CN106554704A - A kind of solar energy reflective insulation coating and preparation method thereof - Google Patents
A kind of solar energy reflective insulation coating and preparation method thereof Download PDFInfo
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- CN106554704A CN106554704A CN201610878262.7A CN201610878262A CN106554704A CN 106554704 A CN106554704 A CN 106554704A CN 201610878262 A CN201610878262 A CN 201610878262A CN 106554704 A CN106554704 A CN 106554704A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
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- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of solar energy reflective insulation coating：In parts by weight, it is made up of following component：Meso-porous titanium dioxide Si powder MCM 41 of 23 parts of Aladdin companies；12 parts of Nano titanium dioxides；16 17 parts of Tao Shi solid epoxy DER671；Oronain hectorite draws in 12 15 parts of departments：34 parts of zinc stearates；34 parts of calcium stearates；12 parts of hydroxypropyl guar gum；23 parts of hydroxypropyl methylcellulose；45 parts of PTPP (potassium tripolyphosphate)；78 parts of butyl carbitols；89 parts of calcium silicates；67 parts of aluminium silicate；11 12 parts of melamine resin powder；12 part of 2 amino benzenethiol；0.3 0.5 parts of γ aminopropyltriethoxywerene werenes；14 15 parts of methyl iso-butyl ketone (MIBK)s；15 16 parts of toluene；89 parts of dimethylbenzene.Insulating moulding coating effect of heat insulation of the present invention is excellent, reflecting rate is high, and acid and alkali-resistance, salt spray resistance, ageing-resistant performance are excellent.
Description
Technical field
The invention belongs to paint field, more particularly to a kind of solar energy reflective insulation coating and preparation method thereof.
Background technology
There is building coating decoration functions, defencive function and livability to improve function.Proportion shared by various functions is because making
It is not quite similar with purpose difference.Decoration functions are the functions of beautifying to improve its appearance value by building.Mainly
The concept of concept and three-dimensional pattern in terms of including plane color, pattern and gloss.But will be with building itself
The size and shape of moulding and base material itself is engaged, and can just fully play out.Defencive function is referred to protects building not
The function of protected from environmental and destruction.It is different types of also different to the content that defencive function is required by protective.Such as
It is indoor just very big with index difference that is reaching required by outdoor application.Some buildings are to mould proof, fire prevention, insulation, corrosion resistant
Erosion etc. has particular/special requirement.Coating act as decorating and protects, and protects the surface for being applied jewelry, prevents from extraneous light, oxygen, change
The erosion of material, solvent etc. is learned, the service life for being applied thing is improved；Paint finishing material surface, change its color, decorative pattern,
Gloss, texture etc., improve the aesthetic value of object.Wherein, a kind of good building coating during solar reflection coating.
104371435 A of CN disclose a kind of solar energy reflective insulation coating for construction and preparation method thereof, the coating pair
In solar radiation spectrum, most of wavelength has high reflectance, reduces the temperature difference of indoor and outdoor, plays function of heat insulation；CN
104194625 A disclose a kind of organic-silicon-modified emulsion and solar energy reflective insulation coating, are reaching good reflective insulation
While effect, with preferable fire protecting performance.But effect of heat insulation of the prior art is less desirable, its synthesis of being exposed to the sun for a long time
Performance such as acid and alkali-resistance, salt spray resistance have different degrees of decline.
The content of the invention
The purpose of the present invention is to overcome deficiency of the prior art, there is provided a kind of solar energy reflective insulation coating, the present invention
Insulating moulding coating effect of heat insulation is excellent, reflecting rate is high, and acid and alkali-resistance, salt spray resistance, ageing-resistant performance are excellent.
According to an aspect of the present invention, the invention provides a kind of solar energy reflective insulation coating：According to parts by weight
Meter, is made up of following component：
Meso-porous titanium dioxide Si powder MCM-41 of 2-3 part Aladdins company；1-2 part Nano titanium dioxides；16-17 parts are made pottery
Family name solid epoxy DER671；Oronain hectorite draws in 12-15 parts department：3-4 part zinc stearates；3-4 part calcium stearates；1-2 parts
Hydroxypropyl guar gum；2-3 part hydroxypropyl methylcellulose；4-5 part PTPP (potassium tripolyphosphate)；7-8 part butyl carbitols；8-9 part calcium silicates；
6-7 part aluminium silicate；11-12 part melamine resin powder；1-2 part 2- amino benzenethiols；0.3-0.5 part gamma-amino propyl group
Triethoxysilane；14-15 part methyl iso-butyl ketone (MIBK)s；15-16 part toluene；8-9 part dimethylbenzene.
The solar energy reflective insulation coating：In parts by weight, it is made up of following component：
Meso-porous titanium dioxide Si powder MCM-41 of 2 parts of Aladdin companies；2 parts of Nano titanium dioxides；17 parts of Tao Shi solids
Epoxy resin DER671；Oronain hectorite draws in 15 parts of departments：4 parts of zinc stearates；4 parts of calcium stearates；2 parts of hydroxypropyl guar gum；3 parts
Hydroxypropyl methylcellulose；5 parts of PTPP (potassium tripolyphosphate)；8 parts of butyl carbitols；9 parts of calcium silicates；7 parts of aluminium silicate；12 parts of tripolycyanamide first
Urea formaldehyde powder；2 parts of 2- amino benzenethiols；0.5 part of γ aminopropyltriethoxy silane；15 parts of methyl iso-butyl ketone (MIBK)s；16 parts of first
Benzene；9 parts of dimethylbenzene.
According to another aspect of the present invention, the invention provides a kind of preparation method of solar energy reflective insulation coating,
Comprise the following steps：
1) weigh each raw material for standby；
2) meso-porous titanium dioxide Si powder MCM-41 is adopted with Nano titanium dioxide, Tao Shi solid epoxies DER671
Mixed at high speed cutter A is uniformly dispersed；
3) in mixed at high speed cutter A methyl iso-butyl ketone (MIBK), toluene, dimethylbenzene is added to be warming up to 65 DEG C of stirring 40min；
4) mixed at high speed cutter A is cooled to 40 DEG C, is subsequently adding department and draws oronain hectorite stirring 10min, is warming up to 50
DEG C add 2- amino benzenethiol and γ aminopropyltriethoxy silane stirring 30min；
5) zinc stearate is added in mixed at high speed cutter B；Calcium stearate；Hydroxypropyl guar gum；Hydroxypropyl methylcellulose；
PTPP (potassium tripolyphosphate)；Butyl carbitol；Calcium silicates；Aluminium silicate；Melamine resin powder shear agitation is uniformly dispersed；
6) material in cutter B is at the uniform velocity added in mixed at high speed cutter A in 2h, in 40 DEG C, 1000rpm turn
Lower high speed shear 2h of speed, is dispersed to granularity less than 20 microns；Then room temperature is cooled to, subpackage obtains solar energy reflective insulation coating.
Insulating moulding coating prepared by the present invention not only has good heat-proof quality, it is seen that luminous reflectance reaches more than 92%,
And with good acid and alkali-resistance, salt spray resistance, ageing-resistant performance.
Specific embodiment
To make the object, technical solutions and advantages of the present invention of greater clarity, with reference to specific embodiment, to this
Invention is further described.It should be understood that these descriptions are simply exemplary, and it is not intended to limit the scope of the present invention.
Meso-porous titanium dioxide Si powder MCM-41 is bought in Sigma-Aldrich (Sigma's Order with Nano titanium dioxide
Ritchie), remaining is by commercially available conventional products.
Embodiment 1
Formula：Meso-porous titanium dioxide Si powder MCM-41 of 3 parts of Aladdin companies；1 part of Nano titanium dioxide；16 parts of Tao Shi
Solid epoxy DER671；Oronain hectorite draws in 12 parts of departments：3 parts of zinc stearates；3 parts of calcium stearates；1 part of hydroxypropyl guar
Glue；2 parts of hydroxypropyl methylcellulose；4 parts of PTPP (potassium tripolyphosphate)；7 parts of butyl carbitols；8 parts of calcium silicates；6 parts of aluminium silicate；11 parts of trimerizations
Cyanamide formaldehyde resin powder；1 part of 2- amino benzenethiol；0.3 part of γ aminopropyltriethoxy silane；14 parts of methyl iso-butyl ketone (MIBK)s；
15 parts of toluene；8 parts of dimethylbenzene.
Preparation method：
1) weigh each raw material for standby；
2) meso-porous titanium dioxide Si powder MCM-41 is adopted with Nano titanium dioxide, Tao Shi solid epoxies DER671
Mixed at high speed cutter A is uniformly dispersed；
3) in mixed at high speed cutter A methyl iso-butyl ketone (MIBK), toluene, dimethylbenzene is added to be warming up to 65 DEG C of stirring 40min；
4) mixed at high speed cutter A is cooled to 40 DEG C, is subsequently adding department and draws oronain hectorite stirring 10min, is warming up to 50
DEG C add 2- amino benzenethiol and γ aminopropyltriethoxy silane stirring 30min；
5) zinc stearate is added in mixed at high speed cutter B；Calcium stearate；Hydroxypropyl guar gum；Hydroxypropyl methylcellulose；
PTPP (potassium tripolyphosphate)；Butyl carbitol；Calcium silicates；Aluminium silicate；Melamine resin powder shear agitation is uniformly dispersed；
6) material in cutter B is at the uniform velocity added in mixed at high speed cutter A in 2h, in 40 DEG C, 1000rpm turn
Lower high speed shear 2h of speed, is dispersed to granularity less than 20 microns；Then room temperature is cooled to, subpackage obtains solar energy reflective insulation coating.
Embodiment 2
Meso-porous titanium dioxide Si powder MCM-41 of 2 parts of Aladdin companies；2 parts of Nano titanium dioxides；17 parts of Tao Shi solids
Epoxy resin DER671；Oronain hectorite draws in 15 parts of departments：4 parts of zinc stearates；4 parts of calcium stearates；2 parts of hydroxypropyl guar gum；3 parts
Hydroxypropyl methylcellulose；5 parts of PTPP (potassium tripolyphosphate)；8 parts of butyl carbitols；9 parts of calcium silicates；7 parts of aluminium silicate；12 parts of tripolycyanamide first
Urea formaldehyde powder；2 parts of 2- amino benzenethiols；0.5 part of γ aminopropyltriethoxy silane；15 parts of methyl iso-butyl ketone (MIBK)s；16 parts of first
Benzene；9 parts of dimethylbenzene.
Preparation method is with embodiment 1
Coating property is detected：The micro- spectrum in coating property detection commission third party testing agency Shanghai is according to GB/T9755-2001
Detection, testing result are as shown in table 1 below:
1 coating property testing result of the present invention of table
Result above shows that the insulating moulding coating of present invention preparation not only has good heat-proof quality, it is seen that luminous reflectance reaches
To more than 92%, and with good acid and alkali-resistance, salt spray resistance, ageing-resistant performance.
Although embodiments of the present invention are described in detail, it should be understood that, without departing from the present invention's
In the case of spirit and scope, embodiments of the present invention can be made with various changes, replace and change.
Claims (3)
1. a kind of solar energy reflective insulation coating：In parts by weight, it is made up of following component：
Meso-porous titanium dioxide Si powder MCM-41 of 2-3 part Aladdins company；1-2 part Nano titanium dioxides；16-17 parts Tao Shi is solid
Body epoxy resin DER671；Oronain hectorite draws in 12-15 parts department：3-4 part zinc stearates；3-4 part calcium stearates；1-2 part hydroxypropyls
Base guar gum；2-3 part hydroxypropyl methylcellulose；4-5 part PTPP (potassium tripolyphosphate)；7-8 part butyl carbitols；8-9 part calcium silicates；6-7
Part aluminium silicate；11-12 part melamine resin powder；1-2 part 2- amino benzenethiols；Three second of 0.3-0.5 part gamma-aminos propyl group
TMOS；14-15 part methyl iso-butyl ketone (MIBK)s；15-16 part toluene；8-9 part dimethylbenzene.
2. a kind of solar energy reflective insulation coating according to claim 1, it is characterised in that：The solar energy reflective insulation
Coating：In parts by weight, it is made up of following component：Meso-porous titanium dioxide Si powder MCM-41 of 2 parts of Aladdin companies；2 parts
Nano titanium dioxide；17 parts of Tao Shi solid epoxy DER671；Oronain hectorite draws in 15 parts of departments：4 parts of zinc stearates；4 parts
Calcium stearate；2 parts of hydroxypropyl guar gum；3 parts of hydroxypropyl methylcellulose；5 parts of PTPP (potassium tripolyphosphate)；8 parts of butyl carbitols；9 parts of silicon
Sour calcium；7 parts of aluminium silicate；12 parts of melamine resin powder；2 parts of 2- amino benzenethiols；0.5 part of three ethoxy of gamma-amino propyl group
Base silane；15 parts of methyl iso-butyl ketone (MIBK)s；16 parts of toluene；9 parts of dimethylbenzene.
3. a kind of solar energy reflective insulation coating preparation method described in a kind of claim 1, comprises the following steps：
1) weigh each raw material for standby；
2) meso-porous titanium dioxide Si powder MCM-41 is adopted at a high speed with Nano titanium dioxide, Tao Shi solid epoxies DER671
Mixing cutter A is uniformly dispersed；
3) in mixed at high speed cutter A methyl iso-butyl ketone (MIBK), toluene, dimethylbenzene is added to be warming up to 65 DEG C of stirring 40min；
4) mixed at high speed cutter A is cooled to 40 DEG C, is subsequently adding department and draws oronain hectorite stirring 10min, is warming up to 50 DEG C and adds
Enter 2- amino benzenethiol and γ aminopropyltriethoxy silane stirring 30min；
5) zinc stearate is added in mixed at high speed cutter B；Calcium stearate；Hydroxypropyl guar gum；Hydroxypropyl methylcellulose；Trimerization
Potassium phosphate；Butyl carbitol；Calcium silicates；Aluminium silicate；Melamine resin powder shear agitation is uniformly dispersed；
6) material in cutter B is at the uniform velocity added in mixed at high speed cutter A in 2h, under 40 DEG C, the rotating speed of 1000rpm
High speed shear 2h, is dispersed to granularity less than 20 microns；Then room temperature is cooled to, subpackage obtains solar energy reflective insulation coating.
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| CN201610878262.7A CN106554704A (en) | 2016-10-08 | 2016-10-08 | A kind of solar energy reflective insulation coating and preparation method thereof |
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| CN201610878262.7A CN106554704A (en) | 2016-10-08 | 2016-10-08 | A kind of solar energy reflective insulation coating and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107446493A (en) * | 2017-08-03 | 2017-12-08 | 安徽新智电力科技有限公司 | A kind of power distribution cabinet insulating moulding coating and preparation method thereof |
| CN110374273A (en) * | 2019-07-12 | 2019-10-25 | 安康学院 | A kind of flat roof structure and its construction method |
| CN110951308A (en) * | 2019-11-29 | 2020-04-03 | 华东交通大学理工学院 | Preparation method of near-infrared reflecting material based on spherical MCM-41 |
| CN111117404A (en) * | 2019-12-31 | 2020-05-08 | 华东交通大学理工学院 | Heat-insulating coating and preparation method thereof |
| CN111234628A (en) * | 2020-02-10 | 2020-06-05 | 华东交通大学理工学院 | Reflective heat-insulating coating for outer wall and preparation method thereof |
| CN112194922A (en) * | 2019-07-08 | 2021-01-08 | 常州市大使涂料有限公司 | Heat-insulating cool adhesive coating and preparation method thereof |
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| CN1800283A (en) * | 2005-01-05 | 2006-07-12 | 中国科学院过程工程研究所 | Insulating mold coating and its uses |
| CN101812269A (en) * | 2010-04-12 | 2010-08-25 | 刘清华 | Solar heat radiation reflection coating |
| JP2013151646A (en) * | 2011-10-23 | 2013-08-08 | Daiwa:Kk | Heat-insulating coating composition, and coated material coated with the heat-insulating coating composition |
| CN104774528A (en) * | 2015-03-12 | 2015-07-15 | 江苏科技大学 | Anticorrosion heat-insulation paint and preparation method thereof |
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2016
- 2016-10-08 CN CN201610878262.7A patent/CN106554704A/en active Pending
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| CN1800283A (en) * | 2005-01-05 | 2006-07-12 | 中国科学院过程工程研究所 | Insulating mold coating and its uses |
| CN101812269A (en) * | 2010-04-12 | 2010-08-25 | 刘清华 | Solar heat radiation reflection coating |
| JP2013151646A (en) * | 2011-10-23 | 2013-08-08 | Daiwa:Kk | Heat-insulating coating composition, and coated material coated with the heat-insulating coating composition |
| CN104774528A (en) * | 2015-03-12 | 2015-07-15 | 江苏科技大学 | Anticorrosion heat-insulation paint and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107446493A (en) * | 2017-08-03 | 2017-12-08 | 安徽新智电力科技有限公司 | A kind of power distribution cabinet insulating moulding coating and preparation method thereof |
| CN112194922A (en) * | 2019-07-08 | 2021-01-08 | 常州市大使涂料有限公司 | Heat-insulating cool adhesive coating and preparation method thereof |
| CN110374273A (en) * | 2019-07-12 | 2019-10-25 | 安康学院 | A kind of flat roof structure and its construction method |
| CN110951308A (en) * | 2019-11-29 | 2020-04-03 | 华东交通大学理工学院 | Preparation method of near-infrared reflecting material based on spherical MCM-41 |
| CN110951308B (en) * | 2019-11-29 | 2021-07-27 | 华东交通大学理工学院 | Preparation method of near-infrared reflecting material based on spherical MCM-41 |
| CN111117404A (en) * | 2019-12-31 | 2020-05-08 | 华东交通大学理工学院 | Heat-insulating coating and preparation method thereof |
| CN111234628A (en) * | 2020-02-10 | 2020-06-05 | 华东交通大学理工学院 | Reflective heat-insulating coating for outer wall and preparation method thereof |
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Application publication date: 20170405 |
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