CN106497250A - Luminous membrane preparation method - Google Patents

Luminous membrane preparation method Download PDF

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Publication number
CN106497250A
CN106497250A CN201611136633.0A CN201611136633A CN106497250A CN 106497250 A CN106497250 A CN 106497250A CN 201611136633 A CN201611136633 A CN 201611136633A CN 106497250 A CN106497250 A CN 106497250A
Authority
CN
China
Prior art keywords
base fabric
plasticizing
baking
pvdf
stabilizer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611136633.0A
Other languages
Chinese (zh)
Inventor
阮长青
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201611136633.0A priority Critical patent/CN106497250A/en
Publication of CN106497250A publication Critical patent/CN106497250A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D127/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers
    • C09D127/02—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
    • C09D127/04—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
    • C09D127/06—Homopolymers or copolymers of vinyl chloride
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
    • C08K13/02—Organic and inorganic ingredients
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/24—Acids; Salts thereof
    • C08K3/26—Carbonates; Bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/22—Luminous paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/24—Acids; Salts thereof
    • C08K3/26—Carbonates; Bicarbonates
    • C08K2003/265—Calcium, strontium or barium carbonate

Abstract

The invention discloses a kind of luminous membrane preparation method for construction material of building material field.Base fabric is woven into by dacron thread, is coated by polrvinyl chloride in base fabric（PVC）, plasticizer（DOP）, heat stabilizer, Calcium Carbonate, light stabilizer, antifungus agent, liquid flame retardant, Benzotriazole Ultraviolet Stabilizer, cross-linking agent, fluorine（pvdf）And strontium aluminate, be stirred coating material and be coated in base fabric, through the baking plasticizing of baking oven high humidity, coat in triplicate and toast plasticizing, the process of PVDF is finally carried out via big cylinder surfaces.Reach extinction, give out light, the performance such as mould proof, antifouling, fire-retardant, self-cleaning.

Description

Luminous membrane preparation method
Technical field
A kind of the present invention relates to building material field, more particularly to luminous membrane preparation method for construction material.
Background technology
The visible ray 5-10 minutes such as luminescent coating, active absorption daylight, light, ultraviolet light, scattered light, just can be in dark Middle continuous illumination more than 8 hours, and the multiple colouramas of the bluish-green purple lamp of reddish yellow can be launched as needed.Its principle of luminosity is point
The electronics of son or atom periphery receives outside energy, such as heat, and light, after ray is excited, from ground state transition to excited state, in non- Steady statue.When after the external world excites stopping, he returns ground state, the electronics of excited state is used amount of heat and gradually sends light. The safety signs such as brushing instrument, highway, plant equipment, fire equipment, antiaircraft aisle are used for, the luminescent substance for being used is most Phosphorescent pigment, phosphorescent pigment after ultraviolet or daylight lasing fluorescence, luminous be only capable of persistently several hours, and easily aging Failure, contains the radioactive substance such as radium or uranium in phosphorescence, harmful.
Content of the invention
The purpose of the present invention is the defect for overcoming prior art to exist, there is provided a kind of system for building surface light emitting membrane material Preparation Method, with tension, strong anti tear, anti-severe cold, light weight, extinction, give out light, smooth surface, anti-fouling and self-cleaning, sound insulation, anti-aging The characteristics of good with pliability.
The purpose of the present invention is realized by technical scheme once：
A kind of luminous membrane preparation method, it is characterised in that：The luminescent film proportioning raw materials are as follows：
Polrvinyl chloride（PVC） 45-85
Calcium Carbonate 0-8
DOP 15-30
Barium cadmium zinc heat stabilizer 2.5-5
Phosphoric acid ester liquid flame retardant 5-20
Antifungus agent 0.5-1.2
Benzotriazole Ultraviolet Stabilizer 0.1-0.5
Cross-linking agent 1-7
Fluorine（pvdf） 1-40
Hindered amine light stabilizer 0.1-0.8
Strontium aluminate 5-45
Said ratio unit is（kg)
Luminescent film processing technology is as follows：
1）Base fabric makes
Dacron thread is woven into base fabric；
2）Luminescent material is prepared
Luminous for coating film raw material is pressed proportioning mixing and stirring；
3）Coating coating
Luminescent material is coated in base fabric, and the base fabric after coating is coated in triplicate and toasted through the baking plasticizing of baking oven high humidity Plasticizing；
4）Surface treatment
Toasted plasticizing base fabric carries out the process of PVDF in 1 vat inner surface；Above-mentioned technical proposal is further described：Institute The baking oven high humidity baking temperature that states is 100 DEG C～180 DEG C, and baking time is 3～10min, and curing humidity is 5%, is formed afterwards Dry film, then places in high temperature furnace, 3～10min of solid state reaction at a temperature of 100 DEG C～180 DEG C, forms luminescent film.
The features such as present invention has anti-aging, good, fire-retardant pliability, good light transmission and long service life.
Description of the drawings
Fig. 1 is luminescent film test report.
Specific embodiment
Present disclosure is further described with reference to specifically specific embodiment：
The luminescent film of the present invention has and can light where dark, for the membrane material on structural construction surface, is a kind of tension, resists The luminescent film of the strong and anti-severe cold of tear.
Base fabric is woven into by dacron thread, is coated by polrvinyl chloride in base fabric（PVC）, plasticizer（DOP）, heat stabilizer, Calcium Carbonate, light stabilizer, antifungus agent, liquid flame retardant, Benzotriazole Ultraviolet Stabilizer, cross-linking agent, fluorine（pvdf）And aluminum Sour strontium, is stirred coating material and is coated in base fabric, through the baking plasticizing of baking oven high humidity, coats in triplicate and toasts plasticizing, The last process for carrying out PVDF via big cylinder surfaces.Reach extinction, give out light, the performance such as mould proof, antifouling, fire-retardant, self-cleaning.
The preferred value of luminescent film proportioning raw materials is as follows：
Polrvinyl chloride（PVC） 65
Calcium Carbonate 2
DOP 18
Barium cadmium zinc heat stabilizer 3
Phosphoric acid ester liquid flame retardant 6
Antifungus agent 1
Benzotriazole Ultraviolet Stabilizer 0.2
Cross-linking agent 2
Fluorine（pvdf） 20
Hindered amine light stabilizer 0.3
Strontium aluminate 28
Upper described specific embodiment is only described in further details to the purpose of the present invention, technical scheme and beneficial effect, with The present invention is not limited to, all any modification, equivalent substitution and improvements that within the spirit and principles in the present invention, is done etc., Should be included within the scope of the present invention.

Claims (2)

1. a kind of luminous membrane preparation method, it is characterised in that：The luminescent film proportioning raw materials are as follows：
Polrvinyl chloride（PVC） 45-85
Calcium Carbonate 0-8
DOP 15-30
Barium cadmium zinc heat stabilizer 2.5-5
Phosphoric acid ester liquid flame retardant 5-20
Antifungus agent 0.5-1.2
Benzotriazole Ultraviolet Stabilizer 0.1-0.5
Cross-linking agent 1-7
Fluorine（pvdf） 1-40
Hindered amine light stabilizer 0.1-0.8
Strontium aluminate 5-45
Said ratio unit is（kg)
Luminescent film processing technology is as follows：
1）Base fabric makes
Dacron thread is woven into base fabric；
2）Luminescent material is prepared
Luminous for coating film raw material is pressed proportioning mixing and stirring；
3）Coating coating
Luminescent material is coated in base fabric, and the base fabric after coating is coated in triplicate and toasted through the baking plasticizing of baking oven high humidity Plasticizing；
4）Surface treatment
Toasted plasticizing base fabric carries out the process of PVDF in 1 vat inner surface.
2. luminous membrane preparation method according to claim 1, it is characterised in that：
Described baking oven high humidity baking temperature is 100 DEG C～180 DEG C, and baking time is 3～10min, and curing humidity is 5%, Form dry film afterwards, then place in high temperature furnace, 3～10min of solid state reaction at a temperature of 100 DEG C～180 DEG C, formed and sent out Light film.
CN201611136633.0A 2016-12-12 2016-12-12 Luminous membrane preparation method Pending CN106497250A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611136633.0A CN106497250A (en) 2016-12-12 2016-12-12 Luminous membrane preparation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611136633.0A CN106497250A (en) 2016-12-12 2016-12-12 Luminous membrane preparation method

Publications (1)

Publication Number Publication Date
CN106497250A true CN106497250A (en) 2017-03-15

Family

ID=58329895

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611136633.0A Pending CN106497250A (en) 2016-12-12 2016-12-12 Luminous membrane preparation method

Country Status (1)

Country Link
CN (1) CN106497250A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108457078A (en) * 2018-05-21 2018-08-28 晒稀布（上海）纳米科技有限公司 Environmental-friendfilm film construction material and its manufacture craft

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4678225B2 (en) * 2005-03-31 2011-04-27 住友金属鉱山株式会社 Infrared shielding material fine particle dispersion and infrared shielding material
CN202644056U (en) * 2012-06-05 2013-01-02 南通大东有限公司 High-wet strength regenerated cellulose fiber towel
CN106046625A (en) * 2016-08-15 2016-10-26 东莞市悠悠美居家居制造有限公司 Polyvinyl chloride blowing glue film and calendaring process thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4678225B2 (en) * 2005-03-31 2011-04-27 住友金属鉱山株式会社 Infrared shielding material fine particle dispersion and infrared shielding material
CN202644056U (en) * 2012-06-05 2013-01-02 南通大东有限公司 High-wet strength regenerated cellulose fiber towel
CN106046625A (en) * 2016-08-15 2016-10-26 东莞市悠悠美居家居制造有限公司 Polyvinyl chloride blowing glue film and calendaring process thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
于洪全主编: "《功能材料》", 30 June 2014 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108457078A (en) * 2018-05-21 2018-08-28 晒稀布（上海）纳米科技有限公司 Environmental-friendfilm film construction material and its manufacture craft

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Application publication date: 20170315