CN106616172A - Solid beverage and preparation method thereof - Google Patents

Solid beverage and preparation method thereof Download PDF

Info

Publication number
CN106616172A
CN106616172A CN201610871220.0A CN201610871220A CN106616172A CN 106616172 A CN106616172 A CN 106616172A CN 201610871220 A CN201610871220 A CN 201610871220A CN 106616172 A CN106616172 A CN 106616172A
Authority
CN
China
Prior art keywords
liquid
solid
extract
phase part
solid beverage
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610871220.0A
Other languages
Chinese (zh)
Inventor
潘鸿飞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yunnan Le Zhizhu Biological Technology Co Ltd
Original Assignee
Yunnan Le Zhizhu Biological Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yunnan Le Zhizhu Biological Technology Co Ltd filed Critical Yunnan Le Zhizhu Biological Technology Co Ltd
Priority to CN201610871220.0A priority Critical patent/CN106616172A/en
Publication of CN106616172A publication Critical patent/CN106616172A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/385Concentrates of non-alcoholic beverages
    • A23L2/39Dry compositions
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/84Clarifying or fining of non-alcoholic beverages; Removing unwanted matter using microorganisms or biological material, e.g. enzymes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Zoology (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The invention discloses a solid beverage. The solid beverage comprises 100-120 parts by weight of a bamboo stem and leaf extract, 1-7 parts by weight of a ginger extract, and 10-20 parts by weight of a polygonatum kingianum extract. The invention further provides a preparation method of the solid beverage. The preparation method comprises the following steps of performing pretreatment on raw materials, performing cold water extraction, performing hot water extraction, performing concentration, and making powder; and then mixing taken materials in a certain proportion so as to obtain the solid beverage disclosed by the invention. The solid beverage disclosed by the invention has the efficacies of soothing the nerves and the brain, expelling toxins, nourishing the lung, eliminating phlegm, nourishing yin, preventing stroke, and reducing blood viscosity, is rich in bamboo fragrance when being put in mouths, and has sweet mouth feel of being bitter firstly and then sweet; and when active components are extracted, volatile materials in plants, and materials including polysaccharide, amino acids and the like which are easy to dissolve in cold water are extracted with cold water, then antioxidants of bamboo leaves in bamboo stems and leaves are extracted, and an extraction method of firstly using cold water and then using hot water is used, so that the content of effective components in the solid beverage is high, wherein aroma components can be effectively reserved, and the solid beverage has special fragrance of the plants and is good in mouth feel.

Description

A kind of solid beverage and preparation method thereof
Technical field
The present invention relates to food-processing industry, and in particular to a kind of solid beverage and preparation method thereof.
Background technology
Investigated according to authoritative institution, the crowd of health accounts for 10%, and sick crowd accounts for 15%, and majority of populations is in Asia Health status, such crowd has accounted for 75%.The online investigation of Chinese talent displays that, the white collar in current China's main flow city Inferior health ratio is up to 76%, and in close the sixty percent of overwork state, " Healthy People " ratio truly is less than 3%.It is existing In the people of inferior health or a lot, initial performance is exactly easily fatigue, insomnia, forgetful etc., at ordinary times on diet and motion Also self health care must be learned.Bread is the staff of life, so the diet of health is particularly important, as the saying goes that Diet cures more than the doctors, institute There can be very big benefit to the body of people with a kind of F&B for having health care concurrently.
Culm leaf clearing heat and eliminating phlegm, relieve restlessness and prevent vomiting, can be used for phlegm-heat cough, insomnia of palpitating with fear, gastropyretic vomiting, pernicious vomiting, tire Dynamic uneasiness.Sealwort has boosting qi and nourishing yin, invigorating the spleen, moistening lung, kidney benefiting functions.And have a sleepless night, these phenomenons of cough with lung heat are due to will not be right The life of people produces king-sized impact, therefore Jing is often ignored by people, it is possible to make a kind of using culm leaf and sealwort Beverage, what is be convenient for people to while playing a role in health care drinks, carries, and good in taste, reaches the effect of integration of drinking and medicinal herbs. The drink for having been processed using culm leaf and sealwort currently on the market, but due to active ingredient in culm leaf and sealwort Content is less, therefore health-care effect is not obvious.
The content of the invention
It is an object of the invention to provide a kind of solid beverage and preparation method thereof, efficiently solves people due to life pressure Power is big or diet is irregular etc. causes insomnia, lung heat, night sweat, the problem that tongue is red and mouth is dry.
To solve above-mentioned technical problem, the invention provides a kind of solid beverage, including culm leaf extract 100-120 Weight portion, ginger extract 1-7 weight portions and P. kingianum extract 10-20 weight portions.
Used as preferred, including culm leaf extract 100-110 weight portions, ginger extract 3-4 weight portions and P. kingianum are carried Take thing 13-17 weight portions.
Present invention also offers a kind of preparation method of solid beverage, comprises the steps:
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extract A3, concentration A4 and powder processed A5;
The processing of P. kingianum extract or ginger extract, including pretreatment B1, cold water extraction B2, hot water extract B3, concentration A4 and powder A5 processed;
Above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are mixed by a certain percentage.
Used as preferred, the pretreatment A1 steps are that fresh culm leaf is carried out brokenly into fibre, i.e., using rolling mill practice by culm Leaf is depressed into gained bamboo fibre diameter≤5mm, and bamboo fibre is cut into the bamboo silk of 3-4cm, and enzymolysis liquid enzymolysis broken wall is added in Xiang Zhusi, Obtain solidliquid mixture a1;The pretreatment B1 steps are that P. kingianum or ginger are crushed to after 20-80 mesh, add enzymolysis liquid enzymolysis Broken wall, obtains solidliquid mixture b1.
Used as preferred, the content of each component is in the enzymolysis liquid:Cellulase volume fraction 1.7-3.2%, pectin Enzyme volume fraction 0.31-0.57%, sucrose 0.41-0.58mol/L, MgSO423-31mmol/L and CaCl211-23mmol/L; The enzymolysis liquid of 40-60ml is added in pretreatment A1 steps in every gram of bamboo silk, at 18-25 degree Celsius 15-24 hours are digested;Pretreatment The enzymolysis liquid of 5-10ml is added in every gram of raw material of B1 steps, at 18-25 degree Celsius 13-18 hours are digested.
As preferred, the cold water extraction A2 step be by solidliquid mixture a1 and 20-30 degree Celsius of cold water according to Solid-liquid mass ratio 1:50-100 mixing Posterior circle is extracted 3-10 time, and 1-10 hours are extracted in circulation altogether, and circulation is carried out after the completion of extracting Separation of solid and liquid obtains liquid phase part a2 and solid fraction a2;The cold water extraction B2 step is by solidliquid mixture b1 and 20-30 Degree Celsius cold water according to solid-liquid mass ratio 1:10-20 mixing Posterior circle is extracted 2-8 time, and 0.5-8 hours, circulation are extracted in circulation altogether Separation of solid and liquid is carried out after the completion of extraction and obtains liquid phase part b2 and solid fraction b2.
Used as preferred, it is according to solid-liquid mass ratio 1 that the hot water extracts A3 steps:20-80 adds in solid phase components a2 Extraction 2-5 time is circulated after the hot water mixing for entering 60-80 degree Celsius, 0.1-5h is extracted in circulation altogether, and circulation extraction completes laggard Row separation of solid and liquid obtains liquid phase part a3 and solid fraction a3;It is according to solid-liquid mass ratio 1 that the hot water extracts B3 steps:10- Extraction 2-4 time is circulated after the hot water mixing that 60-80 degree Celsius is added in 18 to solid phase components b2,0.1- is extracted in circulation altogether 4h, circulation carries out separation of solid and liquid and obtains liquid phase part b3 and solid fraction b3 after the completion of extracting.
Used as preferred, the concentration A4 steps are:
Film concentration is carried out to liquid phase part a2 or liquid phase part b2, film concentration is less than 0.01 micron with membrane aperture is separated, point Do not obtain a4 or b4;
Negative pressure evaporation concentration is carried out to liquid phase part a3 or liquid phase part b3, negative pressure evaporation is concentrated first by liquid phase part a3 Or the pressure of liquid phase part b3 is maintained at vacuum 0.01-0.05MPa 20-60 minutes, is then depressured, pressure is kept in 0.05- 0.1MPa to liquid volume reduces 10-20 times, and wherein negative pressure evaporation concentration overall process liquid keeps less than 80 degrees Celsius.
Used as preferred, the powder A5 steps processed are:
Liquid phase part a2 or liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be that 20-80Pa, temperature are little Freeze under -40 degrees celsius, then in -15 degrees Celsius to -28 degrees Celsius lyophilizations, finally under 35-45 degree Celsius Parsing-desiccation to moisture content is less than 10%;
Liquid phase part a3 or liquid phase part b3 carry out that atomization drying is carried out after negative pressure evaporation concentration to moisture content less than 10%, Atomization drying temperature is 53-60 degree Celsius, and atomizing pressure is 2000-3300KPa;.
As preferred, the lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, obtain culm Leaf extract;The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;Will The lyophilized products obtained as raw material with ginger and atomization drying product mix, and obtain ginger extract.
Compared with prior art, beneficial effects of the present invention are at least one of following:
1) solid beverage of the present invention removes culm leaf and the extraction beyond the region of objective existence of sealwort is also added with ginger extract, and ginger can add straightforward man Body metabolism, degrading the channel, can promote the performance of active ingredient effect in culm leaf and sealwort, and can neutralize culm leaf " cold ", the present invention has functions that to calm the nerves most brain, toxin expelling, moistening lung eliminating the phlegm, enriching yin, prevention of stroke and reduces blood viscosity, and enters Mouth bamboo is aromatic strongly fragrant, and with bitter first ,sweet later sweet mouthfeel is returned.
2) solid beverage of the present invention selects the extract of culm leaf, P. kingianum and ginger to prepare, compared to directly with culm leaf, P. kingianum and ginger is brewed or other processing methods for, active constituent content therein is higher, therefore health-care effect is also more preferable.
3) when the present invention extracts active component in culm leaf, P. kingianum and ginger, for the first time using cold water extraction, plant is extracted Volatile materials in thing and it is soluble in the materials such as polysaccharide, the amino acid of cold water;For cold water extract adopts film concentration technique, Volatile materials can at utmost be retained.Second hot water is extracted, can effectively extract be not readily dissolved in cold water, boiling point it is higher Active ingredient, such as the saponin in tabasheer ketone, sealwort or sealwort composition in culm leaf, because hot water extract's matter is difficult to wave Send out, can be concentrated using negative pressure evaporation technology, can be with reduces cost compared to film concentration.The extracting method of first cold water hot water again So that the active constituent content in solid beverage of the present invention is higher, fragrance component therein can be effectively retained, special with plant Some fragrance, mouthfeel is fabulous.
3) during extracts active ingredients of the present invention, cell membrane is destroyed with enzymolysis liquid first so that active ingredient therein is more held Easily it is extracted, improves the extraction efficiency of active ingredient.
4) existing extracting method is compared, the recovery rate of the present invention can improve 10% or so.
Specific embodiment
In order that the objects, technical solutions and advantages of the present invention become more apparent, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that specific embodiment described herein is not used to only to explain the present invention Limit the present invention.
Embodiment 1:
Present embodiments provide a kind of solid beverage, including the weight portion of culm leaf extract 90, the weight portion of ginger extract 7 and The weight portion of P. kingianum extract 20.
Embodiment 2:
Present embodiments provide a kind of solid beverage, including the weight portion of culm leaf extract 120, the weight portion of ginger extract 1 With the weight portion of P. kingianum extract 10.
Embodiment 3:
Present embodiments provide a kind of solid beverage, including the weight portion of culm leaf extract 105, the weight portion of ginger extract 4 With the weight portion of P. kingianum extract 15.
Embodiment 4:
Present embodiments provide a kind of solid beverage, including the weight portion of culm leaf extract 100, the weight portion of ginger extract 5 With the weight portion of P. kingianum extract 17.
Embodiment 5:
Present embodiments provide a kind of solid beverage, including the weight portion of culm leaf extract 110, the weight portion of ginger extract 3 With the weight portion of P. kingianum extract 13.
The species solid beverage of comparing embodiment 1 to embodiment 5, according in the solid beverage that the formula of embodiment 3 is obtained The fragrance of various extracts can preferably coordinate, and reach optimal mouthfeel.
Embodiment 6:
Present embodiments provide a kind of preparation method of solid beverage, including the processing of culm leaf extract, P. kingianum are carried The processing of thing and the processing of ginger extract are taken, above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are pressed Certain proportion mixes, and obtains solid beverage of the present invention.
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extraction A3, concentration A4 and powder A5 processed:
Pretreatment A1, by fresh culm leaf fibre is carried out brokenly, i.e., culm leaf is depressed into gained bamboo fibre diameter using rolling mill practice ≤ 5mm, by bamboo fibre the bamboo silk of 3-4cm is cut to, and the enzymolysis liquid of 60ml is added in every gram of bamboo silk, little in 25 degrees Celsius of enzymolysis 24 When, broken wall is digested, obtain solidliquid mixture a1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction 3.2%th, pectase volume fraction 0.57%, sucrose 0.58mol/L, MgSO431mmol/L and CaCl223mmol/L;
Cold water extraction A2, by solidliquid mixture a1 and 20 degrees Celsius of cold water according to solid-liquid mass ratio 1:Follow after 100 mixing Ring is extracted 10 times, and circulation altogether is extracted 10 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part a2 and solid phase portion after the completion of extracting Divide a2;
Hot water extracts A3, according to solid-liquid mass ratio 1:Add 80 degrees Celsius of hot water mixing laggard in 80 to solid phase components a2 Row circulation is extracted 5 times, and 5h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part a3 and solid fraction after the completion of extracting a3;
Concentration A4, film concentration is carried out to liquid phase part a2, and film concentration is less than 0.01 micron, obtains a4 with membrane aperture is separated; Negative pressure evaporation concentration is carried out to liquid phase part a3, the pressure of liquid phase part a3 is maintained at vacuum by negative pressure evaporation concentration first 0.05MPa 60 minutes, is then depressured, and keeps pressure to reduce 20 times in 0.1MPa to liquid volume, and wherein negative pressure evaporation concentration is complete Process liquids keep 80 degrees Celsius;
Powder A5 processed, the liquid phase part a2 after film is concentrated is freezed, it is lyophilized be in vacuum be 80Pa, -40 degrees Celsius of temperature Under the conditions of freeze, then in -28 degrees Celsius of lyophilizations, finally in 45 degrees Celsius of lower parsing-desiccations to moisture content 10%;Liquid phase Part a3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 60 degrees Celsius, atomization Pressure is 2000KPa;
The lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, culm leaf extract is obtained.
The processing of P. kingianum extract or ginger extract, including pretreatment B1, cold water extraction B2, hot water extraction B3, concentration A4 and powder A5 processed:
Pretreatment B1, P. kingianum or ginger are crushed to after 20 mesh, and the enzymolysis liquid of 5ml is added in every gram of raw material, Celsius 18 Degree enzymolysis 13 hours, obtains solidliquid mixture b1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction 1.7%, pectase volume fraction 0.31%, sucrose 0.41mol/L, MgSO423mmol/L and CaCl211mmol/L;
Cold water extraction B2, by solidliquid mixture b1 and 20 degrees Celsius of cold water according to solid-liquid mass ratio 1:10 mixing Posterior circles Extract 2 times, circulation altogether is extracted 0.5 hour, and circulation carries out separation of solid and liquid and obtains liquid phase part b2 and solid fraction after the completion of extracting b2;
Hot water extracts B3, according to solid-liquid mass ratio 1:Add 60 degrees Celsius of hot water mixing laggard in 10 to solid phase components b2 Row circulation is extracted 2 times, and 0.1h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part b3 and solid phase portion after the completion of extracting Divide b3;
Concentration A4, film concentration is carried out to liquid phase part b2, and film concentration is less than 0.01 micron, obtains b4 with membrane aperture is separated; Negative pressure evaporation concentration is carried out to liquid phase part b3, the pressure of liquid phase part b3 is maintained at vacuum by negative pressure evaporation concentration first 0.05MPa 20 minutes, is then depressured, and keeps pressure to reduce 10 times in 0.1MPa to liquid volume, and wherein negative pressure evaporation concentration is complete Process liquids keep 80 degrees Celsius;
Powder A5 processed, the liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be 20Pa, -40 degrees Celsius of temperature Under the conditions of freeze, then in -15 degrees Celsius of lyophilizations, finally in 35 degrees Celsius of lower parsing-desiccations to moisture content 10%;To liquid Phase part b3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 53 degrees Celsius, mist Change pressure is 2000KPa;
The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;Will The lyophilized products obtained as raw material with ginger and atomization drying product mix, and obtain ginger extract.
Embodiment 7:
Present embodiments provide a kind of preparation method of solid beverage, including the processing of culm leaf extract, P. kingianum are carried The processing of thing and the processing of ginger extract are taken, above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are pressed Certain proportion mixes, and obtains solid beverage of the present invention.
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extraction A3, concentration A4 and powder A5 processed:
Pretreatment A1, by fresh culm leaf fibre is carried out brokenly, i.e., culm leaf is depressed into gained bamboo fibre diameter using rolling mill practice ≤ 5mm, by bamboo fibre the bamboo silk of 3-4cm is cut to, and the enzymolysis liquid of 40ml is added in every gram of bamboo silk, little in 18 degrees Celsius of enzymolysis 15 When, broken wall is digested, obtain solidliquid mixture a1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction 1.7%th, pectase volume fraction 0.31%, sucrose 0.41mol/L, MgSO423mmol/L and CaCl211mmol/L;
Cold water extraction A2, by solidliquid mixture a1 and 30 degrees Celsius of cold water according to solid-liquid mass ratio 1:50 mixing Posterior circles Extract 3 times, circulation altogether is extracted 1 hour, and circulation carries out separation of solid and liquid and obtains liquid phase part a2 and solid fraction a2 after the completion of extracting;
Hot water extracts A3, according to solid-liquid mass ratio 1:Add 60 degrees Celsius of hot water mixing laggard in 20 to solid phase components a2 Row circulation is extracted 2 times, and 0.1h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part a3 and solid phase portion after the completion of extracting Divide a3;
Concentration A4, film concentration is carried out to liquid phase part a2, and film concentration is less than 0.01 micron, obtains a4 with membrane aperture is separated; Negative pressure evaporation concentration is carried out to liquid phase part a3, the pressure of liquid phase part a3 is maintained at vacuum by negative pressure evaporation concentration first 0.01MPa 20 minutes, is then depressured, and keeps pressure to reduce 10 times in 0.05MPa to liquid volume, wherein negative pressure evaporation concentration Overall process liquid keeps 70 degrees Celsius;
Powder A5 processed, the liquid phase part a2 after film is concentrated is freezed, it is lyophilized be in vacuum be 20Pa, -30 degrees Celsius of temperature Under the conditions of freeze, then in -15 degrees Celsius of lyophilizations, finally 35 degrees Celsius of lower parsing-desiccations to moisture content be less than 10%; Liquid phase part a3 carries out that atomization drying is carried out after negative pressure evaporation concentration to moisture content less than 10%, and atomization drying temperature is 53 Celsius Degree, atomizing pressure is 3300KPa;
The lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, culm leaf extract is obtained.
The processing of P. kingianum extract or ginger extract, including pretreatment B1, cold water extraction B2, hot water extraction B3, concentration A4 and powder A5 processed:
Powder A5 processed, the liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be 20Pa, -40 degrees Celsius of temperature Under the conditions of freeze, then in -15 degrees Celsius of lyophilizations, finally in 35 degrees Celsius of lower parsing-desiccations to moisture content 10%;To liquid Phase part b3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 53 degrees Celsius, mist Change pressure is 2000KPa;
Pretreatment B1, P. kingianum or ginger are crushed to after 80 mesh, and the enzymolysis liquid of 10ml is added in every gram of raw material, Celsius 25 Degree enzymolysis 18 hours, obtains solidliquid mixture b1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction 3.2%, pectase volume fraction 0.57%, sucrose 0.58mol/L, MgSO431mmol/L and CaCl223mmol/L;
Cold water extraction B2, by solidliquid mixture b1 and 30 degrees Celsius of cold water according to solid-liquid mass ratio 1:Follow after 20 mixing Ring is extracted 8 times, and circulation altogether is extracted 8 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part b2 and solid fraction after the completion of extracting b2;
Hot water extracts B3, according to solid-liquid mass ratio 1:Add 80 degrees Celsius of hot water mixing laggard in 18 to solid phase components b2 Row circulation is extracted 4 times, and 4h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part b3 and solid fraction after the completion of extracting b3;
Concentration A4, film concentration is carried out to liquid phase part b2, and film concentration is less than 0.01 micron, obtains b4 with membrane aperture is separated; Negative pressure evaporation concentration is carried out to liquid phase part b3, the pressure of liquid phase part b3 is maintained at vacuum by negative pressure evaporation concentration first 0.01MPa 60 minutes, is then depressured, and keeps pressure to reduce 20 times in 0.05MPa to liquid volume, wherein negative pressure evaporation concentration Overall process liquid keeps 80 degrees Celsius;
Powder A5 processed, the liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be 80Pa, -40 degrees Celsius of temperature Under the conditions of freeze, then in -28 degrees Celsius of lyophilizations, finally 45 degrees Celsius of lower parsing-desiccations to moisture content be less than 10%; Carry out being carried out after negative pressure evaporation concentration atomization drying to liquid phase part b3 to moisture content 10%, atomization drying temperature is 60 Celsius Degree, atomizing pressure is 3300KPa;
The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;Will The lyophilized products obtained as raw material with ginger and atomization drying product mix, and obtain ginger extract.
Embodiment 8:
Present embodiments provide a kind of preparation method of solid beverage, including the processing of culm leaf extract, P. kingianum are carried The processing of thing and the processing of ginger extract are taken, above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are pressed Certain proportion mixes, and obtains solid beverage of the present invention.
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extraction A3, concentration A4 and powder A5 processed:
Pretreatment A1, by fresh culm leaf fibre is carried out brokenly, i.e., culm leaf is depressed into gained bamboo fibre diameter using rolling mill practice ≤ 5mm, by bamboo fibre the bamboo silk of 3-4cm is cut to, and the enzymolysis liquid of 50ml is added in every gram of bamboo silk, little in 23 degrees Celsius of enzymolysis 19 When, broken wall is digested, obtain solidliquid mixture a1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction 2.4%th, pectase volume fraction 0.42%, sucrose 0.51mol/L, MgSO429mmol/L and CaCl218mmol/L;
Cold water extraction A2, by solidliquid mixture a1 and 25 degrees Celsius of cold water according to solid-liquid mass ratio 1:60 mixing Posterior circles Extract 5 times, circulation altogether is extracted 4 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part a2 and solid fraction a2 after the completion of extracting;
Hot water extracts A3, according to solid-liquid mass ratio 1:Add 70 degrees Celsius of hot water mixing laggard in 30 to solid phase components a2 Row circulation is extracted 3 times, and 2h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part a3 and solid fraction after the completion of extracting a3;
Concentration A4, film concentration is carried out to liquid phase part a2, and film concentration is less than 0.01 micron, obtains a4 with membrane aperture is separated; Negative pressure evaporation concentration is carried out to liquid phase part a3, the pressure of liquid phase part a3 is maintained at vacuum by negative pressure evaporation concentration first 0.04MPa 45 minutes, is then depressured, and keeps pressure to reduce 15 times in 0.08MPa to liquid volume, wherein negative pressure evaporation concentration Overall process liquid keeps 80 degrees Celsius;
Powder A5 processed, the liquid phase part a2 after film is concentrated is freezed, it is lyophilized be in vacuum be 60Pa, temperature 6-40 degree Celsius Under the conditions of freeze, then in -22 degrees Celsius of lyophilizations, finally in 40 degrees Celsius of lower parsing-desiccations to moisture content 10%;Liquid phase Part a3 carries out that atomization drying is carried out after negative pressure evaporation concentration to moisture content less than 10%, and atomization drying temperature is 57 degrees Celsius, Atomizing pressure is 2700KPa;
The lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, culm leaf extract is obtained.
The processing of P. kingianum extract or ginger extract, including pretreatment B1, cold water extraction B2, hot water extraction B3, concentration A4 and powder A5 processed:
Pretreatment B1, P. kingianum or ginger are crushed to after 60 mesh, and the enzymolysis liquid of 7ml is added in every gram of raw material, Celsius 22 Degree enzymolysis 26 hours, obtains solidliquid mixture b1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction 2.3%, pectase volume fraction 0.4.6%, sucrose 0.5.2mol/L, MgSO427mmol/L and CaCl217mmol/L;
Cold water extraction B2, by solidliquid mixture b1 and 25 degrees Celsius of cold water according to solid-liquid mass ratio 1:15 mixing Posterior circles Extract 4 times, circulation altogether is extracted 3 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part b2 and solid fraction b2 after the completion of extracting;
Hot water extracts B3, according to solid-liquid mass ratio 1:Add 70 degrees Celsius of hot water mixing laggard in 14 to solid phase components b2 Row circulation is extracted 3 times, and 1h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part b3 and solid fraction after the completion of extracting b3;
Concentration A4, film concentration is carried out to liquid phase part b2, and film concentration is less than 0.01 micron, obtains b4 with membrane aperture is separated; Negative pressure evaporation concentration is carried out to liquid phase part b3, the pressure of liquid phase part b3 is maintained at vacuum by negative pressure evaporation concentration first 0.03MPa 36 minutes, is then depressured, and keeps pressure to reduce 13 times in 0.07MPa to liquid volume, wherein negative pressure evaporation concentration Overall process liquid keeps 80 degrees Celsius;
Powder A5 processed, the liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be 50Pa, -40 degrees Celsius of temperature Under the conditions of freeze, then in -22 degrees Celsius of lyophilizations, finally in 37 degrees Celsius of lower parsing-desiccations to moisture content 10%;To liquid Phase part b3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 59 degrees Celsius, mist Change pressure is 25600KPa;
The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;Will The lyophilized products obtained as raw material with ginger and atomization drying product mix, and obtain ginger extract.
Embodiment 9:
Present embodiments provide a kind of preparation method of solid beverage, including the processing of culm leaf extract, P. kingianum are carried The processing of thing and the processing of ginger extract are taken, above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are pressed Certain proportion mixes, and obtains solid beverage of the present invention.
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extraction A3, concentration A4 and powder A5 processed:
Pretreatment A1, by fresh culm leaf fibre is carried out brokenly, i.e., culm leaf is depressed into gained bamboo fibre diameter using rolling mill practice ≤ 5mm, by bamboo fibre the bamboo silk of 3-4cm is cut to, and the enzymolysis liquid of 60ml is added in every gram of bamboo silk, little in 25 degrees Celsius of enzymolysis 24 When, broken wall is digested, obtain solidliquid mixture a1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction 3.2%th, pectase volume fraction 0.57%, sucrose 0.58mol/L, MgSO431mmol/L and CaCl223mmol/L;
Cold water extraction A2, by solidliquid mixture a1 and 20 degrees Celsius of cold water according to solid-liquid mass ratio 1:60 mixing Posterior circles Extract 5 times, circulation altogether is extracted 6 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part a2 and solid fraction a2 after the completion of extracting;
Hot water extracts A3, according to solid-liquid mass ratio 1:Add 80 degrees Celsius of hot water mixing laggard in 80 to solid phase components a2 Row circulation is extracted 3 times, and 2h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part a3 and solid fraction after the completion of extracting a3;
Concentration A4, film concentration is carried out to liquid phase part a2, and film concentration is less than 0.01 micron, obtains a4 with membrane aperture is separated; Negative pressure evaporation concentration is carried out to liquid phase part a3, the pressure of liquid phase part a3 is maintained at vacuum by negative pressure evaporation concentration first 0.05MPa 60 minutes, is then depressured, and keeps pressure to reduce 20 times in 0.1MPa to liquid volume, and wherein negative pressure evaporation concentration is complete Process liquids keep 80 degrees Celsius;
Powder A5 processed, the liquid phase part a2 after film is concentrated is freezed, it is lyophilized be in vacuum be 80Pa, -40 degrees Celsius of temperature Under the conditions of freeze, then in -28 degrees Celsius of lyophilizations, finally in 45 degrees Celsius of lower parsing-desiccations to moisture content 10%;Liquid phase Part a3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 60 degrees Celsius, atomization Pressure is 2000KPa;
The lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, culm leaf extract is obtained.
The processing of P. kingianum extract or ginger extract, including pretreatment B1, cold water extraction B2, hot water extraction B3, concentration A4 and powder A5 processed:
Pretreatment B1, P. kingianum or ginger are crushed to after 80 mesh, and the enzymolysis liquid of 10ml is added in every gram of raw material, Celsius 25 Degree enzymolysis 18 hours, obtains solidliquid mixture b1;The content of each component is in wherein described enzymolysis liquid:Cellulase volume fraction 1.7%, pectase volume fraction 0.31%, sucrose 0.41mol/L, MgSO 23mmol/L and CaCl211mmol/L;
Cold water extraction B2, by solidliquid mixture b1 and 20 degrees Celsius of cold water according to solid-liquid mass ratio 1:10 mixing Posterior circles Extract 4 times, circulation altogether is extracted 5 hours, and circulation carries out separation of solid and liquid and obtains liquid phase part b2 and solid fraction b2 after the completion of extracting;
Hot water extracts B3, according to solid-liquid mass ratio 1:Add 60 degrees Celsius of hot water mixing laggard in 10 to solid phase components b2 Row circulation is extracted 2 times, and 1h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase part b3 and solid fraction after the completion of extracting b3;
Concentration A4, film concentration is carried out to liquid phase part b2, and film concentration is less than 0.01 micron, obtains b4 with membrane aperture is separated; Negative pressure evaporation concentration is carried out to liquid phase part b3, the pressure of liquid phase part b3 is maintained at vacuum by negative pressure evaporation concentration first 0.05MPa 20 minutes, is then depressured, and keeps pressure to reduce 10 times in 0.1MPa to liquid volume, and wherein negative pressure evaporation concentration is complete Process liquids keep 80 degrees Celsius;
Powder A5 processed, the liquid phase part b2 after film is concentrated is freezed, it is lyophilized be in vacuum be 20Pa, -40 degrees Celsius of temperature Under the conditions of freeze, then in -15 degrees Celsius of lyophilizations, finally in 35 degrees Celsius of lower parsing-desiccations to moisture content 10%;To liquid Phase part b3 carries out being carried out after negative pressure evaporation concentration atomization drying to moisture content 10%, and atomization drying temperature is 53 degrees Celsius, mist Change pressure is 2000KPa;
The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;Will The lyophilized products obtained as raw material with ginger and atomization drying product mix, and obtain ginger extract.
The situation of the extract that the extracting method of active ingredient is obtained is shown in the raw material according to embodiment 6 to embodiment 9 Following table, wherein recovery rate are the percentage that extraction of substance accounts for raw material weight, and the deep or light of fragrance is according to four realities by same raw material The fragrance for applying the extract that the Different Extraction Method in example is obtained is compared, and two denseer as " dense ", fragrance of fragrance are thin Two be " light ".
It is slightly better on extract and fragrance from above table as can be seen that embodiment 9 compares other embodiment. Because cold water extraction temperature is relatively low, therefore wherein volatile material retains more, and aroma substance half is easier to volatilization, therefore The denseer material that can illustrate that cold water extraction goes out of fragrance retains more.
Although reference be made herein to invention has been described for multiple explanatory embodiments of the invention, however, it is to be understood that Those skilled in the art can be designed that a lot of other modification and embodiment, and these modifications and embodiment will fall in this Shen Please be within disclosed spirit and spirit.More specifically, in the range of disclosure and claim, can be to master The building block and/or layout of topic composite configuration carries out various modifications and improvement.Except what is carried out to building block and/or layout Deformation and improvement are outer, and to those skilled in the art, other purposes also will be apparent.

Claims (10)

1. a kind of solid beverage, it is characterised in that including culm leaf extract 90-120 weight portions, ginger extract 1-7 weight portions With P. kingianum extract 10-20 weight portions.
2. solid beverage according to claim 1, it is characterised in that including culm leaf extract 100-110 weight portions, ginger Extract 3-4 weight portions and P. kingianum extract 13-17 weight portions.
3. the preparation method of solid beverage described in a kind of claim 1, it is characterised in that comprise the steps:
The processing of culm leaf extract, including pretreatment A1, cold water extraction A2, hot water extract A3, concentration A4 and powder A5 processed;
The processing of P. kingianum extract or ginger extract, including, pretreatment B1, cold water extraction B2, hot water extract B3, concentration A4 and Powder A5 processed;
Above-mentioned fresh culm leaf extract, fresh P. kingianum extract and fresh ginger extract are mixed by a certain percentage.
4. the preparation method of solid beverage according to claim 3, it is characterised in that
The pretreatment A1 steps are that fresh culm leaf is carried out brokenly into fibre, i.e., culm leaf is depressed into gained bamboo fibre using rolling mill practice Diameter≤5mm, by bamboo fibre the bamboo silk of 3-4cm is cut to, and enzymolysis liquid enzymolysis broken wall is added in Xiang Zhusi, obtains solidliquid mixture a1;
The pretreatment B1 steps are that P. kingianum or ginger are crushed to after 20-80 mesh, add enzymolysis liquid enzymolysis broken wall, obtain solid-liquid Mixture b1.
5. the preparation method of solid beverage according to claim 4, it is characterised in that
The content of each component is in the enzymolysis liquid:Cellulase volume fraction 1.7-3.2%, pectase volume fraction 0.31- 0.57%, sucrose 0.41-0.58mol/L, MgSO423-31mmol/L and CaCl211-23mmol/L;In pretreatment A1 steps The enzymolysis liquid of 40-60ml is added in every gram of bamboo silk, at 18-25 degree Celsius 15-24 hours are digested;Pretreatment B1 every gram of raw material of step The enzymolysis liquid of middle addition 5-10ml, at 18-25 degree Celsius 13-18 hours are digested.
6. the preparation method of solid beverage according to claim 4, it is characterised in that
The cold water extraction A2 step is according to solid-liquid mass ratio 1 by solidliquid mixture a1 and 20-30 degree Celsius of cold water:50- 100 mixing Posterior circles are extracted 3-10 time, and 1-10 hours are extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase after the completion of extracting Part a2 and solid fraction a2;
The cold water extraction B2 step is according to solid-liquid mass ratio 1 by solidliquid mixture b1 and 20-30 degree Celsius of cold water:10- 20 mixing Posterior circles are extracted 2-8 time, and 0.5-8 hours are extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid phase after the completion of extracting Part b2 and solid fraction b2.
7. the preparation method of solid beverage according to claim 6, it is characterised in that
It is according to solid-liquid mass ratio 1 that the hot water extracts A3 steps:20-80 adds 60-80 degree Celsius in solid phase components a2 Extraction 2-5 time is circulated after hot water mixing, 0.1-5h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid after the completion of extracting Phase part a3 and solid fraction a3;
It is according to solid-liquid mass ratio 1 that the hot water extracts B3 steps:10-18 adds 60-80 degree Celsius in solid phase components b2 Extraction 2-4 time is circulated after hot water mixing, 0.1-4h is extracted in circulation altogether, and circulation carries out separation of solid and liquid and obtains liquid after the completion of extracting Phase part b3 and solid fraction b3.
8. the preparation method of solid beverage according to claim 6, it is characterised in that the concentration A4 steps are:
Film concentration is carried out to liquid phase part a2 or liquid phase part b2, film concentration is less than 0.01 micron with membrane aperture is separated, respectively To a4 or b4;
Negative pressure evaporation concentration is carried out to liquid phase part a3 or liquid phase part b3, negative pressure evaporation is concentrated first by liquid phase part a3 or liquid The pressure of phase part b3 is maintained at vacuum 0.01-0.05MPa 20-60 minutes, is then depressured, and keeps pressure in 0.05- 0.1MPa to liquid volume reduces 10-20 times, and wherein negative pressure evaporation concentration overall process liquid keeps less than 80 degrees Celsius.
9. the preparation method of solid beverage according to claim 7, it is characterised in that the powder A5 steps processed are:
Liquid phase part a2 or liquid phase part b2 after film is concentrated is freezed, it is lyophilized be vacuum be 20-80Pa, temperature less than- Freeze under 40 degrees celsius, then in -15 degrees Celsius to -28 degrees Celsius lyophilizations, finally parse under 35-45 degree Celsius It is dried to moisture content and is less than 10%;
Liquid phase part a3 or liquid phase part b3 carry out that atomization drying is carried out after negative pressure evaporation concentration to moisture content less than 10%, atomization Baking temperature is 53-60 degree Celsius, and atomizing pressure is 2000-3300KPa.
10. the preparation method of solid beverage according to claim 8 or claim 9, it is characterised in that
The lyophilized products obtained as raw material with culm leaf and atomization drying product are mixed, culm leaf extract is obtained;
The lyophilized products obtained as raw material with P. kingianum and atomization drying product are mixed, P. kingianum extract is obtained;
The lyophilized products obtained as raw material with ginger and atomization drying product are mixed, ginger extract is obtained.
CN201610871220.0A 2016-09-30 2016-09-30 Solid beverage and preparation method thereof Pending CN106616172A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610871220.0A CN106616172A (en) 2016-09-30 2016-09-30 Solid beverage and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610871220.0A CN106616172A (en) 2016-09-30 2016-09-30 Solid beverage and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106616172A true CN106616172A (en) 2017-05-10

Family

ID=58854028

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610871220.0A Pending CN106616172A (en) 2016-09-30 2016-09-30 Solid beverage and preparation method thereof

Country Status (1)

Country Link
CN (1) CN106616172A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109259027A (en) * 2018-12-20 2019-01-25 烟台五神生物科技有限公司 A kind of health beverages
CN114711407A (en) * 2022-05-07 2022-07-08 海天醋业集团有限公司 Ginger and onion extract and preparation method and application thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1799429A (en) * 2005-09-02 2006-07-12 廖农林 Beverage with bamboo and siberian solomoseal rhizome its preparation method
CN1865290A (en) * 2006-06-23 2006-11-22 天津农学院 Extraction method of polysaccharide from winter jujub
CN101397582A (en) * 2007-09-30 2009-04-01 咸阳宏华生化科技有限公司 Method for producing diosgenin by environment friendly pollution-free holoenzyme method
CN103918830A (en) * 2013-01-15 2014-07-16 北京同仁堂健康药业股份有限公司 Warming tea beverage
CN104095030A (en) * 2014-07-10 2014-10-15 青岛大学 Vacuum freeze-dried gypsophila stems and leaves products and preparation process thereof
CN105558645A (en) * 2014-10-13 2016-05-11 康爱民 Ginger juice health care beverage

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1799429A (en) * 2005-09-02 2006-07-12 廖农林 Beverage with bamboo and siberian solomoseal rhizome its preparation method
CN1865290A (en) * 2006-06-23 2006-11-22 天津农学院 Extraction method of polysaccharide from winter jujub
CN101397582A (en) * 2007-09-30 2009-04-01 咸阳宏华生化科技有限公司 Method for producing diosgenin by environment friendly pollution-free holoenzyme method
CN103918830A (en) * 2013-01-15 2014-07-16 北京同仁堂健康药业股份有限公司 Warming tea beverage
CN104095030A (en) * 2014-07-10 2014-10-15 青岛大学 Vacuum freeze-dried gypsophila stems and leaves products and preparation process thereof
CN105558645A (en) * 2014-10-13 2016-05-11 康爱民 Ginger juice health care beverage

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109259027A (en) * 2018-12-20 2019-01-25 烟台五神生物科技有限公司 A kind of health beverages
CN109259027B (en) * 2018-12-20 2019-04-12 烟台五神生物科技有限公司 A kind of health beverages
CN114711407A (en) * 2022-05-07 2022-07-08 海天醋业集团有限公司 Ginger and onion extract and preparation method and application thereof
CN114711407B (en) * 2022-05-07 2023-10-17 海天醋业集团有限公司 Ginger and onion extracting solution and preparation method and application thereof

Similar Documents

Publication Publication Date Title
CN102488010B (en) Method for making momordica grosvenori milky tea
CN104783248A (en) Passiflora edulis drink
CN104305457B (en) A kind of preparation method of cumquat loquat leaf extract
CN104585448A (en) Processing method of health loquat ginger tea
CN102805396B (en) Kumquat compound pulp and juice beverage and preparation method thereof
CN103828986A (en) Health-care tea beverage and preparation process thereof
CN104126700A (en) Grosvenor momordica fruit-honeysuckle flower herbal tea and preparation method thereof
CN106616172A (en) Solid beverage and preparation method thereof
CN105167075A (en) Ginseng-black fungus juice and preparation method of the ginseng-black fungus juice
CN104921132B (en) A kind of disappearing with moistening the lung and relieve the cough breathes heavily the herbal health care oral liquid of effect
CN106820270A (en) A kind of electronic cigarette tobacco tar and preparation method thereof
CN106721839A (en) A kind of preparation method of the brown sugar ginger electuary for being convenient for carrying and eating
CN106387563A (en) Heat-clearing lung-moistening beverage and preparation method thereof
CN103070388B (en) Delicate tricholoma matsutake active extract and preparation method and application thereof
CN104388258B (en) A kind of Exocarpium Citri Grandis health promoting wine and preparation method thereof
CN106260224A (en) A kind of health white tea and processing technology thereof
CN106107277A (en) A kind of Prunus persicanucipersica Schneider beverage and preparation method thereof
CN107467470A (en) A kind of compound solid beverage containing mulberry leaf, persimmon leaves and loguat leaf and preparation method thereof
CN106616126A (en) Functional radix glehniae drink and preparation method thereof
CN104383232B (en) Clearing heat and detoxicating buccal lozenge of lectuce tea and its production method
CN103725580B (en) Method for preparing sweet orange rum
CN112168944A (en) Traditional Chinese medicine composition and extract for preventing new coronary pneumonia, and preparation method and application thereof
CN104479952A (en) Hollowed wampee bark fruit Chinese rice wine and preparation method thereof
CN107334021A (en) Betelnutpalm male flower drink and preparation method thereof
CN106578210A (en) Intestine-moistening carbonated tea and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20170510

RJ01 Rejection of invention patent application after publication