CN106493364B - A kind of low activation martensitic steel precinct laser fusion increasing material manufacturing technique - Google Patents
A kind of low activation martensitic steel precinct laser fusion increasing material manufacturing technique Download PDFInfo
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- CN106493364B CN106493364B CN201610947008.8A CN201610947008A CN106493364B CN 106493364 B CN106493364 B CN 106493364B CN 201610947008 A CN201610947008 A CN 201610947008A CN 106493364 B CN106493364 B CN 106493364B
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- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
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- B22F10/64—Treatment of workpieces or articles after build-up by thermal means
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- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/20—Direct sintering or melting
- B22F10/28—Powder bed fusion, e.g. selective laser melting [SLM] or electron beam melting [EBM]
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- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
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- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
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- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/30—Process control
- B22F10/36—Process control of energy beam parameters
- B22F10/366—Scanning parameters, e.g. hatch distance or scanning strategy
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- B22F7/00—Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression
- B22F7/06—Manufacture of composite layers, workpieces, or articles, comprising metallic powder, by sintering the powder, with or without compacting wherein at least one part is obtained by sintering or compression of composite workpieces or articles from parts, e.g. to form tipped tools
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- B33—ADDITIVE MANUFACTURING TECHNOLOGY
- B33Y—ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
- B33Y10/00—Processes of additive manufacturing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/30—Process control
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- B22F12/00—Apparatus or devices specially adapted for additive manufacturing; Auxiliary means for additive manufacturing; Combinations of additive manufacturing apparatus or devices with other processing apparatus or devices
- B22F12/10—Auxiliary heating means
- B22F12/13—Auxiliary heating means to preheat the material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Abstract
The invention discloses a kind of low activation martensitic steel precinct laser fusion increasing material manufacturing technique, its feature includes:Material is low activation martensitic steel microsphere powder, and fine powder (200 400 mesh) is 1~1.5 with the powder weight proportioning of meal (50 150 mesh), with preferable compactedness;Using precinct laser fusion rapid molding method, the 300W of laser power 20, the 135um of lasing beam diameter 70, the 2000mm/s of sweep speed 500, the 120um of sweep span 35, the 50um of lift height 20, powder preheats 150 300 DEG C, the 20cm of shaping speed 53/ h, argon gas is protected and pressure maintains 10 20mbar in forming room, and part manufacture is incubated more than 48 hours, finally profiled part is heat-treated, Technology for Heating Processing after finishing at 250 400 DEG C:720 760 DEG C are warming up to stove, be incubated 60 120min, then cooling of coming out of the stove after cooling to less than 100 DEG C with the furnace, to reduce residual stress, the overall performance of raising part;Good part rapid shaping quality can be obtained under this technique.
Description
Technical field
The present invention relates to a kind of low activation martensitic steel precinct laser fusion increasing material manufacturing technique, can be used for fusion reactor blanket
And the rapid shaping of the Advanced Nuclear Energy Systems complex components such as fission-type reactor.
Background technology
Increasing material manufacturing (i.e. 3D printing) is rising in recent years and the emerging fast precise processing and manufacturing technology for developing rapidly,
It is used widely in aerospace field;The technology can process the part that conventional method is difficult to manufacture, with labyrinth
Parts-moulding high precision, production efficiency is high and part be integrally formed effect it is good the advantages of.Due to different material rapid shapings
Technique difference is larger, and part quick shaping process is the key of the technology.Fusion reactor is using low activation martensitic steel as structure
Material, low activation martensitic steel has excellent thermophysical property, Flouride-resistani acid phesphatase swelling performance, anti-liquid metal corrosion performance etc.,
The primary structural material of fusion reactor blanket is chosen as, has been also the main candidate structural wood of following fusion engineering mimoir heap covering
Material;Meanwhile, low activation martensitic steel is also the main candidate structure of the Advanced Nuclear Energy Systems critical components such as lead base heap fuel assembly
Material.The Advanced Nuclear Energy Systems critical component service condition such as fusion reactor blanket and lead base heap fuel assembly is harsh, is subjected to persistent erection
Sub- irradiation, surface heat flow high, nuclear heat high deposition, high pressure and complicated machinery load etc., and these key part structures are complicated, to portion
The Forming Quality and formed precision of part propose requirement higher.
The Advanced Nuclear Energy Systems such as fusion reactor blanket because being deposited with nuclear heat higher, cooling-part typically have high density and
The complicated water runner arrangement at narrow interval.At present, using welding more than shaping of the Advanced Nuclear Energy Systems labyrinth containing runner cooling-part
Method, it is especially to use the less high energy beam in heat affected area (such as electron beam, laser) welding method combination specially-shapeds more
Technique (such as patent:CN201110250136.4) etc.;Meanwhile, it is the global formation performance for further improving complex component, also adopt
With the compound welding technology of special welding method (such as Hot Isostatic Pressing Diffusion, electron beam, laser) (such as patent:
CN200810021143.5), but because weld seam is intensive, causes welding difficulty higher and crackle easily occurs in weld seam, additionally, welding process
Complicated heat input causes part distortion larger, and shaping difficulty is high and later stage orthopedic difficulty, the long preparation period of part, cost
It is high.
3D printing can one-shot forming labyrinth part, part distortion is small, near-net-shape, without following process treatment
Deng the shaping of the suitable part with labyrinth;The precision processing technology of 3D printing rapid shaping is applied into fusion reactor bag
The preparation of the Advanced Nuclear Energy Systems complex components such as layer, with wide development and application prospect, need to carry out fusion reactor special
The research of the complex component quick shaping process of structural material.
The content of the invention
The technical problem to be solved in the invention:Overcome that existing complex components welding processing difficulty is high, welding deformation
Greatly, easily there are the key issues such as crackle in postwelding, there is provided a kind of low activation martensitic steel precinct laser fusion increasing material manufacturing technique, with
Solve the problem of Advanced Nuclear Energy Systems complex components low activation martensitic steel 3D printing rapid shaping.Preferably constituency of the invention
Laser fusion technique carries out the rapid processing manufacture of the Advanced Nuclear Energy Systems such as fusion reactor blanket key complex components, with portion
Part can one-shot forming, the advantage that formed precision is high and Forming Quality is good.
Technical solution of the invention is as follows:A kind of low activation martensitic steel precinct laser fusion increasing material manufacturing technique,
Realize that step is as follows:
(1) raw material are low activation martensitic steel microsphere powder, and fine powder matches by a certain percentage with meal, are filled out with raising
Fill density;
(2) graphic computer description is carried out to the complex components to be molded, the complex components three that will be shaped
In dimension sheet template control computer, the main construction including threedimensional model, according to whether the selection shaping such as addition support
Direction, the thickness and the number of plies of hierarchy slicing, extraction and filling of cross section contour etc. are selected according to the size of part, set slice thick
Degree and total score layer number etc.;
(3) precinct laser fusion technique, laser power 20-300W, beam diameter 70-135um, sweep speed 500- are set
2000mm/s, sweep span 35-120um, lift height 20-50um, powder preheat 150-300 DEG C, shaping speed 5-20cm3/
H, argon gas is protected and pressure maintains 10-20mbar in forming room;
(4) powder mixture ratio, fine powder (200-400 mesh) is 1~1.5 with the powder weight proportioning of meal (50-150 mesh),
It is well mixed under vacuum condition, prevents Powder Oxidation;
(5) powdering and fusing, by powder feeding mechanism, uniform laying a layer thickness is the low activation horse of 0.2-1mm on substrate
Family name's body (CLAM) powdered steel, carries out rapid shaping, subsequently successively according to computer graphical chip formation using laser beam to powder
Powdering and laser beam melts rapid shaping are carried out, until complex components complete shaping;
(6) part manufacture is incubated more than 48 hours after finishing at 300-400 DEG C, finally carries out hot place to profiled part
Reason, Technology for Heating Processing:720-760 DEG C is warming up to stove, is incubated 60-120min, then come out of the stove after cooling to less than 100 DEG C with the furnace cold
But, to reduce residual stress, the overall performance of profiled part is improved;
Present invention advantage compared with prior art:
(1) present invention to complex components can a near-net-shape, within the reachable+0.5mm of dimensional accuracy, surface quality
It is higher, typically without follow-up mechanical process;
(2) complex components are molded and the microscopic structure of material has isotropism with mechanical property after Overheating Treatment
And homogenization;
(3) being molded in argon gas protection environment is carried out, and forming part oxygen element content (being less than 100ppm) meets standard, keeps away
Material oxidation is exempted from, parts-moulding quality is high, even tissue, the defect such as pore-free, crackle and no cofusing particle;
(4) the recyclable recycling of residual powder after being molded, stock utilization is close to 100%, and shaping speed is higher (reachable
To about 80cm3/ h) etc..
Brief description of the drawings
Fig. 1 is China's liquid DFLL the first wall components of covering;
Fig. 2 is that China liquid DFLL coverings cool down board member;
Fig. 3 is the Chinese lead base heap upper and lower tube base part of fuel assembly cladding tubes.
Specific embodiment
Below in conjunction with the accompanying drawings and specific embodiment is discussed in detail the present invention.But following embodiment is only limitted to explain this hair
Bright, protection scope of the present invention should include the full content of claim, be not limited only to the present embodiment.
Embodiment 1, by taking fusion reactor China liquid DFLL covering the first wall components rapid shapings as an example, as shown in figure 1, structure
Material is low activation martensite (CLAM) steel of China;
(1) material is the microsphere powder of low activation martensite (CLAM) steel, and by fine powder (200-350 mesh) and meal (50-
100 mesh) press by weight ratio 1:It is fitted into powder feeding mechanism after 1.5 mixing, powder preheats 300 DEG C;
(2) precinct laser fusion equipment is vacuumized, and treats that vacuum reaches 10-3After Pa magnitudes high-purity Ar is filled with to vacuum chamber2,
After vacuum reaches 1MPa, high-purity Ar is vacuumized and is filled with again2, so prepurging more than 2 times repeatedly;
(3) the CLAM steel fine powder and meal that a layer thickness is 0.5mm are sprawled in powdering plane by powder feeding mechanism first
Mixing match powder;
(4) by the STL form sheet template computers of the part of rapid shaping, area of computer aided graphics process is carried out;
According to the size of part:* * wide long are high=161mm*155mm*205mm, selection lift height is 0.5mm, it is considered to part into
Separated with the processing of substrate after type, total hierarchy number is 4120 layers;
(5) precinct laser fusion technique:Laser power 250W, laser diameter 80um, sweep speed 2000mm/s, scanning room
Away from 90um, lift height 50um, powder preheats 300 DEG C, and argon gas protection in forming room, argon pressure 17mbar is entirely being molded
During ensure shaping indoor temperature at 350 DEG C or so;
(6) laser beam is selectively sintered according to the information of cross section profile under control of the computer, metal dust
Be sintered together under the bombardment of laser beam, and with following molded part adhesive, after ground floor powder fusing after, pass through
Powder feeding mechanism lays second layer powder, and powder thickness is uniform and, such layer upon layer identical with ground floor thickness, until whole zero
All sintering is completed part;
(7) after the completion of part sintering, it is incubated in 350 DEG C of environment in forming room and is cracked with preventing portion part for 72 hours,
Insulation is begun to cool down to room temperature after terminating, and blow-on simultaneously takes out part after reclaiming unnecessary powder filler;
(8) part heat treatment;Part carries out vacuum heat after taking out, should with the remnants reduced during parts-moulding
Power, improves the overall performance of part, Technology for Heating Processing:Be warming up to 740 DEG C with stove, be incubated 120min, cool to the furnace 100 DEG C with
Come out of the stove after lower cooling;
(9) be computed with measurement, the shaping speed of the first wall components is 50cm3/ h, formed precision reaches+0.3mm, metallographic
Tissues observed is uniform, the defect such as pore-free, crackle and no cofusing particle.
Embodiment 2:By taking fusion reactor China liquid DFLL coverings cooling board member rapid shaping as an example, as shown in Fig. 2 structure
Material is low activation martensite (CLAM) steel of China;
(1) material is the microsphere powder of low activation martensite (CLAM) steel, and by fine powder (200-350 mesh) and meal (50-
150 mesh) press by weight ratio 1:It is fitted into powder feeding mechanism after 1.5 mixing, powder preheats 250 DEG C;
(2) precinct laser fusion equipment is vacuumized, and treats that vacuum reaches 10-3After Pa magnitudes high-purity Ar is filled with to vacuum chamber2,
After vacuum reaches 1MPa, high-purity Ar is vacuumized and is filled with again2, so prepurging more than 2 times repeatedly;
(3) the CLAM steel fine powder and meal that a layer thickness is 0.3mm are sprawled in powdering plane by powder feeding mechanism first
Mixing match powder;
(4) by the STL form sheet template computers of the part of rapid shaping, area of computer aided graphics process is carried out;
According to the size of part:* * wide long are high=200mm*101mm*10mm, selection lift height is 0.3mm, it is considered to part into
Separated with the processing of substrate after type, total hierarchy number is 40 layers;
(5) precinct laser fusion technique:Laser power 150W, laser diameter 90um, sweep speed 1000mm/s, scanning room
Away from 100um, lift height 30um, powder preheats 250 DEG C, and argon gas protection in forming room, argon pressure 13mbar is entirely being molded
During ensure shaping indoor temperature at 300 DEG C or so;
(6) laser beam is selectively sintered according to the information of cross section profile under control of the computer, metal dust
Be sintered together under the bombardment of laser beam, and with following molded part adhesive, after ground floor powder fusing after, pass through
Powder feeding mechanism lays second layer powder, and powder thickness is uniform and, such layer upon layer identical with ground floor thickness, until whole zero
All sintering is completed part;
(7) after the completion of part sintering, it is incubated in 300 DEG C of environment in forming room and is cracked with preventing portion part for 60 hours,
Insulation is begun to cool down to room temperature after terminating, and blow-on simultaneously takes out part after reclaiming unnecessary powder filler;
(8) part heat treatment;Part carries out vacuum heat after taking out, should with the remnants reduced during parts-moulding
Power, improves the overall performance of part, Technology for Heating Processing:Be warming up to 760 DEG C with stove, be incubated 120min, cool to the furnace 100 DEG C with
Come out of the stove after lower cooling.
(9) it is computed being about 60cm with measurement, the shaping speed for cooling down board member3/ h, formed precision reaches+0.4mm, gold
Phase tissues observed is uniform, does not find the defects such as stomata, crackle and no cofusing particle.
Embodiment 3:By taking the Chinese upper and lower tube base part rapid shaping of lead base heap fuel assembly cladding tubes as an example, as shown in figure 3,
Structural material is Chinese low activation martensitic steel;
(1) material is the microsphere powder of low activation martensitic steel (CLAM), and by fine powder (200-300 mesh) and meal (80-
150 mesh) press by weight ratio 1:It is fitted into powder feeding mechanism after 1.5 mixing, powder preheats 250 DEG C;
(2) precinct laser fusion equipment is vacuumized, and treats that vacuum reaches 10-3After Pa magnitudes high-purity Ar is filled with to vacuum chamber2,
After vacuum reaches 1MPa, high-purity Ar is vacuumized and is filled with again2, so prepurging more than 2 times repeatedly;
(3) the CLAM steel fine powder and meal that a layer thickness is 0.5mm are sprawled in powdering plane by powder feeding mechanism first
Mixing match powder;
(4) by the STL form sheet template computers of the part of rapid shaping, area of computer aided graphics process is carried out;
According to the size of part:* * wide long are high=117mm*130mm*10mm, selection lift height is 0.2mm, it is considered to part into
Separated with the processing of substrate after type, total hierarchy number is 80 layers;
(5) precinct laser fusion technique:Laser power 80W, laser diameter 70um, sweep speed 700mm/s, sweep span
80um, lift height 20um, powder preheat 250 DEG C, and argon gas protection in forming room, argon pressure 15mbar was molded entirely
Ensure shaping indoor temperature at 350 DEG C or so in journey;
(6) laser beam is selectively sintered according to the information of cross section profile under control of the computer, metal dust
Be sintered together under the bombardment of laser beam, and with following molded part adhesive, after ground floor powder fusing after, pass through
Powder feeding mechanism lays second layer powder, and powder thickness is uniform and, such layer upon layer identical with ground floor thickness, until whole zero
All sintering is completed part;
(7) after the completion of part sintering, it is incubated in 350 DEG C of environment in forming room and is cracked with preventing portion part for 48 hours,
Insulation is begun to cool down to room temperature after terminating, and blow-on simultaneously takes out part after reclaiming unnecessary powder filler;
(8) part heat treatment;Part carries out vacuum heat after taking out, should with the remnants reduced during parts-moulding
Power, improves the overall performance of part, Technology for Heating Processing:Be warming up to 720 DEG C with stove, be incubated 90min, cool to the furnace 100 DEG C with
Come out of the stove after lower cooling;
(9) be computed with measurement, the shaping speed of the tube base part is 75cm3/ h, formed precision reaches+0.2mm, metallographic
Tissues observed is uniform, the defect such as pore-free, crackle and no cofusing particle.
It should be noted that according to the various embodiments described above of the present invention, those skilled in the art are can to realize this hair completely
The four corner of bright claim 1 and appurtenance, implementation process and the same the various embodiments described above of method;And the present invention is not detailed
Elaboration partly belongs to techniques well known.
The above, part specific embodiment only of the present invention, but protection scope of the present invention is not limited thereto, and appoints
What those skilled in the art the invention discloses technical scope in, the change or replacement that can be readily occurred in should all be covered
Within protection scope of the present invention.
Claims (3)
1. a kind of low activation martensitic steel precinct laser fusion increasing material manufacturing technique, it is characterised in that:It is low activation including material
Martensite steel microsphere powder, fine powder 200-400 mesh is 1~1.5 with the powder weight proportioning of meal 50-150 mesh, with preferable
Compactedness;Using precinct laser fusion rapid molding method, laser power 20-300W, lasing beam diameter 70-135um, scanning speed
Degree 500-2000mm/s, sweep span 35-120um, lift height 20-50um, powder preheat 150-300 DEG C, shaping speed 5-
20cm3/ h, argon gas is protected and pressure maintains 10-20mbar in forming room, and profiled part is manufactured after finishing in 250-400 DEG C of temperature
The lower insulation of degree, to prevent from cracking, is finally heat-treated to the part for manufacturing, and to reduce residual stress, improves forming part
The overall performance of part.
2. a kind of low activation martensitic steel precinct laser fusion increasing material manufacturing technique according to claim 1, its feature exists
In:The profiled part manufacture is incubated more than 48 hours after finishing at 250-400 DEG C, prevents crackle.
3. a kind of low activation martensitic steel precinct laser fusion increasing material manufacturing technique according to claim 1, its feature exists
In:The process of thermal treatment:720-760 DEG C is warming up to stove, be incubated 60-120min, then after cooling to less than 100 DEG C with the furnace
Come out of the stove cooling, to reduce residual stress, improve the overall performance of profiled part.
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