-07 | 2010-02-10 | 胡建忠 | Micro-electrolysis water-activating material and preparation method thereof |
| CN104787819A (en) * | 2015-03-31 | 2015-07-22 | 宁波方太厨具有限公司 | Method for preparing microelement replenishing agent and replenishing agent prepared by using same |
Non-Patent Citations (2)
| Title |
|---|
| 张力群，等: "《中国民族民间药物应用大全》", 31 December 2015, 山西出版传媒基团 山西科学技术出版社 * |
| 赖红伟，等: "麦饭石口服液中微量元素测定及其聚类分析", 《安徽农业科学》 * |
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Application publication date: 20170510 |