CN106520330A - Lubricant composition for power-spinning processing process for Hastelloy C-series alloys - Google Patents
Lubricant composition for power-spinning processing process for Hastelloy C-series alloys Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/026—Butene
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- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/02—Hydroxy compounds
- C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
- C10M2207/026—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings with tertiary alkyl groups
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/282—Esters of (cyclo)aliphatic oolycarboxylic acids
- C10M2207/2825—Esters of (cyclo)aliphatic oolycarboxylic acids used as base material
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- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/08—Halogenated waxes
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/064—Di- and triaryl amines
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
- C10M2219/022—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of hydrocarbons, e.g. olefines
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
- C10M2219/024—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of esters, e.g. fats
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/10—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring
- C10M2219/104—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring containing sulfur and carbon with nitrogen or oxygen in the ring
- C10M2219/106—Thiadiazoles
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- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
- C10M2223/045—Metal containing thio derivatives
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- C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
- C10M2229/04—Siloxanes with specific structure
- C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/04—Detergent property or dispersant property
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/72—Extended drain
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- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
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- C10N2040/20—Metal working
- C10N2040/244—Metal working of specific metals
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Abstract
The invention discloses a lubricant composition for a power-spinning processing process for Hastelloy C-series alloys. According to the lubricant composition, HVI90BS with a mass ratio being 50% and dioctyl sebacate with a mass ratio being 50% are compounded as composite base oil which is matched with various composite additives comprising an antioxidant, a metal deactivator, an oiliness agent, a friction improver, an extreme pressure agent, an anti-wear agent, an antirust agent, an anti-foaming agent, an oxygen and corrosion resisting agent, a filler and the like. The composition disclosed by the invention has the characteristics of having good cooling performance, lubricity, extreme-pressure wear-resistant carrying capacity, wettability, diffusivity, d cleaning property, anti-rust property, oxygen and corrosion resistance, anti-oxidation stability, anti-shearing stability, adhesion and high oil film strength, reducing surface scratches, improving processing efficiency and prolonging the service life of a mould.
Description
Technical field
A kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions of the present invention belong to metal working lubricant
Field.
Background technology
It is serial that Hastelloy (Hastelloyalloy) is broadly divided into B, C, G tri-, it be mainly used in iron-based Cr-Ni or
The strong corrosive media occasion that Cr-Ni-Mo rustless steels, nonmetallic materials etc. cannot be used.Each trade mark has specific chemistry
Composition, mechanical performance have his own strong points, it is impossible to which what characteristic Hastelloy of lumping together has.Hastelloy plate is applied to various
Chemical industry containing oxidation and reductant.
Kazakhstan C series is mainly C-276 (00Cr16MO16W4)、C-4(00Cr16MO16)、C-22(00Cr22MO13W3)、C-
2000(00Cr20MO16) etc..By taking C-276 as an example, N:14.5~16.5, Cr:15~17, MO:4.0~7.0, Fe≤0.01, C≤
0.08, Si≤2.5, CO≤ 1.0, Mn≤0.04, P≤0.03, S:3.0~4.5, W≤0.035.
Rotary pressure technology originates from ancient times pottery.He is that one kind combines forging, extruding, draw piece, bending, looping mill rolling, horizontal stroke
Roll the few advanced technologies without machining with the process characteristic such as edging.Generally metal letter base, plate blank or prefabricated blank are used
Tail top is held out against on spinning machine mould, drives plug and blank rotation by main shaft;Material is extruded by spinning wheel from blank side simultaneously
On the core of rotation, material is made to produce the continuous plastic deformation of pointwise, so as to obtain the hollow rotary body of various shape of generatrix
Part.According to the blank thickness situation of change during rotary pressing processing, spinning process is divided into conventional spinning and shear spinning two
Plant, i.e. conventional spinning and shear spinning.
The referred to as general rotation of conventional spinning.During general rotation, the thickness of blank is held essentially constant, and shaping relies primarily on blank edge
The contraction of circumference and along radial direction it is indeformable realizing with length.Which is mainly characterized by forming process, substantially can be seen
Go out the change of blank external diameter.The basic mode of conventional spinning has:Draw spinning (drawing rotation), necking in spindown (contracting rotation) and expanding bulging
Three kinds of (expanding rotation) etc..
Also known as flow turning, shear spinning is a kind of Near net shape grown up on the basis of conventional spinning to shear spinning
Processing method, which is substantially added high pressure in blank using spinning roller, and rotary billet carries out local along shaping dies by external force
Gradually spreading produce plastic deformation and it is thinning, so as to obtain high accuracy Thin-wall Revolving Part.
Tail top is adopted during spinning or blank is fixed on into mould otherwise, mould rotation, spinning roller are made feed motion, make hair
Continuously pointwise is thinning and reclines mould and forms the part of required shape for base, and shear spinning relies primarily on subtracting for sotck thinkness
The thin shaping to realize workpiece.
The content of the invention
It is a kind of good with good stability, lubricity, corrosion resistance that the technical problem to be solved in the present invention is to provide,
The excellent Kazakhstan C series alloy shear spinning processing technique lubricant compositions of thermal oxidation stability.
The present invention solves above-mentioned technical problem by following technical solution:
A kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions, using the HVI90BS of mass ratio 50%
Be complex as base oil with 50% di-n-octyl sebacate, coordinate various compound additives, its each mass percent into packet
Into:
Component | Mass percentage content |
Base oil | Surplus |
Antioxidant | 0.06%~0.6% |
Metal deactivator | 0.03%~0.3% |
Oiliness improver | 4%~8% |
Friction improver | 1%~2% |
Extreme pressure agent | 3%~5% |
Antiwear additive | 3%~5% |
Antirust agent | 0.05%~0.5% |
Anti-foaming agent | 10ppm~30ppm |
Oxidation and corrosion inhibitor | 0.5%~1.2% |
Adhesive agent | 2%~6% |
Filler | 2%~4% |
The mass percent summation of above each component is 100%.
Antioxidant be mass ratio 50% 2,6- di-t-butyls mixed phenol with 50% it is right, to '-di-iso-octyldiphenylamine
T538 is combined.Metal deactivator agent is that the thiadiazole of the thiadiazoles derivative T561 and 50% of mass ratio 50% is combined.
Oiliness improver is sulfuration cottonseed oil T404.Friction improver is sulfur molybdenum phosphate T461.
Extreme pressure agent is chlorinated paraffin T302.Antiwear additive is sulfide isobutene T321.
Antirust agent is that the petroleum sodium sulfonate of the BTA T706 and 50% of mass ratio 50% is combined;
Anti-foaming agent is methyl-silicone oil.Oxidation and corrosion inhibitor is sulfur phosphorus fourth octyl group zinc salt T202.
Adhesive agent is polyisobutylene T603D.Filler is paraffin wax fully refined 66.
A kind of remarkable advantage of Kazakhstan C series alloy shear spinning processing technique lubricant compositions of the present invention has good
Cooling well, lubricity, extreme-pressure anti-wear load, wellability, diffusibility, cleaning, rust-preventing characteristic, antioxygen anti-corrosive properties, antioxygen
Change stability, anti-shearing stability, adhesiveness, film strength is high, reduces galled spotss and cut, improves working (machining) efficiency, extends
Die life.
Specific embodiment
Embodiment 1:
Following each component is pressed the mediation of row mass percent to form:
Above each component mass percentage content summation is 100%.
Embodiment 2:
Following each component is pressed the mediation of row mass percent to form:
Above each component mass percentage content summation is 100%.
Embodiment 3:
Following each component is pressed the mediation of row mass percent to form:
Above each component mass percentage content summation is 100%.
The typical physiochemical techniques index of 1 product of embodiment:
Project | Quality index |
Kinematic viscosity (40 DEG C)/mm2/s-1 | 226.5 |
Viscosity index (VI) | 98 |
Flash-point (opening)/DEG C | 277 |
Condensation point/DEG C | -29 |
Coefficient of friction | 0.055 |
Corrosivity (copper sheet, 100 DEG C, 3h)/level | 1 |
Oxidation stability (rotary oxygen bomb, 150 DEG C)/min | 327 |
Resistance to emulsion (84 DEG C, 40-40-0)/min | 11 |
Tetra-ball machine test/Pb/N | 995 |
Sintering load/PD/N | 6670 |
Terraced nurse agrees/N | 283 |
FZG/ levels | 13 |
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % | 6.7 |
Mechanical admixture, % | 0.003 |
Moisture, % | Vestige |
The typical physiochemical techniques index of 2 product of embodiment:
Project | Quality index |
Kinematic viscosity (40 DEG C)/mm2/s-1 | 229.3 |
Viscosity index (VI) | 98 |
Flash-point (opening)/DEG C | 276 |
Condensation point/DEG C | -28 |
Coefficient of friction | 0.055 |
Corrosivity (copper sheet, 100 DEG C, 3h)/level | 1 |
Oxidation stability (rotary oxygen bomb, 150 DEG C)/min | 337 |
Resistance to emulsion (84 DEG C, 40-40-0)/min | 12 |
Tetra-ball machine test/Pb/N | 978 |
Sintering load/PD/N | 6610 |
Terraced nurse agrees/N | 284 |
FZG/ levels | 13 |
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % | 6.8 |
Mechanical admixture, % | 0.003 |
Moisture, % | Vestige |
The typical physiochemical techniques index of 3 product of embodiment:
Project | Quality index |
Kinematic viscosity (40 DEG C)/mm2/s-1 | 228.7 |
Viscosity index (VI) | 105 |
Flash-point (opening)/DEG C | 266 |
Condensation point/DEG C | -27 |
Coefficient of friction | 0.057 |
Corrosivity (copper sheet, 100 DEG C, 3h)/level | 1 |
Oxidation stability (rotary oxygen bomb, 150 DEG C)/min | 333 |
Resistance to emulsion (84 DEG C, 40-40-0)/min | 13 |
Tetra-ball machine test/Pb/N | 970 |
Sintering load/PD/N | 6560 |
Terraced nurse agrees/N | 286 |
FZG/ levels | 13 |
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % | 7.1 |
Mechanical admixture, % | 0.005 |
Moisture, % | Vestige |
Claims (10)
1. a kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions, it is characterised in that:Using mass ratio 50%
The di-n-octyl sebacate of HVI90BS and 50% be complex as base oil, coordinate various compound additives, its respective mass percent
Into being grouped into:
The mass percent summation of above each component is 100%.
2. a kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist
In antioxidant be mass ratio 50% 2,6- di-t-butyls mixed phenol with 50% it is right, to '-di-iso-octyldiphenylamine T538 is multiple
Close.
3. a kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist
In metal deactivator agent be mass ratio 50% thiadiazoles derivative T561 and 50% thiadiazole be combined.
4. a kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist
In oiliness improver be sulfuration cottonseed oil T404.
5. a kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist
In friction improver be sulfur molybdenum phosphate T461;Extreme pressure agent is chlorinated paraffin T302.
6. a kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist
In antiwear additive be sulfide isobutene T321.
7. a kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist
In antirust agent be mass ratio 50% BTA T706 and 50% petroleum sodium sulfonate be combined.
8. a kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist
In anti-foaming agent be methyl-silicone oil;Oxidation and corrosion inhibitor is sulfur phosphorus fourth octyl group zinc salt T202.
9. a kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature exist
In adhesive agent be polyisobutylene T603D.
10. a kind of Kazakhstan C series alloy shear spinning processing technique lubricant compositions as claimed in claim 1, its feature
Be filler be paraffin wax fully refined 66.
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CN103695135A (en) * | 2013-12-27 | 2014-04-02 | 南宁市禹焱新能源科技有限公司 | Castor-based gas-fired fuel engine oil composition |
CN104450079A (en) * | 2014-11-17 | 2015-03-25 | 广西大学 | Lubricating agent composition for warm forging of stainless steel |
CN104974842A (en) * | 2015-07-20 | 2015-10-14 | 广西大学 | Castor-base rotary cold-forging beryllium alloy lubricant composition |
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2016
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Patent Citations (3)
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CN103695135A (en) * | 2013-12-27 | 2014-04-02 | 南宁市禹焱新能源科技有限公司 | Castor-based gas-fired fuel engine oil composition |
CN104450079A (en) * | 2014-11-17 | 2015-03-25 | 广西大学 | Lubricating agent composition for warm forging of stainless steel |
CN104974842A (en) * | 2015-07-20 | 2015-10-14 | 广西大学 | Castor-base rotary cold-forging beryllium alloy lubricant composition |
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唐晓东: "《石油加工助剂作用原理与应用》", 30 November 2004, 石油工业出版社 * |
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