CN106566615A - 一种机械切割液及其制备方法 - Google Patents

一种机械切割液及其制备方法 Download PDF

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CN106566615A
CN106566615A CN201610928826.3A CN201610928826A CN106566615A CN 106566615 A CN106566615 A CN 106566615A CN 201610928826 A CN201610928826 A CN 201610928826A CN 106566615 A CN106566615 A CN 106566615A
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邓集叶
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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06—Metal compounds
    • C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/085—Phosphorus oxides, acids or salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/16—Naphthenic acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/08—Halogenated waxes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
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    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling

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  • General Chemical & Material Sciences (AREA)
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Abstract

本发明涉及一种机械切割液及其制备方法，由如下重量份数的组分制成：油酸10‑15份、松香8‑11份、乳化剂4‑8份、氢氧化钠水溶液11‑13份、磷酸氢二钠5‑9份、石油磺酸钠6‑12份、氯化石蜡3‑7份、环烷酸铅4‑9份、三乙醇胺油酸皂8‑13份和机油20‑50份。本发明的有益效果是：该切割液稳定性得到了提高，在加工过程中不容易出现油水分离，能够减少对电蚀产物的派出与切割速度的影响，减轻电极丝的损耗。

Description

一种机械切割液及其制备方法
技术领域
本发明涉及机械加工领域，具体涉及一种机械切割液及其制备方法。
背景技术
目前大多数控线切割机床均为慢速走丝，一般采用去离子水为工作液。由于工作液中加入少量的表面活性剂，可使介电液中的微粒减少，因而可以提高电加工工艺效果，但快走丝线切割加工只有在液体介质中进行最为稳定，并且乳化液对加工工艺指标如切割速率、工件表面粗糙度和加工精度等影响很大，快走丝线切割在加工过程中电极丝和工件之间的温度很高很容易造成电极丝的使用寿命变短，且加工是在窄缝中进行的，切割过程中的电蚀产物很难排除，金属表面容易锈蚀。
发明内容
综上所述，为了克服现有技术的不足，本发明所要解决的技术问题是提供一种机械切割液及其制备方法。
本发明解决上述技术问题的技术方案如下：一种机械切割液，由如下重量份数的组分制成：油酸10-15份、松香8-11份、乳化剂4-8份、氢氧化钠水溶液11-13份、磷酸氢二钠5-9份、石油磺酸钠6-12份、氯化石蜡3-7份、环烷酸铅4-9份、三乙醇胺油酸皂8-13份和机油20-50份。
一种机械切割液的制备方法，由如下重量份数的组分制得：
(1)分别称取如下重量份数的各组分：油酸10-15份、松香8-11份、乳化剂4-8份、氢氧化钠水溶液11-13份、磷酸氢二钠5-9份、石油磺酸钠6-12份、氯化石蜡3-7份、环烷酸铅4-9份、三乙醇胺油酸皂8-13份和机油20-50份；
(2)将步骤(1)称取的油酸、松香、乳化剂、氢氧化钠水溶液和机油投入釜中后加热；
(3)待完全熔化后，依次加入不好走(1)称取的磷酸氢二钠、石油磺酸钠、氯化石蜡、环烷酸铅和三乙醇胺油酸皂后降温；
(4)搅拌后冷却至室温即得。
进一步，步骤(2)中加热至110-130℃。
进一步，步骤(3)中降温至50-70℃。
进一步，步骤(4)中搅拌40-60min。
本发明的有益效果是：该切割液稳定性得到了提高，在加工过程中不容易出现油水分离，能够减少对电蚀产物的派出与切割速度的影响，减轻电极丝的损耗。
具体实施方式
以下结合具体实例对本发明的原理和特征进行描述，所举实例只用于解释本发明，并非用于限定本发明的范围。
实施例1
一种机械切割液的制备方法，由如下重量份数的组分制得：
(1)分别称取如下重量份数的各组分：油酸10份、松香8份、乳化剂4份、氢氧化钠水溶液11份、磷酸氢二钠5份、石油磺酸钠6份、氯化石蜡3份、环烷酸铅4份、三乙醇胺油酸皂8份和机油20份；
(2)将步骤(1)称取的油酸、松香、乳化剂、氢氧化钠水溶液和机油投入釜中，加热至110℃；
(3)待完全熔化后，依次加入不好走(1)称取的磷酸氢二钠、石油磺酸钠、氯化石蜡、环烷酸铅和三乙醇胺油酸皂，降温至50℃；
(4)搅拌40min，冷却至室温即得。
实施例2
一种机械切割液的制备方法，由如下重量份数的组分制得：
(1)分别称取如下重量份数的各组分：油酸13份、松香10份、乳化剂5份、氢氧化钠水溶液12份、磷酸氢二钠7份、石油磺酸钠10份、氯化石蜡5份、环烷酸铅7份、三乙醇胺油酸皂11份和机油30份；
(2)将步骤(1)称取的油酸、松香、乳化剂、氢氧化钠水溶液和机油投入釜中，加热至120℃；
(3)待完全熔化后，依次加入不好走(1)称取的磷酸氢二钠、石油磺酸钠、氯化石蜡、环烷酸铅和三乙醇胺油酸皂，降温至60℃；
(4)搅拌50min，冷却至室温即得。
实施例3
一种机械切割液的制备方法，由如下重量份数的组分制得：
(1)分别称取如下重量份数的各组分：油酸15份、松香11份、乳化剂8份、氢氧化钠水溶液13份、磷酸氢二钠9份、石油磺酸钠12份、氯化石蜡7份、环烷酸铅9份、三乙醇胺油酸皂13份和机油50份；
(2)将步骤(1)称取的油酸、松香、乳化剂、氢氧化钠水溶液和机油投入釜中，加热至130℃；
(3)待完全熔化后，依次加入不好走(1)称取的磷酸氢二钠、石油磺酸钠、氯化石蜡、环烷酸铅和三乙醇胺油酸皂，降温至70℃；
(4)搅拌60min，冷却至室温即得。
以上所述仅为本发明的较佳实施例，并不用以限制本发明，凡在本发明的精神和原则之内，所作的任何修改、等同替换、改进等，均应包含在本发明的保护范围之内。

Claims (5)

1.一种机械切割液，其特征在于，由如下重量份数的组分制成：油酸10-15份、松香8-11份、乳化剂4-8份、氢氧化钠水溶液11-13份、磷酸氢二钠5-9份、石油磺酸钠6-12份、氯化石蜡3-7份、环烷酸铅4-9份、三乙醇胺油酸皂8-13份和机油20-50份。
2.一种机械切割液的制备方法，其特征在于，由如下重量份数的组分制得：
(1)分别称取如下重量份数的各组分：油酸10-15份、松香8-11份、乳化剂4-8份、氢氧化钠水溶液11-13份、磷酸氢二钠5-9份、石油磺酸钠6-12份、氯化石蜡3-7份、环烷酸铅4-9份、三乙醇胺油酸皂8-13份和机油20-50份；
(2)将步骤(1)称取的油酸、松香、乳化剂、氢氧化钠水溶液和机油投入釜中后加热；
(3)待完全熔化后，依次加入不好走(1)称取的磷酸氢二钠、石油磺酸钠、氯化石蜡、环烷酸铅和三乙醇胺油酸皂后降温；
(4)搅拌后冷却至室温即得。
3.根据权利要求2所述的制备方法，其特征在于，步骤(2)中加热至110-130℃。
4.根据权利要求2所述的制备方法，其特征在于，步骤(3)中降温至50-70℃。
5.根据权利要求2所述的制备方法，其特征在于，步骤(4)中搅拌40-60min。
CN201610928826.3A 2016-10-31 2016-10-31 一种机械切割液及其制备方法 Pending CN106566615A (zh)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004043537A (ja) * 2002-07-09 2004-02-12 Kyodo Yushi Co Ltd 水溶性潤滑剤組成物
CN102807910A (zh) * 2012-06-30 2012-12-05 无锡成诺精密机械有限公司 乳化切削油
CN104293432A (zh) * 2014-09-28 2015-01-21 无锡阳工机械制造有限公司 一种线切割工作液
CN104946357A (zh) * 2015-06-04 2015-09-30 苏州市宝玛数控设备有限公司 线切割加工用工作液

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004043537A (ja) * 2002-07-09 2004-02-12 Kyodo Yushi Co Ltd 水溶性潤滑剤組成物
CN102807910A (zh) * 2012-06-30 2012-12-05 无锡成诺精密机械有限公司 乳化切削油
CN104293432A (zh) * 2014-09-28 2015-01-21 无锡阳工机械制造有限公司 一种线切割工作液
CN104946357A (zh) * 2015-06-04 2015-09-30 苏州市宝玛数控设备有限公司 线切割加工用工作液

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Application publication date: 20170419