CN106616172A - Solid beverage and preparation method thereof - Google Patents
Solid beverage and preparation method thereof Download PDFInfo
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- CN106616172A CN106616172A CN201610871220.0A CN201610871220A CN106616172A CN 106616172 A CN106616172 A CN 106616172A CN 201610871220 A CN201610871220 A CN 201610871220A CN 106616172 A CN106616172 A CN 106616172A
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- 239000007787 solid Substances 0.000 title claims abstract description 86
- 235000013361 beverage Nutrition 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 239000000284 extract Substances 0.000 claims abstract description 91
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 51
- 241000037826 Polygonatum kingianum Species 0.000 claims abstract description 47
- 238000003809 water extraction Methods 0.000 claims abstract description 37
- 229940002508 ginger extract Drugs 0.000 claims abstract description 33
- 235000020708 ginger extract Nutrition 0.000 claims abstract description 33
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 29
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 29
- 241001330002 Bambuseae Species 0.000 claims abstract description 29
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 29
- 239000011425 bamboo Substances 0.000 claims abstract description 29
- 239000002994 raw material Substances 0.000 claims abstract description 28
- 238000002156 mixing Methods 0.000 claims abstract description 25
- 239000000843 powder Substances 0.000 claims abstract description 24
- 238000000605 extraction Methods 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims description 99
- 239000007791 liquid phase Substances 0.000 claims description 83
- 238000000889 atomisation Methods 0.000 claims description 42
- 238000001704 evaporation Methods 0.000 claims description 42
- 230000008020 evaporation Effects 0.000 claims description 42
- 238000001035 drying Methods 0.000 claims description 39
- 239000000203 mixture Substances 0.000 claims description 30
- 238000000926 separation method Methods 0.000 claims description 24
- 239000000835 fiber Substances 0.000 claims description 18
- 241000234314 Zingiber Species 0.000 claims description 16
- 235000006886 Zingiber officinale Nutrition 0.000 claims description 16
- 235000008397 ginger Nutrition 0.000 claims description 16
- 239000007790 solid phase Substances 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 14
- 238000004108 freeze drying Methods 0.000 claims description 11
- 108010059892 Cellulase Proteins 0.000 claims description 10
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 10
- 229930006000 Sucrose Natural products 0.000 claims description 10
- 239000001110 calcium chloride Substances 0.000 claims description 10
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 10
- 229940106157 cellulase Drugs 0.000 claims description 10
- 239000012528 membrane Substances 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 10
- 239000005720 sucrose Substances 0.000 claims description 10
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 9
- CSNNHWWHGAXBCP-UHFFFAOYSA-L magnesium sulphate Substances [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 9
- 230000000994 depressogenic effect Effects 0.000 claims description 6
- 238000005096 rolling process Methods 0.000 claims description 6
- 239000012071 phase Substances 0.000 claims 3
- 239000003205 fragrance Substances 0.000 abstract description 11
- 239000000463 material Substances 0.000 abstract description 8
- 210000004072 lung Anatomy 0.000 abstract description 5
- 241000196324 Embryophyta Species 0.000 abstract description 4
- 206010062717 Increased upper airway secretion Diseases 0.000 abstract description 4
- 235000009508 confectionery Nutrition 0.000 abstract description 4
- 208000026435 phlegm Diseases 0.000 abstract description 4
- 150000001413 amino acids Chemical class 0.000 abstract description 2
- 239000008280 blood Substances 0.000 abstract description 2
- 210000004369 blood Anatomy 0.000 abstract description 2
- 210000004556 brain Anatomy 0.000 abstract description 2
- 150000004676 glycans Chemical class 0.000 abstract description 2
- 210000005036 nerve Anatomy 0.000 abstract description 2
- 229920001282 polysaccharide Polymers 0.000 abstract description 2
- 239000005017 polysaccharide Substances 0.000 abstract description 2
- 239000003053 toxin Substances 0.000 abstract description 2
- 231100000765 toxin Toxicity 0.000 abstract description 2
- 239000003963 antioxidant agent Substances 0.000 abstract 1
- 108700012359 toxins Proteins 0.000 abstract 1
- 239000004480 active ingredient Substances 0.000 description 7
- 230000036541 health Effects 0.000 description 7
- 230000008859 change Effects 0.000 description 4
- 235000005911 diet Nutrition 0.000 description 4
- 230000037213 diet Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000003595 mist Substances 0.000 description 4
- 208000013738 Sleep Initiation and Maintenance disease Diseases 0.000 description 3
- 206010047700 Vomiting Diseases 0.000 description 3
- 206010022437 insomnia Diseases 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000008673 vomiting Effects 0.000 description 3
- 206010011224 Cough Diseases 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 208000001431 Psychomotor Agitation Diseases 0.000 description 1
- 206010038743 Restlessness Diseases 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 235000008429 bread Nutrition 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 229940088598 enzyme Drugs 0.000 description 1
- 230000003862 health status Effects 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 206010029410 night sweats Diseases 0.000 description 1
- 230000036565 night sweats Effects 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 230000000505 pernicious effect Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/84—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter using microorganisms or biological material, e.g. enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Microbiology (AREA)
- Molecular Biology (AREA)
- Zoology (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The invention discloses a solid beverage. The solid beverage comprises 100-120 parts by weight of a bamboo stem and leaf extract, 1-7 parts by weight of a ginger extract, and 10-20 parts by weight of a polygonatum kingianum extract. The invention further provides a preparation method of the solid beverage. The preparation method comprises the following steps of performing pretreatment on raw materials, performing cold water extraction, performing hot water extraction, performing concentration, and making powder; and then mixing taken materials in a certain proportion so as to obtain the solid beverage disclosed by the invention. The solid beverage disclosed by the invention has the efficacies of soothing the nerves and the brain, expelling toxins, nourishing the lung, eliminating phlegm, nourishing yin, preventing stroke, and reducing blood viscosity, is rich in bamboo fragrance when being put in mouths, and has sweet mouth feel of being bitter firstly and then sweet; and when active components are extracted, volatile materials in plants, and materials including polysaccharide, amino acids and the like which are easy to dissolve in cold water are extracted with cold water, then antioxidants of bamboo leaves in bamboo stems and leaves are extracted, and an extraction method of firstly using cold water and then using hot water is used, so that the content of effective components in the solid beverage is high, wherein aroma components can be effectively reserved, and the solid beverage has special fragrance of the plants and is good in mouth feel.
Description
Technical field
The present invention relates to food-processing industry, and in particular to a kind of solid beverage and preparation method thereof.
Background technology
Investigated according to authoritative institution, the crowd of health accounts for 10%, and sick crowd accounts for 15%, and majority of populations is in Asia
Health status, such crowd has accounted for 75%.The online investigation of Chinese talent displays that, the white collar in current China's main flow city
Inferior health ratio is up to 76%, and in close the sixty percent of overwork state, " Healthy People " ratio truly is less than 3%.It is existing
In the people of inferior health or a lot, initial performance is exactly easily fatigue, insomnia, forgetful etc., at ordinary times on diet and motion
Also self health care must be learned.Bread is the staff of life, so the diet of health is particularly important, as the saying goes that Diet cures more than the doctors, institute
There can be very big benefit to the body of people with a kind of F&B for having health care concurrently.
Culm leaf clearing heat and eliminating phlegm, relieve restlessness and prevent vomiting, can be used for phlegm-heat cough, insomnia of palpitating with fear, gastropyretic vomiting, pernicious vomiting, tire
Dynamic uneasiness.Sealwort has boosting qi and nourishing yin, invigorating the spleen, moistening lung, kidney benefiting functions.And have a sleepless night, these phenomenons of cough with lung heat are due to will not be right
The life of people produces king-sized impact, therefore Jing is often ignored by people, it is possible to make a kind of using culm leaf and sealwort
Beverage, what is be convenient for people to while playing a role in health care drinks, carries, and good in taste, reaches the effect of integration of drinking and medicinal herbs.
The drink for having been processed using culm leaf and sealwort currently on the market, but due to active ingredient in culm leaf and sealwort
Content is less, therefore health-care effect is not obvious.
The content of the invention
It is an object of the invention to provide a kind of solid beverage and preparation method thereof, efficiently solves people due to life pressure
Power is big or diet is irregular etc. causes insomnia, lung heat, night sweat, the problem that tongue is red and mouth is dry.
To solve above-mentioned technical problem, the invention provides a kind of solid beverage, including culm leaf extract 100-120
Weight portion, ginger extract 1-7 weight portions and P. kingianum extract 10-20 weight portions.
Used as preferred, including culm leaf extract 100-110 weight portions, ginger extract 3-4 weight portions and P. kingianum are carried
Take thing 13-17 weight portions.
Present invention also offers a kind of preparation method of solid beverage, comprises the steps:
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extract A3, concentration A4 and powder processed
A5;
The processing of P. kingianum extract or ginger extract, including pretreatment B1, cold water extraction B2, hot water extract B3, concentration
A4 and powder A5 processed;
Above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are mixed by a certain percentage.
Used as preferred, the pretreatment A1 steps are that fresh culm leaf is carried out brokenly into fibre, i.e., using rolling mill practice by culm
Leaf is depressed into gained bamboo fibre diameter≤5mm, and bamboo fibre is cut into the bamboo silk of 3-4cm, and enzymolysis liquid enzymolysis broken wall is added in Xiang Zhusi,
Obtain solidliquid mixture a1;The pretreatment B1 steps are that P. kingianum or ginger are crushed to after 20-80 mesh, add enzymolysis liquid enzymolysis
Broken wall, obtains solidliquid mixture b1.
Used as preferred, the content of each component is in the enzymolysis liquid:Cellulase volume fraction 1.7-3.2%, pectin
Enzyme volume fraction 0.31-0.57%, sucrose 0.41-0.58mol/L, MgSO423-31mmol/L and CaCl211-23mmol/L;
The enzymolysis liquid of 40-60ml is added in pretreatment A1 steps in every gram of bamboo silk, at 18-25 degree Celsius 15-24 hours are digested;Pretreatment
The enzymolysis liquid of 5-10ml is added in every gram of raw material of B1 steps, at 18-25 degree Celsius 13-18 hours are digested.
As preferred, the cold water extraction A2 step be by solidliquid mixture a1 and 20-30 degree Celsius of cold water according to
Solid-liquid mass ratio 1:50-100 mixing Posterior circle is extracted 3-10 time, and 1-10 hours are extracted in circulation altogether, and circulation is carried out after the completion of extracting
Separation of solid and liquid obtains liquid phase part a2 and solid fraction a2;The cold water extraction B2 step is by solidliquid mixture b1 and 20-30
Degree Celsius cold water according to solid-liquid mass ratio 1:10-20 mixing Posterior circle is extracted 2-8 time, and 0.5-8 hours, circulation are extracted in circulation altogether
Separation of solid and liquid is carried out after the completion of extraction and obtains liquid phase part b2 and solid fraction b2.
Used as preferred, it is according to solid-liquid mass ratio 1 that the hot water extracts A3 steps:20-80 adds in solid phase components a2
Extraction 2-5 time is circulated after the hot water mixing for entering 60-80 degree Celsius, 0.1-5h is extracted in circulation altogether, and circulation extraction completes laggard
Row separation of solid and liquid obtains liquid phase part a3 and solid fraction a3;It is according to solid-liquid mass ratio 1 that the hot water extracts B3 steps:10-
Extraction 2-4 time is circulated after the hot water mixing that 60-80 degree Celsius is added in 18 to solid phase components b2,0.1- is extracted in circulation altogether
4h, circulation carries out separation of solid and liquid and obtains liquid phase part b3 and solid fraction b3 after the completion of extracting.
Used as preferred, the concentration A4 steps are:
Film concentration is carried out to liquid phase part a2 or liquid phase part b2, film concentration is less than 0.01 micron with membrane aperture is separated, point
Do not obtain a4 or b4;
Negative pressure evaporation concentration is carried out to liquid phase part a3 or liquid phase part b3, negative pressure evaporation is concentrated first by liquid phase part a3
Or the pressure of liquid phase part b3 is maintained at vacuum 0.01-0.05MPa 20-60 minutes, is then depressured, pressure is kept in 0.05-
0.1MPa to liquid volume reduces 10-20 times, and wherein negative pressure evaporation concentration overall process liquid keeps less than 80 degrees Celsius.
Used as preferred, the powder A5 steps processed are:
Liquid phase part a2 or liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be that 20-80Pa, temperature are little
Freeze under -40 degrees celsius, then in -15 degrees Celsius to -28 degrees Celsius lyophilizations, finally under 35-45 degree Celsius
Parsing-desiccation to moisture content is less than 10%;
Liquid phase part a3 or liquid phase part b3 carry out that atomization drying is carried out after negative pressure evaporation concentration to moisture content less than 10%,
Atomization drying temperature is 53-60 degree Celsius, and atomizing pressure is 2000-3300KPa;.
As preferred, the lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, obtain culm
Leaf extract;The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;Will
The lyophilized products obtained as raw material with ginger and atomization drying product mix, and obtain ginger extract.
Compared with prior art, beneficial effects of the present invention are at least one of following:
1) solid beverage of the present invention removes culm leaf and the extraction beyond the region of objective existence of sealwort is also added with ginger extract, and ginger can add straightforward man
Body metabolism, degrading the channel, can promote the performance of active ingredient effect in culm leaf and sealwort, and can neutralize culm leaf
" cold ", the present invention has functions that to calm the nerves most brain, toxin expelling, moistening lung eliminating the phlegm, enriching yin, prevention of stroke and reduces blood viscosity, and enters
Mouth bamboo is aromatic strongly fragrant, and with bitter first ,sweet later sweet mouthfeel is returned.
2) solid beverage of the present invention selects the extract of culm leaf, P. kingianum and ginger to prepare, compared to directly with culm leaf,
P. kingianum and ginger is brewed or other processing methods for, active constituent content therein is higher, therefore health-care effect is also more preferable.
3) when the present invention extracts active component in culm leaf, P. kingianum and ginger, for the first time using cold water extraction, plant is extracted
Volatile materials in thing and it is soluble in the materials such as polysaccharide, the amino acid of cold water;For cold water extract adopts film concentration technique,
Volatile materials can at utmost be retained.Second hot water is extracted, can effectively extract be not readily dissolved in cold water, boiling point it is higher
Active ingredient, such as the saponin in tabasheer ketone, sealwort or sealwort composition in culm leaf, because hot water extract's matter is difficult to wave
Send out, can be concentrated using negative pressure evaporation technology, can be with reduces cost compared to film concentration.The extracting method of first cold water hot water again
So that the active constituent content in solid beverage of the present invention is higher, fragrance component therein can be effectively retained, special with plant
Some fragrance, mouthfeel is fabulous.
3) during extracts active ingredients of the present invention, cell membrane is destroyed with enzymolysis liquid first so that active ingredient therein is more held
Easily it is extracted, improves the extraction efficiency of active ingredient.
4) existing extracting method is compared, the recovery rate of the present invention can improve 10% or so.
Specific embodiment
In order that the objects, technical solutions and advantages of the present invention become more apparent, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that specific embodiment described herein is not used to only to explain the present invention
Limit the present invention.
Embodiment 1:
Present embodiments provide a kind of solid beverage, including the weight portion of culm leaf extract 90, the weight portion of ginger extract 7 and
The weight portion of P. kingianum extract 20.
Embodiment 2:
Present embodiments provide a kind of solid beverage, including the weight portion of culm leaf extract 120, the weight portion of ginger extract 1
With the weight portion of P. kingianum extract 10.
Embodiment 3:
Present embodiments provide a kind of solid beverage, including the weight portion of culm leaf extract 105, the weight portion of ginger extract 4
With the weight portion of P. kingianum extract 15.
Embodiment 4:
Present embodiments provide a kind of solid beverage, including the weight portion of culm leaf extract 100, the weight portion of ginger extract 5
With the weight portion of P. kingianum extract 17.
Embodiment 5:
Present embodiments provide a kind of solid beverage, including the weight portion of culm leaf extract 110, the weight portion of ginger extract 3
With the weight portion of P. kingianum extract 13.
The species solid beverage of comparing embodiment 1 to embodiment 5, according in the solid beverage that the formula of embodiment 3 is obtained
The fragrance of various extracts can preferably coordinate, and reach optimal mouthfeel.
Embodiment 6:
Present embodiments provide a kind of preparation method of solid beverage, including the processing of culm leaf extract, P. kingianum are carried
The processing of thing and the processing of ginger extract are taken, above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are pressed
Certain proportion mixes, and obtains solid beverage of the present invention.
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extraction A3, concentration A4 and powder A5 processed:
Pretreatment A1, by fresh culm leaf fibre is carried out brokenly, i.e., culm leaf is depressed into gained bamboo fibre diameter using rolling mill practice
≤ 5mm, by bamboo fibre the bamboo silk of 3-4cm is cut to, and the enzymolysis liquid of 60ml is added in every gram of bamboo silk, little in 25 degrees Celsius of enzymolysis 24
When, broken wall is digested, obtain solidliquid mixture a1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction
3.2%th, pectase volume fraction 0.57%, sucrose 0.58mol/L, MgSO431mmol/L and CaCl223mmol/L;
Cold water extraction A2, by solidliquid mixture a1 and 20 degrees Celsius of cold water according to solid-liquid mass ratio 1:Follow after 100 mixing
Ring is extracted 10 times, and circulation altogether is extracted 10 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part a2 and solid phase portion after the completion of extracting
Divide a2;
Hot water extracts A3, according to solid-liquid mass ratio 1:Add 80 degrees Celsius of hot water mixing laggard in 80 to solid phase components a2
Row circulation is extracted 5 times, and 5h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part a3 and solid fraction after the completion of extracting
a3;
Concentration A4, film concentration is carried out to liquid phase part a2, and film concentration is less than 0.01 micron, obtains a4 with membrane aperture is separated;
Negative pressure evaporation concentration is carried out to liquid phase part a3, the pressure of liquid phase part a3 is maintained at vacuum by negative pressure evaporation concentration first
0.05MPa 60 minutes, is then depressured, and keeps pressure to reduce 20 times in 0.1MPa to liquid volume, and wherein negative pressure evaporation concentration is complete
Process liquids keep 80 degrees Celsius;
Powder A5 processed, the liquid phase part a2 after film is concentrated is freezed, it is lyophilized be in vacuum be 80Pa, -40 degrees Celsius of temperature
Under the conditions of freeze, then in -28 degrees Celsius of lyophilizations, finally in 45 degrees Celsius of lower parsing-desiccations to moisture content 10%;Liquid phase
Part a3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 60 degrees Celsius, atomization
Pressure is 2000KPa;
The lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, culm leaf extract is obtained.
The processing of P. kingianum extract or ginger extract, including pretreatment B1, cold water extraction B2, hot water extraction B3, concentration
A4 and powder A5 processed:
Pretreatment B1, P. kingianum or ginger are crushed to after 20 mesh, and the enzymolysis liquid of 5ml is added in every gram of raw material, Celsius 18
Degree enzymolysis 13 hours, obtains solidliquid mixture b1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction
1.7%, pectase volume fraction 0.31%, sucrose 0.41mol/L, MgSO423mmol/L and CaCl211mmol/L;
Cold water extraction B2, by solidliquid mixture b1 and 20 degrees Celsius of cold water according to solid-liquid mass ratio 1:10 mixing Posterior circles
Extract 2 times, circulation altogether is extracted 0.5 hour, and circulation carries out separation of solid and liquid and obtains liquid phase part b2 and solid fraction after the completion of extracting
b2;
Hot water extracts B3, according to solid-liquid mass ratio 1:Add 60 degrees Celsius of hot water mixing laggard in 10 to solid phase components b2
Row circulation is extracted 2 times, and 0.1h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part b3 and solid phase portion after the completion of extracting
Divide b3;
Concentration A4, film concentration is carried out to liquid phase part b2, and film concentration is less than 0.01 micron, obtains b4 with membrane aperture is separated;
Negative pressure evaporation concentration is carried out to liquid phase part b3, the pressure of liquid phase part b3 is maintained at vacuum by negative pressure evaporation concentration first
0.05MPa 20 minutes, is then depressured, and keeps pressure to reduce 10 times in 0.1MPa to liquid volume, and wherein negative pressure evaporation concentration is complete
Process liquids keep 80 degrees Celsius;
Powder A5 processed, the liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be 20Pa, -40 degrees Celsius of temperature
Under the conditions of freeze, then in -15 degrees Celsius of lyophilizations, finally in 35 degrees Celsius of lower parsing-desiccations to moisture content 10%;To liquid
Phase part b3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 53 degrees Celsius, mist
Change pressure is 2000KPa;
The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;Will
The lyophilized products obtained as raw material with ginger and atomization drying product mix, and obtain ginger extract.
Embodiment 7:
Present embodiments provide a kind of preparation method of solid beverage, including the processing of culm leaf extract, P. kingianum are carried
The processing of thing and the processing of ginger extract are taken, above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are pressed
Certain proportion mixes, and obtains solid beverage of the present invention.
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extraction A3, concentration A4 and powder A5 processed:
Pretreatment A1, by fresh culm leaf fibre is carried out brokenly, i.e., culm leaf is depressed into gained bamboo fibre diameter using rolling mill practice
≤ 5mm, by bamboo fibre the bamboo silk of 3-4cm is cut to, and the enzymolysis liquid of 40ml is added in every gram of bamboo silk, little in 18 degrees Celsius of enzymolysis 15
When, broken wall is digested, obtain solidliquid mixture a1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction
1.7%th, pectase volume fraction 0.31%, sucrose 0.41mol/L, MgSO423mmol/L and CaCl211mmol/L;
Cold water extraction A2, by solidliquid mixture a1 and 30 degrees Celsius of cold water according to solid-liquid mass ratio 1:50 mixing Posterior circles
Extract 3 times, circulation altogether is extracted 1 hour, and circulation carries out separation of solid and liquid and obtains liquid phase part a2 and solid fraction a2 after the completion of extracting;
Hot water extracts A3, according to solid-liquid mass ratio 1:Add 60 degrees Celsius of hot water mixing laggard in 20 to solid phase components a2
Row circulation is extracted 2 times, and 0.1h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part a3 and solid phase portion after the completion of extracting
Divide a3;
Concentration A4, film concentration is carried out to liquid phase part a2, and film concentration is less than 0.01 micron, obtains a4 with membrane aperture is separated;
Negative pressure evaporation concentration is carried out to liquid phase part a3, the pressure of liquid phase part a3 is maintained at vacuum by negative pressure evaporation concentration first
0.01MPa 20 minutes, is then depressured, and keeps pressure to reduce 10 times in 0.05MPa to liquid volume, wherein negative pressure evaporation concentration
Overall process liquid keeps 70 degrees Celsius;
Powder A5 processed, the liquid phase part a2 after film is concentrated is freezed, it is lyophilized be in vacuum be 20Pa, -30 degrees Celsius of temperature
Under the conditions of freeze, then in -15 degrees Celsius of lyophilizations, finally 35 degrees Celsius of lower parsing-desiccations to moisture content be less than 10%;
Liquid phase part a3 carries out that atomization drying is carried out after negative pressure evaporation concentration to moisture content less than 10%, and atomization drying temperature is 53 Celsius
Degree, atomizing pressure is 3300KPa;
The lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, culm leaf extract is obtained.
The processing of P. kingianum extract or ginger extract, including pretreatment B1, cold water extraction B2, hot water extraction B3, concentration
A4 and powder A5 processed:
Powder A5 processed, the liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be 20Pa, -40 degrees Celsius of temperature
Under the conditions of freeze, then in -15 degrees Celsius of lyophilizations, finally in 35 degrees Celsius of lower parsing-desiccations to moisture content 10%;To liquid
Phase part b3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 53 degrees Celsius, mist
Change pressure is 2000KPa;
Pretreatment B1, P. kingianum or ginger are crushed to after 80 mesh, and the enzymolysis liquid of 10ml is added in every gram of raw material, Celsius 25
Degree enzymolysis 18 hours, obtains solidliquid mixture b1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction
3.2%, pectase volume fraction 0.57%, sucrose 0.58mol/L, MgSO431mmol/L and CaCl223mmol/L;
Cold water extraction B2, by solidliquid mixture b1 and 30 degrees Celsius of cold water according to solid-liquid mass ratio 1:Follow after 20 mixing
Ring is extracted 8 times, and circulation altogether is extracted 8 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part b2 and solid fraction after the completion of extracting
b2;
Hot water extracts B3, according to solid-liquid mass ratio 1:Add 80 degrees Celsius of hot water mixing laggard in 18 to solid phase components b2
Row circulation is extracted 4 times, and 4h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part b3 and solid fraction after the completion of extracting
b3;
Concentration A4, film concentration is carried out to liquid phase part b2, and film concentration is less than 0.01 micron, obtains b4 with membrane aperture is separated;
Negative pressure evaporation concentration is carried out to liquid phase part b3, the pressure of liquid phase part b3 is maintained at vacuum by negative pressure evaporation concentration first
0.01MPa 60 minutes, is then depressured, and keeps pressure to reduce 20 times in 0.05MPa to liquid volume, wherein negative pressure evaporation concentration
Overall process liquid keeps 80 degrees Celsius;
Powder A5 processed, the liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be 80Pa, -40 degrees Celsius of temperature
Under the conditions of freeze, then in -28 degrees Celsius of lyophilizations, finally 45 degrees Celsius of lower parsing-desiccations to moisture content be less than 10%;
Carry out being carried out after negative pressure evaporation concentration atomization drying to liquid phase part b3 to moisture content 10%, atomization drying temperature is 60 Celsius
Degree, atomizing pressure is 3300KPa;
The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;Will
The lyophilized products obtained as raw material with ginger and atomization drying product mix, and obtain ginger extract.
Embodiment 8:
Present embodiments provide a kind of preparation method of solid beverage, including the processing of culm leaf extract, P. kingianum are carried
The processing of thing and the processing of ginger extract are taken, above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are pressed
Certain proportion mixes, and obtains solid beverage of the present invention.
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extraction A3, concentration A4 and powder A5 processed:
Pretreatment A1, by fresh culm leaf fibre is carried out brokenly, i.e., culm leaf is depressed into gained bamboo fibre diameter using rolling mill practice
≤ 5mm, by bamboo fibre the bamboo silk of 3-4cm is cut to, and the enzymolysis liquid of 50ml is added in every gram of bamboo silk, little in 23 degrees Celsius of enzymolysis 19
When, broken wall is digested, obtain solidliquid mixture a1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction
2.4%th, pectase volume fraction 0.42%, sucrose 0.51mol/L, MgSO429mmol/L and CaCl218mmol/L;
Cold water extraction A2, by solidliquid mixture a1 and 25 degrees Celsius of cold water according to solid-liquid mass ratio 1:60 mixing Posterior circles
Extract 5 times, circulation altogether is extracted 4 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part a2 and solid fraction a2 after the completion of extracting;
Hot water extracts A3, according to solid-liquid mass ratio 1:Add 70 degrees Celsius of hot water mixing laggard in 30 to solid phase components a2
Row circulation is extracted 3 times, and 2h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part a3 and solid fraction after the completion of extracting
a3;
Concentration A4, film concentration is carried out to liquid phase part a2, and film concentration is less than 0.01 micron, obtains a4 with membrane aperture is separated;
Negative pressure evaporation concentration is carried out to liquid phase part a3, the pressure of liquid phase part a3 is maintained at vacuum by negative pressure evaporation concentration first
0.04MPa 45 minutes, is then depressured, and keeps pressure to reduce 15 times in 0.08MPa to liquid volume, wherein negative pressure evaporation concentration
Overall process liquid keeps 80 degrees Celsius;
Powder A5 processed, the liquid phase part a2 after film is concentrated is freezed, it is lyophilized be in vacuum be 60Pa, temperature 6-40 degree Celsius
Under the conditions of freeze, then in -22 degrees Celsius of lyophilizations, finally in 40 degrees Celsius of lower parsing-desiccations to moisture content 10%;Liquid phase
Part a3 carries out that atomization drying is carried out after negative pressure evaporation concentration to moisture content less than 10%, and atomization drying temperature is 57 degrees Celsius,
Atomizing pressure is 2700KPa;
The lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, culm leaf extract is obtained.
The processing of P. kingianum extract or ginger extract, including pretreatment B1, cold water extraction B2, hot water extraction B3, concentration
A4 and powder A5 processed:
Pretreatment B1, P. kingianum or ginger are crushed to after 60 mesh, and the enzymolysis liquid of 7ml is added in every gram of raw material, Celsius 22
Degree enzymolysis 26 hours, obtains solidliquid mixture b1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction
2.3%, pectase volume fraction 0.4.6%, sucrose 0.5.2mol/L, MgSO427mmol/L and CaCl217mmol/L;
Cold water extraction B2, by solidliquid mixture b1 and 25 degrees Celsius of cold water according to solid-liquid mass ratio 1:15 mixing Posterior circles
Extract 4 times, circulation altogether is extracted 3 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part b2 and solid fraction b2 after the completion of extracting;
Hot water extracts B3, according to solid-liquid mass ratio 1:Add 70 degrees Celsius of hot water mixing laggard in 14 to solid phase components b2
Row circulation is extracted 3 times, and 1h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part b3 and solid fraction after the completion of extracting
b3;
Concentration A4, film concentration is carried out to liquid phase part b2, and film concentration is less than 0.01 micron, obtains b4 with membrane aperture is separated;
Negative pressure evaporation concentration is carried out to liquid phase part b3, the pressure of liquid phase part b3 is maintained at vacuum by negative pressure evaporation concentration first
0.03MPa 36 minutes, is then depressured, and keeps pressure to reduce 13 times in 0.07MPa to liquid volume, wherein negative pressure evaporation concentration
Overall process liquid keeps 80 degrees Celsius;
Powder A5 processed, the liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be 50Pa, -40 degrees Celsius of temperature
Under the conditions of freeze, then in -22 degrees Celsius of lyophilizations, finally in 37 degrees Celsius of lower parsing-desiccations to moisture content 10%;To liquid
Phase part b3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 59 degrees Celsius, mist
Change pressure is 25600KPa;
The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;Will
The lyophilized products obtained as raw material with ginger and atomization drying product mix, and obtain ginger extract.
Embodiment 9:
Present embodiments provide a kind of preparation method of solid beverage, including the processing of culm leaf extract, P. kingianum are carried
The processing of thing and the processing of ginger extract are taken, above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are pressed
Certain proportion mixes, and obtains solid beverage of the present invention.
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extraction A3, concentration A4 and powder A5 processed:
Pretreatment A1, by fresh culm leaf fibre is carried out brokenly, i.e., culm leaf is depressed into gained bamboo fibre diameter using rolling mill practice
≤ 5mm, by bamboo fibre the bamboo silk of 3-4cm is cut to, and the enzymolysis liquid of 60ml is added in every gram of bamboo silk, little in 25 degrees Celsius of enzymolysis 24
When, broken wall is digested, obtain solidliquid mixture a1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction
3.2%th, pectase volume fraction 0.57%, sucrose 0.58mol/L, MgSO431mmol/L and CaCl223mmol/L;
Cold water extraction A2, by solidliquid mixture a1 and 20 degrees Celsius of cold water according to solid-liquid mass ratio 1:60 mixing Posterior circles
Extract 5 times, circulation altogether is extracted 6 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part a2 and solid fraction a2 after the completion of extracting;
Hot water extracts A3, according to solid-liquid mass ratio 1:Add 80 degrees Celsius of hot water mixing laggard in 80 to solid phase components a2
Row circulation is extracted 3 times, and 2h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part a3 and solid fraction after the completion of extracting
a3;
Concentration A4, film concentration is carried out to liquid phase part a2, and film concentration is less than 0.01 micron, obtains a4 with membrane aperture is separated;
Negative pressure evaporation concentration is carried out to liquid phase part a3, the pressure of liquid phase part a3 is maintained at vacuum by negative pressure evaporation concentration first
0.05MPa 60 minutes, is then depressured, and keeps pressure to reduce 20 times in 0.1MPa to liquid volume, and wherein negative pressure evaporation concentration is complete
Process liquids keep 80 degrees Celsius;
Powder A5 processed, the liquid phase part a2 after film is concentrated is freezed, it is lyophilized be in vacuum be 80Pa, -40 degrees Celsius of temperature
Under the conditions of freeze, then in -28 degrees Celsius of lyophilizations, finally in 45 degrees Celsius of lower parsing-desiccations to moisture content 10%;Liquid phase
Part a3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 60 degrees Celsius, atomization
Pressure is 2000KPa;
The lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, culm leaf extract is obtained.
The processing of P. kingianum extract or ginger extract, including pretreatment B1, cold water extraction B2, hot water extraction B3, concentration
A4 and powder A5 processed:
Pretreatment B1, P. kingianum or ginger are crushed to after 80 mesh, and the enzymolysis liquid of 10ml is added in every gram of raw material, Celsius 25
Degree enzymolysis 18 hours, obtains solidliquid mixture b1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction
1.7%, pectase volume fraction 0.31%, sucrose 0.41mol/L, MgSO 23mmol/L and CaCl211mmol/L;
Cold water extraction B2, by solidliquid mixture b1 and 20 degrees Celsius of cold water according to solid-liquid mass ratio 1:10 mixing Posterior circles
Extract 4 times, circulation altogether is extracted 5 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part b2 and solid fraction b2 after the completion of extracting;
Hot water extracts B3, according to solid-liquid mass ratio 1:Add 60 degrees Celsius of hot water mixing laggard in 10 to solid phase components b2
Row circulation is extracted 2 times, and 1h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part b3 and solid fraction after the completion of extracting
b3;
Concentration A4, film concentration is carried out to liquid phase part b2, and film concentration is less than 0.01 micron, obtains b4 with membrane aperture is separated;
Negative pressure evaporation concentration is carried out to liquid phase part b3, the pressure of liquid phase part b3 is maintained at vacuum by negative pressure evaporation concentration first
0.05MPa 20 minutes, is then depressured, and keeps pressure to reduce 10 times in 0.1MPa to liquid volume, and wherein negative pressure evaporation concentration is complete
Process liquids keep 80 degrees Celsius;
Powder A5 processed, the liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be 20Pa, -40 degrees Celsius of temperature
Under the conditions of freeze, then in -15 degrees Celsius of lyophilizations, finally in 35 degrees Celsius of lower parsing-desiccations to moisture content 10%;To liquid
Phase part b3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 53 degrees Celsius, mist
Change pressure is 2000KPa;
The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;Will
The lyophilized products obtained as raw material with ginger and atomization drying product mix, and obtain ginger extract.
The situation of the extract that the extracting method of active ingredient is obtained is shown in the raw material according to embodiment 6 to embodiment 9
Following table, wherein recovery rate are the percentage that extraction of substance accounts for raw material weight, and the deep or light of fragrance is according to four realities by same raw material
The fragrance for applying the extract that the Different Extraction Method in example is obtained is compared, and two denseer as " dense ", fragrance of fragrance are thin
Two be " light ".
It is slightly better on extract and fragrance from above table as can be seen that embodiment 9 compares other embodiment.
Because cold water extraction temperature is relatively low, therefore wherein volatile material retains more, and aroma substance half is easier to volatilization, therefore
The denseer material that can illustrate that cold water extraction goes out of fragrance retains more.
Although reference be made herein to invention has been described for multiple explanatory embodiments of the invention, however, it is to be understood that
Those skilled in the art can be designed that a lot of other modification and embodiment, and these modifications and embodiment will fall in this Shen
Please be within disclosed spirit and spirit.More specifically, in the range of disclosure and claim, can be to master
The building block and/or layout of topic composite configuration carries out various modifications and improvement.Except what is carried out to building block and/or layout
Deformation and improvement are outer, and to those skilled in the art, other purposes also will be apparent.
Claims (10)
1. a kind of solid beverage, it is characterised in that including culm leaf extract 90-120 weight portions, ginger extract 1-7 weight portions
With P. kingianum extract 10-20 weight portions.
2. solid beverage according to claim 1, it is characterised in that including culm leaf extract 100-110 weight portions, ginger
Extract 3-4 weight portions and P. kingianum extract 13-17 weight portions.
3. the preparation method of solid beverage described in a kind of claim 1, it is characterised in that comprise the steps:
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extract A3, concentration A4 and powder A5 processed;
The processing of P. kingianum extract or ginger extract, including, pretreatment B1, cold water extraction B2, hot water extract B3, concentration A4 and
Powder A5 processed;
Above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are mixed by a certain percentage.
4. the preparation method of solid beverage according to claim 3, it is characterised in that
The pretreatment A1 steps are that fresh culm leaf is carried out brokenly into fibre, i.e., culm leaf is depressed into gained bamboo fibre using rolling mill practice
Diameter≤5mm, by bamboo fibre the bamboo silk of 3-4cm is cut to, and enzymolysis liquid enzymolysis broken wall is added in Xiang Zhusi, obtains solidliquid mixture
a1;
The pretreatment B1 steps are that P. kingianum or ginger are crushed to after 20-80 mesh, add enzymolysis liquid enzymolysis broken wall, obtain solid-liquid
Mixture b1.
5. the preparation method of solid beverage according to claim 4, it is characterised in that
The content of each component is in the enzymolysis liquid:Cellulase volume fraction 1.7-3.2%, pectase volume fraction 0.31-
0.57%, sucrose 0.41-0.58mol/L, MgSO423-31mmol/L and CaCl211-23mmol/L;In pretreatment A1 steps
The enzymolysis liquid of 40-60ml is added in every gram of bamboo silk, at 18-25 degree Celsius 15-24 hours are digested;Pretreatment B1 every gram of raw material of step
The enzymolysis liquid of middle addition 5-10ml, at 18-25 degree Celsius 13-18 hours are digested.
6. the preparation method of solid beverage according to claim 4, it is characterised in that
The cold water extraction A2 step is according to solid-liquid mass ratio 1 by solidliquid mixture a1 and 20-30 degree Celsius of cold water:50-
100 mixing Posterior circles are extracted 3-10 time, and 1-10 hours are extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase after the completion of extracting
Part a2 and solid fraction a2;
The cold water extraction B2 step is according to solid-liquid mass ratio 1 by solidliquid mixture b1 and 20-30 degree Celsius of cold water:10-
20 mixing Posterior circles are extracted 2-8 time, and 0.5-8 hours are extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase after the completion of extracting
Part b2 and solid fraction b2.
7. the preparation method of solid beverage according to claim 6, it is characterised in that
It is according to solid-liquid mass ratio 1 that the hot water extracts A3 steps:20-80 adds 60-80 degree Celsius in solid phase components a2
Extraction 2-5 time is circulated after hot water mixing, 0.1-5h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid after the completion of extracting
Phase part a3 and solid fraction a3;
It is according to solid-liquid mass ratio 1 that the hot water extracts B3 steps:10-18 adds 60-80 degree Celsius in solid phase components b2
Extraction 2-4 time is circulated after hot water mixing, 0.1-4h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid after the completion of extracting
Phase part b3 and solid fraction b3.
8. the preparation method of solid beverage according to claim 6, it is characterised in that the concentration A4 steps are:
Film concentration is carried out to liquid phase part a2 or liquid phase part b2, film concentration is less than 0.01 micron with membrane aperture is separated, respectively
To a4 or b4;
Negative pressure evaporation concentration is carried out to liquid phase part a3 or liquid phase part b3, negative pressure evaporation is concentrated first by liquid phase part a3 or liquid
The pressure of phase part b3 is maintained at vacuum 0.01-0.05MPa 20-60 minutes, is then depressured, and keeps pressure in 0.05-
0.1MPa to liquid volume reduces 10-20 times, and wherein negative pressure evaporation concentration overall process liquid keeps less than 80 degrees Celsius.
9. the preparation method of solid beverage according to claim 7, it is characterised in that the powder A5 steps processed are:
Liquid phase part a2 or liquid phase part b2 after film is concentrated is freezed, it is lyophilized be vacuum be 20-80Pa, temperature less than-
Freeze under 40 degrees celsius, then in -15 degrees Celsius to -28 degrees Celsius lyophilizations, finally parse under 35-45 degree Celsius
It is dried to moisture content and is less than 10%;
Liquid phase part a3 or liquid phase part b3 carry out that atomization drying is carried out after negative pressure evaporation concentration to moisture content less than 10%, atomization
Baking temperature is 53-60 degree Celsius, and atomizing pressure is 2000-3300KPa.
10. the preparation method of solid beverage according to claim 8 or claim 9, it is characterised in that
The lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, culm leaf extract is obtained;
The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;
The lyophilized products obtained as raw material with ginger and atomization drying product are mixed, ginger extract is obtained.
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CN1799429A (en) * | 2005-09-02 | 2006-07-12 | 廖农林 | Beverage with bamboo and siberian solomoseal rhizome its preparation method |
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