CN106498371A - Film formation device and film build method - Google Patents

Film formation device and film build method Download PDF

Info

Publication number
CN106498371A
CN106498371A CN201610188203.7A CN201610188203A CN106498371A CN 106498371 A CN106498371 A CN 106498371A CN 201610188203 A CN201610188203 A CN 201610188203A CN 106498371 A CN106498371 A CN 106498371A
Authority
CN
China
Prior art keywords
electrode
film
workpiece
temperature
chamber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610188203.7A
Other languages
Chinese (zh)
Inventor
徳嵩佑
尾崎悟
吉冈尚规
田中优
西原隆治
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shimadzu Corp
Original Assignee
Shimadzu Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shimadzu Corp filed Critical Shimadzu Corp
Publication of CN106498371A publication Critical patent/CN106498371A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/50Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating using electric discharges
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/34Sputtering
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/54Controlling or regulating the coating process
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/52Controlling or regulating the coating process

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Plasma & Fusion (AREA)
  • Chemical Vapour Deposition (AREA)
  • Plasma Technology (AREA)

Abstract

The present invention provides a kind of film formation device and film build method, reduces film forming matter from stripping electrode.Film formation device includes:Chamber, deposits workpiece;Electrode, configures in chamber interior, in order to carry out film forming on workpiece and supply electric power;And temperature adjustment device, the temperature of adjustment electrode, so that carry out a succession of in film process of film forming on workpiece, is carried out in the operation beyond the film formation process of film forming and film formation process on workpiece, the temperature of electrode is for approximately fixed, in order to avoid the film forming matter of electrode is piled up in from stripping electrode.

Description

Film formation device and film build method
Technical field
The present invention relates to one kind is configured with film formation device and the film forming of electrode in chamber (chamber) Method.
Background technology
As the film formation device for carrying out film forming in process object workpiece (work), using there is plasma Body (plasma) chemical vapor deposition (Chemical Vapor Deposition, CVD) device splashes Plating (sputter) device etc..In these film formation devices, in film formation process, film forming matter can also be deposited in The internal face of chamber is deposited on the surface of the electrode for being configured at chamber interior.Because these film forming matters from Chamber or stripping electrode are simultaneously attached on workpiece, and the film quality that can produce film of the film forming on workpiece declines The problems such as.Thus, for example being ground configuring the countermeasures such as anti-adhesion plate to the internal face for covering chamber Study carefully (referring for example to patent document 1).
Prior art literature
Patent document
Patent document 1:Japanese Patent Laid-Open 2007-012907 publication
Content of the invention
[invention problem to be solved]
Because of the within the chamber in plasma CVD equipment, to be exposed to plasma medium, is generally disposed at chamber The temperature of indoor electrode can rise in film forming processing procedure.Thus, electrode can be expanded.Separately On the one hand, when workpiece is changed, because carrying out atmosphere opening to chamber, so as to the temperature of electrode can be because cold But decline.Thus, electrode can shrink.Due to being sent out according to temperature change as electrode meeting so Change shape, so as to the difference because of electrode with the coefficient of thermal expansion of film forming matter causes film forming matter from stripping electrode.Its As a result, the problems such as film forming matter being produced and is attached to workpiece.
In view of the problem points, it is an object of the invention to provide a kind of film forming matter that reduces is shelled from electrode From film formation device and film build method.
[technological means of solve problem]
According to a form of the present invention, there is provided a kind of film formation device, its are used for carrying out film forming in workpiece, The film formation device includes:(A) chamber, deposits workpiece;(B) electrode, configures in chamber interior, In order to carry out film forming on workpiece and supply electric power;And (C) temperature adjustment device, adjust electrode Temperature, so that carrying out a succession of in film process of film forming on workpiece, carries out film forming on workpiece Film formation process and film formation process beyond operation in, the temperature of electrode is approximately fixed, in order to avoid pile up In electrode film forming matter from stripping electrode.
According to the present invention another form, there is provided a kind of film build method, its a succession of in film process, The temperature of adjustment electrode, so that beyond carrying out the film formation process of film forming and film formation process on workpiece In operation, the temperature of electrode is approximately fixed, in order to avoid be piled up in the film forming matter of electrode from stripping electrode, Described a succession of comprise the following steps into film process:By film forming process object Workpiece storage within the chamber; By the power supply of regulation to the electrode for being configured within the chamber, to carry out film forming on workpiece;And it is right After workpiece carries out film forming, atmosphere opening is carried out to chamber.
(The effect of invention)
In accordance with the invention it is possible to provide a kind of reduce film forming matter from the film formation device of stripping electrode and into Film method.
Description of the drawings
Fig. 1 is the schematic diagram of the structure of the film formation device of the 1st embodiment for representing the present invention.
Fig. 2 is for carrying out to the film build method of film formation device of the 1st embodiment using the present invention The flow chart of explanation.
Fig. 3 is the schematic diagram of the structure of the film formation device of the 2nd embodiment for representing the present invention.
Fig. 4 is the schematic diagram that the action of the film formation device of the 2nd embodiment to the present invention is illustrated.
Fig. 5 is the schematic diagram of the structure of the film formation device for representing another embodiment of the present invention.
[explanation of symbol]
1:Film formation device
10:Chamber
20:Electrode
30:Temperature adjustment device
40:Power supply
50:Gas supply mechanism
60:Exhaust gear
70:Workpiece holder
100:Workpiece
101:1st processing region
102:2nd processing region
201:Target
202:Target electrode
203:Sputter power supply
204:Gear lock
510:Unstrpped gas
Specific embodiment
Next, being explained with reference to embodiments of the present invention.In the record of following accompanying drawing, For same or similar part marks same or similar symbol.But should be noted that, accompanying drawing is only Schematic person.And, embodiment shown below is to illustrate the technological thought tool for by the present invention The device of body or method, in embodiments of the present invention, the structure of constituent part, configuration etc. are not It is defined in described below person.Embodiments of the present invention can add various changes in detail in the claims.
(the 1st embodiment)
The film formation device 1 of the 1st embodiment of the present invention is as shown in figure 1, possess:Chamber 10, deposits Put process object workpiece 100;Electrode 20, configures in the inside of chamber 10, in order on workpiece 100 Carry out film forming and supply electric power;And temperature adjustment device 30, adjust the temperature of electrode 20.
Film formation device 1 shown in Fig. 1 is carried out on workpiece 100 by plasma CVD method The plasma CVD equipment of film, possesses power supply 40, the gas supply machine to 20 supply electric power of electrode Structure 50 and exhaust gear 60.Power supply 40 is, for example, high frequency electric source.Gas supply mechanism 50 will be formed The unstrpped gas 510 of the film on the workpiece 100 is supplied to the inside of chamber 10.Exhaust gear 60 Gas in chamber 10 is discharged to the outside.Possesses the gas tune for omitting diagram in exhaust gear 60 Pressure in chamber 10 is remained fixation by pressure valve.
In film formation device 1, in the electrode 20 being configured in chamber 10 opposite to each other with workpiece 100 and take Carry between the workpiece holder (work holder) 70 of workpiece 100, formation unstrpped gas 510 etc. Gas ions.For example, workpiece holder 70 is made by electrode 20 as negative electrode (cathode) electrode For anode (anode) electrode.By workpiece 100 is exposed to the plasma being formed in inside chamber 10 In body so that film of the contained raw material with unstrpped gas 510 as principal component on workpiece 100 into Film.
Hereinafter, the example of the method by the formation film of film formation device 1 is described with reference to Fig. 2.
In step S11, electrode 20 is adjusted to by temperature adjustment device 30 for regulation temperature.Connect Get off, in step S12, temperature that electrode 20 is adjusted to regulation, and film forming is dealt with objects workpiece 100 deposit to chamber 10.Subsequently, make to become vacuum in chamber 10 by exhaust gear 60.
In step S13, unstrpped gas 510 is directed in chamber 10 by gas supply mechanism 50. Next, by exhaust gear 60 to reducing pressure in chamber 10, by the unstrpped gas in chamber 10 510 adjust to the air pressure of regulation.
The step of film formation process in S14, power supply 40 is turned on (ON) and the electric power of regulation is supplied Give to electrode 20.Thus, the unstrpped gas 510 in chamber 10 is in plasma.Formed etc. Exciting in gas ions is planted and is reacted on the surface of workpiece 100, so as to the surface shape in workpiece 100 Into film.In the film formation process, the temperature of electrode 20 is adjusted also by temperature adjustment device 30. That is, electrode 20 is adjusted to the temperature of regulation, and carries out the film forming of workpiece 100.
After forming the film of regulation thickness on workpiece 100, power supply 40 is disconnected in step S15 (OFF), terminate film formation process.Next, by exhaust gear 60 by unstrpped gas 510 from chamber 10 discharge.Subsequently, in step s 16, electrode 20 is adjusted to set point of temperature and chamber 10 is entered Row atmosphere opening, from the workpiece 100 that chamber 10 takes out of film forming.
By described a succession of into film process, the film that film forming specifies on workpiece 100.In addition, In the case of continuously running film formation device 1, return to step S11, by untreated new workpiece 100 Deposit to chamber 10.
Temperature adjustment device 30 adjusts the temperature of electrode 20, so that in reference to illustrated by Fig. 2 Consecutive in film process, the temperature of electrode 20 for fixing, in order to avoid be piled up in the film forming matter of electrode 20 from Electrode 20 is peeled off.That is, in film formation device 1, carry out on workpiece 100 film formation process of film forming with into In other operations beyond membrane process, the temperature of electrode 20 is retained as fixing.For example, in order to more When changing 100 grade of workpiece and carrying out atmosphere opening to chamber 10 with film formation process in, the temperature of electrode 20 For fixation.Therefore, the deformation of the electrode 20 for causing because of temperature change is suppressed.As a result, can press down Make the difference because of electrode with the coefficient of thermal expansion of film forming matter and cause film forming matter from stripping electrode.
Temperature adjustment device 30 shown in Fig. 1 has and is configured at adjustment portion 31 in electrode 20 and right The configuration part 32 set by the temperature of adjustment portion 31.For example, as adjustment portion 31, in electrode 20 Inside arrange for warm water flowing circulation waterway.Also, the temperature that the portion that is set 32 have adjusted temperature Water is supplied to adjustment portion 31, makes warm water in the inner loop of electrode 20, to adjust the temperature of electrode 20. Or, also can be for adjustment portion 31 be using heating element heaters such as heaters (heater), by configuration part 32 controlling the heating element heater, electrode 20 is adjusted to the temperature of regulation.
By film formation device 1, for example can be by including HMDO (Hexamethyldisiloxane)(HMDSO:O[Si(CH3)3]2) and oxygen (O2) unstrpped gas 510 carry out plasma polymerization and obtain with SiOXCY:The film of H structure is used as barrier (barrier) film, and film forming is carried out on the workpiece 100 as resinous wood.Now, if to electrode 20 materials'use metal material such as copper (Cu), the then barrier film of film forming and electrode on workpiece 100 The difference of 20 thermal coefficient of expansion is big.Therefore, if electrode 20 is because of the temperature between film formation process and other operations Degree changes and deforms, then can be because of electrode 20 and the thermal expansion of the film forming matter being piled up on electrode 20 The difference of rate and cause film forming matter to be peeled off from electrode 20.
However, in film formation device 1, from the beginning of workpiece 100 is deposited to chamber 10, through film forming work Sequence, till workpiece 100 is taken out of from chamber 10, adjusts electricity by temperature adjustment device 30 The temperature of pole 20, so that the temperature of electrode 20 is approximately fixed.Therefore, electrode 20 will not become Shape, film forming matter are suppressed from the stripping of electrode 20.The so-called temperature by electrode 20 is maintained substantially Fixed, refer to and be maintained what electrode 20 only will not deform from the degree that electrode 20 is peeled off in film forming matter Temperature, the preferably temperature of electrode 20 are maintained fixed completely, so that electrode 20 is completely not Can deform.
The temperature of electrode 20 arbitrarily can set.For example, electrode chamber 10 being subject to during atmosphere opening It is roughly the same temperature that 20 temperature is adjusted to the temperature of the electrode 20 in film formation process, to suppress Because chamber 10 atmosphere opening when the temperature drop of electrode 20 that causes of radiating.Or, also can root Internal temperature according to chamber 10 of the rate of film build (rate) when high is adjusting the temperature of electrode 20.Especially, The temperature of electrode 20 is adjusted to rate of film build height preferably and the film of required film quality can be made in workpiece The temperature of film forming well on 100.
For example, as described below, electrode 20 is set according to the temperature of the workpiece 100 during film formation process Temperature.In the case where workpiece 100 is resin, sometimes for carry out film forming and it is preferred that by workpiece 100 Temperature be set higher than room temperature.For example in the case where film forming is carried out using HMDSO, if work The temperature of part 100 is 60 DEG C~80 DEG C, then film can be adhered well on workpiece 100.By so As be set as that the workpiece 100 of set point of temperature is deposited in chamber 10 in the case of, the temperature of electrode 20 Set also according to the temperature of workpiece 100.Thereby, it is possible to suppress the temperature change of workpiece 100. Therefore, the temperature of electrode 20 is set as 60 DEG C~80 DEG C by temperature adjustment device 30.
In addition, also the temperature of electrode 20 can be set as to chamber 10 by temperature adjustment device 30 Carry out the temperature in atmosphere opening.The temperature of the electrode 20 in film formation process than atmosphere opening in electricity In the case of the temperature height of pole 20, such as by using peltier (Peltier) element to adjustment portion 31 Deng so as to the temperature of the electrode 20 in film formation process can be reduced.
But, by improving the temperature of electrode 20, can be reduced by bakeing (baking) effect The moisture being adsorbed in atmosphere opening on 10 internal face of chamber etc..Thereby, it is possible to suppress to chamber 10 The increase of time that is exhausted of inside.It is therefore preferable that the temperature of electrode 20 is higher than room temperature.Therefore, The high temperature of temperature of the electrode 20 to be subject to than chamber 10 during atmosphere opening, by the temperature of electrode 20 It is adjusted to fixed.For example, the temperature of electrode 20 also can be adjusted by temperature adjustment device 30, with The temperature being fixed as in the temperature highest film formation process of electrode 20.
And, carry out greatly except the temperature of the electrode 20 of rising in film formation process and to chamber 10 Beyond temperature change between the temperature of the electrode 20 that gas declines when opening, electrode 20 can also produce temperature Degree change.For example, in the case where the electric power supplied by electrode 20 changes, the temperature of electrode 20 Degree can change.And, in the case of film formation time length or change workpiece 100 In the case of being carried out continuously into film process, the temperature of electrode 20 can be gradually increasing.If thus, not to electricity The temperature of pole 20 is adjusted, then electrode 20 can be caused to produce because of a variety of causes into during film process every time Temperature change.
On the other hand, in the film formation device 1 of the 1st embodiment of the invention, including film formation process A succession of in film process, the temperature of electrode 20 is adjusted to fixed.Therefore, can suppress because of electrode 20 temperature change causes film forming matter to peel off from electrode 20.As a result, according to film formation device 1, can prevent The problems such as only film forming matter is attached to workpiece 100 and causes film quality generation deterioration or thickness to become uneven.
(the 2nd embodiment)
The film formation device 1 of the 2nd embodiment of the present invention is different from the film formation device 1 shown in Fig. 1 Part is:As shown in figure 3, the inner setting in chamber 10 has The multiple processing regions for processing.Other structures are identical with the 1st embodiment.
Fig. 3 is represented and is set with the 1st processing region 101 and the 2nd processing region 102 in chamber 10 Example as multiple processing regions.Workpiece holder 70 makes workpiece 100 interior throughout the 1st in chamber 10 Processing region 101 and the 2nd processing region 102 and move.
Film formation device 1 shown in Fig. 3 is illustrated:1st processing region 101 be by sputtering method and The sputter processing region of film forming is carried out on workpiece 100, and the 2nd processing region 102 is by plasma CVD and carry out the example of the plasma CVD processing region of film forming on workpiece 100.1st In processing region 101, target (target) 201 is installed on target electrode 202.Target electrode 202 Be connected to supply high frequency (radio frequency (Radio Freqency, RF)) electric power or direct current (Direct Current, DC) the sputter power supply 203 of electric power.The structure of the 2nd processing region 102 and the film forming dress shown in Fig. 1 Put 1 identical.
Hereinafter, to being carried out continuously in the process in sputter processing region and plasma CVD processing region The situation of process illustrate.
First, electrode 20 is adjusted to the temperature of regulation by temperature adjustment device 30, and by workpiece 100 deposit in chamber 10, as shown in figure 3, workpiece 100 is configured at the 1st processing region 101 In.Also, from the inert gas supply source 52 of gas supply mechanism 50 by inertia such as argon (Ar) gas Gas 520 is imported in chamber 10.From sputter power supply 203 to 202 supply electric power of target electrode so that inertia Gas 520 discharges, so as to form plasma in the gas phase of the near surface of target 201.Wait It is subject to the cation of the inert gas 520 for accelerating to collide to the surface of target 201 in gas ions, passes through Sputter and discharge target atom.The atom discharged from the surface of target 201 adheres to/it is piled up in workpiece 100 surface, and form film.
After the sputter process in the 1st processing region 101 terminates, as shown in figure 4, being equipped on workpiece Workpiece 100 on fixed mount 70 moves to the 2nd processing region 102 from the 1st processing region 101.With Afterwards, in the 2nd processing region 102, by referring to the film build method illustrated by Fig. 2, by electrode 20 The temperature of regulation is adjusted to, and workpiece 100 is carried out based on plasma CVD method into film process. That is, the inside of the chamber 10 of vacuum is vented to by exhaust gear 60, from gas supply mechanism 50 unstrpped gas supply source 51 imports unstrpped gas 510.Then, unstripped gas is made in chamber 10 Body 510 is plasmarized, forms film on the surface of workpiece 100.Subsequently, take out of from chamber 10 The workpiece 100 that handles well.
Described above whole in film process, electrode 20 is adjusted by temperature adjustment device 30 Temperature so that the temperature of electrode 20 for fix.
In addition, in the 1st processing region 101, being configured with by lift 205 and in chamber 10 The gear lock (shutter) 204 for moving along the vertical direction.In the 2nd processing region 102 into film process During, as shown in figure 4, protecting the surface of target 201 by the gear lock 204 of rising.And, During atmosphere opening being carried out when 100 grade of workpiece is changed to chamber 10, also by gear lock 204 The surface of protection target 201.On the other hand, during sputter process, as shown in figure 3, gear lock 204 decline.
As described above, according to the film formation device 1 of the 2nd embodiment of the present invention, can pass through true Empty continuously carrying out the process in the process in the 1st processing region 101 and the 2nd processing region 102. Therefore, compared with the chamber is set to the situation of vacuum when per treatment, total (total) place can be shortened The reason time.And, workpiece 100 will not be exposed in air, thus, for example can prevent from being formed at There is rotten or impurity and be attached on film in the film on workpiece 100.
Further, in the film formation device 1 of the 2nd embodiment, also identical with the 1st embodiment, In film formation process based on plasma CVD method and other operations in addition to film formation process, pass through Temperature adjustment device 30 is adjusting the temperature of electrode 20, so that the temperature of electrode 20 is for fixing.Therefore, The deformation of the electrode 20 caused because of temperature change is suppressed, so as to because of electrode 20 and the heat of film forming matter The film forming matter that the difference of expansion rate causes is suppressed from the stripping of electrode 20.As a result, implementing the 2nd In the film formation device 1 of mode, it is attached on workpiece 100 prevented also from the film forming matter that peels off from electrode 20 The problems such as.Other are substantially the same with the 1st embodiment, thus omit the record for repeating.
In addition, the process in the 1st processing region 101 is to appoint with the processing sequence in the 2nd processing region Meaning.For example, both can as mentioned above as processed in the 1st processing region 101 after, the 2nd Processed in processing region 102, or also process can have been carried out in the 2nd processing region 102 Afterwards, processed in the 1st processing region 101.
Film formation device 1 shown in Fig. 3 is used for the decorative use of ejection formation plastics (plastic) product Deng.For example, it is suitable for making the auto parts such as door handle (doorknob) or meters present gold Category texture, and make the situation of the film forming such as aluminium film, stainless steel (SUS) film, titanium film.And, it is also possible to Decorative use in family's electrical article, toy, cosmetics containers, the hornbook of clock and watch etc..
For example, in the 1st film (the such as aluminium for forming easily oxidation by sputtering method on workpiece 100 Film etc.) after, continuous using vacuum, formed with covering the 1st film by plasma CVD method anti- Only the 2nd film of the 1st film oxidation is using as diaphragm.For example, the film build method is before manufacture automobile During speculum (reflector) of headlight (head light) etc., aluminium film is formed on the surface of resin parts In the case of wait effectively.
(other embodiment)
As described above, describing the present invention by embodiment, but should not be construed as constituting the disclosure The discussion and accompanying drawing of a part defines the present invention.According to the disclosure, those skilled in the art should energy Understand various replacement embodiments, embodiment and application technology.
In described, the example that workpiece 100 is flatly equipped on workpiece holder 70, but this is illustrated Invention is equally applicable to for example shown in Fig. 5, and workpiece 100 is vertically equipped on boat type (boat type) In the film formation device 1 of workpiece holder 70.In film formation device 1 shown in Fig. 5, electrode 20 be with Workpiece 100 is extends in the vertical direction opposite to each other.
And, the situation that film formation device 1 is plasma CVD equipment is illustratively illustrated, but Can be the film formation device using other film build methods, present invention can be suitably applied to configuration within the chamber The film formation device of electrode.For example, by temperature adjustment device 30 by the temperature of the target electrode of sputtering unit Degree is set as fixing, so as to suppress stripping of the film forming matter from target electrode.
Thus, the present invention is certainly comprising various embodiments that does not record etc. herein.Therefore, according to institute State bright, the technical scope of the present invention is only by the specific item defined of invention of appropriate claims.

Claims (5)

1. a kind of film formation device, for carrying out film forming on workpiece, the film formation device is characterised by Including:
Chamber, deposits the workpiece;
Electrode, configures in the chamber interior, in order to carry out film forming on the workpiece and supply electric power; And
Temperature adjustment device, adjusts the temperature of the electrode, so that carrying out film forming on the workpiece A succession of in film process, carry out the film formation process and the film formation process of film forming on the workpiece In operation in addition, the temperature of the electrode for fixing, in order to avoid be piled up in the film forming matter of the electrode from The stripping electrode.
2. film formation device according to claim 1, it is characterised in that
The temperature of the electrode when chamber atmosphere is opened by the temperature adjustment device be adjusted to The temperature identical temperature of the electrode in the film formation process, to suppress because of the air of the chamber The temperature drop that radiating when open is caused.
3. film formation device according to claim 1 and 2, it is characterised in that
Carry out on the workpiece film forming a succession of into film process be from by the Workpiece storage to described Chamber starts, through the film formation process, till the workpiece is taken out of from the chamber everywhere Reason.
4. film formation device according to claim 1 and 2, it is characterised in that further include:
Power supply, supplies the electric power to the electrode;And
Gas supply mechanism, unstrpped gas is supplied to the inside of the chamber,
The power supply supplies the electric power to the electrode, to form the plasma of the unstrpped gas,
By the workpiece is exposed in the plasma, so that with institute in the unstrpped gas Film on the workpiece film forming of the raw material for containing for principal component.
5. a kind of film build method, it is characterised in that
A succession of comprise the following steps into film process:
By film forming process object Workpiece storage within the chamber;
By the power supply of regulation to the electrode for being configured at the within the chamber, to carry out on the workpiece Film forming;And
The workpiece is carried out after film forming, atmosphere opening is carried out to the chamber,
Described a succession of in film process,
The temperature of the electrode is adjusted, so that carrying out film formation process and the institute of film forming on the workpiece State in the operation beyond film formation process, the temperature of the electrode is for fixing, in order to avoid it is piled up in the electrode Film forming matter from the stripping electrode.
CN201610188203.7A 2015-09-03 2016-03-29 Film formation device and film build method Pending CN106498371A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2015173437A JP6565502B2 (en) 2015-09-03 2015-09-03 Film forming apparatus and film forming method
JP2015-173437 2015-09-03

Publications (1)

Publication Number Publication Date
CN106498371A true CN106498371A (en) 2017-03-15

Family

ID=58278964

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610188203.7A Pending CN106498371A (en) 2015-09-03 2016-03-29 Film formation device and film build method

Country Status (2)

Country Link
JP (1) JP6565502B2 (en)
CN (1) CN106498371A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114807886A (en) * 2022-04-13 2022-07-29 北京北方华创微电子装备有限公司 Process chamber and process method

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6187691B1 (en) * 1999-05-14 2001-02-13 Asm Japan K.K. Method of forming film on semiconductor substrate in film-forming apparatus
CN103451725A (en) * 2012-06-01 2013-12-18 夏普株式会社 Vapor phase growth device and producing method of nitride semiconductor illuminating element
CN103534383A (en) * 2011-05-20 2014-01-22 株式会社岛津制作所 Thin film forming device
CN104485277A (en) * 2009-04-10 2015-04-01 应用材料公司 Hvpe chamber hardware

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02197575A (en) * 1989-01-26 1990-08-06 Canon Inc Microwave plasma cvd method and device therefor
JPH02236279A (en) * 1989-03-08 1990-09-19 Fujitsu Ltd Device for forming thin amorphous silicon film
US20080299326A1 (en) * 2007-05-30 2008-12-04 Asm Japan K.K. Plasma cvd apparatus having non-metal susceptor
JP2015220288A (en) * 2014-05-15 2015-12-07 三菱電機株式会社 Plasma cvd device and plasma cvd method using the same

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6187691B1 (en) * 1999-05-14 2001-02-13 Asm Japan K.K. Method of forming film on semiconductor substrate in film-forming apparatus
CN104485277A (en) * 2009-04-10 2015-04-01 应用材料公司 Hvpe chamber hardware
CN103534383A (en) * 2011-05-20 2014-01-22 株式会社岛津制作所 Thin film forming device
CN103451725A (en) * 2012-06-01 2013-12-18 夏普株式会社 Vapor phase growth device and producing method of nitride semiconductor illuminating element

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114807886A (en) * 2022-04-13 2022-07-29 北京北方华创微电子装备有限公司 Process chamber and process method
CN114807886B (en) * 2022-04-13 2024-05-17 北京北方华创微电子装备有限公司 Process chamber and process method

Also Published As

Publication number Publication date
JP2017048433A (en) 2017-03-09
JP6565502B2 (en) 2019-08-28

Similar Documents

Publication Publication Date Title
CN113025972B (en) Manufacturing method of aluminum target
EP2310554B1 (en) Process and installation for depositing films onto a substrate
WO2010045595A3 (en) Method for improving process control and film conformality of pecvd films
US10378095B2 (en) TiB2 layers and manufacture thereof
CN111748789B (en) Device and method for depositing pure DLC (Diamond like carbon) by enhancing glow discharge through graphite cathode arc
CN107267916A (en) It is a kind of in method of the carbide surface by Deposited By Dc Magnetron Sputtering W N hard films
CN107532290A (en) For the method for the substrate for producing coating
CN102912306B (en) Device and process for computerized automatic control high power pulsed magnetron spluttering
CN103938166A (en) High-energy pulse-type magnetron sputtering method and magnetron sputtering device
KR102408543B1 (en) High-power pulse coating method
CN106498371A (en) Film formation device and film build method
JP2000109979A (en) Surface treatment method by dc arc discharge plasma
KR20060041306A (en) Film forming method
US20040040833A1 (en) Apparatus and method for plasma treating an article
US20070009670A9 (en) Sputter method or device for the production of natural voltage optimized coatings
TW201531585A (en) Apparatus and method for the reduction of impurities in films
CN110656313B (en) Zirconium aluminum nitride/aluminum oxide composite coating firmly combined with hard alloy and preparation method thereof
JP5901571B2 (en) Deposition method
US20190276932A1 (en) Film forming apparatus and film forming method
CN109072418B (en) Apparatus and method for creating gradient layer defining properties in a sputtering apparatus multilayer coating system
CN111118479A (en) Process method for graphite boat saturation
KR20120061013A (en) Metal thin film forming apparatus and forming method of three-dimensional polymer using linear CD source and electron beam sputter
CN219449844U (en) Coating device
CN109837522A (en) A kind of forming diamond-like carbon film on surface of infrared optical element coating process
US20220044930A1 (en) Pulsed-plasma deposition of thin film layers

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20170315