CN106591092A - Making method of pomegranate fruit vinegar - Google Patents
Making method of pomegranate fruit vinegar Download PDFInfo
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- CN106591092A CN106591092A CN201611176320.8A CN201611176320A CN106591092A CN 106591092 A CN106591092 A CN 106591092A CN 201611176320 A CN201611176320 A CN 201611176320A CN 106591092 A CN106591092 A CN 106591092A
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- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
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Abstract
The invention belongs to the technical field of biology and particularly relates to a making method of pomegranate fruit vinegar. The method comprises the following steps of 1, raw material treatment; 2, enzymolysis; 3, filtering; 4, alcoholic fermentation treatment, wherein some fruit juice is added into a traditional Chinese medicine mixed solution composed of gymnema sylvestre schult, codonopsis pilosula, caladium, radix polygonati officinalis, oriental wormwood, dendrobium officinale, leonurus, dandelion, Chinese lobelia, licorice roots and platycodon grandiflorum, then, activated complex zymocyte is added, fermentation is performed for 5-8 d under the temperature of 25-28 DEG C, and a pomegranate fruit wine body can be obtained; juice and the traditional Chinese medicine mixing solution are mixed according to the volume size being 15:(2-4), and the added amount of the activated complex zymocyte is 0.01 that of the total mass of the juice and traditional Chinese medicine mixed solution; 5, acetic fermentation treatment; 6, sterilization of pomegranate fruit vinegar pulp under the temperature of 65 DEG C for 10-15 min, so that the pomegranate fruit vinegar is obtained. The method is easy and convenient to implement, and soft and mellow in vinegar flavor, has the layering sense, has rich fragrance and has the certain healthcare and health-preserving effect.
Description
【Technical field】
The invention belongs to biological technical field, and in particular to a kind of preparation method of red pomegranate fruit vinegar.
【Background technology】
Red pomegranate is a kind of Punica granatum L., because after maturation, peel is gained the name for pink.Red pomegranate has：The red stone in Yimeng
Pomegranate, beautiful purchase red pomegranate.The former is gained the name because of the main product of red pomegranate ground, and the latter is process technology and the raw material application because of red pomegranate
And gain the name.Red pomegranate nature and flavor are sweet, sour and astringent, warm, containing materials such as abundant vitamin C, Punica granatum L. polyphenol and anthocyanidin in fruit, have
Good toxin expelling, anti-oxidation efficacy.It is all very effective in terms of medicinal, beauty, dietetic therapy.
Traditional red pomegranate fruit vinegar manufacture method is that first the sarcocarp of red pomegranate fruit is squeezed the juice, and is then carried out red pomegranate fruit juice
Jing allotments after alcohol fermentation and acetic fermentation are made, and after red pomegranate fruit is squeezed the juice, remaining marc is not utilized, and not only makes
Into certain waste, and the yield of red pomegranate fruit vinegar is not also high, and the manufacture method of the red pomegranate fruit vinegar beverage of the present invention will fruit
Juice and marc are all utilized, and not only reduce cost, and nutritive value is also above traditional red pomegranate fruit vinegar beverage.
【The content of the invention】
It is an object of the invention to：A kind of preparation method of red pomegranate fruit vinegar, simple to operation, the soft alcohol of the smell of vinegar are provided
It is thick, with stereovision, have dense fragrance, and with certain health care's effect.
To achieve these goals, the technical solution used in the present invention is as follows：
A kind of preparation method of red pomegranate fruit vinegar, specifically includes following steps：
A：Feedstock treating：Red pomegranate fruit is cleaned with clear water, then shell is separated with sarcocarp, then by the seed in sarcocarp
Remove, take pulp, antioxidant is added toward in pulp, then carry out microwave treatment 30-50S, it is stand-by；Wherein, antioxidation
The addition of additive accounts for the 1/200-1/100 of pulp volume；
B：Enzymolysis：Pulp after processing in A is added into pectase, is digested 3 hours under the conditions of temperature is for 38 DEG C, Ran Hou
Sterilize under the conditions of 160 DEG C；
C：Filter：After pulp after sterilizing is centrifuged, is filtered, marc and fruit parts are obtained, it is stand-by；Filter
Drainage screen mesh number be 500 mesh；
D：Alcohol fermentation is processed：Take fruit parts add by Largeleaf Gymnema, Radix Codonopsis, Rhizoma Caladii Bicoloriss, Rhizoma Polygonati Odorati, Herba Artemisiae Scopariae, Herba Dendrobii,
Chinese medicine mixed liquor made by Herba Leonuri, Herba Taraxaci, Herba Lobeliae Chinensis, Radix Glycyrrhizae, Radix Platycodoniss, is subsequently adding with activation composite zymocyte, in 25-
28 DEG C fermentation 5-8 days after red pomegranate fruit wine body is obtained；Wherein fruit juice and the volume ratio of Chinese medicine mixed liquor are 15:2-4, adds
The amount of activation composite zymocyte be 0.01 times of fruit juice and Chinese medicine mixed liquor gross mass；
E：Acetic fermentation process：By red pomegranate fruit wine body be adjusted to 14 °, pH be 5 after, into wine body add marc, acetic acid
Bacterium, ferments 5-6 days at 30-35 DEG C in temperature, and air inflow during fermentation is controlled in 9-10m3/ T.hr, when detect red pomegranate fruit
When the acidity of wine body is more than 5.0g/100ml, stops ventilation, obtain red pomegranate fruit vinegar oleo stock；
F：Red pomegranate fruit vinegar oleo stock is sterilized at 65 DEG C 10-15min, red pomegranate fruit vinegar is obtained.
In the present invention, further illustrate, in step, the antioxidant be to be mixed by following raw material and
Into the tertiary butyl pair that specially mass concentration is the sodium hexametaphosphate solution of 0.5-0.8%, mass concentration is 0.01-0.02%
Resorcinol solution and mass concentration are 1-2 according to mass ratio for the ascorbic acid solution of 0.8-1.0%:2-5：After 10-20 mixing
Obtain.
In the present invention, further illustrate, in step, the frequency of the microwave treatment is 250-400MHz.
In the present invention, further illustrate, in step D, the Chinese medicine mixed liquor is by the spoon of 25-28 weight portions
Rattan, 15-25 weight portion Herba Dendrobii, 13-24 weight portion Rhizoma Caladii Bicoloriss, 7-13 weight portion Radix Platycodoniss, 8-15 weight portion Rhizoma Polygonati Odorati, 6-10 weights
Amount part Herba Artemisiae Scopariae, 8-12 weight portion Herba Leonuris, 8-14 weight portion Herba Taraxacis, 10-15 weight portion Herba Lobeliae Chinensis, 6-10 weight portion Radix Codonopsis,
5-10 weight portion Radix Glycyrrhizaes are made.
In the present invention, further illustrate, in step D, the concrete method for making of the Chinese medicine mixed liquor is：
A. in parts by weight, mixing after the chopping of Radix Codonopsis, Radix Glycyrrhizae and Herba Lobeliae Chinensis is added and is decocted in container, added appropriate
Water is heated to boiling to submergence raw material after immersion 10-20min, and after decocting 40-60min, cooling is centrifuged being filtrated to get filter
Liquid and residue, according still further to said method to residue decoction 2-3 time, last merging filtrate mix homogeneously, are obtained mixed liquor I, treat
With；
B. in parts by weight, Rhizoma Polygonati Odorati, Herba Artemisiae Scopariae, Herba Leonuri, Herba Taraxaci are crushed to mix coarse powder, with volumetric concentration is
After the swelling 2-3h of 95% ethanol load percolation equipment in, with 95% alcohol dipping 18h after, start to ooze with the speed of 3.5mL/min
Filter process, collect the percolate of 8 times of medical material amounts, it is stand-by；
C. in parts by weight, weighing addition volumetric concentration after Largeleaf Gymnema, Herba Dendrobii, Rhizoma Caladii Bicoloriss, Radix Platycodoniss are crushed is
Reflux, extract, is carried out after the immersion of 70% ethanol, extracting solution is collected after extracting repeatedly at least 20 times, the mixed extract for obtaining is treated
With；
D. the mixed liquor I that step a, b, c obtained, percolate, obtain Chinese medicine mixed liquor after mixed extract mixing.
In the present invention, further illustrate, in stepb, the size of the coarse powder is less than 5mm.
In the present invention, further illustrate, in step D, the activation composite zymocyte includes rice wine yeast, medicated beer
The combination of more than three kinds in yeast, yellow wine yeast, fruit wine yeast, wine yeast.
In the present invention, part Chinese herbal medicine efficacy effect is described below：
Largeleaf Gymnema, Chinese medicine name.For asclepiadaceae Largeleaf Gymnema fruit platymiscium Largeleaf Gymnema Gymnemasylvestre (Retz.)
Schult. root or browse.Mildly bitter flavor, it is cool in nature.GUIXIN, liver, spleen channel.The effect of with wind-expelling pain-stopping, removing toxic substances and promoting subsidence of swelling.For
Rheumatic arthralgia, laryngopharynx swelling and pain, scrofula, acute mastitis, sore scabies, eczema, innominate toxic swelling, venom.
Herba Dendrobii (scientific name：Dendrobium officinale Kimura et Migo) flavor efficacy：Sweet in the mouth, property are micro-
It is cold.Promote the production of body fluid nourishing the stomach；Nourishing YIN and clearing away heat；Lung moistening kidney tonifying；The strong waist of improving eyesight.
The perennial tuberous plant of Rhizoma Caladii Bicoloriss, often makees annual crop cultivation.Blade peltate, petiole length and it is loose, green or
Aubergine；Plant base portion forms shortening stem, and it is loose into meat bulb, referred to as " Fructus Colocasiae Esculentae " or " female taro " to build up nutrient, spherical,
It is avette, oval or block etc..Female taro has often saved a brain bud, but most strong with the axillary bud energy of middle and lower part section position, occurs
Primary tiller, forms little bulb and is referred to as " sub- taro ", then " grandson taro " occurs from sub- taro, under optimum conditions, can form great-grandson
Or great-great-grandson taro etc..Toil, temperature, with removing toxic substances and promoting subsidence of swelling, eliminating stasis to stop pain, dispelling the wind and dampness pathogens pain, treating swelling and pain by traumatic injury.
Radix Platycodoniss (Platycodon grandiflorus), another name burden flower, Radix Platycodonis, mitral flower are that perennial herb is planted
Thing, stem are high 20～120 centimetres, generally without hair, even close by undercoat, not branch, few top branch.Leaf is all verticillate, and part is taken turns
Raw stockless or to have extremely short handle to whole alternates, blade is avette, ovate-elliptic to lanceolar, and leaf is avette or ovate drapes over one's shoulders pin
Shape, flower skipper or dark violet white, can make ornamental flower；Its root can be used as medicine, and have eliminating phlegm and stopping cough, lung qi dispersing, evacuation of pus etc. to act on, the traditional Chinese medical science
Common medicine.
Rhizoma Polygonati Odorati, scientific name：Polygonatum odoratum (Mill.) Druce, is Liliaceae herbaceos perennial.Root
Stem it is horizontal walk, meat yellow-white, close raw majority fibrous roots.Blade face green, below Lycoperdon polymorphum Vitt.Flower axil life, usual 1～3 cluster life.In originating in
State southwest, but wild distribution is very wide.Cold-resistant, also shade tolerant, likes wet environment, and suitable growth is loose in what is enriched containing humus
Soil.《Collective Notes to Canon of Materia Medica》" stem is tetanic, like bamboo arrow shaft, has section for cloud." therefore have the name of Rhizoma Polygonati Odorati.The rhizome of plant can hyoscine,
Chinese medicine name is also Rhizoma Polygonati Odorati, and autumn excavates, clean, shines to softness, rubs repeatedly, and dry in the sun is dried to without hard-core, or after steaming thoroughly,
Rub to translucent, dry, cut sheet or section is used.It is sweet, put down.Attach to the lung and stomach meridians.Rhizoma Polygonati Odorati is extracted flavonoid substances and is taken off with Folium Mori extract
Oxygen nojirimycin combines to form a kind of novel substance --- and clear sugar element (cics) of pancreas is washed, is acted on blood sugar lowering, blood fat, blood pressure etc..
Herba Artemisiae Scopariae, another name Adeps Bovis seu Bubali, Tian Naili, because of dirt, Ma Xian, capillary wormwood, floss Artemisia, Herba Artemisiae Sieversianae, spire Herba Artemisiae Annuae, An Lvcao, Latin
Literary fame ArtemisiacapillarisThunb. tubular flower mesh, Compositae, origanum Artemisia Jing winters be not dead, old of Chun Zeyin and
It is raw, it is therefore named because of old or Herba Artemisiae Scopariae.Then it is changed into Artemisia to its Seedling of summer, therefore also known as Herba Artemisiae Scopariae.Folks of china now still have with rice flour make Herba Artemisiae Scopariae cake,
The custom of group.Herba Artemisiae Scopariae is cooked, and will adopt tender Seedling, it is old it is medicinal be Herba Artemisiae Scopariae.Therefore have the saying of " February Herba Artemisiae Scopariae, May Artemisia ".Distribution
Riverbank, low hillside area in the low altitude area of the country such as China, Japan, Korea, Mongolia.Herba Artemisiae Scopariae has two collection period, spring
The habit adopted in season claims " capillary wormwood "；The habit that autumn adopts claims " Herba Artemisiae Scopariae ".Meridian distribution of property and flavor：It is bitter, pungent, it is slightly cold.Returns spleen, stomach, liver, gallbladder meridian.
Can flu-prevention, control heatstroke, flu, headache heavy sensation of the body, stomachache, vomiting, fullness in chest, vapour lock dyspepsia, food stagnation of child abdominal distention, abdomen
Rush down, the disease such as menorrhagia, bleeding not during menses, skin itching and edema.
Herba Leonuri Classification system：Leonurus artemisia (Laur.) S.Y.Hu F, are Labiatae, mother wort plant
Thing, summer-flowering.Its dry aerial parts is conventional Chinese medicine, and most of China area is produced, raw to use or endure cream use.1 year or two
Year SHENGCAO this national most area is distributed, and is born in hill wasteland, ridge, meadow etc..Spend incomplete in summer riotous growth
Pluck when opening, acrid in the mouth is bitter, cool, invigorate blood circulation, silts of dispelling, regulating menstruation, disappear water, treats menoxenia, vaginal bleeding during pregnancy difficult labour, retention of placenta, product
Bruise afterwards, abdominal pain due to blood stasis, metrorrhagia and metrostaxises, rush down blood at hematuria, carbuncle swells sore.
Herba Taraxaci (Classification system：Taraxacum mongolicum Hand.-Mazz.) Compositae, Dandelion is perennial
Herbaceous plant.Root is coniform, surface sepia, shrinkage, and limb edge has wave-formed mouth or pinniform drastic crack sometimes, base portion gradually narrow Cheng Ye
, often with reddish violet, scape top aubergine is close by the long pubescence of spider's thread shape white for handle, petiole and master pulse；Head inflorescence, involucre clock
Shape, achene crineous, long pappus white, 4～October of flowering fruit bearing stage.Sweet in the mouth, puts down, nontoxic.It is sweet, it is flat to be slightly cold.Enter liver, stomach.Cure mainly
Heat-clearing and toxic substances removing, diuresis eliminating stagnation.Acute mastitiss are controlled, lymphadenitises, scrofula, malignant boil carbuncle toxin, acute conjunctivitiss, cold, fever are anxious
Property tonsillitiss, acute bronchitiss, gastritis, hepatitis, cholecystitis, urinary tract infection.
Herba Lobeliae Chinensis (scientific name：Lobelia chinensis Lour.), campanulaceae lobelia perennial herb.Stem is thin and delicate,
Crawl, take root on section, branch is upright.Leaf alternate, stockless or nearly stockless, ellipticity lanceolar is to bar shaped.Usual 1 is spent, it is estranged
The top axil of branch；Bennet is thin, and squamella is without hair；Calyx cylinder falls long cone shape；Corolla pink or white.Capsule inverted cone shape, it is long
About 6 millimeters.Seed ellipticity, slightly flat pressure are near yellowish pink.The flowering fruit bearing stage 5-10 months.Be distributed in Yangtze River in China middle and lower reaches and on the south each province
Area；Other various countries of Asia to the east of India are also distributed.Herb is medicinal, containing various alkaloids, have heat-clearing and toxic substances removing, inducing diuresis to remove edema it
Effect, controls venom, cirrhotic ascites, advanced schistosomiasises ascites, appendicitis effect etc..Cortex Acanthopanciss, Chinese medicine name.For Araliaceae
The dry root skin of plant acanthopanax gracilistyluses Acanthopanar gracilist μ lusW.W.Smith.Summer, two season of autumn excavation root,
Clean, strip root bark, dry.Acrid in the mouth, hardship, it is warm in nature.Liver and kidney channel.For Bi condition, muscles and bones impotence, children's walking retardation in children, body void are weary
Power, edema, tinea pedis.
Radix Codonopsis (scientific name；Codonopsis pilosula (Franch.) Nannf.) Codonopsises of Radix Linderae section, perennial herb
Plant, has milk.Stem foot tool majority warty stem trace, the normal hypertrophy of root are in fusiform or fusiform cylinder, and stem winds, sterile or first
End is blossomed, yellow green or yellow-white, and alternate of the leaf on stem and side shoot, petiole have thin short seta, and blade is avette or narrow avette,
Edge has wavy crenation, above green, below celadon, spend, and petiole alternate or be bordering on opposite, on corolla
Position, wealthy mitriform, sliver equilateral triangle, flower pesticide are elongated, and seed is most, and avette, the 7-10 months yield positive results.With invigorating the spleen and replenishing QI, it is good for
The effect of spleen lung benefiting.
Radix Glycyrrhizae (scientific name：Glycyrrhiza uralensis Fisch) another name：State is old, Herba Hedyotis cantonensis, Glycyrrhiza uralensis Fisch., sweet
Son.Pulse family, Glycyrrhiza perennial herb, root are sturdy with root stock, are a kind of tonification Chinese herbal medicine.To a kind of good medicine of human body,
Medicinal part is root and rhizome, and Medicinal Materials Characters root is in cylindrical, 25～100 centimetres of length, 0.6～3.5 centimetre of diameter.Crust is elastic
Differ, surface rufous or taupe brown.In cylinder, there is bud scar on surface, has marrow in the middle part of section rhizome.Feeble QI, taste are sweet and special.
Indication heat-clearing and toxic substances removing, expelling phlegm for arresting cough, gastral cavity abdomen etc..
In sum, as a result of above-mentioned technical proposal, the invention has the beneficial effects as follows：
1st, the effect of the Chinese medicine mixed liquor added in the present invention, is to increase the wind of red pomegranate fruit wine after alcohol fermentation first
Taste and stereovision, second, increase health-care effect, specially Largeleaf Gymnema has blood sugar lowering reducing blood pressure and blood fat, wind-dispelling removing heat from blood, detumescence
Pain relieving, stomach invigorating diuresis, Herba Dendrobii have nourishing the stomach of promoting the production of body fluid, the effect of lung moistening kidney tonifying, Rhizoma Caladii Bicoloriss removing toxic substances and promoting subsidence of swelling, eliminating stasis to stop pain, Fructus Citri tangerinae
Stalk is acted on lung qi dispersing, eliminating phlegm and relieving cough, is had enhancing antiinflammatory and immunization, is monarch drug altogether；Rhizoma Polygonati Odorati yin nourishing, moisturize, relieving restlessness, Herba Artemisiae Scopariae
Clearing away damp-heat, Herba Leonuri promoting blood circulation, inducing diuresis to remove edema, Herba Taraxaci heat-clearing and toxic substances removing are ministerial drug altogether；Herba Lobeliae Chinensis diuresis antibacterial, Radix Codonopsis invigorating middle warmer benefit
Gas, strengthening spleen and tonifying lung, are adjuvant drug altogether；Radix Glycyrrhizae mediation property of medicine makes medicine；Follow monarch principle compatibility between active compound, all medicines share,
Respectively arrogate to oneself its work(, bring out the best in each other again, play appetite-stimulating indigestion-relieving altogether, benefiting qi and nourishing blood, the work(of suppressing liver-YANG and reach reducing blood sugar and blood fat blood pressure lowering
Effect.Meanwhile, the Chinese medicine mixed liquor added serves the intension of abundant red pomegranate fruit vinegar, Chinese medicine mixing during the fermentation
Liquid contains the effective ingredient in every medical material, adds broken red pomegranate pulp body adjust the solid-liquid of slurry in liquid form
Content ratio, can also control the content of total acid in alcoholic fermentation process, be avoided that the later stage of deacidification is processed.It is multiple through the applicant
Test prove, by very add the application Chinese medicine mixed liquor after, the total acid content in alcoholic fermentation process in below 5g/L, and
And, the backflow that Largeleaf Gymnema, Herba Dendrobii, Rhizoma Caladii Bicoloriss, Radix Platycodoniss are obtained without reflux, extract, but directly carry out after steaming and decocting
During the Chinese medicine mixed liquor of compatibility adds pulp, the total acid content in alcoholic fermentation process reaches 10g/L, by Rhizoma Polygonati Odorati, Herba Artemisiae Scopariae, Herba Leonuri
Grass, Herba Taraxaci obtain percolate without seepage pressure effects but the Chinese medicine mixed liquor addition pulp of compatibility are carried out after direct steaming and decocting
In, the total acid content in alcoholic fermentation process reaches 13g/L.Comprehensively get on very well, the Chinese medicine mixed liquor of addition can adjust ethanol and send out
Ferment factor, and health-care effect can be increased to red pomegranate fruit slurry raw material, increase the mouthfeel level of red pomegranate fruit vinegar.
2nd, the combination of the antioxidant of described the application, will isolate after carrying out crushing in view of red pomegranate fruit first
The acidic materials such as substantial amounts of acidic materials, overall slurry meta-acid, the red pomegranate fruit acid for itself discharging, citric acid have certain
Oxidation resistance, other Organic substances while crushing in red pomegranate fruit are from free state (vitamin, saccharide, protein, fat
Etc.), with the aerial time lengthening of broken exposure, afterwards, content of organics is reduced 2 hours after crushing and being broken
8%-15%, in order to prevent Organic substance in free state easily with air contact and be oxidized so that the content of organics in slurry
Reduce, the applicant has certain effect to the slurry for crushing in extra addition antioxidant through research, and what detection was obtained has
The content of machine thing compare not additionally add antioxidant slurry content of organics be higher by 5%-10%, add first
Stable in properties in sour environment containing ascorbic acid in antioxidant, the stable effect for playing promotion suppresses vitamin
C decomposes, and the red pomegranate fruit slurry after additionally the ascorbic acid of addition prevents to crush is from keeping original acidity, it will destruction is red
The former composition dynamic model of Punica granatum L., will certainly lose the content of material of red pomegranate fruit script, try through this research worker for this
Issue after examination and approval so that Yuanping City's weighing apparatus of red pomegranate fruit slurry is not broken
Bad, sodium hexametaphosphate solution can improve the viscosity of slurry in addition, suppress vitamin to decompose, and can play certain sedimentation work
With so that the ion of free state can be in the state of supernatant, and more conducively antioxidant plays which prevents slurry from aoxidizing
Effect, and the tert-butylhydroquinone of one of component of antioxidant has a higher oxidation resistance, can be rapidly
The substance protection of supernatant free state is got up, and after supernatant has non-oxidizability in the material of sedimentation, is played
Certain insulation blocking is deposited in the effect of the material of bottom, and the combination of the antioxidant of the application is not only only capable of single
The effect for having played them cleverly can also combine realize strengthen antioxidation and safeguard red pomegranate fruit slurry dynamic put down
Weighing apparatus；Three key of unstability double bond in the dissociant in broken slurry can be will be switched off in stable after additional microwave treatment
Phase, reinforces the stability of material.
3rd, the characteristics of mulriple yeasts of the invention have preferably active, every Yeasts have which peculiar, it is contained
Yeast flora is different, each have their own profitable strain, and also has different physical characteristics, cooperates and would be even more beneficial to send out
Ferment, improves the efficiency of fermentation, reduces the time of fermentation.
【Specific embodiment】
All features disclosed in this specification, or disclosed all methods or during the step of, except mutually exclusive
Feature and/or step beyond, can combine by any way.
Any feature disclosed in this specification (including any accessory claim, summary), unless specifically stated otherwise,
Replaced by other equivalent or alternative features with similar purpose.I.e., unless specifically stated otherwise, each feature is a series of
An example in equivalent or similar characteristics.
Embodiment 1：
A kind of preparation method of red pomegranate fruit vinegar, specifically includes following steps：
A：Feedstock treating：Red pomegranate fruit is cleaned with clear water, then shell is separated with sarcocarp, then by the seed in sarcocarp
Remove, take pulp, it is 0.01% to add toward in pulp by the sodium hexametaphosphate solution, mass concentration that mass concentration is 0.5%
It is 1 according to mass ratio that tert-butylhydroquinone solution and mass concentration are 0.8% ascorbic acid solution:2：Obtain after 10 mixing
Antioxidant, then frequency be 250MHz under the conditions of carry out microwave treatment 30S, it is stand-by；Wherein, antioxidant
Addition account for the 1/200 of pulp volume；
B：Enzymolysis：Pulp after processing in A is added into pectase, is digested 3 hours under the conditions of temperature is for 38 DEG C, Ran Hou
Sterilize under the conditions of 160 DEG C；
C：Filter：After pulp after sterilizing is centrifuged, is filtered, marc and fruit parts are obtained, it is stand-by；Filter
Drainage screen mesh number be 500 mesh；
D：Alcohol fermentation is processed：Take fruit parts to add by the Largeleaf Gymnema of 25 weight portions, 15 weight portion Herba Dendrobii, 13 weights
Amount part Rhizoma Caladii Bicoloriss, 7 weight portion Radix Platycodoniss, 8 weight portion Rhizoma Polygonati Odorati, 6 weight portion Herba Artemisiae Scopariaes, 8 weight portion Herba Leonuris, 8 weight portion Herba Taraxacis, 10
Weight portion Herba Lobeliae Chinensis, 6 weight portion Radix Codonopsis, Chinese medicine mixed liquor made by 5 weight portion Radix Glycyrrhizaes, are subsequently adding with by rice wine yeast, beer
Brewer yeast, yellow wine yeast are 1 according to volume ratio:2:The 1 activation composite zymocyte for combining, after fermenting 5-8 days at 25 DEG C i.e.
Red pomegranate fruit wine body is obtained；Wherein fruit juice and the volume ratio of Chinese medicine mixed liquor are 15:2, the activation composite zymocyte of addition
Measure 0.01 times for fruit juice and Chinese medicine mixed liquor gross mass；
The concrete method for making of the Chinese medicine mixed liquor is：
A. in parts by weight, mixing after the chopping of Radix Codonopsis, Radix Glycyrrhizae and Herba Lobeliae Chinensis is added and is decocted in container, added appropriate
Water after immersion 10min, is heated to boiling to submergence raw material, and after decocting 40min, cooling is centrifuged being filtrated to get filtrate and residual
Slag, according still further to said method to residue decoction 2 times, last merging filtrate mix homogeneously, is obtained mixed liquor I, stand-by；
B. in parts by weight, it is that size is thick less than the mixing of 5mm Rhizoma Polygonati Odorati, Herba Artemisiae Scopariae, Herba Leonuri, Herba Taraxaci to be crushed
Powder, with volumetric concentration be the swelling 2h of 95% ethanol after load percolation equipment in, with 95% alcohol dipping 18h after, with 3.5mL/min
Speed start percolation process, collect 8 times of medical material amounts percolate, it is stand-by；
C. in parts by weight, weighing addition volumetric concentration after Largeleaf Gymnema, Herba Dendrobii, Rhizoma Caladii Bicoloriss, Radix Platycodoniss are crushed is
Reflux, extract, is carried out after the immersion of 70% ethanol, extracting solution is collected after extracting repeatedly at least 20 times, the mixed extract for obtaining is treated
With；
D. the mixed liquor I that step a, b, c obtained, percolate, obtain Chinese medicine mixed liquor after mixed extract mixing
E：Acetic fermentation process：By red pomegranate fruit wine body be adjusted to 14 °, pH be 5 after, into wine body add marc, acetic acid
Bacterium, ferments 6 days at 35 DEG C in temperature, and air inflow during fermentation is controlled in 10m3/ T.hr, when the acid for detecting red pomegranate fruit wine body
When degree is more than 5.0g/100ml, stops ventilation, obtain red pomegranate fruit vinegar oleo stock；
F：Red pomegranate fruit vinegar oleo stock is sterilized at 65 DEG C 15min, red pomegranate fruit vinegar is obtained.
Embodiment 2：
A kind of preparation method of red pomegranate fruit vinegar, specifically includes following steps：
A：Feedstock treating：Red pomegranate fruit is cleaned with clear water, then shell is separated with sarcocarp, then by the seed in sarcocarp
Remove, take pulp, it is 0.012% to add toward in pulp by the sodium hexametaphosphate solution, mass concentration that mass concentration is 0.65%
Tert-butylhydroquinone solution and ascorbic acid solution that mass concentration is 0.9% be 2 according to mass ratio:5：After 20 mixing
The antioxidant for arriving, then carries out microwave treatment 50S under the conditions of frequency is 400MHz, stand-by；Wherein, antioxidation addition
The addition of agent accounts for the 1/100 of pulp volume；
B：Enzymolysis：Pulp after processing in A is added into pectase, is digested 3 hours under the conditions of temperature is for 38 DEG C, Ran Hou
Sterilize under the conditions of 160 DEG C；
C：Filter：After pulp after sterilizing is centrifuged, is filtered, marc and fruit parts are obtained, it is stand-by；Filter
Drainage screen mesh number be 500 mesh；
D：Alcohol fermentation is processed：Take fruit parts to add by the Largeleaf Gymnema of 28 weight portions, 25 weight portion Herba Dendrobii, 24 weights
Amount part Rhizoma Caladii Bicoloriss, 13 weight portion Radix Platycodoniss, 15 weight portion Rhizoma Polygonati Odorati, 10 weight portion Herba Artemisiae Scopariaes, 12 weight portion Herba Leonuris, 8-14 weight portion Pus
Herba Taraxaci, 15 weight portion Herba Lobeliae Chinensis, 10 weight portion Radix Codonopsis, Chinese medicine mixed liquor made by 10 weight portion Radix Glycyrrhizaes, are subsequently adding with by beer
Brewer yeast, yellow wine yeast, fruit wine yeast, wine yeast are 1 according to volume ratio:2:1：The 1 activation composite fermentation for combining
Bacterium, is obtained red pomegranate fruit wine body after fermenting 8 days at 28 DEG C；Wherein fruit juice and the volume ratio of Chinese medicine mixed liquor are 15:4, plus
The amount of the activation composite zymocyte for entering is 0.01 times of fruit juice and Chinese medicine mixed liquor gross mass；
The concrete method for making of the Chinese medicine mixed liquor is：
A. in parts by weight, mixing after the chopping of Radix Codonopsis, Radix Glycyrrhizae and Herba Lobeliae Chinensis is added and is decocted in container, added appropriate
Water after immersion 20min, is heated to boiling to submergence raw material, and after decocting 60min, cooling is centrifuged being filtrated to get filtrate and residual
Slag, according still further to said method to residue decoction 3 times, last merging filtrate mix homogeneously, is obtained mixed liquor I, stand-by；
B. in parts by weight, it is that size is thick less than the mixing of 5mm Rhizoma Polygonati Odorati, Herba Artemisiae Scopariae, Herba Leonuri, Herba Taraxaci to be crushed
Powder, with volumetric concentration be the swelling 3h of 95% ethanol after load percolation equipment in, with 95% alcohol dipping 18h after, with 3.5mL/min
Speed start percolation process, collect 8 times of medical material amounts percolate, it is stand-by；
C. in parts by weight, weighing addition volumetric concentration after Largeleaf Gymnema, Herba Dendrobii, Rhizoma Caladii Bicoloriss, Radix Platycodoniss are crushed is
Reflux, extract, is carried out after the immersion of 70% ethanol, extracting solution is collected after extracting repeatedly at least 20 times, the mixed extract for obtaining is treated
With；
D. the mixed liquor I that step a, b, c obtained, percolate, obtain Chinese medicine mixed liquor after mixed extract mixing
E：Acetic fermentation process：By red pomegranate fruit wine body be adjusted to 14 °, pH be 5 after, into wine body add marc, acetic acid
Bacterium, ferments 5 days at 30 DEG C in temperature, and air inflow during fermentation is controlled in 9m3/ T.hr, when the acid for detecting red pomegranate fruit wine body
When degree is more than 5.0g/100ml, stops ventilation, obtain red pomegranate fruit vinegar oleo stock；
F：Red pomegranate fruit vinegar oleo stock is sterilized at 65 DEG C 10min, red pomegranate fruit vinegar is obtained.
Embodiment 3：
A kind of preparation method of red pomegranate fruit vinegar, specifically includes following steps：
A：Feedstock treating：Red pomegranate fruit is cleaned with clear water, then shell is separated with sarcocarp, then by the seed in sarcocarp
Remove, take pulp, it is 0.02% to add toward in pulp by the sodium hexametaphosphate solution, mass concentration that mass concentration is 0.8%
It is 2 according to mass ratio that tert-butylhydroquinone solution and mass concentration are 1.0% ascorbic acid solution:3：Obtain after 12 mixing
Antioxidant, then frequency be 300MHz under the conditions of carry out microwave treatment 40S, it is stand-by；Wherein, antioxidant
Addition account for the 1/150 of pulp volume；
B：Enzymolysis：Pulp after processing in A is added into pectase, is digested 3 hours under the conditions of temperature is for 38 DEG C, Ran Hou
Sterilize under the conditions of 160 DEG C；
C：Filter：After pulp after sterilizing is centrifuged, is filtered, marc and fruit parts are obtained, it is stand-by；Filter
Drainage screen mesh number be 500 mesh；
D：Alcohol fermentation is processed：Take fruit parts to add by the Largeleaf Gymnema of 26 weight portions, 19 weight portion Herba Dendrobii, 16 weights
Amount part Rhizoma Caladii Bicoloriss, 9 weight portion Radix Platycodoniss, 10 weight portion Rhizoma Polygonati Odorati, 7 weight portion Herba Artemisiae Scopariaes, 10 weight portion Herba Leonuris, 11 weight portion Pus are public
English, 12 weight portion Herba Lobeliae Chinensis, 8 weight portion Radix Codonopsis, Chinese medicine mixed liquor made by 7 weight portion Radix Glycyrrhizaes, are subsequently adding with by yellow wine ferment
Mother, fruit wine yeast, wine yeast are 1 according to volume ratio:2:The 1 activation composite zymocyte for combining, ferments at 25-28 DEG C
Red pomegranate fruit wine body is obtained after 7 days；Wherein fruit juice and the volume ratio of Chinese medicine mixed liquor are 15:3, the activation of addition is compound to be sent out
The amount of yeast-like fungi is 0.01 times of fruit juice and Chinese medicine mixed liquor gross mass；
The concrete method for making of the Chinese medicine mixed liquor is：
A. in parts by weight, mixing after the chopping of Radix Codonopsis, Radix Glycyrrhizae and Herba Lobeliae Chinensis is added and is decocted in container, added appropriate
Water after immersion 15min, is heated to boiling to submergence raw material, and after decocting 50min, cooling is centrifuged being filtrated to get filtrate and residual
Slag, according still further to said method to residue decoction 3 times, last merging filtrate mix homogeneously, is obtained mixed liquor I, stand-by；
B. in parts by weight, it is that size is thick less than the mixing of 5mm Rhizoma Polygonati Odorati, Herba Artemisiae Scopariae, Herba Leonuri, Herba Taraxaci to be crushed
Powder, with volumetric concentration be the swelling 2.5h of 95% ethanol after load percolation equipment in, with 95% alcohol dipping 18h after, with 3.5mL/
The speed of min starts percolation process, collects the percolate of 8 times of medical material amounts, stand-by；
C. in parts by weight, weighing addition volumetric concentration after Largeleaf Gymnema, Herba Dendrobii, Rhizoma Caladii Bicoloriss, Radix Platycodoniss are crushed is
Reflux, extract, is carried out after the immersion of 70% ethanol, extracting solution is collected after extracting repeatedly at least 20 times, the mixed extract for obtaining is treated
With；
D. the mixed liquor I that step a, b, c obtained, percolate, obtain Chinese medicine mixed liquor after mixed extract mixing
E：Acetic fermentation process：By red pomegranate fruit wine body be adjusted to 14 °, pH be 5 after, into wine body add marc, acetic acid
Bacterium, ferments 5.5 days at 32 DEG C in temperature, and air inflow during fermentation is controlled in 9.5m3/ T.hr, when detecting red pomegranate fruit wine body
Acidity be more than 5.0g/100ml when, stop ventilation, obtain red pomegranate fruit vinegar oleo stock；
F：Red pomegranate fruit vinegar oleo stock is sterilized at 65 DEG C 12min, red pomegranate fruit vinegar is obtained.
Comparative example 1：
Concrete steps are same as Example 3, and difference is to be not added with antioxidation addition after red pomegranate fruit is broken in step A
Agent, enters next step after directly using microwave treatment.
Comparative example 2：
Concrete steps are substantially the same manner as Example 3, and difference is that Chinese medicine mixing is not added with during the alcohol fermentation of step D is processed
Liquid.
Comparative example 3：
Concrete steps are same as Example 3, and the activation composite zymocyte added in step D of difference is single rice wine ferment
It is female.
The red pomegranate fruit vinegar that embodiment 1-3 and comparative example 1-3 are prepared carries out total acid content detection, and what is used is identical
Fruit is crushed red pomegranate, is detected that the total content in Organic substance is 284mg/L, is then used embodiment 1-3 and comparative example respectively
Slurry after the A process of the step of 1-3, after placing 2 hours, detects the total content (A) of Organic substance again；When completing acetic fermentation
Between, testing result see the table below：.
1 testing result information slip of table
As seen from the above table, controlled all in antioxidation, fermentation natural law reduction, total acid content using technical scheme
With obvious advantage.
The red pomegranate fruit vinegar that embodiment 1-3 is obtained is to young (22-29 year), middle aged (30-40 year), old age (50-60
Year) people taste, randomly select per group of 50 people in stage, before having a meal every night, drink 100mL, with appetizing effect, and
The crowd for being adapted to have " three high " (hypertension, hyperlipidemia, hyperglycemia) drinks, and is had a meal after eating again, blood pressure blood fat blood glucose
Content is not higher by 2.5% before not drinking.And the vinegar obtained using technical solution of the present invention is presented pale red and is all clarified
Bright, no suspended substance, the smell of vinegar it is soft it is mellow, with stereovision, have dense fragrance.
Described above is the detailed description for preferably possible embodiments of the invention, but embodiment is not limited to this
Bright patent claim, the equal change completed under the technical spirit suggested by all present invention or modification change, all should belong to
In the covered the scope of the claims of the present invention.
Claims (7)
1. a kind of preparation method of red pomegranate fruit vinegar, it is characterised in that：Specifically include following steps：
A：Feedstock treating：Red pomegranate fruit is cleaned with clear water, then shell is separated with sarcocarp, then the seed in sarcocarp is gone
Remove, take pulp, antioxidant is added toward in pulp, then carry out microwave treatment 30-50S, it is stand-by；Wherein, antioxidation adds
Plus the addition of agent accounts for the 1/200-1/100 of pulp volume；
B：Enzymolysis：Pulp after processing in A is added into pectase, is digested 3 hours under the conditions of temperature is for 38 DEG C, then 160
Sterilize under the conditions of DEG C；
C：Filter：After pulp after sterilizing is centrifuged, is filtered, marc and fruit parts are obtained, it is stand-by；The mistake of filtration
The mesh number of filter screen is 500 mesh；
D：Alcohol fermentation is processed：Take fruit parts to add by Largeleaf Gymnema, Radix Codonopsis, Rhizoma Caladii Bicoloriss, Rhizoma Polygonati Odorati, Herba Artemisiae Scopariae, Herba Dendrobii, Herba Leonuri
Chinese medicine mixed liquor made by grass, Herba Taraxaci, Herba Lobeliae Chinensis, Radix Glycyrrhizae, Radix Platycodoniss, is subsequently adding with activation composite zymocyte, at 25-28 DEG C
Fermentation was obtained red pomegranate fruit wine body after 5-8 days；Wherein fruit juice and the volume ratio of Chinese medicine mixed liquor are 15:2-4, the work of addition
The amount for changing composite zymocyte is 0.01 times of fruit juice and Chinese medicine mixed liquor gross mass；
E：Acetic fermentation process：By red pomegranate fruit wine body be adjusted to 14 °, pH be 5 after, into wine body add marc, acetic acid bacteria,
Temperature is fermented 5-6 days at 30-35 DEG C, and air inflow during fermentation is controlled in 9-10m3/ T.hr, when detecting red pomegranate fruit wine body
When acidity is more than 5.0g/100ml, stops ventilation, obtain red pomegranate fruit vinegar oleo stock；
F：Red pomegranate fruit vinegar oleo stock is sterilized at 65 DEG C 10-15min, red pomegranate fruit vinegar is obtained.
2. method according to claim 1, it is characterised in that：In step, the antioxidant is by following original
Material is mixed, and specially mass concentration is the sodium hexametaphosphate solution of 0.5-0.8%, mass concentration for 0.01-0.02%'s
Tert-butylhydroquinone solution and mass concentration are 1-2 according to mass ratio for the ascorbic acid solution of 0.8-1.0%:2-5：10-
Obtain after 20 mixing.
3. method according to claim 1, it is characterised in that：In step, the frequency of the microwave treatment is 250-
400MHz。
4. method according to claim 1, it is characterised in that：In step D, the Chinese medicine mixed liquor is by 25-28 weights
The Largeleaf Gymnema of amount part, 15-25 weight portion Herba Dendrobii, 13-24 weight portion Rhizoma Caladii Bicoloriss, 7-13 weight portion Radix Platycodoniss, 8-15 weight portions
Rhizoma Polygonati Odorati, 6-10 weight portion Herba Artemisiae Scopariaes, 8-12 weight portion Herba Leonuris, 8-14 weight portion Herba Taraxacis, 10-15 weight portion Herba Lobeliae Chinensis, 6-10
Weight portion Radix Codonopsis, 5-10 weight portion Radix Glycyrrhizaes are made.
5. method according to claim 4, it is characterised in that：In step D, the specifically side of making of the Chinese medicine mixed liquor
Method is：
A. in parts by weight, mixing after the chopping of Radix Codonopsis, Radix Glycyrrhizae and Herba Lobeliae Chinensis is added and is decocted in container, add appropriate water extremely
Submergence raw material, after immersion 10-20min, is heated to boiling, after decocting 40-60min, cooling, be centrifuged being filtrated to get filtrate and
Residue, according still further to said method to residue decoction 2-3 time, last merging filtrate mix homogeneously, is obtained mixed liquor I, stand-by；
B. in parts by weight, Rhizoma Polygonati Odorati, Herba Artemisiae Scopariae, Herba Leonuri, Herba Taraxaci are crushed to mix coarse powder, is 95% second with volumetric concentration
After the swelling 2-3h of alcohol load percolation equipment in, with 95% alcohol dipping 18h after, with the speed of 3.5mL/min start percolation process,
The percolate of 8 times of medical material amounts is collected, it is stand-by；
C. in parts by weight, weigh and after Largeleaf Gymnema, Herba Dendrobii, Rhizoma Caladii Bicoloriss, Radix Platycodoniss are crushed, add volumetric concentration to be 70% second
Reflux, extract, is carried out after alcohol immersion, after extracting repeatedly at least 20 times, extracting solution is collected, it is by the mixed extract for obtaining, stand-by；
D. the mixed liquor I that step a, b, c obtained, percolate, obtain Chinese medicine mixed liquor after mixed extract mixing.
6. method according to claim 5, it is characterised in that：In stepb, the size of the coarse powder is less than 5mm.
7. method according to claim 1, it is characterised in that：In step D, the activation composite zymocyte includes rice wine
The combination of more than three kinds in yeast, beer yeast, yellow wine yeast, fruit wine yeast, wine yeast.
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Application publication date: 20170426 |