CN106588492A - Special organic fertilizer for camellia nitidissima - Google Patents
Special organic fertilizer for camellia nitidissima Download PDFInfo
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- CN106588492A CN106588492A CN201611194913.7A CN201611194913A CN106588492A CN 106588492 A CN106588492 A CN 106588492A CN 201611194913 A CN201611194913 A CN 201611194913A CN 106588492 A CN106588492 A CN 106588492A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D5/00—Fertilisers containing magnesium
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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Abstract
The invention discloses a special organic fertilizer for camellia nitidissima. The special organic fertilizer is prepared from, by weight, 100-200 parts of bagasse, 100-200 parts of bean curd residue, 50-120 parts of cassava residue, 30-50 parts of shrimp and crab shells, 3-12 parts of EM bacteria, 30-80 parts of animal carcasses, 60-90 parts of attapulgite soil, 30-80 parts of livestock manure, 20-50 parts of pine needles meal, 20-40 parts of silkworm excrements, 30-50 parts of tobacco leaves, 15-30 parts of chitooligosaccharides and 1-6 parts of trace elements. According to the special organic fertilizer, the camellia nitidissima is more resistant to diseases and insects, and the quality and yield are improved. The special organic fertilizer is easily absorbed and transformed by the camellia nitidissima, the effective utilization ratio of the special organic fertilizer for the camellia nitidissima is significantly enhanced, the growth period of the camellia nitidissima is shortened, the flowering period is advanced and the flowering number of flowering period is increased.
Description
Technical field
The present invention relates to technical field of fertilizers, and in particular to a kind of Camellia nitidissima fertilizer special for organic and preparation method thereof.
Background technology
Camellia nitidissima belongs to Theaceae, Camellia, is twin sisters with tea, camellia, South Mountain tea, oil tea, tea plum etc., is country
One of first class of protection plant.Camellia nitidissima spends golden yellow, dazzling brilliant, seemingly applies coating of wax, sparkling and crystal-clear and glossy, seemingly has semi-transparent
Bright sense.Camellia nitidissima is singly born in axil, when the flowers are in blossom, there is cup-shaped, gyalectiform or bowl-shape, delicate and charming colourful, beautiful grace.With
Before, people did not see the golden yellow species of pattern.Nineteen sixty, Chinese science worker is found that first in the band of Nanning one
A kind of flavous camellia, is named as Camellia nitidissima.Foreign countries are referred to as magical " Dongfang " magic tea, are described as " plant kingdom great Xiong
Cat ", " tea race queen ".According to Nutrition and Food Safety Office of China Disease Prevention and control Centre, Guangxi Zhuang Autonomous Region prevention from suffering from the diseases
Control centre, Guangxi Zhuang Autonomous Region sanitary monitoring test center, the center nutrition of Beijing disease prevention and control center and food peace
The authoritative institutions such as full institute, Analysis-Test Research Center, Guangxi Zhuang Autonomous Region, Colleges Of Traditional Chinese Medicine Of Guangxi, Guangxi Agriculture College experimental center
Inspection shows：The nontoxic level of golden flower Camellias, containing more than 400 kinds of nutriments, have no toxic side effect.Rich in tea polysaccharide, Tea Polyphenols, total soap
Glucoside, general flavone, Tea Pigment, caffeine, protein, vitamin B1, B2, vitamin C, vitamin E, folic acid, aliphatic acid, B- Hu trailing plants
Various natural nutrition compositions such as Bu Su；Camellia nitidissima contains tens kinds of amino acid such as theanine, threonine, and various right rich in having
Human body has the trace elements such as natural organic germanium (Ge), selenium (Se), molybdenum (Mo), zinc (Zn), the vanadium (V) of important health-care effect, and
The macroelements such as potassium (K), calcium (Ca), magnesium (Mg).As Camellia nitidissima has special medical value and economic worth, Camellia nitidissima kind
Gradually industrialization is planted, in the market Camellia nitidissima special fertilizer is relatively fewer, and single function, usually promote Camellia nitidissima to be grown to
It is main.
The content of the invention
It is an object of the present invention to provide a kind of Camellia nitidissima fertilizer special for organic, present invention raising Camellia nitidissima Resistant energy
Power, significantly improves Camellia nitidissima quality and yield, and the present invention significantly improves Camellia nitidissima special organic easily by golden flower tea tree sorption enhanceds
The effective rate of utilization of fertilizer, shortens the growth period of Camellia nitidissima, in advance the quantity of blooming at florescence and increase florescence.
The present invention provide technical scheme be：
A kind of Camellia nitidissima fertilizer special for organic, the Camellia nitidissima fertilizer special for organic is made including following weight portion material：Sugarcane
Slag 100-200 parts, soybean residue 100-200 parts, manioc waste 50-120 parts, shrimp and crab shells 30-50 parts, EM bacterium 3-12 parts, spoil
30-80 parts, attapulgite 60-90 parts, fowl and animal excrement 30-80 parts, pine needle meal 20-50 parts, silkworm excrement 20-40 parts, tobacco leaf 30-50
Part, chitosan oligosaccharide 15-30 parts, trace element 1-6 parts；Wherein, the trace element is made up of following weight portion material：Sodium selenite
10-15 parts, ferrous sulfate 5-10 parts, zinc sulfate 5-15 parts, water-soluble sodium molybdate 3-8 parts, manganese sulfate 5-8 parts, cobaltous sulfate, iodate
Sodium 1-5 parts, magnesium sulfate 5-8 parts.
Preferably, the Camellia nitidissima fertilizer special for organic is made up of following weight portion material：Bagasse 120-180 parts, beans
Rotten slag 150-190 parts, manioc waste 80-100 parts, shrimp and crab shells 35-45 parts, EM bacterium 5-8 parts, spoil 50-60 parts, attapulgite
75-85 parts, fowl and animal excrement 55-65 parts, pine needle meal 30-40 parts, silkworm excrement 25-35 parts, tobacco leaf 35-45 parts, chitosan oligosaccharide 20-25 parts,
Micro- 2-4 parts, 2mol/L hydrochloric acid solution 150-180 parts, NaOH 10-50 parts.
Preferably, the Camellia nitidissima fertilizer special for organic is made up of following weight portion material：175 parts of bagasse, soybean residue
165 parts, 95 parts of manioc waste, 40 parts of shrimp and crab shells, 6 parts of EM bacterium, 55 parts of spoil, 80 parts of attapulgite, 60 parts of fowl and animal excrement, pine
35 parts of pin powder, 30 parts of silkworm excrement, 40 parts of tobacco leaf, 22 parts of chitosan oligosaccharide, 3 parts of trace element, 170 parts of 2mol/L hydrochloric acid solutions, hydroxide
25 parts of sodium；Wherein, the trace element is made up of following weight portion material：12 parts of sodium selenite, 7 parts of ferrous sulfate, zinc sulfate
12 parts, water-soluble 5 parts of sodium molybdate, 6 parts of manganese sulfate, cobaltous sulfate, 4 parts of sodium iodide, 6 parts of magnesium sulfate.
The present invention also provides a kind of preparation method of described Camellia nitidissima fertilizer special for organic, comprises the following steps：
Step 1, tobacco leaf is added water using after ultrasonic grind, suction filtration obtains the first filtrate and the first filter residue, toward filter residue
After middle addition ethanol is extracted 1 hour, suction filtration obtains the second filtrate and the second filter residue, subtracts after the first filtrate and the second filtrate are merged
Pressure is concentrated into the first filtrate and the second filtrate cumulative volume 1/4 obtains extract；
Step 2, by shrimp and crab shells, spoil be dried after mechanical crushing, add 2mol/L hydrochloric acid solutions, in autoclave
In, after reaction 3-6 hours, filtrate being filtrated to get, filtrate evaporation to be reclaimed and obtain protein concentrated solution after hydrochloric acid；
Step 3, EM bacterium are divided into two parts, first part of weight ratio with second part is 7: 3, by bagasse, soybean residue, cassava
Slag, attapulgite, fowl and animal excrement, pine needle meal, silkworm excrement are mixed into fermentation base-material, add after first part of EM bacterium, water mixing using step
The hydrochloric acid reclaimed in rapid 2 adjusts PH to 4-5 after fermentation vat sealing and fermenting 2-3 days, and fermentation temperature is 55 DEG C, is centrifuged for the first time
Filter obtains the first fermentation filter residue and the first zymotic fluid, is obtained using step 2 after the first fermentation residue adds second part of EM bacterium, water mixing
PH to 4-5 is adjusted in fermentation vat sealing and fermenting 1-2 days, fermentation temperature is 50 DEG C, second centrifugal filtration to the hydrochloric acid for reclaiming
To the second fermentation filter residue and the second zymotic fluid, adopt after the first zymotic fluid is merged with the second zymotic fluid NaOH regulation PH to
6-7 obtains zymotic fluid；
Step 4, nanometer pulverization will be carried out after trace element to particle diameter less than 10 microns, obtain powder；
Zymotic fluid, step that protein concentrated solution that step 5, the extract that step 1 is obtained, step 2 are obtained, step 3 are obtained
The powder obtained in rapid 4 obtains the Camellia nitidissima fertilizer special for organic after being well mixed with chitosan oligosaccharide.
Preferably, tobacco leaf and the weight ratio of water are 1: 2 in step 1, and the first filter residue is 1: 2 with the weight ratio of ethanol.
Preferably, the pressure of step 2 mesohigh reactor is 20-30Mpa, and temperature is 50-60 DEG C.
Preferably, in step 3 ferment base-material with add water weight ratio be 1: 5, first fermentation filter residue with add
The weight ratio of water is 1: 3.
Beneficial effects of the present invention are as follows：
1), the macromolecular in fertilizer can not only be resolved into small molecule and easily be absorbed by golden flower tea trees by bacterium containing EM of the invention, be promoted
Enter the yield that golden flower growth of tea plant significantly improves Camellia nitidissima, optimization improves soil texture, and the tobacco leaf of addition is through extracting what is obtained
Extract can not only prevent and treat the insect in soil, while golden flower tea trees resistant to diseases and insects itself can be improved, reduce chemical insecticide
Use, the present invention contains various trace elements, significantly improves Camellia nitidissima quality, present invention addition soybean residue, manioc waste, shrimp crab
Shell etc., there is provided multiple protein amino acid and multivitamin, trace element, plays twice laid, the cost for substantially reducing, silkworm
Containing abundant chlorophyll in sand, easily absorbed by golden flower tea trees, promote the growth of golden flower Camellias to shorten growth cycle.
2), preparation method of the invention is simple to operation, and Production Time is short, wherein shrimp and crab shells and spoil, Jing Guoti
Small molecule amino acid is obtained, is easily absorbed by tea tree, while tobacco leaf extracts active principle improves pre- preventing disease and pest ability, and sent out
Beneficiating ingredient decomposes through microorganism in ferment, can be easier to be absorbed into energy, improves having for Camellia nitidissima fertilizer special for organic
Effect utilization rate.
Specific embodiment
With reference to specific embodiment, the present invention is described in further detail, to make those skilled in the art's reference say
Bright book word can be implemented according to this.
Embodiment 1：
A kind of Camellia nitidissima fertilizer special for organic, including following weight portion material makes：100 parts of bagasse, 100 parts of soybean residue,
5 parts of manioc waste, 30 parts of shrimp and crab shells, 3 parts of EM bacterium, 30 parts of spoil, 60 parts of attapulgite, 30 parts of fowl and animal excrement, pine needle meal 20
Part, 20 parts of silkworm excrement, 30 parts of tobacco leaf, 15 parts of chitosan oligosaccharide, 1 part of trace element；Wherein, the trace element is by following weight portion material
Composition：10 parts of sodium selenite, 5 parts of ferrous sulfate, 5 parts of zinc sulfate, water-soluble 3 parts of sodium molybdate, 5 parts of manganese sulfate, cobaltous sulfate, iodate
1 part of sodium, 5 parts of magnesium sulfate.
The preparation method of described Camellia nitidissima fertilizer special for organic, comprises the following steps：
Step 1, tobacco leaf is added water using after ultrasonic grind, suction filtration obtains the first filtrate and the first filter residue, toward filter residue
After middle addition ethanol is extracted 1 hour, suction filtration obtains the second filtrate and the second filter residue, subtracts after the first filtrate and the second filtrate are merged
Pressure is concentrated into the first filtrate and the second filtrate cumulative volume 1/4 obtains extract；
Step 2, by shrimp and crab shells, spoil be dried after mechanical crushing, add 2mol/L hydrochloric acid solutions, in autoclave
In, after reacting 5 hours, filtrate being filtrated to get, filtrate evaporation to be reclaimed and obtain protein concentrated solution after hydrochloric acid；
Step 3, EM bacterium are divided into two parts, first part of weight ratio with second part is 7: 3, by bagasse, soybean residue, cassava
Slag, attapulgite, fowl and animal excrement, pine needle meal, silkworm excrement are mixed into fermentation base-material, add after first part of EM bacterium, water mixing using step
The hydrochloric acid reclaimed in rapid 2 adjusts PH to 4-5 after fermentation vat sealing and fermenting 3 days, and fermentation temperature is 55 DEG C, first time centrifugal filtration
The first fermentation filter residue and the first zymotic fluid are obtained, is obtained using step 2 after the first fermentation residue adds second part of EM bacterium, water mixing
The hydrochloric acid of recovery adjusts PH to 4-5 in fermentation vat sealing and fermenting 2 days, and fermentation temperature is 50 DEG C, second centrifugal filtration to the
Two fermentation filter residues and the second zymotic fluid, PH to 6-7 is adjusted after the first zymotic fluid is merged with the second zymotic fluid using NaOH
Obtain zymotic fluid；
Step 4, nanometer pulverization will be carried out after trace element to particle diameter less than 10 microns, obtain powder；
Zymotic fluid, step that protein concentrated solution that step 5, the extract that step 1 is obtained, step 2 are obtained, step 3 are obtained
The powder obtained in rapid 4 obtains the Camellia nitidissima fertilizer special for organic after being well mixed with chitosan oligosaccharide.
Embodiment 2
A kind of Camellia nitidissima fertilizer special for organic, including following weight portion material makes：200 parts of bagasse, 200 parts of soybean residue,
120 parts of manioc waste, 50 parts of shrimp and crab shells, 12 parts of EM bacterium, 80 parts of spoil, 90 parts of attapulgite, 80 parts of fowl and animal excrement, pine needle meal
50 parts, 40 parts of silkworm excrement, 50 parts of tobacco leaf, 30 parts of chitosan oligosaccharide, trace element 6 parts；Wherein, the trace element is by following weight portion material
Material composition：15 parts of sodium selenite, 10 parts of ferrous sulfate, 15 parts of zinc sulfate, water-soluble 8 parts of sodium molybdate, 8 parts of manganese sulfate, cobaltous sulfate,
5 parts of sodium iodide, 8 parts of magnesium sulfate.
The preparation method of described Camellia nitidissima fertilizer special for organic, comprises the following steps：
Step 1, tobacco leaf is added water using after ultrasonic grind, suction filtration obtains the first filtrate and the first filter residue, toward filter residue
After middle addition ethanol is extracted 1 hour, suction filtration obtains the second filtrate and the second filter residue, subtracts after the first filtrate and the second filtrate are merged
Pressure is concentrated into the first filtrate and the second filtrate cumulative volume 1/4 obtains extract；
Step 2, by shrimp and crab shells, spoil be dried after mechanical crushing, add 2mol/L hydrochloric acid solutions, in autoclave
In, after reacting 4 hours, filtrate being filtrated to get, filtrate evaporation to be reclaimed and obtain protein concentrated solution after hydrochloric acid；
Step 3, EM bacterium are divided into two parts, first part of weight ratio with second part is 7: 3, by bagasse, soybean residue, cassava
Slag, attapulgite, fowl and animal excrement, pine needle meal, silkworm excrement are mixed into fermentation base-material, add after first part of EM bacterium, water mixing using step
The hydrochloric acid reclaimed in rapid 2 adjusts PH to 4-5 after fermentation vat sealing and fermenting 3 days, and fermentation temperature is 55 DEG C, first time centrifugal filtration
The first fermentation filter residue and the first zymotic fluid are obtained, is obtained using step 2 after the first fermentation residue adds second part of EM bacterium, water mixing
The hydrochloric acid of recovery adjusts PH to 4-5 in fermentation vat sealing and fermenting 1 day, and fermentation temperature is 50 DEG C, second centrifugal filtration to the
Two fermentation filter residues and the second zymotic fluid, PH to 6-7 is adjusted after the first zymotic fluid is merged with the second zymotic fluid using NaOH
Obtain zymotic fluid；
Step 4, nanometer pulverization will be carried out after trace element to particle diameter less than 10 microns, obtain powder；
Zymotic fluid, step that protein concentrated solution that step 5, the extract that step 1 is obtained, step 2 are obtained, step 3 are obtained
The powder obtained in rapid 4 obtains the Camellia nitidissima fertilizer special for organic after being well mixed with chitosan oligosaccharide.
Embodiment 3
A kind of Camellia nitidissima fertilizer special for organic, is made up of following weight portion material：120 parts of bagasse, 150 parts of soybean residue, wood
80 parts of potato slag, 35 parts of shrimp and crab shells, 5 parts of EM bacterium, 50 parts of spoil, 75 parts of attapulgite, 55 parts of fowl and animal excrement, pine needle meal 30
Part, 25 parts of silkworm excrement, 35 parts of tobacco leaf, 20 parts of chitosan oligosaccharide, 2 parts of trace element, 150 parts of 2mol/L hydrochloric acid solutions, 10 parts of NaOH.
The preparation method of described Camellia nitidissima fertilizer special for organic, comprises the following steps：
Step 1, tobacco leaf is added water using after ultrasonic grind, suction filtration obtains the first filtrate and the first filter residue, toward filter residue
After middle addition ethanol is extracted 1 hour, suction filtration obtains the second filtrate and the second filter residue, subtracts after the first filtrate and the second filtrate are merged
Pressure is concentrated into the first filtrate and the second filtrate cumulative volume 1/4 obtains extract；
Step 2, by shrimp and crab shells, spoil be dried after mechanical crushing, add 2mol/L hydrochloric acid solutions, in autoclave
In, after reacting 5 hours, filtrate being filtrated to get, filtrate evaporation to be reclaimed and obtain protein concentrated solution after hydrochloric acid；
Step 3, EM bacterium are divided into two parts, first part of weight ratio with second part is 7: 3, by bagasse, soybean residue, cassava
Slag, attapulgite, fowl and animal excrement, pine needle meal, silkworm excrement are mixed into fermentation base-material, add after first part of EM bacterium, water mixing using step
The hydrochloric acid reclaimed in rapid 2 adjusts PH to 4-5 after fermentation vat sealing and fermenting 2 days, and fermentation temperature is 55 DEG C, first time centrifugal filtration
The first fermentation filter residue and the first zymotic fluid are obtained, is obtained using step 2 after the first fermentation residue adds second part of EM bacterium, water mixing
The hydrochloric acid of recovery adjusts PH to 4-5 in fermentation vat sealing and fermenting 2 days, and fermentation temperature is 50 DEG C, second centrifugal filtration to the
Two fermentation filter residues and the second zymotic fluid, PH to 6-7 is adjusted after the first zymotic fluid is merged with the second zymotic fluid using NaOH
Obtain zymotic fluid；
Step 4, nanometer pulverization will be carried out after trace element to particle diameter less than 10 microns, obtain powder；
Zymotic fluid, step that protein concentrated solution that step 5, the extract that step 1 is obtained, step 2 are obtained, step 3 are obtained
The powder obtained in rapid 4 obtains the Camellia nitidissima fertilizer special for organic after being well mixed with chitosan oligosaccharide.
Preferably, tobacco leaf and the weight ratio of water are 1: 2 in step 1, and the first filter residue is 1: 2 with the weight ratio of ethanol.
Preferably, the pressure of step 2 mesohigh reactor is 25Mpa, and temperature is 55 DEG C.
Preferably, in step 3 ferment base-material with add water weight ratio be 1: 5, first fermentation filter residue with add
The weight ratio of water is 1: 3.
Embodiment 4
A kind of Camellia nitidissima fertilizer special for organic, is made up of following weight portion material：180 parts of bagasse, 190 parts of soybean residue, wood
100 parts of potato slag, 45 parts of shrimp and crab shells, 8 parts of EM bacterium, 60 parts of spoil, 85 parts of attapulgite, 65 parts of fowl and animal excrement, pine needle meal 40
Part, 35 parts of silkworm excrement, 45 parts of tobacco leaf, 25 parts of chitosan oligosaccharide, 4 parts of trace element, 180 parts of 2mol/L hydrochloric acid solutions, 50 parts of NaOH.
The preparation method of described Camellia nitidissima fertilizer special for organic, comprises the following steps：
Step 1, tobacco leaf is added water using after ultrasonic grind, suction filtration obtains the first filtrate and the first filter residue, toward filter residue
After middle addition ethanol is extracted 1 hour, suction filtration obtains the second filtrate and the second filter residue, subtracts after the first filtrate and the second filtrate are merged
Pressure is concentrated into the first filtrate and the second filtrate cumulative volume 1/4 obtains extract；
Step 2, by shrimp and crab shells, spoil be dried after mechanical crushing, add 2mol/L hydrochloric acid solutions, in autoclave
In, after reaction 3-6 hours, filtrate being filtrated to get, filtrate evaporation to be reclaimed and obtain protein concentrated solution after hydrochloric acid；
Step 3, EM bacterium are divided into two parts, first part of weight ratio with second part is 7: 3, by bagasse, soybean residue, cassava
Slag, attapulgite, fowl and animal excrement, pine needle meal, silkworm excrement are mixed into fermentation base-material, add after first part of EM bacterium, water mixing using step
The hydrochloric acid reclaimed in rapid 2 adjusts PH to 4-5 after fermentation vat sealing and fermenting 3 days, and fermentation temperature is 55 DEG C, first time centrifugal filtration
The first fermentation filter residue and the first zymotic fluid are obtained, is obtained using step 2 after the first fermentation residue adds second part of EM bacterium, water mixing
The hydrochloric acid of recovery adjusts PH to 4-5 in fermentation vat sealing and fermenting 2 days, and fermentation temperature is 50 DEG C, second centrifugal filtration to the
Two fermentation filter residues and the second zymotic fluid, PH to 6-7 is adjusted after the first zymotic fluid is merged with the second zymotic fluid using NaOH
Obtain zymotic fluid；
Step 4, nanometer pulverization will be carried out after trace element to particle diameter less than 10 microns, obtain powder；
Zymotic fluid, step that protein concentrated solution that step 5, the extract that step 1 is obtained, step 2 are obtained, step 3 are obtained
The powder obtained in rapid 4 obtains the Camellia nitidissima fertilizer special for organic after being well mixed with chitosan oligosaccharide.
Tobacco leaf and the weight ratio of water are 1: 2 in step 1, and the first filter residue is 1: 2 with the weight ratio of ethanol.
The pressure of step 2 mesohigh reactor is 30Mpa, and temperature is 60 DEG C.
Fermentation base-material and the weight ratio of the water for adding are 1: 5 in step 3, the weight ratio of the first fermentation filter residue and the water for adding
For 1: 3.
Embodiment 5
A kind of Camellia nitidissima fertilizer special for organic, is made up of following weight portion material：175 parts of bagasse, 165 parts of soybean residue, wood
95 parts of potato slag, 40 parts of shrimp and crab shells, 6 parts of EM bacterium, 55 parts of spoil, 80 parts of attapulgite, 60 parts of fowl and animal excrement, pine needle meal 35
Part, 30 parts of silkworm excrement, 40 parts of tobacco leaf, 22 parts of chitosan oligosaccharide, 3 parts of trace element, 170 parts of 2mol/L hydrochloric acid solutions, 25 parts of NaOH；
Wherein, the trace element is made up of following weight portion material：12 parts of sodium selenite, 7 parts of ferrous sulfate, 12 parts of zinc sulfate, water
5 parts of dissolubility sodium molybdate, 6 parts of manganese sulfate, cobaltous sulfate, 4 parts of sodium iodide, 6 parts of magnesium sulfate.
The preparation method of described Camellia nitidissima fertilizer special for organic, comprises the following steps：
Step 1, tobacco leaf is added water using after ultrasonic grind, suction filtration obtains the first filtrate and the first filter residue, toward filter residue
After middle addition ethanol is extracted 1 hour, suction filtration obtains the second filtrate and the second filter residue, subtracts after the first filtrate and the second filtrate are merged
Pressure is concentrated into the first filtrate and the second filtrate cumulative volume 1/4 obtains extract；
Step 2, by shrimp and crab shells, spoil be dried after mechanical crushing, add 2mol/L hydrochloric acid solutions, in autoclave
In, after reacting 3 hours, filtrate being filtrated to get, filtrate evaporation to be reclaimed and obtain protein concentrated solution after hydrochloric acid；
Step 3, EM bacterium are divided into two parts, first part of weight ratio with second part is 7: 3, by bagasse, soybean residue, cassava
Slag, attapulgite, fowl and animal excrement, pine needle meal, silkworm excrement are mixed into fermentation base-material, add after first part of EM bacterium, water mixing using step
The hydrochloric acid reclaimed in rapid 2 adjusts PH to 4-5 after fermentation vat sealing and fermenting 2 days, and fermentation temperature is 55 DEG C, first time centrifugal filtration
The first fermentation filter residue and the first zymotic fluid are obtained, is obtained using step 2 after the first fermentation residue adds second part of EM bacterium, water mixing
The hydrochloric acid of recovery adjusts PH to 4-5 in fermentation vat sealing and fermenting 1 day, and fermentation temperature is 50 DEG C, second centrifugal filtration to the
Two fermentation filter residues and the second zymotic fluid, PH to 6-7 is adjusted after the first zymotic fluid is merged with the second zymotic fluid using NaOH
Obtain zymotic fluid；
Step 4, nanometer pulverization will be carried out after trace element to particle diameter less than 10 microns, obtain powder；
Zymotic fluid, step that protein concentrated solution that step 5, the extract that step 1 is obtained, step 2 are obtained, step 3 are obtained
The powder obtained in rapid 4 obtains the Camellia nitidissima fertilizer special for organic after being well mixed with chitosan oligosaccharide.
Wherein, tobacco leaf and the weight ratio of water are 1: 2 in step 1, and the first filter residue is 1: 2 with the weight ratio of ethanol.
The pressure of step 2 mesohigh reactor is 20Mpa, and temperature is 50 DEG C.
Fermentation base-material and the weight ratio of the water for adding are 1: 5 in step 3, the weight ratio of the first fermentation filter residue and the water for adding
For 1: 3.
Although embodiment of the present invention is disclosed as above, it is not restricted to listed in specification and embodiment
With, it can be applied to completely various suitable the field of the invention, for those skilled in the art, can be easily
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, the present invention is not limited
In specific details and shown here as the embodiment with description.
Claims (7)
1. a kind of Camellia nitidissima fertilizer special for organic, it is characterised in that the Camellia nitidissima fertilizer special for organic includes following weight portion material
Make：Bagasse 100-200 parts, soybean residue 100-200 parts, manioc waste 50-120 parts, shrimp and crab shells 30-50 parts, EM bacterium 3-12 parts,
Spoil 30-80 parts, attapulgite 60-90 parts, fowl and animal excrement 30-80 parts, pine needle meal 20-50 parts, silkworm excrement 20-40 parts, cigarette
Leaf 30-50 parts, chitosan oligosaccharide 15-30 parts, trace element 1-6 parts；Wherein, the trace element is made up of following weight portion material：
Sodium selenite 10-15 parts, ferrous sulfate 5-10 parts, zinc sulfate 5-15 parts, water-soluble sodium molybdate 3-8 parts, manganese sulfate 5-8 parts, sulphur
Sour cobalt, sodium iodide 1-5 parts, magnesium sulfate 5-8 parts.
2. Camellia nitidissima fertilizer special for organic as claimed in claim 1, it is characterised in that the Camellia nitidissima fertilizer special for organic is by following
Weight portion material is made：Bagasse 120-180 parts, soybean residue 150-190 parts, manioc waste 80-100 parts, shrimp and crab shells 35-45 parts,
EM bacterium 5-8 parts, spoil 50-60 parts, attapulgite 75-85 parts, fowl and animal excrement 55-65 parts, pine needle meal 30-40 parts, silkworm excrement
25-35 parts, tobacco leaf 35-45 parts, chitosan oligosaccharide 20-25 parts, trace element 2-4 parts, 2mol/L hydrochloric acid solution 150-180 parts, hydrogen-oxygen
Change sodium 10-50 parts.
3. Camellia nitidissima fertilizer special for organic as claimed in claim 2, it is characterised in that the Camellia nitidissima fertilizer special for organic is by following
Weight portion material is made：175 parts of bagasse, 165 parts of soybean residue, 95 parts of manioc waste, 40 parts of shrimp and crab shells, 6 parts of EM bacterium, spoil
55 parts, 80 parts of attapulgite, 60 parts of fowl and animal excrement, 35 parts of pine needle meal, 30 parts of silkworm excrement, 40 parts of tobacco leaf, 22 parts of chitosan oligosaccharide, micro unit
3 parts of element, 170 parts of 2mol/L hydrochloric acid solutions, 25 parts of NaOH；Wherein, the trace element is made up of following weight portion material：
12 parts of sodium selenite, 7 parts of ferrous sulfate, 12 parts of zinc sulfate, water-soluble 5 parts of sodium molybdate, 6 parts of manganese sulfate, cobaltous sulfate, sodium iodide 4
Part, 6 parts of magnesium sulfate.
4. the preparation method of the Camellia nitidissima fertilizer special for organic as described in claim 1-3 arbitrarily, it is characterised in that including following
Step：
Step 1, tobacco leaf is added water using after ultrasonic grind, suction filtration obtains the first filtrate and the first filter residue, adds toward filter residue
Enter after ethanol extracts 1 hour, suction filtration obtains the second filtrate and the second filter residue, will the first filtrate and the second filtrate merge after reduce pressure dense
It is reduced to the first filtrate and the second filtrate cumulative volume 1/4 obtains extract；
Step 2, by shrimp and crab shells, spoil be dried after mechanical crushing, add 2mol/L hydrochloric acid solutions, in autoclave,
After reaction 3-6 hours, filtrate is filtrated to get, filtrate evaporation to be reclaimed and obtain protein concentrated solution after hydrochloric acid；
Step 3, EM bacterium are divided into two parts, first part of weight ratio with second part is 7: 3, by bagasse, soybean residue, manioc waste,
Attapulgite, fowl and animal excrement, pine needle meal, silkworm excrement are mixed into fermentation base-material, to add and adopt step 2 after first part of EM bacterium, water mixing
The hydrochloric acid of middle recovery adjusts PH to 4-5 after fermentation vat sealing and fermenting 2-3 days, and fermentation temperature is 55 DEG C, first time centrifugal filtration
The first fermentation filter residue and the first zymotic fluid are obtained, is obtained using step 2 after the first fermentation residue adds second part of EM bacterium, water mixing
The hydrochloric acid of recovery adjusts PH to 4-5 in fermentation vat sealing and fermenting 1-2 days, fermentation temperature is 50 DEG C, and second centrifugal filtration is arrived
Second fermentation filter residue and the second zymotic fluid, PH to 6- is adjusted after the first zymotic fluid is merged with the second zymotic fluid using NaOH
7 obtain zymotic fluid；
Step 4, nanometer pulverization will be carried out after trace element to particle diameter less than 10 microns, obtain powder；
In zymotic fluid, step 4 that protein concentrated solution that step 5, the extract that step 1 is obtained, step 2 are obtained, step 3 are obtained
The powder for obtaining obtains the Camellia nitidissima fertilizer special for organic after being well mixed with chitosan oligosaccharide.
5. the preparation method of Camellia nitidissima fertilizer special for organic as claimed in claim 4, it is characterised in that tobacco leaf and water in step 1
Weight ratio be 1: 2, the weight ratio of the first filter residue and ethanol is 1: 2.
6. the preparation method of Camellia nitidissima fertilizer special for organic as claimed in claim 4, it is characterised in that step 2 mesohigh reacts
The pressure of kettle is 20-30Mpa, and temperature is 50-60 DEG C.
7. the preparation method of Camellia nitidissima fertilizer special for organic as claimed in claim 4, it is characterised in that ferment base-material in step 3
It is 1: 5 with the weight ratio of the water for adding, the first fermentation filter residue is 1: 3 with the weight ratio of the water for adding.
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| CN107445689A (en) * | 2017-08-03 | 2017-12-08 | 钟山县良丰生态农业有限公司 | A kind of cow dung organic fertilizer and preparation method thereof |
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