CN106587912B - The processing method of the dedicated yellow glue mud of colored glaze ceramics seal - Google Patents

The processing method of the dedicated yellow glue mud of colored glaze ceramics seal Download PDF

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CN106587912B
CN106587912B CN201611021599.2A CN201611021599A CN106587912B CN 106587912 B CN106587912 B CN 106587912B CN 201611021599 A CN201611021599 A CN 201611021599A CN 106587912 B CN106587912 B CN 106587912B
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yellow glue
glue mud
mud
tumbling
yellow
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CN106587912A (en
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姜涛
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/13Compounding ingredients
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28CPREPARING CLAY; PRODUCING MIXTURES CONTAINING CLAY OR CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28C1/00Apparatus or methods for obtaining or processing clay
    • B28C1/003Plant; Methods
    • B28C1/006Methods
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B41PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41KSTAMPS; STAMPING OR NUMBERING APPARATUS OR DEVICES
    • B41K1/00Portable hand-operated devices without means for supporting or locating the articles to be stamped, i.e. hand stamps; Inking devices or other accessories therefor
    • B41K1/02Portable hand-operated devices without means for supporting or locating the articles to be stamped, i.e. hand stamps; Inking devices or other accessories therefor with one or more flat stamping surfaces having fixed images
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/02Frit compositions, i.e. in a powdered or comminuted form
    • C03C8/10Frit compositions, i.e. in a powdered or comminuted form containing lead
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/24Manufacture of porcelain or white ware
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/32Burning methods
    • C04B33/34Burning methods combined with glazing

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Structural Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Cosmetics (AREA)
  • Ceramic Products (AREA)

Abstract

A kind of processing method of the dedicated yellow glue mud of colored glaze ceramics seal, steps are as follows: S1. places the yellow glue mud taken 48 hours in shady and cool place, is preferred with loseing the cement floor of sunlight, is then fed into pulverizer and is ground into tiny particle, be preferred with 20-30 mesh screen;S2. smashed yellow glue mud is sent into tumbler and carries out tumbling processing, and when tumbling vacuumized primary every 5-8 minute, is exhausted after vacuum every time tumbling 5-10 minute, then vacuum pumping, such to recycle 2-4 times;S3. the yellow glue mud after tumbling is put into stainless cylinder of steel, in stainless-steel heating tank plus water covers yellow glue mud, then closes stainless-steel heating tank, is heated to 75-80 DEG C, and is kept for 15-18 minutes;S4. the yellow glue mud after heating is sent into pug mill and carries out pugging processing, comply with base needs, yellow glue mud, which is placed on shady place storage, after the completion can be used to base in 2-5 days.Present invention process is simple, practical, and obtained yellow glue mud plasticity is good, and deformation rate is low, and final product quality is high.

Description

The processing method of the dedicated yellow glue mud of colored glaze ceramics seal
Technical field
The present invention relates to ancient painted pottery technical fields, and in particular to a kind of processing method of the dedicated yellow glue mud of colored glaze ceramics seal.
Background technique
China is ceramic ancient country, talks about ceramics, and the foreigner just expects China.Pottery art is a kind of biomorphogenic.Ceramic form Basic material be soil, water, fire.People has only grasped the plasticity of water and soil kneading, rheological characteristic and forming method and sintering rule Rule, can just facilitate the generation and evolution of pottery art form, and ceramic implement is made to generate the form of beauty.Focus on moulding simultaneously has with what is decorated Machine combines, and by the inspiration and creativity consciousness of people's acumen, captures and the plasticity beauty, flexible beauty and performance for disclosing soil are lived Power is grasped by the people of wisdom, developed, innovated in this way there have been completely new pottery art form.Any artistic development is to certain rank Section, can all form complete skill.
Tao Yin has it from ancient times, starts from quotient's week, is contained in Qin Han.For China ancients using soil as material, digging cave is kiln, applies chisel in chalk soil On greenwave, exquisite low temperature pottery is burnt out.Potting skill is handed down from age to age, until the Sui Dynasty, the local circle head given there has been shaft kiln Burn the history of pottery, the first placed in the middle former innerland in boundary connects the Yellow River context, be with tri-coloured glazed pottery place of production Luoyang it is adjacent, boundary head tri-coloured glazed pottery device by Appearance.After thousand, the boundary head that boundary's head tri-coloured glazed pottery has evolved as today portrayed glazed colored pottery.
The remaining years are longer than this, drink the water of the Yinhe River, are from childhood companion with clay.It is slightly long, painting and calligraphy seal cutting is liked, arts institutions are read, increasing is read It goes through, increases one's knowledge.Ten Yu Nianlai explore examination with Chinese Painting and Calligraphy seal cutting art involvement circle head and portray the creation of glazed colored pottery skill, make to watch Property is integrated with practicability, is brought out the best in each other, magnificent mansion.But traditional ancient painted pottery method for cooking is not suitable for the requirement with seal, It needs to carry out innovation improvement to it.
Summary of the invention
A kind of at low cost technical problem to be solved by the present invention lies in improving, the simple colored glaze ceramics seal of method is dedicated The processing method of yellow glue mud.
The technical problems to be solved by the invention are realized using following technical scheme:
A kind of processing method of the dedicated yellow glue mud of colored glaze ceramics seal, steps are as follows:
S1. the yellow glue mud taken is placed 48 hours in shady and cool place, is preferred with loseing the cement floor of sunlight, is then sent Enter pulverizer and be ground into tiny particle, is preferred with 20-30 mesh screen;
S2. smashed yellow glue mud is sent into tumbler and carries out tumbling processing, and when tumbling vacuumized once every 5-8 minute, It exhausts after vacuum every time tumbling 5-10 minutes, then vacuum pumping, so recycles 2-4 times, so that yellow glue mud energy in tumbling procedure Enough achieve the effect that breathing massage, makes its softening, improve its plasticity;
S3. the yellow glue mud after tumbling is put into stainless cylinder of steel, in stainless-steel heating tank plus water covers yellow glue mud, then Stainless-steel heating tank is closed, is heated to 75-80 DEG C, and is kept for 15-18 minutes;It plays sterilizing, reduce activity function, Ke Yixian Writing reduces the deformation after blank is fired;
S4. the yellow glue mud after heating is sent into pug mill and carries out pugging processing, comply with base needs, it after the completion will be yellow Clay, which is placed on shady place storage, can be used to base in 2-5 days.
Yellow glue mud made from this method, can be improved the intensity of seal and the degrees of fusion of blank and glaze, and applicant is logical It crosses long period of experiments discovery to need to carry out pugging to the yellow glue mud of ecosystem, the biscuit shapeliness after firing in this way is easy to glaze Fusion, save for a long time colour-fast.
The yellow glue mud that above-mentioned yellow glue mud selects Jieshou City field battalion township domain to produce, boundary head portray the clay that glazed colored pottery print uses It is taken from local yellow glue mud, also referred to as " the Yellow River silt ", i.e., the Yellow River deposits the yellow clay to get off after spreading unchecked, and property is soft, can Plasticity is stronger, and the boundary head that can make moulding various kinds portrays glazed colored pottery print.
Further, it needs that the humidity adjustment of yellow glue mud is conducive to tumbling and is worked 20% or so in S2 step tumbling Progress.
Further, the water being added in the S3 step is pure water.
Further, the storage temperature of yellow glue mud is maintained at 18-23 DEG C in S4 step.
It is a further object to provide a kind of manufacture crafts of colored glaze seal containing above-mentioned yellow glue mud, specific to walk It is rapid as follows:
(1) seal base is made
Yellow glue mud condiments is with the hands rubbed, it is ever-changing to fall the moulding such as mud rectangularity, square or circle for disk mud moulding Tao Yinzhang base;
(2) silt is applied
To silt twice on seal base, first upper laterite, upper carclazyte is in base face afterwards, then dries in the air to half-dried;It is preferred, is avoided with drying in the shade Solar exposure;
(3) seal side money is scribed
It is scribed with iron label or bamboo stick, with the gimmicks such as picking, carving, scrape, free sketching Chinese painting (flower-and-bird painting, enjoyable scenery with hills and waters, people Object is drawn) it is engraved on seal four sides, it conveniently portrays, so that picture is generated black, white, grey artistic effect, then carved characters and fallen in print face with seal cutter Side money, not only natural interest, but also the taste of aobvious metal and stone show unique artistic effect;
(4) print face is scribed
It dries in the air after seal base to after absolutely dry, then marks, the seal cutting art of China is dissolved into the scribing of Tao Yin, chalk soil pine It is soft, it cuts down, pen integration, printed text content may be either name, and poem epigram also can be various Xiao's shapes, the lines point carved Draw it is straggly move back and forth, reasonable organization, extraordinary efficacy is unrestrained, spectacular;
(5) it is fired into kiln
It fires in two times, for the first time into kiln biscuiting, red white effect is presented;Then glazing, opposite side money part glazing, according to Picture needs, the green glaze on appropriate place, prints face part not glazing;It carries out firing into kiln for second after the completion;In terms of firing, First dehumidifying, for biscuiting temperature generally at 700 DEG C to 800 DEG C, finished product portrays Tao Yin for brick-red, is fired by glaze after biscuiting, that is, is coated with glaze It is put into after material in the saggar of ceramic, is gradually increased temperature, reach 980 DEG C, burnt two days two nights, the Tao Yin after kiln discharge is reddish brown in off-white Red, accessories are emerald green and colour of loess glaze colours, three colored glaze of self-assembling formation, four unifications are to portray glazed colored pottery print.
Boundary's head ancient painted pottery is that the mankind constantly observe in long-term production practices, in social life, constantly discover, constantly refine The crystallization constantly created.The township for being grown on ancient painted pottery is given, is inspired, the middle letter of credence oneself pursued diligently over 30 years are incorporated Seal cutting art is drawn, is repeatedly practised, rule is grasped, induction and conclusion has produced " boundary head portrays glazed colored pottery print ", extended boundary head quarter Ancient painted pottery skill is drawn, boundary head is enriched and portrays ancient painted pottery type, especially realizes the ornamental value pottery art culture mutually unified with practicability.
The glaze is formulated by the prescription of following weight percent: regeneration lead powder 5-20%, silica 40- 60%, kaolin 20-40%;In order to further increase the performance of reviver, the regeneration lead powder in glaze has carried out special work Skill processing keeps the seal color after firing vivider, the holding time is more long to improve its performance;And glaze after glaze firing Face is smooth, light, pore-free, without pinprick, and without splitting, green body is indeformable, and glaze thermal expansion coefficient is from RTT~transition temperature point after tested α < 6.0 × 10-6/℃;The middle layer of about 52 μ thickness is generated between base glaze, guarantees that base glaze has firm binding performance.
The treatment process of above-mentioned reviver is as follows:
(1) collecting the scrap lead cream generated in waste lead acid battery dismantling can form according to the difference of scrap lead cream sulfur content The interior ore pulp for adding water to be configured to mass fraction 55%-75% scrap lead cream of the reaction kettle of strong convection;
(2) the interior addition sodium carbonate into the ore pulp of step (1), wherein the additional amount of sodium carbonate is the 1.3- of theoretical amount It 1.4 times, is continuously stirred 25-35 minutes after adding sodium carbonate, process does not need to heat;
(3) by ore pulp be put into one with strong impaction, extruding, rubbing action equipment in react, while using high Concentration ore pulp material particles form frictional force, will apply in sweetening process in PbSO4The PbCO on surface3Layer open makes PbSO4Molten In liquid with Na2CO3It comes into full contact with, after reaction 20-30 minutes, reactant is separated by solid-liquid separation, the desulfurization containing sodium carbonate is obtained Mother liquor and desulfurization lead plaster;
(4) desulfurization lead plaster is sent into solidification room, chemical substance is carried out to desulfurization lead plaster with certain temperature and humidity Conversion and moisture evaporation make its moisture content≤5% by the solidification and three phases drying in 2 stages;
(5) desulfurization lead plaster after drying is ground and is sieved collection, the granularity of desulfurization lead plaster is obtained in 80-95 mesh To regeneration lead powder.
Solidify in above-mentioned steps (4) and dry design parameter be as follows:
S1. the first stage solidifies, and 80 DEG C of temperature, humidity 99.9%, time 3h is humidified using steam or atomized water;
S2. second stage solidifies, and 85 DEG C of temperature, humidity 99.9%, time 3h is humidified using steam or atomized water;
S3. the phase III is dry, and 80 DEG C of temperature, humidity 0.0%, time 36h forbids humidifying;
S4. fourth stage is dry, temperature 70 C, humidity 0.0%, and time 1.2h forbids humidifying;
S5. the 5th stage is dry, temperature 60 C, humidity 0.0%, and time 2h forbids humidifying.
The beneficial effects of the present invention are: present invention process is simple, practical, obtained yellow glue mud plasticity is good, deformation Rate is low, and final product quality is high, and the product holding time is long, colour-fast, realizes the ornamental value pottery art culture mutually unified with practicability.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below Specific embodiment is closed, the present invention is further explained.
Embodiment 1
A kind of processing method of the dedicated yellow glue mud of colored glaze ceramics seal, steps are as follows:
S1. the yellow glue mud taken is placed 48 hours in shady and cool place, is preferred with loseing the cement floor of sunlight, is then sent Enter pulverizer and be ground into tiny particle, is preferred with 20-30 mesh screen;
S2. smashed yellow glue mud is sent into tumbler and carries out tumbling processing, and when tumbling vacuumized once every 5-8 minute, It exhausts after vacuum every time tumbling 5-10 minutes, then vacuum pumping, so recycles 2-4 times, so that yellow glue mud energy in tumbling procedure Enough achieve the effect that breathing massage, makes its softening, improve its plasticity;
S3. the yellow glue mud after tumbling is put into stainless cylinder of steel, in stainless-steel heating tank plus water covers yellow glue mud, then Stainless-steel heating tank is closed, is heated to 75-80 DEG C, and is kept for 15-18 minutes;It plays sterilizing, reduce activity function, Ke Yixian Writing reduces the deformation after blank is fired;
S4. the yellow glue mud after heating is sent into pug mill and carries out pugging processing, comply with base needs, it after the completion will be yellow Clay, which is placed on shady place storage, can be used to base in 2-5 days.
Yellow glue mud made from this method, can be improved the intensity of seal and the degrees of fusion of blank and glaze, and applicant is logical It crosses long period of experiments discovery to need to carry out pugging to the yellow glue mud of ecosystem, the biscuit shapeliness after firing in this way is easy to glaze Fusion, save for a long time colour-fast.
The yellow glue mud that above-mentioned yellow glue mud selects Jieshou City field battalion township domain to produce, boundary head portray the clay that glazed colored pottery print uses It is taken from local yellow glue mud, also referred to as " the Yellow River silt ", i.e., the Yellow River deposits the yellow clay to get off after spreading unchecked, and property is soft, can Plasticity is stronger, and the boundary head that can make moulding various kinds portrays glazed colored pottery print.
Embodiment 2
A kind of processing method of the dedicated yellow glue mud of colored glaze ceramics seal, steps are as follows:
S1. the yellow glue mud taken is placed 48 hours in shady and cool place, is preferred with loseing the cement floor of sunlight, is then sent Enter pulverizer and be ground into tiny particle, is preferred with 20-30 mesh screen;
S2. smashed yellow glue mud is sent into tumbler and carries out tumbling processing, by the humidity adjustment of yellow glue mud 20% or so, Conducive to the progress of tumbling work;It vacuumized every 5-8 minutes primary when tumbling, exhausts after vacuum tumbling 5-10 minutes every time, so Vacuum pumping afterwards, so circulation 2-4 times make its softening so that yellow glue mud can achieve the effect that breathing massage in tumbling procedure, Improve its plasticity;
S3. the yellow glue mud after tumbling is put into stainless cylinder of steel, in stainless-steel heating tank plus pure water covers yellow glue mud, so Stainless-steel heating tank is closed afterwards, is heated to 75-80 DEG C, and is kept for 15-18 minutes;It plays sterilizing, reduce activity function, it can be with Significantly reduce the deformation after blank is fired;
S4. the yellow glue mud after heating is sent into pug mill and carries out pugging processing, comply with base needs, it after the completion will be yellow Clay, which is placed on shady place storage, can be used to base in 2-5 days.
Yellow glue mud made from this method, can be improved the intensity of seal and the degrees of fusion of blank and glaze, and applicant is logical It crosses long period of experiments discovery to need to carry out pugging to the yellow glue mud of ecosystem, the biscuit shapeliness after firing in this way is easy to glaze Fusion, save for a long time colour-fast.
The yellow glue mud that above-mentioned yellow glue mud selects Jieshou City field battalion township domain to produce, boundary head portray the clay that glazed colored pottery print uses It is taken from local yellow glue mud, also referred to as " the Yellow River silt ", i.e., the Yellow River deposits the yellow clay to get off after spreading unchecked, and property is soft, can Plasticity is stronger, and the boundary head that can make moulding various kinds portrays glazed colored pottery print.
Embodiment 3
A kind of processing method of the dedicated yellow glue mud of colored glaze ceramics seal, steps are as follows:
S1. the yellow glue mud taken is placed 48 hours in shady and cool place, is preferred with loseing the cement floor of sunlight, is then sent Enter pulverizer and be ground into tiny particle, is preferred with 20-30 mesh screen;
S2. smashed yellow glue mud is sent into tumbler and carries out tumbling processing, by the humidity adjustment of yellow glue mud 20% or so, Conducive to the progress of tumbling work;It vacuumized every 5-8 minutes primary when tumbling, exhausts after vacuum tumbling 5-10 minutes every time, so Vacuum pumping afterwards, so circulation 2-4 times make its softening so that yellow glue mud can achieve the effect that breathing massage in tumbling procedure, Improve its plasticity;
S3. the yellow glue mud after tumbling is put into stainless cylinder of steel, in stainless-steel heating tank plus pure water covers yellow glue mud, so Stainless-steel heating tank is closed afterwards, is heated to 75-80 DEG C, and is kept for 15-18 minutes;It plays sterilizing, reduce activity function, it can be with Significantly reduce the deformation after blank is fired;
S4. the yellow glue mud after heating is sent into pug mill and carries out pugging processing, comply with base needs, it after the completion will be yellow Clay, which is placed on shady place storage, can be used to base in 2-5 days, and storage temperature is maintained at 18-23 DEG C.
Yellow glue mud made from this method, can be improved the intensity of seal and the degrees of fusion of blank and glaze, and applicant is logical It crosses long period of experiments discovery to need to carry out pugging to the yellow glue mud of ecosystem, the biscuit shapeliness after firing in this way is easy to glaze Fusion, save for a long time colour-fast.
The yellow glue mud that above-mentioned yellow glue mud selects Jieshou City field battalion township domain to produce, boundary head portray the clay that glazed colored pottery print uses It is taken from local yellow glue mud, also referred to as " the Yellow River silt ", i.e., the Yellow River deposits the yellow clay to get off after spreading unchecked, and property is soft, can Plasticity is stronger, and the boundary head that can make moulding various kinds portrays glazed colored pottery print.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (5)

1. a kind of processing method of the dedicated yellow glue mud of colored glaze ceramics seal, it is characterised in that steps are as follows:
S1. the yellow glue mud taken is placed 48 hours in shady and cool place, using the cement floor for loseing sunlight as set-point, is then sent Enter pulverizer and be ground into tiny particle, crosses 20-30 mesh screen;
S2. smashed yellow glue mud is sent into tumbler and carries out tumbling processing, and when tumbling vacuumized once, every time every 5-8 minute Tumbling 5-10 minutes are exhausted after vacuum, then vacuum pumping, so circulation 2-4 times;
S3. the yellow glue mud after tumbling is put into stainless cylinder of steel, in stainless-steel heating tank plus water covers yellow glue mud, then will not The steel heating tank that becomes rusty is closed, and is heated to 75-80 DEG C, and kept for 15-18 minutes;
S4. the yellow glue mud after heating is sent into pug mill and carries out pugging processing, base needs are complied with, after the completion by yellow glue mud Being placed on shady place storage can be used to base in 2-5 days.
2. the processing method of the dedicated yellow glue mud of colored glaze ceramics seal according to claim 1, which is characterized in that above-mentioned yellow glue The yellow glue mud that mud selects Jieshou City field battalion township domain to produce.
3. the processing method of the dedicated yellow glue mud of colored glaze ceramics seal according to claim 1, which is characterized in that in S2 step It needs to adjust the humidity of yellow glue mud 20% in tumbling.
4. the processing method of the dedicated yellow glue mud of colored glaze ceramics seal according to claim 1, which is characterized in that in S3 step The water of middle addition is pure water.
5. the processing method of the dedicated yellow glue mud of colored glaze ceramics seal according to claim 1, which is characterized in that in S4 step The storage temperature of middle yellow glue mud is maintained at 18-23 DEG C.
CN201611021599.2A 2016-11-21 2016-11-21 The processing method of the dedicated yellow glue mud of colored glaze ceramics seal Expired - Fee Related CN106587912B (en)

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CN107522465B (en) * 2017-09-19 2018-08-24 界首市伟盛古窑彩陶制作发展有限公司 A kind of preparation method of high-quality ceramics seal
CN107932702B (en) * 2017-11-14 2019-09-24 马铭 A kind of preparation method of seal
CN108911698B (en) * 2018-08-13 2020-05-22 福建省德化环宇陶瓷有限公司 Preparation method of corrosion-resistant high-permeability environment-friendly ceramic

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