CN106590180A - Anti-rust specimen holder - Google Patents
Anti-rust specimen holder Download PDFInfo
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- CN106590180A CN106590180A CN201611145293.8A CN201611145293A CN106590180A CN 106590180 A CN106590180 A CN 106590180A CN 201611145293 A CN201611145293 A CN 201611145293A CN 106590180 A CN106590180 A CN 106590180A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D101/00—Coating compositions based on cellulose, modified cellulose, or cellulose derivatives
- C09D101/08—Cellulose derivatives
- C09D101/26—Cellulose ethers
- C09D101/28—Alkyl ethers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Lubricants (AREA)
- Paints Or Removers (AREA)
Abstract
The invention provides an anti-rust specimen holder. A layer of anti-rust film is arranged outside the specimen holder. The anti-rust film is prepared from, by mass, 15-23 parts of sodium hexametaphosphate, 5-11 parts of sodium oxide, 11-16 parts of methyl cellulose, 3-7 parts of magnesium chloride, 5-13 parts of monopotassium phosphate, 2-8 parts of aluminum hydroxide, 2-6 parts of zirconium oxide, 5-8 parts of citric acid, 1-4 parts of triethanolamine, 3-8 parts of hydroxy propyl distarch phosphate, 3-7 parts of nano silicon dioxide, 10-17 parts of sodium dodecyl benzene sulfonate, 3-6 parts of organic silicon and ethylene glycol copolymer wax, 0.3-0.7 part of auxiliary material, 2-4 parts of cross-linking agent, 1-3 parts of anti-rust auxiliary, 1-3 parts of adhesive and 10-20 parts of deionized water. The anti-rust performance of the specimen holder is improved, and the service life is prolonged.
Description
Technical field
The present invention relates to a kind of specimen mounting, a kind of particularly antirust specimen mounting.
Background technology
To extend the service life of mild steel or low-alloy steel, often to its brush coating, steel structure coating coating it
Before, it is necessary to the tarnish resistance of steel construction Service Environment is seen clearly, to select rational coating system and coating process；Often try now
Sample rack all has corrosion resistant performance, and corrosion resistant but seldom has, and antirusting paint can protect metal surfaces from big gas and water etc.
Chemistry or the coating of electrochemical corrosion, coating antirusting paint in metal surface can effectively avoid various corrosive goodses in air
The direct invasion of matter so that maximized prolongation metal useful life.Steel construction, chemical industry equipment, pipeline and machinery set
It is standby often to apply antirusting paint to protect material.
The content of the invention
The technical problem to be solved is the shortcoming for overcoming prior art, there is provided a kind of good antirust property, is used
The specimen mounting of life-span length.
The present invention solves the technical scheme of above technical problem：A kind of antirust specimen mounting is provided,：Outside the specimen mounting
One layer of antirust film is provided with, the antirust film includes according to the mass fraction following：Calgon：15-23 parts, sodium oxide molybdena：
5-11 parts, methylcellulose：11-16 parts, magnesium chloride：3-7 parts, potassium dihydrogen phosphate：5-13 parts, aluminium hydroxide：2-8 parts, oxidation
Zirconium：2-6 parts, citric acid：5-8 parts, triethanolamine：1-4 parts, hydroxypropyl PASELLI EASYGEL：3-8 parts, nano silicon：3-
7 parts, neopelex：10-17 parts, organosilicon ethylene glycol EVA wax：3-6 parts, auxiliary material：0.3-0.7 parts, You Jirong
Agent：2-5 parts, crosslinking agent：2-4 parts, antirust auxiliary agent：1-3 parts, binding agent：1-3 parts, deionized water：10-20 parts；
The auxiliary material is compound rare-earth, and the compound rare-earth includes by mass percentage following components：Dysprosium：12-14%, cerium：
23-26%, praseodymium：9-14%, neodymium：3-6%, remaining is lanthanum element, and above lanthanide rare each component sum is 100%；
The crosslinking agent is polyethylene or haloflex；
The antirust auxiliary agent includes following components according to percentage by weight：Potassium dihydrogen phosphate：33-35%, urea：25-35%, alkyl
Phenol polyethenoxy ether：4-7%, balance of water；
The binding agent includes according to the mass fraction following components：Polyoxyethylene aliphatic alcohol ether：5-13 parts, polyether modified silicon oil：
3-8 parts, dimethyl silicone polymer：11-16 parts, surfactant：3-7 parts, high-molecular organic material：5-11 parts, the surface
Activating agent is one or more mixture in odium stearate, stearic acid potassium or calcium stearate, and the macromolecular material is poly- third
Acrylamide.
The further restriction technical scheme of the present invention：
Aforesaid antirust film includes according to the mass fraction following：Calgon：17-23 parts, sodium oxide molybdena：8-11 parts, methyl
Cellulose：13-16 parts, magnesium chloride：5-7 parts, potassium dihydrogen phosphate：8-13 parts, aluminium hydroxide：2-6 portionings, zirconium oxide：2-4 parts,
Citric acid：5-7 parts, triethanolamine：1-3 parts, hydroxypropyl PASELLI EASYGEL：3-6 parts, nano silicon：3-5 parts, 12
Sodium alkyl benzene sulfonate：10-14 parts, organosilicon ethylene glycol EVA wax：3-5 parts, auxiliary material：0.3-0.5 parts, organic solvent：2-4
Part, crosslinking agent：2-3 parts, antirust auxiliary agent：1-2 parts, binding agent：1-2 parts, deionized water：14-20 parts；
The auxiliary material is compound rare-earth, and the compound rare-earth includes by mass percentage following components：Dysprosium：12-13%, cerium：
23-25%, praseodymium：9-12%, neodymium：3-5%, remaining is lanthanum element, and above lanthanide rare each component sum is 100%；
The crosslinking agent is haloflex；
The antirust auxiliary agent includes following components according to percentage by weight：Potassium dihydrogen phosphate：33-34%, urea：29-35%, alkyl
Phenol polyethenoxy ether：4-5%, balance of water；
The binding agent includes according to the mass fraction following components：Polyoxyethylene aliphatic alcohol ether：7-13 parts, polyether modified silicon oil：
3-6 parts, dimethyl silicone polymer：11-14 parts, surfactant：3-5 parts, high-molecular organic material：5-10 parts, the surface
Activating agent is one or more mixture in odium stearate, stearic acid potassium or calcium stearate, and the macromolecular material is poly- third
Acrylamide.
Aforesaid antirust film includes according to the mass fraction following：Calgon：17-21 parts, sodium oxide molybdena：8-10 point,
Methylcellulose：13-14 parts, magnesium chloride：5-6 parts, potassium dihydrogen phosphate：8-11 parts, aluminium hydroxide：4-6 portionings, zirconium oxide：3-4
Part, citric acid：6-7 parts, triethanolamine：2-3 parts, hydroxypropyl PASELLI EASYGEL：5-6 parts, nano silicon：4-5 parts, ten
Dialkyl benzene sulfonic acids sodium：12-14 parts, organosilicon ethylene glycol EVA wax：4-5 parts, auxiliary material：0.4-0.5 parts, organic solvent：3-4
Part, crosslinking agent：2 parts, antirust auxiliary agent：2 parts, binding agent：2 parts, deionized water：17-20 parts；
The auxiliary material is compound rare-earth, and the compound rare-earth includes by mass percentage following components：Dysprosium：12%, cerium：23%,
Praseodymium：10%, neodymium：3%, remaining is lanthanum element, and above lanthanide rare each component sum is 100%；
The crosslinking agent is haloflex；
The antirust auxiliary agent includes following components according to percentage by weight：Potassium dihydrogen phosphate：33%, urea：30%, alkyl phenol polyoxy
Vinethene：5%, balance of water；
The binding agent includes according to the mass fraction following components：Polyoxyethylene aliphatic alcohol ether：7-10 parts, polyether modified silicon oil：
5-6 parts, dimethyl silicone polymer：13-14 parts, surfactant：4-5 parts, high-molecular organic material：7-10 parts, the surface
Activating agent is one or more mixture in odium stearate, stearic acid potassium or calcium stearate, and the macromolecular material is poly- third
Acrylamide.
Aforesaid antirust film preparation method is comprised the following steps：
Step one：According to said ratio by calgon, sodium oxide molybdena, base cellulose, potassium dihydrogen phosphate, citric acid, organosilicon
Ethylene glycol EVA wax and deionized water are added in reactor, and agitator is stirred with 450-560r/min, stir 30-
40min, temperature rises to 53-65 DEG C, is subsequently adding aluminium hydroxide, zirconium oxide and neopelex, continues to stir, temperature
70-80 DEG C is risen to, 1-2h is incubated, room temperature is then down to, it is standby；
Step 2：Hydroxypropyl PASELLI EASYGEL, nano silicon, triethanolamine and crosslinking agent are added according to said ratio
To in reactor, with 620-680r/min stirrings, the time is 45-55min, is subsequently adding auxiliary material, organic solvent and antirust auxiliary agent,
Continue with 700-750r/min stirrings, the time is 1-2h, temperature rises to 95-102 DEG C, is incubated 2-3h, and temperature is down to room temperature；
Step 3：The raw material that step one and step 2 are obtained is mixed, and with 400-450r/min 1-2h is stirred, and temperature rises to
60-70 DEG C, binding agent is added, continue to stir, temperature rises to 80-98 DEG C, is incubated 3-5h, is cooled to 50-55 DEG C, is then pulled out
Film, finally dries.
The invention has the beneficial effects as follows：Antirusting paint environmental protection of the present invention, to health and to production, accumulating,
Construction safety non-hazardous；Organic solvent is added, the dispersiveness of the various composition added during coating is improved, compound rare-earth is added,
Mechanical performance and anti-corrosive properties are improve, service life is also extended, binding agent is with the addition of, adhesion of thin film is improve by force,
Even if in moist surface construction, still adhesion-tight.
Specific embodiment
Embodiment 1
The present embodiment provides a kind of antirust specimen mounting, and one layer of antirust film is provided with outside specimen mounting, and antirust film presses mass fraction
Meter includes following：Calgon：18 parts, sodium oxide molybdena：9 parts, methylcellulose：15 parts, magnesium chloride：6 parts, potassium dihydrogen phosphate：
11 parts, aluminium hydroxide：4 parts, zirconium oxide：3 parts, citric acid：6 parts, triethanolamine：2 parts, hydroxypropyl PASELLI EASYGEL：5 parts,
Nano silicon：4 parts, neopelex：12 parts, organosilicon ethylene glycol EVA wax：4 parts, auxiliary material：0.3 part, have
Machine solvent：3 parts, crosslinking agent：2 parts, antirust auxiliary agent：2 parts, binding agent：1 part, deionized water：16 parts；
Auxiliary material is compound rare-earth, and the compound rare-earth includes by mass percentage following components：Dysprosium：12%, cerium：24%, praseodymium：
11%, neodymium：4%, remaining is lanthanum element, and above lanthanide rare each component sum is 100%；
Crosslinking agent is haloflex；
Antirust auxiliary agent includes following components according to percentage by weight：Potassium dihydrogen phosphate：34%, urea：35%, alkyl phenol polyoxy second
Alkene ether：5%, balance of water；
Binding agent includes according to the mass fraction following components：Polyoxyethylene aliphatic alcohol ether：12 parts, polyether modified silicon oil：5 parts, it is poly-
Dimethyl siloxane：13 parts, surfactant：4 parts, high-molecular organic material：8 parts, surfactant is odium stearate, hard
Mixture in sour potassium or calcium stearate, macromolecular material is polyacrylamide.
A kind of antirust film preparation method of antirust specimen mounting of the present embodiment is comprised the following steps：
Step one：According to said ratio by calgon, sodium oxide molybdena, base cellulose, potassium dihydrogen phosphate, citric acid, organosilicon
Ethylene glycol EVA wax and deionized water are added in reactor, and agitator is stirred with 480r/min, stir 33min, temperature
Degree rises to 58 DEG C, is subsequently adding aluminium hydroxide, zirconium oxide and neopelex, continues to stir, and temperature rises to 73 DEG C, protects
Warm 1.5h, is then down to room temperature, standby；
Step 2：Hydroxypropyl PASELLI EASYGEL, nano silicon, triethanolamine and crosslinking agent are added according to said ratio
To in reactor, with 650r/min stirrings, the time is 50min, is subsequently adding auxiliary material, organic solvent and antirust auxiliary agent, continue with
700r/min is stirred, and the time is 1.5h, and temperature rises to 98 DEG C, is incubated 2h, and temperature is down to room temperature；
Step 3：The raw material that step one and step 2 are obtained is mixed, and with 400r/min 2h is stirred, and temperature rises to 63 DEG C,
Binding agent is added, continues to stir, temperature rises to 90 DEG C, is incubated 4h, is cooled to 52 DEG C, then carries out pulling out film, finally dries.
Embodiment 2
The present embodiment provides a kind of antirust specimen mounting, and one layer of antirust film is provided with outside specimen mounting, and antirust film presses mass fraction
Meter includes following：Calgon：20 parts, sodium oxide molybdena：10 parts, methylcellulose：13 parts, magnesium chloride：5 parts, potassium dihydrogen phosphate：
9 parts, aluminium hydroxide：5 parts, zirconium oxide：4 parts, citric acid：7 parts, triethanolamine：3 parts, hydroxypropyl PASELLI EASYGEL：6 parts, receive
Rice silica：5 parts, neopelex：13 parts, organosilicon ethylene glycol EVA wax：5 parts, auxiliary material：0.4 part, it is organic
Solvent：4 parts, crosslinking agent：2 parts, antirust auxiliary agent：2 parts, binding agent：1 part, deionized water：18 parts；
Auxiliary material is compound rare-earth, and the compound rare-earth includes by mass percentage following components：Dysprosium：12%, cerium：24%, praseodymium：
11%, neodymium：4%, remaining is lanthanum element, and above lanthanide rare each component sum is 100%；
Crosslinking agent is haloflex；
Antirust auxiliary agent includes following components according to percentage by weight：Potassium dihydrogen phosphate：34%, urea：35%, alkylphenol-polyethenoxy
Ether：5%, balance of water；
Binding agent includes according to the mass fraction following components：Polyoxyethylene aliphatic alcohol ether：10 parts, polyether modified silicon oil：6 parts, it is poly-
Dimethyl siloxane：14 parts, surfactant：5 parts, high-molecular organic material：7 parts, surfactant is odium stearate, hard
Mixture in sour potassium or calcium stearate, macromolecular material is polyacrylamide.
A kind of antirust film preparation method of antirust specimen mounting of the present embodiment is comprised the following steps：
Step one：According to said ratio by calgon, sodium oxide molybdena, base cellulose, potassium dihydrogen phosphate, citric acid, organosilicon
Ethylene glycol EVA wax and deionized water are added in reactor, and agitator is stirred with 500r/min, stir 30min, temperature
Degree rises to 63 DEG C, is subsequently adding aluminium hydroxide, zirconium oxide and neopelex, continues to stir, and temperature rises to 78 DEG C, protects
Warm 2h, is then down to room temperature, standby；
Step 2：Hydroxypropyl PASELLI EASYGEL, nano silicon, triethanolamine and crosslinking agent are added according to said ratio
To in reactor, with 680r/min stirrings, the time is 45min, is subsequently adding auxiliary material, organic solvent and antirust auxiliary agent, continue with
720r/min is stirred, and the time is 1h, and temperature rises to 100 DEG C, is incubated 1.5h, and temperature is down to room temperature；
Step 3：The raw material that step one and step 2 are obtained is mixed, and with 430r/min 1.5h is stirred, and temperature rises to 67
DEG C, binding agent is added, continue to stir, temperature rises to 96 DEG C, is incubated 4h, is cooled to 54 DEG C, then carries out pulling out film, finally dries.
In addition to the implementation, the present invention can also have other embodiment, all employing equivalents or equivalent transformation shape
Into technical scheme, all fall within the protection domain of application claims.
Claims (4)
1. a kind of antirust specimen mounting, is provided with one layer of antirust film outside the specimen mounting, it is characterised in that：The antirust film is pressed
Mass fraction meter includes following：Calgon：15-23 parts, sodium oxide molybdena：5-11 parts, methylcellulose：11-16 parts, chlorination
Magnesium：3-7 parts, potassium dihydrogen phosphate：5-13 parts, aluminium hydroxide：2-8 parts, zirconium oxide：2-6 parts, citric acid：5-8 parts, triethanolamine：
1-4 parts, hydroxypropyl PASELLI EASYGEL：3-8 parts, nano silicon：3-7 parts, neopelex：10-17 parts, have
Machine silicon ethylene glycol EVA wax：3-6 parts, auxiliary material：0.3-0.7 parts, organic solvent：2-5 parts, crosslinking agent：2-4 parts, antirust auxiliary agent：
1-3 parts, binding agent：1-3 parts, deionized water：10-20 parts；
The auxiliary material is compound rare-earth, and the compound rare-earth includes by mass percentage following components：Dysprosium：12-14%, cerium：
23-26%, praseodymium：9-14%, neodymium：3-6%, remaining is lanthanum element, and above lanthanide rare each component sum is 100%；
The crosslinking agent is polyethylene or haloflex；
The antirust auxiliary agent includes following components according to percentage by weight：Potassium dihydrogen phosphate：33-35%, urea：25-35%, alkyl
Phenol polyethenoxy ether：4-7%, balance of water；
The binding agent includes according to the mass fraction following components：Polyoxyethylene aliphatic alcohol ether：5-13 parts, polyether modified silicon oil：
3-8 parts, dimethyl silicone polymer：11-16 parts, surfactant：3-7 parts, high-molecular organic material：5-11 parts, the surface
Activating agent is one or more mixture in odium stearate, stearic acid potassium or calcium stearate, and the macromolecular material is poly- third
Acrylamide.
2. antirust specimen mounting according to claim 1, it is characterised in that the antirust film include according to the mass fraction with
Under：Calgon：17-23 parts, sodium oxide molybdena：8-11 parts, methylcellulose：13-16 parts, magnesium chloride：5-7 parts, biphosphate
Potassium：8-13 parts, aluminium hydroxide：2-6 portionings, zirconium oxide：2-4 parts, citric acid：5-7 parts, triethanolamine：1-3 parts, hydroxypropyl two
Starch phosphate：3-6 parts, nano silicon：3-5 parts, neopelex：10-14 parts, organosilicon ethylene glycol copolymerization
Body wax：3-5 parts, auxiliary material：0.3-0.5 parts, organic solvent：2-4 parts, crosslinking agent：2-3 parts, antirust auxiliary agent：1-2 parts, binding agent：
1-2 parts, deionized water：14-20 parts；
The auxiliary material is compound rare-earth, and the compound rare-earth includes by mass percentage following components：Dysprosium：12-13%, cerium：
23-25%, praseodymium：9-12%, neodymium：3-5%, remaining is lanthanum element, and above lanthanide rare each component sum is 100%；
The crosslinking agent is haloflex；
The antirust auxiliary agent includes following components according to percentage by weight：Potassium dihydrogen phosphate：33-34%, urea：29-35%, alkyl
Phenol polyethenoxy ether：4-5%, balance of water；
The binding agent includes according to the mass fraction following components：Polyoxyethylene aliphatic alcohol ether：7-13 parts, polyether modified silicon oil：
3-6 parts, dimethyl silicone polymer：11-14 parts, surfactant：3-5 parts, high-molecular organic material：5-10 parts, the surface
Activating agent is one or more mixture in odium stearate, stearic acid potassium or calcium stearate, and the macromolecular material is poly- third
Acrylamide.
3. antirust specimen mounting according to claim 1, it is characterised in that the antirust film include according to the mass fraction with
Under：Calgon：17-21 parts, sodium oxide molybdena：8-10 point, methylcellulose：13-14 parts, magnesium chloride：5-6 parts, biphosphate
Potassium：8-11 parts, aluminium hydroxide：4-6 portionings, zirconium oxide：3-4 parts, citric acid：6-7 parts, triethanolamine：2-3 parts, hydroxypropyl two
Starch phosphate：5-6 parts, nano silicon：4-5 parts, neopelex：12-14 parts, organosilicon ethylene glycol copolymerization
Body wax：4-5 parts, auxiliary material：0.4-0.5 parts, organic solvent：3-4 parts, crosslinking agent：2 parts, antirust auxiliary agent：2 parts, binding agent：2 parts,
Deionized water：17-20 parts；
The auxiliary material is compound rare-earth, and the compound rare-earth includes by mass percentage following components：Dysprosium：12%, cerium：23%,
Praseodymium：10%, neodymium：3%, remaining is lanthanum element, and above lanthanide rare each component sum is 100%；
The crosslinking agent is haloflex；
The antirust auxiliary agent includes following components according to percentage by weight：Potassium dihydrogen phosphate：33%, urea：30%, alkyl phenol polyoxy
Vinethene：5%, balance of water；
The binding agent includes according to the mass fraction following components：Polyoxyethylene aliphatic alcohol ether：7-10 parts, polyether modified silicon oil：
5-6 parts, dimethyl silicone polymer：13-14 parts, surfactant：4-5 parts, high-molecular organic material：7-10 parts, the surface
Activating agent is one or more mixture in odium stearate, stearic acid potassium or calcium stearate, and the macromolecular material is poly- third
Acrylamide.
4. the antirust specimen mounting according to claim 1-3, it is characterised in that：One layer of antirust film is provided with outside the specimen mounting
Preparation method is comprised the following steps：
Step one：According to said ratio by calgon, sodium oxide molybdena, base cellulose, potassium dihydrogen phosphate, citric acid, organosilicon
Ethylene glycol EVA wax and deionized water are added in reactor, and agitator is stirred with 450-560r/min, stir 30-
40min, temperature rises to 53-65 DEG C, is subsequently adding aluminium hydroxide, zirconium oxide and neopelex, continues to stir, temperature
70-80 DEG C is risen to, 1-2h is incubated, room temperature is then down to, it is standby；
Step 2：Hydroxypropyl PASELLI EASYGEL, nano silicon, triethanolamine and crosslinking agent are added according to said ratio
To in reactor, with 620-680r/min stirrings, the time is 45-55min, is subsequently adding auxiliary material, organic solvent and antirust auxiliary agent,
Continue with 700-750r/min stirrings, the time is 1-2h, temperature rises to 95-102 DEG C, is incubated 2-3h, and temperature is down to room temperature；
Step 3：The raw material that step one and step 2 are obtained is mixed, and with 400-450r/min 1-2h is stirred, and temperature rises to
60-70 DEG C, binding agent is added, continue to stir, temperature rises to 80-98 DEG C, is incubated 3-5h, is cooled to 50-55 DEG C, is then pulled out
Film, finally dries.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611145293.8A CN106590180A (en) | 2016-12-13 | 2016-12-13 | Anti-rust specimen holder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611145293.8A CN106590180A (en) | 2016-12-13 | 2016-12-13 | Anti-rust specimen holder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106590180A true CN106590180A (en) | 2017-04-26 |
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ID=58801092
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611145293.8A Pending CN106590180A (en) | 2016-12-13 | 2016-12-13 | Anti-rust specimen holder |
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| CN (1) | CN106590180A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109091835A (en) * | 2018-09-07 | 2018-12-28 | 江苏叙然信息科技有限公司 | Basketball stands outside a kind of corrosion-resistant antirust room |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104530855A (en) * | 2014-11-20 | 2015-04-22 | 马鞍山市金韩涂料制造有限公司 | Water-based rust conversion and prevention paint |
| CN105017962A (en) * | 2014-04-24 | 2015-11-04 | 张振英 | Constant, long-acting and anti-pollution flashover coating HRTV |
| CN105838188A (en) * | 2016-04-28 | 2016-08-10 | 江苏金源腾峰换热设备有限公司 | Treating process of high-temperature-resistant tubular product for waste-heat utilization device |
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| CN105017962A (en) * | 2014-04-24 | 2015-11-04 | 张振英 | Constant, long-acting and anti-pollution flashover coating HRTV |
| CN104530855A (en) * | 2014-11-20 | 2015-04-22 | 马鞍山市金韩涂料制造有限公司 | Water-based rust conversion and prevention paint |
| CN105838188A (en) * | 2016-04-28 | 2016-08-10 | 江苏金源腾峰换热设备有限公司 | Treating process of high-temperature-resistant tubular product for waste-heat utilization device |
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| CN109091835A (en) * | 2018-09-07 | 2018-12-28 | 江苏叙然信息科技有限公司 | Basketball stands outside a kind of corrosion-resistant antirust room |
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Application publication date: 20170426 |