CN106635729A - Preparation method of hawthorn vinegar - Google Patents
Preparation method of hawthorn vinegar Download PDFInfo
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- CN106635729A CN106635729A CN201611177466.4A CN201611177466A CN106635729A CN 106635729 A CN106635729 A CN 106635729A CN 201611177466 A CN201611177466 A CN 201611177466A CN 106635729 A CN106635729 A CN 106635729A
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- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
- C12J1/00—Vinegar; Preparation or purification thereof
- C12J1/04—Vinegar; Preparation or purification thereof from alcohol
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Abstract
The invention belongs to the technical field of biology, and particularly relates to a preparation method of hawthorn vinegar. The method comprises the following steps of (A) raw material treatment; (B) enzymolysis; (C) filtering; (D) alcoholic fermentation treatment: adding one part of taken fruit juice to a traditional Chinese medicinal mixed solution prepared from gymnema sylvestre, liquorice, houttuynia cordata, black gardenia jasminoides peel, trogopterus dung, dendrobium officinale, radix scrophulariae, wampee roots, poria cocos, astragalus membranaceus and fig leaves, adding activated compound zymophyte and fermenting at 25-28 DEG C for 5-8 days to obtain hawthorn wine, wherein the volume ratio of the fruit juice to the traditional Chinese medicinal mixed solution is 15:(2-4), and the amount of the added activated compound zymophyte is 0.01 times of total mass of the fruit juice and the traditional Chinese medicinal mixed solution; (E) acetic fermentation treatment; and (F) sterilizing hawthorn vinegar puree at 65 DEG C for 10-15 minutes to obtain the hawthorn vinegar. The method is simple and convenient to operate, and the hawthorn vinegar is soft and mellow in taste, has a sense of depth and a thick aroma and also has certain healthcare and health-preservation effects.
Description
【Technical field】
The invention belongs to biological technical field, and in particular to a kind of preparation method of Hawthorn Vinegar.
【Background technology】
Containing abundant carbohydrate, dietary fiber, calcium, iron, potassium and vitamin C in hawthorn, with very high nutrition
And medical value.Often eating haw products can whet the appetite, and improve the health care of sleep, and keep constant, the prevention of arterial of calcium in bone and blood
It is atherosis, make one to promote longevity, therefore hawthorn is considered as " long-lived fruit " by people.Hawthorn is cultivated as the special product fruit tree of China
It is with a long history, aboundresources, the history eaten raw using it, be used as medicine and processed nearly 3000, its tree body strong stress resistance, pest and disease damage
It is few, it is easy to produce pollution-free, safety, high-quality, health, nutritious green fruit and Organic Fruit.
Relevant formula, theory and modern pharmacology, nutrition according to Chinese medicated food, using modern food technique
, advanced animal nutrition, hawthorn are appropriately coordinated with other materials, the development of new products, and the depth of Efforts To Develop hawthorn adds
Work technical research, improves traditional processing method, and the loss of hawthorn function factor is reduced as far as possible, gives full play to hawthorn uniqueness
" edible+medicinal " value, health-care series foodstuff of the Devoting Major Efforts To Developing based on hawthorn, the frontier that developing hawthorn utilizes will be produced
Fabulous economic benefit and social benefit.
Vinegar is a kind of traditional food of China.In China, vinegar being brewageed and eats as long as history has more than one thousand years.It is Chinese many
There is the custom of vinegar in area.With the development of food scientific technology, people have deeper understanding to effect of vinegar.Modern section
Think that vinegar plays the role of following aspect to health of curing the disease：1st, dispelling fatigue；2nd, the acid-base balance of blood is adjusted, people is maintained
Vivo environment it is relatively stable；3rd, help digest, be conducive to the absorption of nutrient content in food；4th, anti-aging, suppresses and reduces
The formation of peroxide in human aging process；5th, with very strong sterilizing ability, staphylococcus in enteron aisle, big can be killed
Enterobacteria, Halophiles etc.；6th, strengthen liver function, enhance metabolism；7th, expansion of blood vessels, advantageously reduces blood pressure, prevents the heart
The generation of vascular diseases；8th, strengthen renal function, there are diuresis, and glucose in urine content can be reduced；9th, fat excessive in vivo can be made
Fat is changed into physical consumption and falls, and promotes the metabolism of sugar and protein, can prevent and treat obesity；10th, cancer-resisting substance is also contained in vinegar.
Traditional Hawthorn Vinegar preparation method is that first the pulp of hawthorn is squeezed the juice, and then haw juice is carried out into alcoholic fermentation and vinegar
After acid fermentation Jing allotment be made, hawthorn after squeezing the juice remaining pomace be not utilized, not only cause certain waste, and
The yield of Hawthorn Vinegar is not also high, and the preparation method of the Hawthorn vinegar beverage of the present invention is all utilized fruit juice and pomace, not only
Cost is reduced, nutritive value is also above traditional Hawthorn vinegar beverage.
【The content of the invention】
It is an object of the invention to：A kind of preparation method of Hawthorn Vinegar is provided, it is simple to operation, the smell of vinegar it is soft it is mellow,
With stereovision, there is dense fragrance, and with certain health care's effect.
To achieve these goals, the technical solution used in the present invention is as follows：
A kind of preparation method of Hawthorn Vinegar, specifically includes following steps：
A：Feedstock treating：Hawthorn is cleaned with clear water, then separates shell and pulp, then the seed in pulp is gone
Remove, take pulp, antioxidant is added toward in pulp, then carry out microwave treatment 35-55S, it is stand-by；Wherein, it is anti-oxidant to add
Plus the addition of agent accounts for the 1/350-1/200 of pulp volume；
B：Enzymolysis：Pulp after processing in A is added into pectase, is digested 2 hours under the conditions of temperature is for 45 DEG C, Ran Hou
Sterilize under the conditions of 180 DEG C；
C：Filter：After pulp after sterilizing is centrifuged, is filtered, pomace and fruit parts are obtained, it is stand-by；Its
In, the mesh number of the screen pack of filtration is 200 mesh；
D：Alcoholic fermentation is processed：Take fruit parts to add by gymnema sylvestre, Radix Glycyrrhizae, cordate houttuynia, Fructus Gardeniae skin, excrementum pteropi, iron
Chinese medicine mixed liquor made by the skin stem of noble dendrobium, radix scrophulariae, Chinese wampee root, Poria cocos, the Radix Astragali, common fig leaf juice, is subsequently adding with activation composite fermentation
Bacterium, after fermenting 5-8 days at 25-28 DEG C Hawthorn Fruit Wine body is obtained；Wherein fruit juice and the volume ratio of Chinese medicine mixed liquor are 15:2-4,
The amount of the activation composite zymocyte of addition is 0.01 times of fruit juice and Chinese medicine mixed liquor gross mass；
E：Acetic fermentation process：By Hawthorn Fruit Wine body be adjusted to 14 °, pH be 5 after, into wine body add pomace, acetic acid bacteria,
Temperature is fermented 5-6 days at 30-35 DEG C, and air inflow during fermentation is controlled in 9-10m3/ T.hr, when the acidity for detecting Hawthorn Fruit Wine body
During more than 5.0g/100ml, stop ventilation, obtain Hawthorn Vinegar magma；
F：By Hawthorn Vinegar magma at 65 DEG C sterilization 10-15min, obtain Hawthorn Vinegar.
In the present invention, further illustrate, in step, the antioxidant be to be mixed by following raw material and
Into the tertiary butyl pair that specially mass concentration is the sodium hexametaphosphate solution of 0.5-0.8%, mass concentration is 0.01-0.02%
Resorcinol solution and mass concentration are 1-2 according to mass ratio for the ascorbic acid solution of 0.8-1.0%:2-5：After 10-20 mixing
Obtain.
In the present invention, further illustrate, in step, the frequency of the microwave treatment is 250-400MHz.
In the present invention, further illustrate, in step D, the Chinese medicine mixed liquor is by the spoon of 25-28 weight portions
Rattan, 15-25 weight portion dendrobium candidums, 13-24 weight portion cordate houttuynias, 7-13 weight portion common fig leaf juicves, 8-15 weight portion Fructus Gardeniaes
Skin, 6-10 weight portion excrementum pteropis, 8-12 weight portion radix scrophulariaes, 8-14 weight portion Chinese wampee roots, 10-15 weight portion Poria cocos, 6-10 weight
Part Radix Glycyrrhizae, the 5-10 weight portion Radixs Astragali are made.
In the present invention, further illustrate, in step D, the concrete method for making of the Chinese medicine mixed liquor is：
A. in parts by weight, mixing after the chopping of Radix Glycyrrhizae, the Radix Astragali and Poria cocos is added and is decocted in container, add appropriate water
To submergence raw material, after immersion 10-20min, boiling is heated to, after decocting 40-60min, cooling is centrifuged being filtrated to get filtrate
And residue, residue is decocted 2-3 time according still further to said method, last merging filtrate is simultaneously well mixed, and mixed liquor I is obtained, stand-by；
B. in parts by weight, Fructus Gardeniae skin, excrementum pteropi, radix scrophulariae, Chinese wampee root are crushed to mix meal, uses volumetric concentration
To be fitted in diacolation equipment after the swelling 2-3h of 95% ethanol, with 95% alcohol dipping 18h after, started with the speed of 3.5mL/min
Diacolation process, collects the percolate of 8 times of medicinal material amounts, stand-by；
C. in parts by weight, weigh after gymnema sylvestre, dendrobium candidum, cordate houttuynia, common fig leaf juice are crushed and add volumetric concentration
To carry out refluxing extraction after the immersion of 70% ethanol, extract is collected after at least 20 times are extracted repeatedly, by the mixed extract for obtaining,
It is stand-by；
D. Chinese medicine mixed liquor is obtained after the mixed liquor I, percolate, the mixed extract mixing that obtain step a, b, c.
In the present invention, further illustrate, in stepb, the particle size of the meal is less than 5mm.
In the present invention, further illustrate, in step D, the activation composite zymocyte includes rice wine yeast, beer
The combination of more than three kinds in yeast, yellow wine yeast, fruit wine yeast, wine yeast.
Part Chinese herbal medicine efficacy effect is described below in the present invention：
Gymnema sylvestre, Chinese medicine name.For Asclepiadaceae gymnema sylvestre fruit platymiscium gymnema sylvestre Gymnemasylvestre (Retz.)
Schult. root or browse.Mildly bitter flavor, it is cool in nature.The thoughts of returning home, liver, the spleen channel.The effect of with wind-expelling pain-stopping, removing toxicity for detumescence.For
Arthralgia due to wind-dampness, abscess of throat, scrofula, acute mastitis, sore scabies, eczema, nameless sores or boils, venomous snake bite.
Dendrobium candidum (scientific name：Dendrobium officinale Kimura et Migo) flavor efficacy：Sweet, property is micro-
It is cold.Promote the production of body fluid nourishing the stomach；Nourishing Yin and clearing heat；Moistening lung kidney-nourishing；The strong waist of improving eyesight.
Common fig leaf juice scientific name Ficus carica L., cure mainly diarrhea due to damp-heat, under band, hemorrhoid, carbuncle swells pain, scrofula.It is used as medicine
Position leaf.Nature and flavor are sweet, micro-pungent, mild-natured.Return through enter the heart, large intestine channel.Effect clearing away damp-heat, solves sore, swelling and pain relieving.
Cordate houttuynia (Latin Houttuynia Cordala Thunb), it is pungent, tremble with fear, return lung Jing.Can subside a swelling and treat sore, diuresis is removed
It is wet, stomach strengthening and digestion promoting, with controlling real heat, heat toxin, damp evil, hemorrhoidal hemorrhage, retention of heat in the spleen and stomach etc..
Excrementum pteropi Latin literary fame:Angelica sinensis, it is sweet, it is warm in nature.Excrementum pteropi effect and effect：Promoting blood circulation to remove blood stasis,
Fries charcoal hemostasis.For trusted subordinate's extravasated blood, dysmenorrhoea, blood stasis is through closing, curing postpartum bleeding is suffered from abdominal pain；Fry charcoal and control metrostaxis.
Fructus Gardeniae skin Latin literary fame：Itoa orientalis Hemsl., bitter is cold in nature.Enter the heart, liver, lung, stomach.Tool
There are heat-clearing, purging intense heat, removing toxic substances, cool blood.
Radix scrophulariae Latin literary fame:Calceolaria crenatiflora. are sweet, bitter, salty；Cold nature.Return lung, stomach, kidney
Jing.Clearing heat and cooling blood, purging intense heat and detonicating, enriching yin.Control warm heresy to join the army, cave in pericardium, febrile virulent maculae, the deep red polydipsia of consumption of YIN caused by febrile disease, tongue, Tianjin wound
Constipation, hectic fever due to yin labor is coughed, hot eyes, pharyngalgia, scrofula, diphtheria, carbuncle sore tumefacting virus.
Poria cocos Latin literary fame:Poria cocos (schw.) Wolf, property slightly sweet flavor is put down, enter the heart, lung, the spleen channel.With excreting dampness
Li Shui, strengthening the spleen and stomach, effect of antitoxic heart-soothing and sedative.
Chinese wampee root (Latin literary fame:Root of Chinese Wampee), pungent slight bitter is warm in nature.Return stomach, Liver Channel.Main gas
Indigestion pain, stomachache, colic, treating rheumatic ostealgia, dysmenorrhoea.
Radix Glycyrrhizae (scientific name：Glycyrrhiza uralensis Fisch) another name：State is old, Herba Hedyotis cantonensis, Glycyrrhiza Uralensis, sweet
Son.Pulse family, Glycyrrhiza perennial herb, root is sturdy with root-like stock, is a kind of help Chinese herbal medicine.To a kind of good medicine of human body,
Medicinal part is root and rhizome, and Medicinal Materials Characters root is long 25～100 centimetres in cylinder, 0.6～3.5 centimetre of diameter.Crust is elastic
Differ, surface rufous or taupe brown.In cylinder, there is bud scar on surface to rhizome, and there is marrow at section middle part.Gas is micro-, and taste is sweet and special.
Indication is clearing heat and detoxicating, expelling phlegm and arresting coughing, gastral cavity abdomen etc..
Radix Astragali Radix Astragali, nature and flavor：It is sweet, tepor.Return through：Return lung, spleen, liver and kidney channel.It has enhancing body to exempt from
Epidemic disease function, liver protection, diuresis, anti-aging, resisting stress, step-down and wide antibacterial action.
In sum, as a result of above-mentioned technical proposal, the invention has the beneficial effects as follows：
1st, the effect of the Chinese medicine mixed liquor added in the present invention, be first will increase after alcoholic fermentation the local flavor of Hawthorn Fruit Wine and
Stereovision, second, increase health-care effect, there is specially gymnema sylvestre hypoglycemic reducing blood pressure and blood fat, wind-dispelling cool blood, detumescence to stop
Bitterly, stomach invigorating diuresis, dendrobium candidum have nourishing the stomach of promoting the production of body fluid, the effect of moistening lung kidney-nourishing, cordate houttuynia antipyretic and antidote functions, common fig leaf juice tool
There is a surname's lung, eliminating phlegm and relieving cough effect has enhancing anti-inflammatory and immunization, is altogether monarch drug in a prescription；Fructus Gardeniae skin yin-nourishing, moisturize, it is relieving restlessness, five clever
Fat liver protection cardiac stimulant, radix scrophulariae promoting blood circulation, inducing diuresis to remove edema, Chinese wampee root open chest gas, control herria, control hernia, are altogether ministerial drug；Poria cocos profit
Urine antibacterial, Radix Glycyrrhizae mediation property of medicine are altogether adjutant；Radix Astragali invigorating qi for consolidating superficies, inducing diuresis for removing edema are used as making medicine；The monarch and his subjects' assistant is followed between active compound
Principle compatibility, all medicines share is respectively arrogated to oneself its work(, is brought out the best in each other again, play appetite-stimulating indigestion-relieving altogether, benefiting qi and nourishing blood, the work(of suppressing liver-YANG and
Up to the hypotensive effect of reducing blood sugar and blood fat.Meanwhile, the Chinese medicine mixed liquor added serves during the fermentation abundant hawthorn
The intension of vinegar, Chinese medicine mixed liquor contains the active ingredient in every medicinal material, and in liquid form the broken hawthorn slurry of addition can also
The solid-liquid content ratio of adjustment slurry, can also control the content of total acid in alcoholic fermentation process, and the later stage for being avoided that deacidification is processed.Jing
Crossing the applicant's test of many times proves, after the Chinese medicine mixed liquor for adding very much the application, the total acid in alcoholic fermentation process contains
Amount is in below 5g/L, also, the phegma that gymnema sylvestre, dendrobium candidum, cordate houttuynia, common fig leaf juice are obtained without refluxing extraction
But the Chinese medicine mixed liquor that compatibility is directly carried out after boiling is added in pulp, the total acid content in alcoholic fermentation process reaches 10g/
L, obtains Fructus Gardeniae skin, excrementum pteropi, radix scrophulariae, Chinese wampee root percolate but directly carries out compatibility after boiling without seepage pressure effects
Chinese medicine mixed liquor add pulp in, the total acid content in alcoholic fermentation process reaches 13g/L.Comprehensively get on very well, the Chinese medicine of addition
Mixed liquor can adjust alcoholic fermentation factor, and can increase health-care effect to hawthorn slurry raw material, increase the mouthfeel layer of Hawthorn Vinegar
It is secondary.
2nd, the combination of the antioxidant of described the application, carries out to isolate after crushing in a large number first in view of hawthorn
Acidic materials, overall slurry meta-acid, the acidic materials such as crataegolic acid, citric acid of release itself have certain anti-oxidant energy
Power, other organic matters while crushing in hawthorn from free state (vitamin, carbohydrate, protein, fat etc.), with broken
Broken to expose aerial time lengthening, afterwards, content of organics reduces 8%-15% to 2 hours after crushing and being broken, is
Prevent organic matter in free state easily with air contact and be oxidized so that the content of organics reduction in slurry, the application
People has certain effect in extra addition antioxidant through research to the slurry for crushing, and detects the content phase of the organic matter for obtaining
5%-10% is higher by than the slurry content of organics without extra addition antioxidant, the antioxidant for adding first
In it is stable in properties in sour environment containing ascorbic acid, the stable effect for playing promotion suppresses vitamin C to decompose, and additionally adds
Plus ascorbic acid prevent it is broken after hawthorn slurry from keeping original acidity, it will the former composition dynamic analog of destruction hawthorn
Type, will certainly lose the content of material of hawthorn script, find along with calgon is molten through this researcher test for this
The comprehensively certain acidic materials of liquid energy so that Yuanping City's weighing apparatus of hawthorn slurry is not destroyed, and in addition sodium hexametaphosphate solution can be improved
The viscosity of slurry, suppresses vitamin to decompose, and can play certain settlement action so that the ion of free state can be presented
The state of clear liquid, more conducively antioxidant play its prevent slurry aoxidize effect, and the component of antioxidant it
One tert-butylhydroquinone has higher oxidation resistance, rapidly can play the substance protection of supernatant free state
Come, and supernatant has after non-oxidizability in the material of sedimentation, serves certain insulation blocking and is deposited in bottom
The effect of material, the combination of the antioxidant of the application is not only only capable of the single effect for having played them can also be cleverly
Combination is realized plus strong antioxidant action and the dynamic equilibrium for safeguarding hawthorn slurry；Energy after additional microwave treatment is by broken slurry
Dissociant in the key of unstability double bond three will be switched off in stable phase, reinforce the stability of material.
3rd, the characteristics of mulriple yeasts of the invention have preferably active, every Yeasts have its peculiar, it is contained
Yeast flora is different, each have their own profitable strain, and also has different physical characteristics, cooperates and would be even more beneficial to send out
Ferment, improves the efficiency of fermentation, reduces the time of fermentation.
【Specific embodiment】
All features disclosed in this specification, or disclosed all methods or during the step of, except mutually exclusive
Feature and/or step beyond, can combine by any way.
Any feature disclosed in this specification (including any accessory claim, summary), unless specifically stated otherwise,
Equivalent by other or with similar purpose alternative features are replaced.I.e., unless specifically stated otherwise, each feature is a series of
An example in equivalent or similar characteristics.
Embodiment 1：
A kind of preparation method of Hawthorn Vinegar, specifically includes following steps：
A：Feedstock treating：Hawthorn is cleaned with clear water, then separates shell and pulp, then the seed in pulp is gone
Remove, take pulp, add toward in pulp by the sodium hexametaphosphate solution that mass concentration is 0.5%, the spy that mass concentration is 0.01%
It is 1 according to mass ratio that butylhydroquinone's solution and mass concentration are 0.8% ascorbic acid solution:2：Obtain after 10 mixing
Antioxidant, then carries out microwave treatment 35S under the conditions of frequency is 250MHz, stand-by；Wherein, antioxidant
Addition accounts for the 1/200 of pulp volume；
B：Enzymolysis：Pulp after processing in A is added into pectase, is digested 2 hours under the conditions of temperature is for 45 DEG C, Ran Hou
Sterilize under the conditions of 180 DEG C；
C：Filter：After pulp after sterilizing is centrifuged, is filtered, pomace and fruit parts are obtained, it is stand-by；Its
In, the mesh number of the screen pack of filtration is 200 mesh；
D：Alcoholic fermentation is processed：Take fruit parts to add by gymnema sylvestre, 15 weight portion dendrobium candidums, 13 weights of 25 weight portions
Amount part cordate houttuynia, 7 weight portion common fig leaf juicves, 8 weight portion Fructus Gardeniae skins, 6 weight portion excrementum pteropis, 8 weight portion radix scrophulariaes, 8 weight portions
Chinese wampee root, 10 weight portion Poria cocos, 6 weight portion Radix Glycyrrhizaes, Chinese medicine mixed liquor made by the 5 weight portion Radixs Astragali, are subsequently adding with by rice wine
Yeast, brewer's yeast, yellow wine yeast are 1 according to volume ratio:2:The 1 activation composite zymocyte for combining, ferment 5-8 at 25 DEG C
Hawthorn Fruit Wine body is obtained after it；Wherein fruit juice and the volume ratio of Chinese medicine mixed liquor are 15:2, the activation composite zymocyte of addition
Amount be 0.01 times of fruit juice and Chinese medicine mixed liquor gross mass；
The concrete method for making of the Chinese medicine mixed liquor is：
A. in parts by weight, mixing after the chopping of Radix Glycyrrhizae, the Radix Astragali and Poria cocos is added and is decocted in container, add appropriate water
To submergence raw material, after immersion 10min, boiling is heated to, after decocting 40min, cooling is centrifuged being filtrated to get filtrate and residual
Slag, decocts 2 times according still further to said method to residue, and last merging filtrate is simultaneously well mixed, and mixed liquor I is obtained, stand-by；
B. in parts by weight, Fructus Gardeniae skin, excrementum pteropi, radix scrophulariae, Chinese wampee root are crushed and is less than the mixed of 5mm for particle size
Close meal, with volumetric concentration be the swelling 2h of 95% ethanol after be fitted in diacolation equipment, with 95% alcohol dipping 18h after, with
The speed of 3.5mL/min starts diacolation process, collects the percolate of 8 times of medicinal material amounts, stand-by；
C. in parts by weight, weigh after gymnema sylvestre, dendrobium candidum, cordate houttuynia, common fig leaf juice are crushed and add volumetric concentration
To carry out refluxing extraction after the immersion of 70% ethanol, extract is collected after at least 20 times are extracted repeatedly, by the mixed extract for obtaining,
It is stand-by；
D. Chinese medicine mixed liquor is obtained after the mixed liquor I, percolate, the mixed extract mixing that obtain step a, b, c
E：Acetic fermentation process：By Hawthorn Fruit Wine body be adjusted to 14 °, pH be 5 after, into wine body add pomace, acetic acid bacteria,
Temperature is fermented 6 days at 35 DEG C, and air inflow during fermentation is controlled in 10m3/ T.hr, when the acidity for detecting Hawthorn Fruit Wine body is more than
During 5.0g/100ml, stop ventilation, obtain Hawthorn Vinegar magma；
F：By Hawthorn Vinegar magma at 65 DEG C sterilization 15min, obtain Hawthorn Vinegar.
Embodiment 2：
A kind of preparation method of Hawthorn Vinegar, specifically includes following steps：
A：Feedstock treating：Hawthorn is cleaned with clear water, then separates shell and pulp, then the seed in pulp is gone
Remove, take pulp, it is 0.012% to add toward in pulp by the sodium hexametaphosphate solution, mass concentration that mass concentration is 0.65%
It is 2 according to mass ratio that tert-butylhydroquinone solution and mass concentration are 0.9% ascorbic acid solution:5：Obtain after 20 mixing
Antioxidant, then frequency be 400MHz under the conditions of carry out microwave treatment 55S, it is stand-by；Wherein, antioxidant
Addition account for the 1/100 of pulp volume；
B：Enzymolysis：Pulp after processing in A is added into pectase, is digested 2 hours under the conditions of temperature is for 45 DEG C, Ran Hou
Sterilize under the conditions of 180 DEG C；
C：Filter：After pulp after sterilizing is centrifuged, is filtered, pomace and fruit parts are obtained, it is stand-by；Its
In, the mesh number of the screen pack of filtration is 200 mesh；
D：Alcoholic fermentation is processed：Take fruit parts to add by gymnema sylvestre, 25 weight portion dendrobium candidums, 24 weights of 28 weight portions
Amount part cordate houttuynia, 13 weight portion common fig leaf juicves, 15 weight portion Fructus Gardeniae skins, 10 weight portion excrementum pteropis, 12 weight portion radix scrophulariaes, 8-14
Weight portion Chinese wampee root, 15 weight portion Poria cocos, 10 weight portion Radix Glycyrrhizaes, Chinese medicine mixed liquor made by the 10 weight portion Radixs Astragali, are subsequently adding
With by brewer's yeast, yellow wine yeast, fruit wine yeast, wine yeast according to volume ratio be 1:2:1：1 activation for combining is answered
Zymophyte is closed, Hawthorn Fruit Wine body is obtained after fermenting 8 days at 28 DEG C；Wherein fruit juice and the volume ratio of Chinese medicine mixed liquor are 15:4,
The amount of the activation composite zymocyte of addition is 0.01 times of fruit juice and Chinese medicine mixed liquor gross mass；
The concrete method for making of the Chinese medicine mixed liquor is：
A. in parts by weight, mixing after the chopping of Radix Glycyrrhizae, the Radix Astragali and Poria cocos is added and is decocted in container, add appropriate water
To submergence raw material, after immersion 20min, boiling is heated to, after decocting 60min, cooling is centrifuged being filtrated to get filtrate and residual
Slag, decocts 3 times according still further to said method to residue, and last merging filtrate is simultaneously well mixed, and mixed liquor I is obtained, stand-by；
B. in parts by weight, Fructus Gardeniae skin, excrementum pteropi, radix scrophulariae, Chinese wampee root are crushed and is less than the mixed of 5mm for particle size
Close meal, with volumetric concentration be the swelling 3h of 95% ethanol after be fitted in diacolation equipment, with 95% alcohol dipping 18h after, with
The speed of 3.5mL/min starts diacolation process, collects the percolate of 8 times of medicinal material amounts, stand-by；
C. in parts by weight, weigh after gymnema sylvestre, dendrobium candidum, cordate houttuynia, common fig leaf juice are crushed and add volumetric concentration
To carry out refluxing extraction after the immersion of 70% ethanol, extract is collected after at least 20 times are extracted repeatedly, by the mixed extract for obtaining,
It is stand-by；
D. Chinese medicine mixed liquor is obtained after the mixed liquor I, percolate, the mixed extract mixing that obtain step a, b, c
E：Acetic fermentation process：By Hawthorn Fruit Wine body be adjusted to 14 °, pH be 5 after, into wine body add pomace, acetic acid bacteria,
Temperature is fermented 5 days at 30 DEG C, and air inflow during fermentation is controlled in 9m3/ T.hr, when the acidity for detecting Hawthorn Fruit Wine body is more than
During 5.0g/100ml, stop ventilation, obtain Hawthorn Vinegar magma；
F：By Hawthorn Vinegar magma at 65 DEG C sterilization 10min, obtain Hawthorn Vinegar.
Embodiment 3：
A kind of preparation method of Hawthorn Vinegar, specifically includes following steps：
A：Feedstock treating：Hawthorn is cleaned with clear water, then separates shell and pulp, then the seed in pulp is gone
Remove, take pulp, add toward in pulp by the sodium hexametaphosphate solution that mass concentration is 0.8%, the spy that mass concentration is 0.02%
It is 2 according to mass ratio that butylhydroquinone's solution and mass concentration are 1.0% ascorbic acid solution:3：Obtain after 12 mixing
Antioxidant, then carries out microwave treatment 40S under the conditions of frequency is 300MHz, stand-by；Wherein, antioxidant
Addition accounts for the 1/150 of pulp volume；
B：Enzymolysis：Pulp after processing in A is added into pectase, is digested 2 hours under the conditions of temperature is for 45 DEG C, Ran Hou
Sterilize under the conditions of 180 DEG C；
C：Filter：After pulp after sterilizing is centrifuged, is filtered, pomace and fruit parts are obtained, it is stand-by；Its
In, the mesh number of the screen pack of filtration is 200 mesh；
D：Alcoholic fermentation is processed：Take fruit parts to add by gymnema sylvestre, 19 weight portion dendrobium candidums, 16 weights of 26 weight portions
Amount part cordate houttuynia, 9 weight portion common fig leaf juicves, 10 weight portion Fructus Gardeniae skins, 7 weight portion excrementum pteropis, 10 weight portion radix scrophulariaes, 11 weight
Part Chinese wampee root, 12 weight portion Poria cocos, 8 weight portion Radix Glycyrrhizaes, Chinese medicine mixed liquor made by the 7 weight portion Radixs Astragali, are subsequently adding with by Huang
Brewer yeast, fruit wine yeast, wine yeast are 1 according to volume ratio:2:The 1 activation composite zymocyte for combining, at 25-28 DEG C
Fermentation is obtained Hawthorn Fruit Wine body after 7 days；Wherein fruit juice and the volume ratio of Chinese medicine mixed liquor are 15:3, the activation of addition is compound to be sent out
The amount of yeast-like fungi is 0.01 times of fruit juice and Chinese medicine mixed liquor gross mass；
The concrete method for making of the Chinese medicine mixed liquor is：
A. in parts by weight, mixing after the chopping of Radix Glycyrrhizae, the Radix Astragali and Poria cocos is added and is decocted in container, add appropriate water
To submergence raw material, after immersion 15min, boiling is heated to, after decocting 50min, cooling is centrifuged being filtrated to get filtrate and residual
Slag, decocts 3 times according still further to said method to residue, and last merging filtrate is simultaneously well mixed, and mixed liquor I is obtained, stand-by；
B. in parts by weight, Fructus Gardeniae skin, excrementum pteropi, radix scrophulariae, Chinese wampee root are crushed and is less than the mixed of 5mm for particle size
Close meal, with volumetric concentration be the swelling 2.5h of 95% ethanol after be fitted in diacolation equipment, with 95% alcohol dipping 18h after, with
The speed of 3.5mL/min starts diacolation process, collects the percolate of 8 times of medicinal material amounts, stand-by；
C. in parts by weight, weigh after gymnema sylvestre, dendrobium candidum, cordate houttuynia, common fig leaf juice are crushed and add volumetric concentration
To carry out refluxing extraction after the immersion of 70% ethanol, extract is collected after at least 20 times are extracted repeatedly, by the mixed extract for obtaining,
It is stand-by；
D. Chinese medicine mixed liquor is obtained after the mixed liquor I, percolate, the mixed extract mixing that obtain step a, b, c
E：Acetic fermentation process：By Hawthorn Fruit Wine body be adjusted to 14 °, pH be 5 after, into wine body add pomace, acetic acid bacteria,
Temperature is fermented 5.5 days at 32 DEG C, and air inflow during fermentation is controlled in 9.5m3/ T.hr, when the acidity for detecting Hawthorn Fruit Wine body is more than
During 5.0g/100ml, stop ventilation, obtain Hawthorn Vinegar magma；
F：By Hawthorn Vinegar magma at 65 DEG C sterilization 12min, obtain Hawthorn Vinegar.
Comparative example 1：
Concrete steps are same as Example 3, and difference is that hawthorn is not added with antioxidant after crushing in step A, directly
Connect using after microwave treatment enter next step.
Comparative example 2：
Concrete steps are substantially the same manner as Example 3, and difference is that Chinese medicine mixing is not added with during the alcoholic fermentation of step D is processed
Liquid.
Comparative example 3：
Concrete steps are same as Example 3, and the activation composite zymocyte added in step D of difference is single rice wine ferment
It is female.
The Hawthorn Vinegar that embodiment 1-3 and comparative example 1-3 are prepared carries out total acid content detection, the identical hawthorn for using
Crushed, detected that the total content in organic matter is 284mg/L, then respectively using embodiment 1-3 and the step of comparative example 1-3
Slurry after A process, after placing 2 hours, detects the total content (A) of organic matter again；Complete acetic fermentation time, testing result
See the table below：.
The testing result situation table of table 1
| Detection project | A(mg/L) | Total acid content g/L | Fermentation number of days/day |
| Embodiment 1 | 254 | 4.5 | 6 |
| Embodiment 2 | 289 | 4.1 | 5 |
| Embodiment 3 | 278 | 4.4 | 5.5 |
| Comparative example 1 | 213 | 4.1 | 5.5 |
| Comparative example 2 | 275 | 13 | 5.5 |
| Comparative example 3 | 272 | 4.2 | 5.5 |
As seen from the above table, controlled all in anti-oxidant, fermentation number of days reduction, total acid content using technical scheme
With obvious advantage.
The Hawthorn Vinegar that embodiment 1-3 is obtained is to young (22-29 year), middle aged (30-40 year), old (50-60 year)
People tastes, and randomly selects per group of 50 people in stage, and before having a meal every night 50mL is drunk, and with appetizing effect, and is adapted to have
The crowd of " three high " (hypertension, high fat of blood, hyperglycaemia) drinks, and is had a meal again after eating, and the content of blood pressure blood fat blood sugar is not
2.5% be higher by before not drinking.And pale red is presented for the vinegar obtained using technical solution of the present invention and all clear, nothing are outstanding
Float, the smell of vinegar it is soft it is mellow, with stereovision, have dense fragrance.
Described above is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this
Bright patent claim, the equal change completed under the technical spirit suggested by all present invention or modification change, all should belong to
Cover the scope of the claims in the present invention.
Claims (7)
1. a kind of preparation method of Hawthorn Vinegar, specifically includes following steps：
A：Feedstock treating：Hawthorn is cleaned with clear water, then separates shell and pulp, then the seed in pulp is removed, take
Pulp, antioxidant is added toward in pulp, then carries out microwave treatment 35-55S, stand-by；Wherein, antioxidant
Addition accounts for the 1/350-1/200 of pulp volume；
B：Enzymolysis：Pulp after processing in A is added into pectase, is digested 2 hours under the conditions of temperature is for 45 DEG C, then 180
Sterilize under the conditions of DEG C；
C：Filter：After pulp after sterilizing is centrifuged, is filtered, pomace and fruit parts are obtained, it is stand-by；Wherein, mistake
The mesh number of the screen pack of filter is 200 mesh；
D：Alcoholic fermentation is processed：Take fruit parts to add by gymnema sylvestre, Radix Glycyrrhizae, cordate houttuynia, Fructus Gardeniae skin, excrementum pteropi, iron sheet stone
Chinese medicine mixed liquor made by dry measure used in former times, radix scrophulariae, Chinese wampee root, Poria cocos, the Radix Astragali, common fig leaf juice, is subsequently adding and uses activation composite zymocyte,
25-28 DEG C fermentation 5-8 days after Hawthorn Fruit Wine body is obtained；Wherein fruit juice and the volume ratio of Chinese medicine mixed liquor are 15:2-4, adds
The amount of activation composite zymocyte be 0.01 times of fruit juice and Chinese medicine mixed liquor gross mass；
E：Acetic fermentation process：By Hawthorn Fruit Wine body be adjusted to 14 °, pH be 5 after, into wine body add pomace, acetic acid bacteria, in temperature
Ferment 5-6 days at 30-35 DEG C, air inflow during fermentation is controlled in 9-10m3/ T.hr, when the acidity for detecting Hawthorn Fruit Wine body is more than
During 5.0g/100ml, stop ventilation, obtain Hawthorn Vinegar magma；
F：By Hawthorn Vinegar magma at 65 DEG C sterilization 10-15min, obtain Hawthorn Vinegar.
2. method according to claim 1, it is characterised in that in step, the antioxidant is by following original
Material is mixed, and specially mass concentration is sodium hexametaphosphate solution, the mass concentration of 0.5-0.8% for 0.01-0.02%'s
Tert-butylhydroquinone solution and mass concentration are 1-2 according to mass ratio for the ascorbic acid solution of 0.8-1.0%:2-5：10-
Obtain after 20 mixing.
3. method according to claim 1, it is characterised in that in step, the frequency of the microwave treatment is 250-
400MHz。
4. method according to claim 1, it is characterised in that in step D, the Chinese medicine mixed liquor is by 25-28 weights
The gymnema sylvestre of amount part, 15-25 weight portion dendrobium candidums, 13-24 weight portion cordate houttuynias, 7-13 weight portion common fig leaf juicves, 8-15 weights
Amount part Fructus Gardeniae skin, 6-10 weight portion excrementum pteropis, 8-12 weight portion radix scrophulariaes, 8-14 weight portion Chinese wampee roots, 10-15 weight portion Fu
Siberian cocklebur, 6-10 weight portion Radix Glycyrrhizaes, the 5-10 weight portion Radixs Astragali are made.
5. method according to claim 1, it is characterised in that in step D, the specifically side of making of the Chinese medicine mixed liquor
Method is：
A. in parts by weight, will mix in addition decoction container after the chopping of Radix Glycyrrhizae, the Radix Astragali and Poria cocos, add appropriate water to leaching
No raw material, after immersion 10-20min, be heated to boiling, after decocting 40-60min, cooling is centrifuged being filtrated to get filtrate and residual
Slag, decocts 2-3 time according still further to said method to residue, and last merging filtrate is simultaneously well mixed, and mixed liquor I is obtained, stand-by；
B. in parts by weight, Fructus Gardeniae skin, excrementum pteropi, radix scrophulariae, Chinese wampee root are crushed to mix meal, is with volumetric concentration
Be fitted into after the swelling 2-3h of 95% ethanol in diacolation equipment, with 95% alcohol dipping 18h after, start to ooze with the speed of 3.5mL/min
Filter process, collect the percolate of 8 times of medicinal material amounts, it is stand-by；
C. in parts by weight, weighing addition volumetric concentration after gymnema sylvestre, dendrobium candidum, cordate houttuynia, common fig leaf juice are crushed is
Refluxing extraction is carried out after the immersion of 70% ethanol, after at least 20 times are extracted repeatedly extract is collected, the mixed extract for obtaining is treated
With；
D. Chinese medicine mixed liquor is obtained after the mixed liquor I, percolate, the mixed extract mixing that obtain step a, b, c.
6. method according to claim 5, it is characterised in that in stepb, the particle size of the meal is less than 5mm.
7. method according to claim 1, it is characterised in that in step D, the activation composite zymocyte includes rice wine
The combination of more than three kinds in yeast, brewer's yeast, yellow wine yeast, fruit wine yeast, wine yeast.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108570397A (en) * | 2018-06-21 | 2018-09-25 | 广西壮族自治区林业科学研究院 | A kind of preparation method of crataegus jingxiensis Li vinegar |
| CN108902598A (en) * | 2018-06-21 | 2018-11-30 | 广西壮族自治区林业科学研究院 | A kind of crataegus jingxiensis Li health-care vinegar beverage and preparation method thereof |
| CN115386449A (en) * | 2022-08-23 | 2022-11-25 | 张传福 | Traditional Chinese medicine solid vinegar and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103387926A (en) * | 2013-07-18 | 2013-11-13 | 苏州市天灵中药饮片有限公司 | Fruit vinegar for clearing heat and moistening intestines and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103387926A (en) * | 2013-07-18 | 2013-11-13 | 苏州市天灵中药饮片有限公司 | Fruit vinegar for clearing heat and moistening intestines and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108570397A (en) * | 2018-06-21 | 2018-09-25 | 广西壮族自治区林业科学研究院 | A kind of preparation method of crataegus jingxiensis Li vinegar |
| CN108902598A (en) * | 2018-06-21 | 2018-11-30 | 广西壮族自治区林业科学研究院 | A kind of crataegus jingxiensis Li health-care vinegar beverage and preparation method thereof |
| CN108902598B (en) * | 2018-06-21 | 2021-08-13 | 广西壮族自治区林业科学研究院 | Jingxi fig hawthorn health-care vinegar beverage and preparation method thereof |
| CN108570397B (en) * | 2018-06-21 | 2021-08-13 | 广西壮族自治区林业科学研究院 | Preparation method of Jingxi Daguo hawthorn vinegar |
| CN115386449A (en) * | 2022-08-23 | 2022-11-25 | 张传福 | Traditional Chinese medicine solid vinegar and preparation method thereof |
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