CN106520371A - Passion fruit perfume - Google Patents
Passion fruit perfume Download PDFInfo
- Publication number
- CN106520371A CN106520371A CN201610847567.1A CN201610847567A CN106520371A CN 106520371 A CN106520371 A CN 106520371A CN 201610847567 A CN201610847567 A CN 201610847567A CN 106520371 A CN106520371 A CN 106520371A
- Authority
- CN
- China
- Prior art keywords
- passifolra edulis
- perfume
- passion fruit
- quintessence oil
- perfume according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The invention discloses a passion fruit perfume comprising the following component raw materials in parts by weight: 1-4 parts of passion fruit essential oil, 0.5-1.5 parts of strawberry essential oil, 0.3-1.7 parts of lemon essential oil, 0.1-0.3 part of sodium sulfate, 0.5-0.6 part of turbo cornutus solander operculum, 0.1-0.4 part of hydrogenated castor oil, 0.4-0.5 part of procyanidine, and 100 parts of a solvent. A dandelion powder is added in an extraction process of the passion fruit essential oil; in a carbon dioxide supercritical extraction process, essence effective components in passion fruit can be effectively extracted, the extracted passion fruit essence is rich in smell, and an original flavor is not destroyed. The passion fruit perfume has the passion fruit fragrance and unique faint scent smell, has no side effects on a human body, and is suitable for the majority of people.
Description
Technical field
The present invention relates to a kind of perfume, more particularly to a kind of Passifolra edulis perfume.
Background technology
The way for extracting natural plant spice from natural aromatic plant is present for a long time, and China is that production natural perfume material is gone through
One of earliest country of history, can produce hundreds of kind.Fruit flavouring perfume is applied to all types of crowds, and this kind of perfume fragrance is happy
People, and fragrance is especially, it is deep to be liked by broad masses.But at present this kind of perfume be mostly relatively stimulated by fragrance such as Citrus, it is strong
Fruit do raw material and prepare fruit flavouring.Passifolra edulis fragrance fragrance, the taste with unique delicate fragrance, but because of its fragrance widow
Light, elongated, after extraction, fragrance is light, it is more difficult to for making perfume, therefore, almost there is no the perfume (or spice) of Passifolra edulis taste in the market
Water.
The information for being disclosed in the background section is merely intended to increase the understanding of the general background to the present invention, and should not
When the prior art for being considered to recognize or imply the information structure in any form well known to persons skilled in the art.
The content of the invention
The present invention invents a kind of Passifolra edulis perfume for solving above-mentioned technical problem, it is desirable to provide a kind of fragrance fragrance, have
The perfume of the distinctive delicate fragrance taste of Passifolra edulis.
For achieving the above object, the technical scheme that the present invention is provided is as follows：
A kind of Passifolra edulis perfume, according to ratio of weight and number, is made up of following components raw material：1～4 part of Passifolra edulis quintessence oil, grass
0.5～1.5 part of certain kind of berries quintessence oil, 0.3～1.7 part of Fructus Citri Limoniae quintessence oil, 0.1～0.3 part of mirabilite, 0.5～0.6 part of Turbo cornutus Solander, hydrogenated castor
0.1～0.4 part of oil, 0.4～0.5 part of procyanidin, 100 parts of solvent.
Wherein, described Turbo cornutus Solander is to mix Turbo cornutus Solander with Herba Cymbopogonis Citrari, Fructus Gleditsia, is added water, and is cooked by slow fire 6～12 hours, takes out drip
Dry, attrition grinding is crossed 180～220 mesh sieves, is obtained final product.
Wherein, described Turbo cornutus Solander, Herba Cymbopogonis Citrari, Fructus Gleditsia are into 10:3:4 mass ratioes, i.e. Turbo cornutus Solander：Herba Cymbopogonis Citrari：Fructus Gleditsia=10:3:3 mass
Than；1～2 times for Herba Cymbopogonis Citrari quality of the water of addition.
Wherein, described solvent is ethanol solution that volumetric concentration is 65～75%.
Wherein, described Passifolra edulis quintessence oil is prepared by following methods, and its operating procedure is：
(1) pretreated Passifolra edulis are taken to be put in reactor, is added water, added Herba Taraxaci powder, be passed through carbon dioxide
(CO2), reacted；
(2) by gained reacting liquid filtering in step (1), filtrate is taken, vacuum distillation is carried out, Passifolra edulis quintessence oil is obtained final product.
Wherein, pretreated Passifolra edulis and water in step (1), Herba Taraxaci powder are into 1:2～5:0.3～0.5 mass ratio,
I.e. pretreated Passifolra edulis：Water：Herba Taraxaci powder=1:2～5:0.3～0.5.
Wherein, for taking new fresh Herba Taraxaci, it is 10～15% to dry to mass water content to described Herba Taraxaci powder, grinding,
220 mesh sieves are crossed, is obtained final product.
Wherein, in step (1), in reactor, reaction pressure is 7397kPa, and temperature is 35 DEG C, reacts 0.5～2.5h.
Wherein, the temperature of the vacuum distillation described in step (2) is 55～65 DEG C, and pressure is 15.7～25kPa, and the time is
0.5～1.0h.
Wherein, the pretreated Passifolra edulis are to take medium well fresh Passifolra edulis, shell, take sarcocarp.
Compared with prior art, the present invention has the advantages that：
(1) present invention adds Herba Taraxaci powder in Passifolra edulis quintessence oil extraction process, in carbon dioxide supercritical fluid extraction mistake
Cheng Zhong, can effectively extract essence effective ingredient in Passifolra edulis, and extraction gained Passifolra edulis essence taste is stronger, and does not destroy which
Original flavor；
(2) Passifolra edulis perfume of the present invention has Passifolra edulis fragrance, the taste of unique delicate fragrance, and human body is had no side effect, and fits
Close many people to use.
Specific embodiment
It is described in detail with reference to specific embodiment, it is to be understood that protection scope of the present invention is not by concrete
The restriction of embodiment.
Embodiment 1
Passifolra edulis quintessence oil is prepared by following methods：
(1) new fresh Herba Taraxaci is taken, it is 10% to dry to mass water content, and grinding is crossed 220 mesh sieves, obtains final product Herba Taraxaci powder,
It is standby；Taking medium well fresh Passifolra edulis carries out pretreatment, that is, shell, take sarcocarp, pretreated Passifolra edulis are put into
In the high-pressure reactor of 2.0L, add water, add Herba Taraxaci powder, holding flow is 500m3/ h is passed through carbon dioxide (CO2), protect
It is 7397kPa to hold pressure in high-pressure reactor, and keeping temperature is 35 DEG C, reacts 0.5h；Wherein, pretreated Passifolra edulis with plus
The water that enters, Herba Taraxaci powder are into 1:2:0.3 mass ratio, i.e., pretreated Passifolra edulis：Water：Herba Taraxaci powder=1:2:0.3；
(2) by gained reacting liquid filtering in step (1), filtrate is taken, carries out vacuum distillation, vacuum distillation temperature is 55 DEG C,
Pressure is 15.7kPa, and the time is 1.0h, obtains final product Passifolra edulis quintessence oil, standby；
By Turbo cornutus Solander, Herba Cymbopogonis Citrari, Fructus Gleditsia into 10:3:4 mass ratioes, i.e. Turbo cornutus Solander：Herba Cymbopogonis Citrari：Fructus Gleditsia=10:3:3 mass ratioes, by Turbo cornutus Solander
Mix with Herba Cymbopogonis Citrari, Fructus Gleditsia, according to adding water for 1 times that water is Herba Cymbopogonis Citrari quality, be cooked by slow fire 6 hours, taking-up is drained, attrition grinding,
180 mesh sieves are crossed, is obtained final product, it is standby；
A kind of Passifolra edulis perfume, in units of g, weighs following component raw material：Passifolra edulis quintessence oil 4g obtained by above-mentioned extraction,
Fructus Fragariae Ananssae quintessence oil 1.5g, Fructus Citri Limoniae quintessence oil 1.7g, mirabilite 0.3g, above-mentioned standby Turbo cornutus Solander 0.6g, castor oil hydrogenated 0.4g, former cyanine
Plain 0.5g, solvent volume concentration are 65% ethanol 100g, mixing, are obtained final product.
Embodiment 2
Passifolra edulis quintessence oil is prepared by following methods：
(1) new fresh Herba Taraxaci is taken, it is 15% to dry to mass water content, and grinding is crossed 220 mesh sieves, obtains final product Herba Taraxaci powder,
It is standby；Taking medium well fresh Passifolra edulis carries out pretreatment, that is, shell, take sarcocarp, pretreated Passifolra edulis are put into
In the high-pressure reactor of 2.0L, add water, add Herba Taraxaci powder, holding flow is 500m3/ h is passed through carbon dioxide (CO2), protect
It is 7397kPa to hold pressure in high-pressure reactor, and keeping temperature is 35 DEG C, reacts 2.5h；Wherein, pretreated Passifolra edulis with plus
The water that enters, Herba Taraxaci powder are into 1:5:0.5 mass ratio, i.e., pretreated Passifolra edulis：Water：Herba Taraxaci powder=1:5:0.5；
(2) by gained reacting liquid filtering in step (1), filtrate is taken, carries out vacuum distillation, vacuum distillation temperature is 65 DEG C,
Pressure is 25kPa, and the time is 0.5h, obtains final product Passifolra edulis quintessence oil, standby；
By Turbo cornutus Solander, Herba Cymbopogonis Citrari, Fructus Gleditsia into 10:3:4 mass ratioes, i.e. Turbo cornutus Solander：Herba Cymbopogonis Citrari：Fructus Gleditsia=10:3:3 mass ratioes, by Turbo cornutus Solander
Mix with Herba Cymbopogonis Citrari, Fructus Gleditsia, according to adding water for 2 times that water is Herba Cymbopogonis Citrari quality, be cooked by slow fire 12 hours, taking-up is drained, attrition grinding,
220 mesh sieves are crossed, is obtained final product, it is standby；
A kind of Passifolra edulis perfume, in units of g, weighs following component raw material：Passifolra edulis quintessence oil 1g obtained by above-mentioned extraction,
Fructus Fragariae Ananssae quintessence oil 0.5g, Fructus Citri Limoniae quintessence oil 0.3g, mirabilite 0.1g, above-mentioned standby Turbo cornutus Solander 0.5g, castor oil hydrogenated 0.1g, former cyanine
Plain 0.4g, solvent volume concentration are 75% ethanol 100g, mixing, are obtained final product.
Embodiment 3
Passifolra edulis quintessence oil is prepared by following methods：
(1) new fresh Herba Taraxaci is taken, it is 13% to dry to mass water content, and grinding is crossed 220 mesh sieves, obtains final product Herba Taraxaci powder,
It is standby；Taking medium well fresh Passifolra edulis carries out pretreatment, that is, shell, take sarcocarp, pretreated Passifolra edulis are put into
In the high-pressure reactor of 2.0L, add water, add Herba Taraxaci powder, holding flow is 500m3/ h is passed through carbon dioxide (CO2), protect
It is 7397kPa to hold pressure in high-pressure reactor, and keeping temperature is 35 DEG C, reacts 1.5h；Wherein, pretreated Passifolra edulis with plus
The water that enters, Herba Taraxaci powder are into 1:3.5:0.4 mass ratio, i.e., pretreated Passifolra edulis：Water：Herba Taraxaci powder=1:3.5:
0.4；
(2) by gained reacting liquid filtering in step (1), filtrate is taken, carries out vacuum distillation, vacuum distillation temperature is 60 DEG C,
Pressure is 20kPa, and the time is 0.75h, obtains final product Passifolra edulis quintessence oil, standby；
By Turbo cornutus Solander, Herba Cymbopogonis Citrari, Fructus Gleditsia into 10:3:4 mass ratioes, i.e. Turbo cornutus Solander：Herba Cymbopogonis Citrari：Fructus Gleditsia=10:3:3 mass ratioes, by Turbo cornutus Solander
Mix with Herba Cymbopogonis Citrari, Fructus Gleditsia, according to adding water for 2 times that water is Herba Cymbopogonis Citrari quality, be cooked by slow fire 6～12 hours, taking-up is drained, and crushing is ground
Mill, crosses 200 mesh sieves, obtains final product, standby；
A kind of Passifolra edulis perfume, in units of g, weighs following component raw material：Passifolra edulis quintessence oil obtained by above-mentioned extraction
2.5g, Fructus Fragariae Ananssae quintessence oil 1.0g, Fructus Citri Limoniae quintessence oil 1.0g, mirabilite 0.2g, above-mentioned standby Turbo cornutus Solander 0.5g, castor oil hydrogenated 0.25g,
Procyanidin 0.45g, solvent volume concentration are 70% ethanol 100g, mixing, are obtained final product.
Solvent of the present invention is made up of ethanol, important component part of the ethanol as solvent, can be dissolved quintessence oil and be risen
To the effect of uniform dilution quintessence oil, and ethanol evaporation rate is fast, and range of scatter is little, can be rapidly separated quintessence oil molecule, allows perfume
The taste of oneself is given play to.Meanwhile, and ethanol has functions that to prevent organic substance oxidation deterioration in quintessence oil, extends the guarantor of perfume
The matter phase, is the excellent selection of perfume solvent.
The further present invention adopts carbon dioxide supercritical fluid extraction during extraction Passifolra edulis essence, can be more effectively
Passifolra edulis essence effective ingredient is extracted, and, Herba Taraxaci powder can play agent for capturing in carbon dioxide supercritical fluid extraction solvent
Effect, can by the scattered essence aggregation being dispersed in extractant, more favorably in the aggregation of Passifolra edulis essence effective ingredient, after
Continuous distillation, obtains the Passifolra edulis essence of better quality.
It is aforementioned to the present invention specific illustrative embodiment description be in order to illustrate and illustration purpose.These descriptions
It is not wishing to limit the invention to disclosed precise forms, and it will be apparent that according to above-mentioned teaching, much can be changed
And change.The purpose of selecting and describing the exemplary embodiment is that explaining that the certain principles and its reality of the present invention should
With so that those skilled in the art can realize and using the present invention a variety of exemplaries and
A variety of selections and change.The scope of the present invention is intended to be limited by claims and its equivalents.
Claims (10)
1. a kind of Passifolra edulis perfume, it is characterised in that according to ratio of weight and number, be made up of following components raw material：Passifolra edulis quintessence oil 1
～4 parts, 0.5～1.5 part of Fructus Fragariae Ananssae quintessence oil, 0.3～1.7 part of Fructus Citri Limoniae quintessence oil, 0.1～0.3 part of mirabilite, 0.5～0.6 part of Turbo cornutus Solander,
0.1～0.4 part of castor oil hydrogenated, 0.4～0.5 part of procyanidin, 100 parts of solvent.
2. Passifolra edulis perfume according to claim 1, it is characterised in that：Described Turbo cornutus Solander is to mix Turbo cornutus Solander with Herba Cymbopogonis Citrari, Fructus Gleditsia
Close, add water, be cooked by slow fire 6～12 hours, taking-up is drained, attrition grinding, cross 180～220 mesh sieves, obtain final product.
3. Passifolra edulis perfume according to claim 2, it is characterised in that：Described Turbo cornutus Solander, Herba Cymbopogonis Citrari, Fructus Gleditsia are into 10:3:4 mass
Than i.e. Turbo cornutus Solander：Herba Cymbopogonis Citrari：Fructus Gleditsia=10:3:3 mass ratioes；1～2 times for Herba Cymbopogonis Citrari quality of the water of addition.
4. Passifolra edulis perfume according to claim 1, it is characterised in that：Described solvent is 65～75% for volumetric concentration
Ethanol solution.
5. Passifolra edulis perfume according to claim 1, it is characterised in that described Passifolra edulis quintessence oil is prepared into by following methods
Arrive, its operating procedure is：
(1) pretreated Passifolra edulis are taken to be put in reactor, is added water, add Herba Taraxaci powder, be passed through carbon dioxide (CO2),
Reacted；
(2) by gained reacting liquid filtering in step (1), filtrate is taken, vacuum distillation is carried out, Passifolra edulis quintessence oil is obtained final product.
6. Passifolra edulis perfume according to claim 5, it is characterised in that：Pretreated Passifolra edulis and water, Pu in step (1)
Herba Taraxaci powder is into 1:2～5:0.3～0.5 mass ratio.
7. Passifolra edulis perfume according to claim 5, it is characterised in that：Described Herba Taraxaci powder is to take new fresh Herba Taraxaci,
It is 10～15% to dry to mass water content, and grinding is crossed 220 mesh sieves, obtained final product.
8. Passifolra edulis perfume according to claim 5, it is characterised in that：In step (1), in reactor, reaction pressure is
7397kPa, temperature are 35 DEG C, react 0.5～2.5h.
9. Passifolra edulis perfume according to claim 5, it is characterised in that：The temperature of the vacuum distillation described in step (2) is
55～65 DEG C, pressure is 15.7～25kPa, and the time is 0.5～1.0h.
10. Passifolra edulis perfume according to claim 5, it is characterised in that：The pretreated Passifolra edulis are medium well for taking
Fresh Passifolra edulis, shell, take sarcocarp.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610847567.1A CN106520371A (en) | 2016-09-23 | 2016-09-23 | Passion fruit perfume |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610847567.1A CN106520371A (en) | 2016-09-23 | 2016-09-23 | Passion fruit perfume |
Publications (1)
| Publication Number | Publication Date |
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| CN106520371A true CN106520371A (en) | 2017-03-22 |
Family
ID=58344142
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610847567.1A Pending CN106520371A (en) | 2016-09-23 | 2016-09-23 | Passion fruit perfume |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113403146A (en) * | 2021-07-17 | 2021-09-17 | 广州芬豪香精有限公司 | Preparation method of fruit essence |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113403146A (en) * | 2021-07-17 | 2021-09-17 | 广州芬豪香精有限公司 | Preparation method of fruit essence |
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Application publication date: 20170322 |