CN106544103A - A kind of hydraulic guide rail oil and preparation method thereof - Google Patents

A kind of hydraulic guide rail oil and preparation method thereof Download PDF

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Publication number
CN106544103A
CN106544103A CN201610948872.XA CN201610948872A CN106544103A CN 106544103 A CN106544103 A CN 106544103A CN 201610948872 A CN201610948872 A CN 201610948872A CN 106544103 A CN106544103 A CN 106544103A
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parts
oil
minutes
guide rail
hydraulic guide
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金福英
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04Mixtures of base-materials and additives
    • C10M169/045Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
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    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
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    • C10M2201/041Carbon; Graphite; Carbon black
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    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08Inorganic acids or salts thereof
    • C10M2201/082Inorganic acids or salts thereof containing nitrogen
    • C10M2201/083Inorganic acids or salts thereof containing nitrogen nitrites
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    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
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    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10Carboxylix acids; Neutral salts thereof
    • C10M2207/12Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
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    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10Carboxylix acids; Neutral salts thereof
    • C10M2207/12Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
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    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28Esters
    • C10M2207/286Esters of polymerised unsaturated acids
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    • C10M2207/40Fatty vegetable or animal oils
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    • C10M2215/08Amides
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    • C10M2219/00Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/02Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
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    • C10M2223/00Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04Phosphate esters
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    • C10M2229/04Siloxanes with specific structure
    • C10M2229/0405Siloxanes with specific structure used as base material
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    • C10N2020/00Specified physical or chemical properties or characteristics, i.e. function, of component of lubricating compositions
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    • C10N2040/08Hydraulic fluids, e.g. brake-fluids

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Abstract

The invention provides a kind of hydraulic guide rail oil and preparation method thereof.It is prepared from by following steps:(1)By white oil, hydroisomerizing dewaxing and Petiolus Trachycarpi oil mixing, 60 80 DEG C are heated to, are stirred 5 10 minutes;(2)Polyisobutylene, aluminum oleate, silicone oil, palmitic acid, single Tryfac 5573, sulfuration arctic sperm oil, ternary polycarboxylic acids and lauroylamidopropyl betaine are added, is stirred 20 40 minutes under 300 500r/min of rotating speed;(3)Nano diamond and sodium nitrite are added, is stirred 10 30 minutes under 200 400r/min of rotating speed, ultrasound is carried out in being put into Ultrasound Instrument 38 minutes;(4)After being down to room temperature, it is ground 30 60 minutes in adding grinder and obtains final product.It is an object of the invention to provide a kind of hydraulic guide rail oil, with higher viscosity index (VI), using wide temperature range, anti-creep performance is remarkable, while antioxygenic property is good, the up time is long, life-span length.

Description

A kind of hydraulic guide rail oil and preparation method thereof
Technical field
The present invention relates to fine chemistry industry Material Field, and in particular to a kind of hydraulic guide rail oil and preparation method thereof.
Background technology
Guide rail is one of important moving parts of lathe, and its motion mode is reciprocal, pause alternate motion, usually can Generation creeping phenomenon.There is confficient of static friction of the reason for the creeping mainly between upper and lower rails more than the coefficient of kinetic friction in lathe, Quiet coefficient of kinetic friction difference is bigger, and generation is creeped more serious.Slide creeping, has had a strong impact on machining accuracy and the surface of product Fineness, also shortens lathe and cutting-tool's used life.And machine tool guideway produce creep and lubricant has larger relation, Thus require oiliness fabulous and the appropriate lubricating oil of viscosity, to keep the mixing of the fluid lubrication or approximate fluid applications of thin oil film Lubricating status.It is exactly the precision machine tool lubricating oil for being used for hydraulic pressure and guide rail lubrication for an oil piping system that hydraulic guide rail oil is, because This requirement is provided simultaneously with the dual performance of hydraulic oil and rail oil.Hydraulic guide rail oil is except requiring good antioxidant, resisting Outside mill property, breaking and anti-foaming property, slide creeping to be most importantly prevented, therefore, research and development non-oxidizability is good, anti-to creep Can get well and the hydraulic guide rail oil of long service life has great importance and is worth.
The content of the invention
Technical problem to be solved:It is an object of the invention to provide a kind of hydraulic guide rail oil, with higher viscosity index (VI), Using wide temperature range, anti-creep performance is remarkable, while antioxygenic property is good, the up time is long, life-span length.
Technical scheme:A kind of hydraulic guide rail oil, is prepared from weight portion by following component:White oil 50-70 parts, hydrogenation are different Structure dewaxing 15-30 parts, Petiolus Trachycarpi oil 10-20 parts, polyisobutylene 3-5 parts, Nano diamond 0.5-1 parts, aluminum oleate 1-3 parts, silicone oil 2-5 parts, palmitic acid 3-6 parts, single Tryfac 5573 2-5 parts, sulfuration arctic sperm oil 2-5 parts, ternary polycarboxylic acids 1-2 parts, Laurel Amido propyl betaine 1-3 parts, sodium nitrite 0.5-1 parts.
It is further preferred that a kind of described hydraulic guide rail oil, is prepared from weight portion by following component:White oil 55- 65 parts, hydroisomerizing dewaxing 20-25 parts, Petiolus Trachycarpi oil 12-18 parts, polyisobutylene 3.5-4.5 parts, Nano diamond 0.6-0.9 parts, Aluminum oleate 1.5-2.5 parts, silicone oil 3-4 parts, palmitic acid 4-5 parts, single Tryfac 5573 3-4 parts, sulfuration arctic sperm oil 3-4 parts, Ternary polycarboxylic acids 1.2-1.8 parts, lauroylamidopropyl betaine 1.5-2.5 parts, sodium nitrite 0.6-0.9 parts.
The preparation method of above-mentioned degradable packaging material is comprised the following steps:
(1)By white oil, hydroisomerizing dewaxing and Petiolus Trachycarpi oil mixing, 60-80 DEG C is heated to, 5-10 minutes are stirred;
(2)Add polyisobutylene, aluminum oleate, silicone oil, palmitic acid, single Tryfac 5573, sulfuration arctic sperm oil, the poly- carboxylic of ternary Acid and lauroylamidopropyl betaine, stir 20-40 minutes under rotating speed 300-500r/min;
(3)Nano diamond and sodium nitrite are added, is stirred 10-30 minutes under rotating speed 200-400r/min, is put into Ultrasound Instrument In carry out ultrasonic 3-8 minutes;
(4)After being down to room temperature, 30-60 minutes are ground in adding grinder and are obtained final product.
It is further preferred that step(1)In be heated to 65-75 DEG C, mixing time be 6-9 minutes.
It is further preferred that step(2)Middle rotating speed is 350-450r/min, and mixing time is 25-35 minutes.
It is further preferred that step(3)Middle rotating speed be 250-350r/min, mixing time be 15-25 minutes, ultrasonic time For 4-6 minutes.
It is further preferred that step(4)Middle milling time is 40-50 minutes.
Beneficial effect:A kind of hydraulic guide rail oil of the present invention, with higher viscosity index (VI), reaches as high as 114, using temperature Degree scope is wide, and static and dynamic friction coefficient difference is only 0.078, and anti-creep performance is remarkable, meanwhile, the rotary oxygen bomb time up to 269min, Antioxygenic property is good, and use time is long, life-span length.
Specific embodiment
Embodiment 1
A kind of hydraulic guide rail oil, is prepared from weight portion by following component:50 parts of white oil, hydroisomerizing dewaxing 15 parts, Petiolus Trachycarpi 10 parts of oil, 3 parts of polyisobutylene, 0.5 part of Nano diamond, 1 part of aluminum oleate, 2 parts of silicone oil, 3 parts of palmitic acid, single Tryfac 5573 2 parts, sulfuration 2 parts of arctic sperm oil, 1 part of ternary polycarboxylic acids, 1 part of lauroylamidopropyl betaine, 0.5 part of sodium nitrite.
The preparation method of above-mentioned degradable packaging material is:
(1)By white oil, hydroisomerizing dewaxing and Petiolus Trachycarpi oil mixing, 60 DEG C are heated to, are stirred 5 minutes;
(2)Add polyisobutylene, aluminum oleate, silicone oil, palmitic acid, single Tryfac 5573, sulfuration arctic sperm oil, the poly- carboxylic of ternary Acid and lauroylamidopropyl betaine, stir 20 minutes under rotating speed 300r/min;
(3)Nano diamond and sodium nitrite are added, is stirred 10 minutes under rotating speed 200r/min, is carried out in being put into Ultrasound Instrument Ultrasound 3 minutes;
(4)After being down to room temperature, it is ground 30 minutes in adding grinder and obtains final product.
Embodiment 2
A kind of hydraulic guide rail oil, is prepared from weight portion by following component:55 parts of white oil, hydroisomerizing dewaxing 20 parts, Petiolus Trachycarpi 12 parts of oil, 3.5 parts of polyisobutylene, 0.6 part of Nano diamond, 1.5 parts of aluminum oleate, 3 parts of silicone oil, 4 parts of palmitic acid, single lauryl phosphorus 3 parts of acid esters, 3 parts of arctic sperm oil of sulfuration, 1.2 parts of ternary polycarboxylic acids, 1.5 parts of lauroylamidopropyl betaine, sodium nitrite 0.6 Part.
The preparation method of above-mentioned degradable packaging material is:
(1)By white oil, hydroisomerizing dewaxing and Petiolus Trachycarpi oil mixing, 65 DEG C are heated to, are stirred 6 minutes;
(2)Add polyisobutylene, aluminum oleate, silicone oil, palmitic acid, single Tryfac 5573, sulfuration arctic sperm oil, the poly- carboxylic of ternary Acid and lauroylamidopropyl betaine, stir 25 minutes under rotating speed 350r/min;
(3)Nano diamond and sodium nitrite are added, is stirred 15 minutes under rotating speed 250r/min, is carried out in being put into Ultrasound Instrument Ultrasound 4 minutes;
(4)After being down to room temperature, it is ground 40 minutes in adding grinder and obtains final product.
Embodiment 3
A kind of hydraulic guide rail oil, is prepared from weight portion by following component:60 parts of white oil, 22.5 parts of hydroisomerizing dewaxing, palm fibre 15 parts of palmitic acid oil, 4 parts of polyisobutylene, 0.75 part of Nano diamond, 2 parts of aluminum oleate, 3.5 parts of silicone oil, 4.5 parts of palmitic acid, single Laurel 3.5 parts of base phosphate ester, 3.5 parts of arctic sperm oil of sulfuration, 1.5 parts of ternary polycarboxylic acids, 2 parts of lauroylamidopropyl betaine, nitrous acid 0.75 part of sodium.
The preparation method of above-mentioned degradable packaging material is:
(1)By white oil, hydroisomerizing dewaxing and Petiolus Trachycarpi oil mixing, 70 DEG C are heated to, are stirred 7 minutes;
(2)Add polyisobutylene, aluminum oleate, silicone oil, palmitic acid, single Tryfac 5573, sulfuration arctic sperm oil, the poly- carboxylic of ternary Acid and lauroylamidopropyl betaine, stir 30 minutes under rotating speed 400r/min;
(3)Nano diamond and sodium nitrite are added, is stirred 20 minutes under rotating speed 300r/min, is carried out in being put into Ultrasound Instrument Ultrasound 5 minutes;
(4)After being down to room temperature, it is ground 50 minutes in adding grinder and obtains final product.
Embodiment 4
A kind of hydraulic guide rail oil, is prepared from weight portion by following component:65 parts of white oil, hydroisomerizing dewaxing 25 parts, Petiolus Trachycarpi 18 parts of oil, 4.5 parts of polyisobutylene, 0.9 part of Nano diamond, 2.5 parts of aluminum oleate, 4 parts of silicone oil, 5 parts of palmitic acid, single lauryl phosphorus 4 parts of acid esters, 4 parts of arctic sperm oil of sulfuration, 1.8 parts of ternary polycarboxylic acids, 2.5 parts of lauroylamidopropyl betaine, sodium nitrite 0.9 Part.
The preparation method of above-mentioned degradable packaging material is:
(1)By white oil, hydroisomerizing dewaxing and Petiolus Trachycarpi oil mixing, 75 DEG C are heated to, are stirred 9 minutes;
(2)Add polyisobutylene, aluminum oleate, silicone oil, palmitic acid, single Tryfac 5573, sulfuration arctic sperm oil, the poly- carboxylic of ternary Acid and lauroylamidopropyl betaine, stir 35 minutes under rotating speed 450r/min;
(3)Nano diamond and sodium nitrite are added, is stirred 25 minutes under rotating speed 350r/min, is carried out in being put into Ultrasound Instrument Ultrasound 6 minutes;
(4)After being down to room temperature, it is ground 50 minutes in adding grinder and obtains final product.
Embodiment 5
A kind of hydraulic guide rail oil, is prepared from weight portion by following component:70 parts of white oil, hydroisomerizing dewaxing 30 parts, Petiolus Trachycarpi 20 parts of oil, 5 parts of polyisobutylene, 1 part of Nano diamond, 3 parts of aluminum oleate, 5 parts of silicone oil, 6 parts of palmitic acid, single Tryfac 5573 5 Part, 5 parts of arctic sperm oil of sulfuration, 2 parts of ternary polycarboxylic acids, 3 parts of lauroylamidopropyl betaine, 1 part of sodium nitrite.
The preparation method of above-mentioned degradable packaging material is:
(1)By white oil, hydroisomerizing dewaxing and Petiolus Trachycarpi oil mixing, 80 DEG C are heated to, are stirred 10 minutes;
(2)Add polyisobutylene, aluminum oleate, silicone oil, palmitic acid, single Tryfac 5573, sulfuration arctic sperm oil, the poly- carboxylic of ternary Acid and lauroylamidopropyl betaine, stir 40 minutes under rotating speed 500r/min;
(3)Nano diamond and sodium nitrite are added, is stirred 30 minutes under rotating speed 400r/min, is carried out in being put into Ultrasound Instrument Ultrasound 8 minutes;
(4)After being down to room temperature, it is ground 60 minutes in adding grinder and obtains final product.
Comparative example 1
The present embodiment is not contain Nano diamond and aluminum oleate with the difference of embodiment 2.Specifically:
A kind of hydraulic guide rail oil, is prepared from weight portion by following component:55 parts of white oil, hydroisomerizing dewaxing 20 parts, Petiolus Trachycarpi 12 parts of oil, 3.5 parts of polyisobutylene, 3 parts of silicone oil, 4 parts of palmitic acid, single 3 parts of Tryfac 5573,3 parts of arctic sperm oil of sulfuration, ternary 1.2 parts of polycarboxylic acids, 1.5 parts of lauroylamidopropyl betaine, 0.6 part of sodium nitrite.
The preparation method of above-mentioned degradable packaging material is:
(1)By white oil, hydroisomerizing dewaxing and Petiolus Trachycarpi oil mixing, 65 DEG C are heated to, are stirred 6 minutes;
(2)Add polyisobutylene, silicone oil, palmitic acid, single Tryfac 5573, sulfuration arctic sperm oil, ternary polycarboxylic acids and Laurel Amido propyl betaine, stirs 25 minutes under rotating speed 350r/min;
(3)Sodium nitrite is added, is stirred 15 minutes under rotating speed 250r/min, ultrasound is carried out in being put into Ultrasound Instrument 4 minutes;
(4)After being down to room temperature, it is ground 40 minutes in adding grinder and obtains final product.
The property indices of the hydraulic guide rail oil of the present invention see the table below, it may be seen that there is higher viscosity to refer to for which Number, reaches as high as 114, and using wide temperature range, the method for evaluation rail oil anti-creep performance is more at present, but does not also have both at home and abroad The unified, method that countries in the world are general, anti-creep stick-slip characteristic test method(s) (the more elegant type stick-slip characteristic examination of China's rail oil Test machine method) determine, it can be seen that the static and dynamic friction coefficient difference of this material is only 0.078, and anti-creep performance is remarkable, meanwhile, this material The material rotary oxygen bomb time, antioxygenic property was good, and use time is long, life-span length up to 269min.
The property indices of 1 hydraulic guide rail oil of table
Name of product Viscosity index (VI) Static and dynamic friction coefficient difference(0.8mm2/s 1960N) Rotary oxygen bomb(min)
Embodiment 1 107 0.087 267
Embodiment 2 109 0.085 268
Embodiment 3 111 0.081 268
Embodiment 4 114 0.078 269
Embodiment 5 112 0.082 268
Comparative example 1 101 0.093 246

Claims (7)

1. a kind of hydraulic guide rail oil, it is characterised in that:It is prepared from weight portion by following component:White oil 50-70 parts, hydrogenation are different Structure dewaxing 15-30 parts, Petiolus Trachycarpi oil 10-20 parts, polyisobutylene 3-5 parts, Nano diamond 0.5-1 parts, aluminum oleate 1-3 parts, silicone oil 2-5 parts, palmitic acid 3-6 parts, single Tryfac 5573 2-5 parts, sulfuration arctic sperm oil 2-5 parts, ternary polycarboxylic acids 1-2 parts, Laurel Amido propyl betaine 1-3 parts, sodium nitrite 0.5-1 parts.
2. a kind of hydraulic guide rail oil according to claim 1, it is characterised in that:By following component with prepared by weight portion Into:White oil 55-65 parts, hydroisomerizing dewaxing 20-25 parts, Petiolus Trachycarpi oil 12-18 parts, polyisobutylene 3.5-4.5 parts, Nano diamond Perfume (or spice) is smeared in 0.6-0.9 parts, aluminum oleate 1.5-2.5 parts, silicone oil 3-4 parts, palmitic acid 4-5 parts, single Tryfac 5573 3-4 parts, sulfuration Whale oil 3-4 parts, ternary polycarboxylic acids 1.2-1.8 parts, lauroylamidopropyl betaine 1.5-2.5 parts, sodium nitrite 0.6-0.9 parts.
3. the preparation method of a kind of hydraulic guide rail oil described in any one of claim 1 to 2, it is characterised in that:Including following step Suddenly:
(1)By white oil, hydroisomerizing dewaxing and Petiolus Trachycarpi oil mixing, 60-80 DEG C is heated to, 5-10 minutes are stirred;
(2)Add polyisobutylene, aluminum oleate, silicone oil, palmitic acid, single Tryfac 5573, sulfuration arctic sperm oil, ternary polycarboxylic acids And lauroylamidopropyl betaine, stir 20-40 minutes under rotating speed 300-500r/min;
(3)Nano diamond and sodium nitrite are added, is stirred 10-30 minutes under rotating speed 200-400r/min, is put into Ultrasound Instrument In carry out ultrasonic 3-8 minutes;
(4)After being down to room temperature, 30-60 minutes are ground in adding grinder and are obtained final product.
4. the preparation method of a kind of hydraulic guide rail oil according to claim 3, it is characterised in that:The step(1)In plus To 65-75 DEG C, mixing time is 6-9 minutes to heat.
5. the preparation method of a kind of hydraulic guide rail oil according to claim 3, it is characterised in that:The step(2)Transfer Speed is 350-450r/min, and mixing time is 25-35 minutes.
6. the preparation method of a kind of hydraulic guide rail oil according to claim 3, it is characterised in that:The step(3)Transfer Speed is 250-350r/min, and mixing time is 15-25 minutes, and ultrasonic time is 4-6 minutes.
7. the preparation method of a kind of hydraulic guide rail oil according to claim 3, it is characterised in that:The step(4)In grind Consume time as 40-50 minutes.
CN201610948872.XA 2016-11-03 2016-11-03 A kind of hydraulic guide rail oil and preparation method thereof Pending CN106544103A (en)

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Application publication date: 20170329