CN106614594A - Composition with plant growth regulation function and preparation method - Google Patents

Composition with plant growth regulation function and preparation method Download PDF

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Publication number
CN106614594A
CN106614594A CN201611223031.9A CN201611223031A CN106614594A CN 106614594 A CN106614594 A CN 106614594A CN 201611223031 A CN201611223031 A CN 201611223031A CN 106614594 A CN106614594 A CN 106614594A
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China
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preparation
composition
plant growth
stabilizer
cosolvent
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CN201611223031.9A
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Chinese (zh)
Inventor
吴炜
付明
张和林
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/36Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
    • A01N43/38Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/06Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
    • A01N43/08Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/22Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom rings with more than six members

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a composition with a plant growth regulation function. The composition is prepared from the following raw materials in percentage by weight: 0.001 to 90 percent of ascorbic acid, 0.0001 to 40 percent of brassinolide, 0.0001 to 25 percent of indoleacetic acid, 1 to 15 percent of dispersant, 0.5 to 15 percent of cosolvent, 0 to 5 percent of stabilizer and the balance of distilled water. According to the composition disclosed by the invention, the preparation technology is simple and easy, the product quality is safe and reliable, the application range is wide, remarkable production and income increasing effects on crops are obtained, the market development prospect is very good, and the social and economic benefits are huge.

Description

A kind of composition with plant growth regulating function and preparation method
Technical field
The invention belongs to agricultural technology field, and in particular to a kind of composition with plant growth regulating function and preparation Method.
Background technology
In recent years, in order to obtain crop, the veterinary antibiotics of high yield, exceeded use agricultural chemicals, chemical fertilizer cause to change in agricultural product Fertilizer, residues of pesticides are exceeded, soil and water pollution, cause a series of broken ring of environment and ecocatastrophe.Seriously threaten mankind's life Deposit and development.For these problems, some bio-organic fertilizers and agricultural chemicals are have developed both at home and abroad.Shape in vegetable material retort process Into organic mixture, with various biological effects.Japan last century end be used as feed addictive, soil deodorant and Organic fertilizer fermentation agent.And compared with systematic research these materials to germination of vegetable seeds, the impact of seedling development.China Research shows effectively prevent the damping-off of seedling and other diseases.The kind of frost flower and marigold is processed with this organic mixture Son, cuttings and root system, can improve the root quantity of germination percentage, rooting percent and the seedling of seed.Also it is used as bio-fertilizer The leavening of material.Although there are some products both at home and abroad and having longer applicating history, it is difficult to adapt to Chinese Economy Development and life The demand of state environmental construction.
Plant growth regulator is generally also referred to as plant hormone.It is chemist the structure for having understood natural hormone with Afterwards, in view of plant endogenous hormones content is very low, it is impossible to extract in large quantities for production, therefore carry out it is artificial synthesized, and Find in derivative from these compounds or the like with natural hormone have equal efficiency even more effectively, it is more superior Artificial synthesized hormone.Plant growth regulator can be used to regulate and control the synthesis of nucleic acid, protein and enzyme in plant body, can be to planting Different phase in thing growth and development process is such as germinateed, takes root, cell elongation, Organ Differentiation, bud differentiation, bloom, result, fall Regulation and control action are played in leaf, dormancy etc..The protein that can improve plant, sugared equal size that they have, what is had can change it Form, the ability of the strengthened plant cold resistance having, drought resisting, salt resistance alkali and disease and insect resistance.Since half a century, plant growth regulating Research, production and the application of agent obtains rapidly development.It shows most fast development speed in whole pesticide industry.
The content of the invention
It is an object of the invention to provide a kind of composition with plant growth regulating function, can not only meet plant life Long demand, and there is very significant effect of increasing production to multiple kinds of crops.
The technical scheme is that:
A kind of composition with plant growth regulating function, is prepared from by the raw material of following weight percents:Ascorbic acid 0.001%~90%, brassin lactones 0.0001%~40%, heteroauxin 0.0001%~25%, dispersant 1%~15%, cosolvent 0.5%~15%, stabilizer 0%~5%, balance of distilled water.
A kind of preparation method of the composition of plant growth regulating function, step is as follows:
(1)Stabilizer is stirred, fine powder is pulverized into, 50-100 mesh sieves are crossed, it is standby;
(2)To in stainless steel autoclave, brassin lactones and heteroauxin are added, be then slowly added into ascorbic acid and dispersion Agent, airtight heating stirs 5-9 hours to 55-75 DEG C, is subsequently adding distilled water, cosolvent and step(1)Stablizing after process Agent, keeping temperature is 33 DEG C, continues to stir 35 minutes, obtains mixed solution, standby;
(3)By step(2)Gained mixed solution is lyophilized into powder, encapsulates, and obtains final product.
A kind of preparation method of the composition of plant growth regulating function, preferred scheme is that the stabilizer is by marine alga Sour sodium, microcrystalline cellulose and converted starch are 3 according to mass ratio:1:0.1 is formulated.
A kind of preparation method of the composition of plant growth regulating function, preferred scheme is that the dispersant is by trimerization Sodium phosphate and stearic acid list glyceride are 2.2 according to mass ratio:0.7 is formulated.
A kind of preparation method of the composition of plant growth regulating function, preferred scheme is, the cosolvent be methyl alcohol, One or two in propylene glycol monomethyl ether and ethyl acetate.
A kind of preparation method of the composition of plant growth regulating function, preferred scheme is, step(1)Cross 80 mesh sieves.
A kind of preparation method of the composition of plant growth regulating function, preferred scheme is, step(2)Airtight heating is extremely 65℃。
A kind of preparation method of the composition of plant growth regulating function, preferred scheme is, step(2)Stirring 7 hours.
A kind of purposes of composition with plant growth regulating function in terms of coordinate plant growth.
The excellent results of the present invention are also manifested by:
(1)Preparation is simple for the present composition, pollution-free, Product quality and safety reliability, easy to use;
(2)The composition applied range by obtained in the present invention, there is significant the effect of increasing income to crop, with fabulous city Field DEVELOPMENT PROSPECT and huge Social benefit and economic benefit.
Specific embodiment
Technical scheme, but protection domain not limited to this are described in detail with reference to embodiment and experimental example.
Embodiment 1:A kind of composition with plant growth regulating function, by the raw material preparation of following weight percents Into:Ascorbic acid 0.001kg, brassin lactones 40kg, heteroauxin 25kg, dispersant 1kg, cosolvent 0.5kg, stabilizer 1kg, balance of distilled water supplies 100kg.
A kind of preparation method of above-mentioned composition with plant growth regulating function is:
(1)Stabilizer is stirred, fine powder is pulverized into, 50 mesh sieves are crossed, standby, the stabilizer is fine by sodium alginate, crystallite Dimension element and converted starch are 3 according to mass ratio:1:0.1 is formulated;
(2)To in stainless steel autoclave, brassin lactones and heteroauxin are added, be then slowly added into ascorbic acid and dispersion Agent, airtight heating is stirred 5 hours to 55 DEG C, is subsequently adding distilled water, cosolvent and step(1)Stabilizer after process, keeps Temperature is 33 DEG C, continues to stir 35 minutes, obtains mixed solution, and standby, the dispersant is sweet by sodium tripolyphosphate and stearic acid list Grease is 2.2 according to mass ratio:0.7 is formulated, and the cosolvent is methyl alcohol;
(3)By step(2)Gained mixed solution is lyophilized into powder, encapsulates, and obtains final product.
Embodiment 2:A kind of composition with plant growth regulating function, by the raw material preparation of following weight percents Into:Ascorbic acid 90kg, brassin lactones 0.0001kg, heteroauxin 0.0001kg, dispersant 1kg, cosolvent 0.5kg, surely Determine agent 1kg, balance of distilled water supplies 100kg.
A kind of preparation method of above-mentioned composition with plant growth regulating function is:
(1)Stabilizer is stirred, fine powder is pulverized into, 100 mesh sieves are crossed, standby, the stabilizer is by sodium alginate, crystallite Cellulose and converted starch are 3 according to mass ratio:1:0.1 is formulated;
(2)To in stainless steel autoclave, brassin lactones and heteroauxin are added, be then slowly added into ascorbic acid and dispersion Agent, airtight heating is stirred 9 hours to 75 DEG C, is subsequently adding distilled water, cosolvent and step(1)Stabilizer after process, keeps Temperature is 33 DEG C, continues to stir 35 minutes, obtains mixed solution, and standby, the dispersant is sweet by sodium tripolyphosphate and stearic acid list Grease is 2.2 according to mass ratio:0.7 is formulated, and the cosolvent is propylene glycol monomethyl ether and ethyl acetate;
(3)By step(2)Gained mixed solution is lyophilized into powder, encapsulates, and obtains final product.
Embodiment 3:A kind of composition with plant growth regulating function, by the raw material preparation of following weight percents Into:Ascorbic acid 40kg, brassin lactones 20kg, heteroauxin 12.5kg, dispersant 1kg, cosolvent 0.5kg, stabilizer 1kg, balance of distilled water supplies 100kg.
A kind of preparation method of above-mentioned composition with plant growth regulating function is:
(1)Stabilizer is stirred, fine powder is pulverized into, 80 mesh sieves are crossed, standby, the stabilizer is fine by sodium alginate, crystallite Dimension element and converted starch are 3 according to mass ratio:1:0.1 is formulated;
(2)To in stainless steel autoclave, brassin lactones and heteroauxin are added, be then slowly added into ascorbic acid and dispersion Agent, airtight heating is stirred 7 hours to 65 DEG C, is subsequently adding distilled water, cosolvent and step(1)Stabilizer after process, keeps Temperature is 33 DEG C, continues to stir 35 minutes, obtains mixed solution, and standby, the dispersant is sweet by sodium tripolyphosphate and stearic acid list Grease is 2.2 according to mass ratio:0.7 is formulated, and the cosolvent is propylene glycol monomethyl ether and methyl alcohol;
(3)By step(2)Gained mixed solution is lyophilized into powder, encapsulates, and obtains final product.
A kind of experimental study of the composition with plant growth regulating function of test example present invention gained:
1.1 subjects
In 2014, with peanut(Kind:Spend No. 14 in Shandong)For the object application present composition, research experiment.
1.2 experimental design
1 mu of peanut experimental plot is chosen, four trial zones are divided into, is respectively control group(1)And test group(3), in April 5 Day is sowed at four trial zones, and depth of planting is 3-4cm, and spacing in the rows 15cm, line-spacing is 40cm.After peanut rudiment 30 days, Different growth regulators are applied to peanut.Wherein control group applies paclobutrazol(Purchase public affairs limited in the favorable to the people agrochemical of Yancheng, Jiangsu Province Department), application process:Per mu is watered 40kg by 30g, carries out foliage-spray.Test group applies respectively three embodiment institutes of the invention Obtain composition, application process:Per mu is watered 40kg by 30g, carries out foliage-spray.
1.3 results and analysis
The impact of control group and test group to peanut yield, as shown in table 1.
The control group of table 1 and experimental group peanut yield are contrasted
From the data in table 1, it can be seen that growth of the different plant growth regulator to peanut has differences, wherein a kind of tool of present invention gained The composition for having plant growth regulating function affects to be significantly better than that and control group on peanut yield(Paclobutrazol).It is indicated above that Three embodiment resulting compositions of the invention have significant effect of increasing production to peanut, and peanut yield increases 1.034-1.469 kg/hm2Amount of increase in production is 18.93%-26.89%, and for effect of increasing production, the gained compound of the embodiment of the present invention three is to peanut Effect of increasing production is more notable.
It should be pointed out that specific embodiment is the more representational example of the present invention, it is clear that the skill of the present invention Art scheme is not limited to above-described embodiment, can also there is many variations.One of ordinary skill in the art, it is clearly public with institute of the invention Written description open or according to file is undoubted to be obtained, and is considered as this patent scope of the claimed.

Claims (9)

1. a kind of composition with plant growth regulating function, it is characterised in that prepared by the raw material of following weight percents Form:Ascorbic acid 0.001%~90%, brassin lactones 0.0001%~40%, heteroauxin 0.0001%~25%, dispersant 1% ~15%, cosolvent 0.5%~15%, stabilizer 0%~5%, balance of distilled water.
2. a kind of preparation method of the composition of plant growth regulating function according to claim 1, it is characterised in that step It is rapid as follows:
(1)Stabilizer is stirred, fine powder is pulverized into, 50-100 mesh sieves are crossed, it is standby;
(2)To in stainless steel autoclave, brassin lactones and heteroauxin are added, be then slowly added into ascorbic acid and dispersion Agent, airtight heating stirs 5-9 hours to 55-75 DEG C, is subsequently adding distilled water, cosolvent and step(1)Stablizing after process Agent, keeping temperature is 33 DEG C, continues to stir 35 minutes, obtains mixed solution, standby;
(3)By step(2)Gained mixed solution is lyophilized into powder, encapsulates, and obtains final product.
3. preparation method according to claim 2, it is characterised in that the stabilizer is by sodium alginate, microcrystalline cellulose With converted starch according to mass ratio be 3:1:0.1 is formulated.
4. preparation method according to claim 2, it is characterised in that the dispersant is by sodium tripolyphosphate and stearic acid list Glyceride is 2.2 according to mass ratio:0.7 is formulated.
5. preparation method according to claim 2, it is characterised in that the cosolvent is methyl alcohol, propylene glycol monomethyl ether and vinegar One or two in acetoacetic ester.
6. preparation method according to claim 2, it is characterised in that step(1)Cross 80 mesh sieves.
7. preparation method according to claim 2, it is characterised in that step(2)Airtight heating is to 65 DEG C.
8. preparation method according to claim 2, it is characterised in that step(2)Stirring 7 hours.
9. purposes of the composition according to claim 1 in terms of coordinate plant growth.
CN201611223031.9A 2016-12-27 2016-12-27 Composition with plant growth regulation function and preparation method Pending CN106614594A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113661994A (en) * 2021-09-15 2021-11-19 多农多收技术研究(江苏)有限公司 Product capable of improving disease resistance of plants and optimizing plant growth and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1069256A (en) * 1992-08-25 1993-02-24 桂林市农业科学研究所 A kind of efficient, multifunctional foliage fertilizer and preparation method thereof
CN1137344A (en) * 1995-06-06 1996-12-11 四川省自然资源研究所 Composite for regulating transport and distribution of xylophyte substance heeled in or injected in xylem
CN103125490A (en) * 2013-03-15 2013-06-05 刘克 Plant growth regulating agent and production process thereof
CN104521970A (en) * 2014-12-01 2015-04-22 江之光 New plant growth regulator
CN104642318A (en) * 2013-11-20 2015-05-27 任青松 Plant growth regulator
CN105613501A (en) * 2014-11-05 2016-06-01 江苏龙灯化学有限公司 Plant-growth regulator composition

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1069256A (en) * 1992-08-25 1993-02-24 桂林市农业科学研究所 A kind of efficient, multifunctional foliage fertilizer and preparation method thereof
CN1137344A (en) * 1995-06-06 1996-12-11 四川省自然资源研究所 Composite for regulating transport and distribution of xylophyte substance heeled in or injected in xylem
CN103125490A (en) * 2013-03-15 2013-06-05 刘克 Plant growth regulating agent and production process thereof
CN104642318A (en) * 2013-11-20 2015-05-27 任青松 Plant growth regulator
CN105613501A (en) * 2014-11-05 2016-06-01 江苏龙灯化学有限公司 Plant-growth regulator composition
CN104521970A (en) * 2014-12-01 2015-04-22 江之光 New plant growth regulator

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* Cited by examiner, † Cited by third party
Title
潘瑞炽: "重视植物生长调节剂的残毒问题", 《生物学通报》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113661994A (en) * 2021-09-15 2021-11-19 多农多收技术研究(江苏)有限公司 Product capable of improving disease resistance of plants and optimizing plant growth and preparation method thereof

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Application publication date: 20170510