CN106490041A - 一种检验科用抑菌消毒液及其制备方法 - Google Patents
一种检验科用抑菌消毒液及其制备方法 Download PDFInfo
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Abstract
本发明公开了一种检验科用抑菌消毒液及其制备方法，由以下重量份的原料制成：晚香玉4‑10份、大蒜12‑24份、常青藤10‑22份、花椒9‑15份、石榴皮12‑18份、紫藤6‑12份、八角莲20‑26份、地胆草12‑24份、败酱草8‑14份、苦豆子6‑18份、斑鸠菊20‑32份、防葵6‑12份、艾叶油4‑10份、柑橘精油10‑16份；本发明采用纯天然植物成分，能有效的对病房内多种细菌、真菌进行灭除和抑制其生长繁殖，并且气味天然清新、对人体安全无害，具备消毒、抑菌、清热、润肺的功效。
Description
技术领域
本发明属于中药技术领域，具体是一种检验科用抑菌消毒液及其制备方法。
背景技术
检验科是病原微生物比较集中的场所，它集中了临床各科室送检的人体体液、血液、呼吸道分泌物、胃肠道排泄物等标本，是医院感染预防和控制的重点科室，检验人员也是医院感染监测的重点人员之一；因此，加强检验科工作人员的安全防护及对环境的严格消毒非常重要。
现有技术中，检验科室内空间的杀菌灭菌，常用的方法有化学试剂灭菌、射线灭菌、干热灭菌、温热灭菌和过滤除菌以及杀菌药物熏蒸灭菌；这几类消毒方式虽然起到一定的消毒作用，但易消毒不彻底、有刺激味，易损伤检验人员的皮肤、不稳定，甚至只能起到净化空气的作用，不具备对人体保健的功效，严重影响检验科人员的呼吸系统与样品检验结果的准确性。
检验科用抑菌消毒液必须安全、有效、无毒副作用，而中药学作为我国的传统医学，具有作用强、见效快、药效持久等优点，且没有依赖性、耐药性以及毒副作用，易溶于水、稳定性高，因此选择检验科用抑菌消毒液，对于检验科室的环境具有十分重要的意义。
发明内容
本发明的目的在于提供一种检验科用抑菌消毒液及其制备方法，以解决上述背景技术中提出的问题。
为实现上述目的，本发明提供如下技术方案：
一种检验科用抑菌消毒液，由以下重量份的原料制成：晚香玉4-10份、大蒜12-24份、常青藤10-22份、花椒9-15份、石榴皮12-18份、紫藤6-12份、八角莲20-26份、地胆草12-24份、败酱草8-14份、苦豆子6-18份、斑鸠菊20-32份、防葵6-12份、艾叶油4-10份、柑橘精油10-16份。
作为本发明进一步的方案：所述检验科用抑菌消毒液，由以下重量份的原料制成：晚香玉5-9份、大蒜16-20份、常青藤14-18份、花椒11-13份、石榴皮13-17份、紫藤7-11份、八角莲21-25份、地胆草14-22份、败酱草9-13份、苦豆子8-16份、斑鸠菊22-30份、防葵7-11份、艾叶油5-9份、柑橘精油11-15份。
作为本发明再进一步的方案：所述检验科用抑菌消毒液，由以下重量份的原料制成：晚香玉7份、大蒜18份、常青藤16份、花椒12份、石榴皮15份、紫藤9份、八角莲23份、地胆草18份、败酱草11份、苦豆子12份、斑鸠菊26份、防葵9份、艾叶油7份、柑橘精油13份。
作为本发明再进一步的方案：所述晚香玉、苦豆子采用植物新鲜花瓣；八角莲、地胆草、斑鸠菊取新鲜植株。
作为本发明再进一步的方案：所述检验科用抑菌消毒液的制备方法，包括以下步骤：
1)将配方量的常青藤、紫藤、败酱草、防葵、石榴皮、花椒和大蒜捣碎后加入5-8倍重量的盐水中，武火煎开转文火煎煮20-30min，过滤得煎煮液冷却备用；
2)将配方量的晚香玉、苦豆子新鲜植物花瓣捣碎，加入8-10倍重量的乙醇溶液中浸泡20-24h，再用超声波处理1-2h，过滤取乙醇提取液备用；
3)将配方量的八角莲、地胆草和斑鸠菊捣碎与柑橘精油混合，置于反应釜中，加入5-8倍重量的去离子水，加热至80℃恒温浸泡1-2h，过滤得滤液备用；
4)将步骤1)中的煎煮液、步骤2)中的乙醇提取液、步骤3)中的滤液，加入搅拌罐中混合，在1200-1600r/min的转速下搅拌15-20min，再加入配方量的艾叶油，调整转速至600-800r/min搅拌10-15min，过滤并低温浓缩至原液体的15％，得到本发明的抑菌消毒液。
作为本发明再进一步的方案：所述步骤1)中的盐水，以盐:水＝1∶25的质量比配置而成。
作为本发明再进一步的方案：所述步骤2)中的乙醇溶液为体积分数80％-85％的乙醇水溶液。
本发明所用的中药药性如下：
1.晚香玉：味微甘、淡；性凉，有清肝明目、拔毒生肌的功效，常被用来主治痈疮肿毒。
2.大蒜：生辛，热；熟甘，温；入脾、胃、肺经；解毒杀虫，消肿止痛，止泻止痢，治肺，驱虫，此外还有温脾暖胃；治痈疽肿毒，白秃癣疮，痢疾泄泻，肺痨顿咳，蛔虫蛲虫，饮食积滞，脘腹冷痛，水肿胀满；
3.常青藤：甘、凉，无毒；入肝、脾二经；善于祛风除湿，凉血止痛，疏风通络，常用于风热痹痛、产后感风，腰部疼痛等症。
4.花椒：可用于温中散寒，除湿，止痛，杀虫，解鱼腥毒。治积食停饮，心腹冷痛，呕吐，噫呃，咳嗽气逆，风寒湿痹，泄泻，痢疾，疝痛，齿痛，蛔虫病，蛲虫病，阴痒，疮疥等症。
5.石榴皮：味酸，涩，性温，小毒；归大肠经；主治中耳炎、创伤出血、月经不调、红崩白带、牙痛、吐血、久泻、久痢、便血、脱肛、滑精、崩漏、带下、虫积腹痛、疥癣等症状。
6.紫藤：甘，微温，有小毒；具有杀虫、止痛、祛风通络等功效，可治筋骨疼、风痹痛、蛲虫病等。
7.八角莲：味苦，辛，性凉，有毒；肺，肝经；化痰散结、祛瘀止痛、清热解毒；用于咳嗽、咽喉肿痛、瘰疬、瘿瘤、痈肿、疔疮、毒蛇咬伤、跌打损伤、痹证。
8.地胆草：性寒，味苦辛；能够清热解毒，利尿消肿。用于感冒，急性扁桃体炎，咽喉炎，眼结膜炎，流行性乙型脑炎，百日咳，急性黄疸型肝炎，肝硬化腹水，急、慢性肾炎，疖肿，湿疹。
9.败酱草：味辛、苦，微寒；归肝、胃、大肠经；能够清热解毒，凉血，消痈排脓，祛瘀止痛；用于肠痈，肺痈高热，咳吐脓血，热毒疮疔，疮疖痛肿，胸腹疼痛，阑尾炎，肠炎、痢疾，产后腹痛，痛经。
10.苦豆子：苦、寒。有毒。归胃、大肠经；能够清热燥湿，止痛，杀虫。
11.斑鸠菊：味甘，涩，性凉；能清热解毒，生肌敛疮；主治阑尾炎；疮疖；烫火伤。
12.防葵：辛，寒，无毒；能】:降逆止咳、清热通淋、益气填精、除邪镇惊、行气散结；主治咳逆上气、膀胱热结、少尿、膀胱宿水、小腹支满胀痛、五脏气虚、癫痫惊狂、邪气惊狂、腹中气、血、痰、邪气结块。
与现有技术相比，本发明的有益效果是：本发明采用纯天然中药成分配方，符合中医药和现代医药理论，具有清热解毒、抑菌杀菌、杀虫消炎、易溶于水、稳定性高等特点，且对人体皮肤无刺激，稳定性高、安全无毒副作用，可广泛应用于检验科人员皮肤以及对室内环境的消毒。
具体实施方式
下面结合具体实施方式对本专利的技术方案作进一步详细地说明。
实施例1
一种检验科用抑菌消毒液，由以下重量份的原料制成：晚香玉4-10份、大蒜12-24份、常青藤10份、花椒9份、石榴皮12份、紫藤6份、八角莲20份、地胆草12份、败酱草8份、苦豆子6份、斑鸠菊20份、防葵6份、艾叶油4份、柑橘精油10份。
所述检验科用抑菌消毒液的制备方法，包括以下步骤：
1)将配方量的常青藤、紫藤、败酱草、防葵、石榴皮、花椒和大蒜捣碎后加入5-8倍重量的盐水中，盐水以盐:水＝1∶25的质量比配置而成；武火煎开转文火煎煮20-30min，过滤得煎煮液冷却备用；
2)将配方量的晚香玉、苦豆子新鲜植物花瓣捣碎，加入8-10倍重量、体积分数为80％-85％的乙醇水溶液中浸泡20-24h，再用超声波处理1-2h，过滤取乙醇提取液备用；
3)将配方量的八角莲、地胆草和斑鸠菊捣碎与柑橘精油混合，置于反应釜中，加入5-8倍重量的去离子水，加热至80℃恒温浸泡1-2h，过滤得滤液备用；
4)将步骤1)中的煎煮液、步骤2)中的乙醇提取液、步骤3)中的滤液，加入搅拌罐中混合，在1200-1600r/min的转速下搅拌15-20min，再加入配方量的艾叶油，调整转速至600-800r/min搅拌10-15min，过滤并低温浓缩至原液体的15％，得到本发明的抑菌消毒液。
实施例2
一种检验科用抑菌消毒液，由以下重量份的原料制成：晚香玉10份、大蒜24份、常青藤22份、花椒15份、石榴皮18份、紫藤12份、八角莲26份、地胆草24份、败酱草14份、苦豆子18份、斑鸠菊32份、防葵12份、艾叶油10份、柑橘精油10-16份。
所述检验科用抑菌消毒液的制备方法，包括以下步骤：
1)将配方量的常青藤、紫藤、败酱草、防葵、石榴皮、花椒和大蒜捣碎后加入5-8倍重量的盐水中，盐水以盐:水＝1∶25的质量比配置而成；武火煎开转文火煎煮20-30min，过滤得煎煮液冷却备用；
2)将配方量的晚香玉、苦豆子新鲜植物花瓣捣碎，加入8-10倍重量、体积分数为80％-85％的乙醇水溶液中浸泡20-24h，再用超声波处理1-2h，过滤取乙醇提取液备用；
3)将配方量的八角莲、地胆草和斑鸠菊捣碎与柑橘精油混合，置于反应釜中，加入5-8倍重量的去离子水，加热至80℃恒温浸泡1-2h，过滤得滤液备用；
4)将步骤1)中的煎煮液、步骤2)中的乙醇提取液、步骤3)中的滤液，加入搅拌罐中混合，在1200-1600r/min的转速下搅拌15-20min，再加入配方量的艾叶油，调整转速至600-800r/min搅拌10-15min，过滤并低温浓缩至原液体的15％，得到本发明的抑菌消毒液。
实施例3
一种检验科用抑菌消毒液，由以下重量份的原料制成：晚香玉5份、大蒜16份、常青藤14份、花椒11份、石榴皮13份、紫藤7份、八角莲21份、地胆草14份、败酱草9份、苦豆子8份、斑鸠菊22份、防葵7份、艾叶油5份、柑橘精油11份。
所述检验科用抑菌消毒液的制备方法，包括以下步骤：
1)将配方量的常青藤、紫藤、败酱草、防葵、石榴皮、花椒和大蒜捣碎后加入5-8倍重量的盐水中，盐水以盐:水＝1∶25的质量比配置而成；武火煎开转文火煎煮20-30min，过滤得煎煮液冷却备用；
2)将配方量的晚香玉、苦豆子新鲜植物花瓣捣碎，加入8-10倍重量、体积分数为80％-85％的乙醇水溶液中浸泡20-24h，再用超声波处理1-2h，过滤取乙醇提取液备用；
3)将配方量的八角莲、地胆草和斑鸠菊捣碎与柑橘精油混合，置于反应釜中，加入5-8倍重量的去离子水，加热至80℃恒温浸泡1-2h，过滤得滤液备用；
4)将步骤1)中的煎煮液、步骤2)中的乙醇提取液、步骤3)中的滤液，加入搅拌罐中混合，在1200-1600r/min的转速下搅拌15-20min，再加入配方量的艾叶油，调整转速至600-800r/min搅拌10-15min，过滤并低温浓缩至原液体的15％，得到本发明的抑菌消毒液。
实施例4
一种检验科用抑菌消毒液，由以下重量份的原料制成：晚香玉9份、大蒜20份、常青藤18份、花椒13份、石榴皮17份、紫藤11份、八角莲25份、地胆草22份、败酱草13份、苦豆子16份、斑鸠菊30份、防葵11份、艾叶油9份、柑橘精油15份。
所述检验科用抑菌消毒液的制备方法，包括以下步骤：
1)将配方量的常青藤、紫藤、败酱草、防葵、石榴皮、花椒和大蒜捣碎后加入5-8倍重量的盐水中，盐水以盐:水＝1∶25的质量比配置而成；武火煎开转文火煎煮20-30min，过滤得煎煮液冷却备用；
2)将配方量的晚香玉、苦豆子新鲜植物花瓣捣碎，加入8-10倍重量、体积分数为80％-85％的乙醇水溶液中浸泡20-24h，再用超声波处理1-2h，过滤取乙醇提取液备用；
3)将配方量的八角莲、地胆草和斑鸠菊捣碎与柑橘精油混合，置于反应釜中，加入5-8倍重量的去离子水，加热至80℃恒温浸泡1-2h，过滤得滤液备用；
4)将步骤1)中的煎煮液、步骤2)中的乙醇提取液、步骤3)中的滤液，加入搅拌罐中混合，在1200-1600r/min的转速下搅拌15-20min，再加入配方量的艾叶油，调整转速至600-800r/min搅拌10-15min，过滤并低温浓缩至原液体的15％，得到本发明的抑菌消毒液。
实施例5
一种检验科用抑菌消毒液，由以下重量份的原料制成：晚香玉7份、大蒜18份、常青藤16份、花椒12份、石榴皮15份、紫藤9份、八角莲23份、地胆草18份、败酱草11份、苦豆子12份、斑鸠菊26份、防葵9份、艾叶油7份、柑橘精油13份。
所述检验科用抑菌消毒液的制备方法，包括以下步骤：
1)将配方量的常青藤、紫藤、败酱草、防葵、石榴皮、花椒和大蒜捣碎后加入5-8倍重量的盐水中，盐水以盐:水＝1∶25的质量比配置而成；武火煎开转文火煎煮20-30min，过滤得煎煮液冷却备用；
2)将配方量的晚香玉、苦豆子新鲜植物花瓣捣碎，加入8-10倍重量、体积分数为80％-85％的乙醇水溶液中浸泡20-24h，再用超声波处理1-2h，过滤取乙醇提取液备用；
3)将配方量的八角莲、地胆草和斑鸠菊捣碎与柑橘精油混合，置于反应釜中，加入5-8倍重量的去离子水，加热至80℃恒温浸泡1-2h，过滤得滤液备用；
4)将步骤1)中的煎煮液、步骤2)中的乙醇提取液、步骤3)中的滤液，加入搅拌罐中混合，在1200-1600r/min的转速下搅拌15-20min，再加入配方量的艾叶油，调整转速至600-800r/min搅拌10-15min，过滤并低温浓缩至原液体的15％，得到本发明的抑菌消毒液。
实验例1
对本发明的灭菌效果进行测试：
1.实验对象：本发明实施例1-5所得的产品为实验组，市面上普通的消毒剂为对照组。
2.实验方法：把实验组和对照组的消毒剂加入已培养一段时间的常见有害菌类的培养基中，一段时间后观察培养基内菌类生长情况，其中培养的常见有害菌类包括大肠杆菌、金黄色葡萄球菌、黑曲霉等有害细菌；
3.实验结果：如表1所示：
表1本发明消毒液的灭菌效果测试实验
由上述实验可知本发明的抑菌消毒液在灭菌方面比市面上普通的消毒剂灭菌效果更快、效率更高、灭菌效果也更持久。
通过以上实验可知本发明实施例5所制得消毒液比实施例1-4所制得消毒液在杀菌消毒的效果上更为优越，即实施例5为本发明最佳方案。
上面对本专利的较佳实施方式作了详细说明，但是本专利并不限于上述实施方式，在本领域的普通技术人员所具备的知识范围内，还可以在不脱离本专利宗旨的前提下作出各种变化。
Claims (7)
1.一种检验科用抑菌消毒液，其特征在于，由以下重量份的原料制成：晚香玉4-10份、大蒜12-24份、常青藤10-22份、花椒9-15份、石榴皮12-18份、紫藤6-12份、八角莲20-26份、地胆草12-24份、败酱草8-14份、苦豆子6-18份、斑鸠菊20-32份、防葵6-12份、艾叶油4-10份、柑橘精油10-16份。
2.根据权利要求1所述检验科用抑菌消毒液，其特征在于，由以下重量份的原料制成：晚香玉5-9份、大蒜16-20份、常青藤14-18份、花椒11-13份、石榴皮13-17份、紫藤7-11份、八角莲21-25份、地胆草14-22份、败酱草9-13份、苦豆子8-16份、斑鸠菊22-30份、防葵7-11份、艾叶油5-9份、柑橘精油11-15份。
3.根据权利要求1所述检验科用抑菌消毒液，其特征在于，由以下重量份的原料制成：晚香玉7份、大蒜18份、常青藤16份、花椒12份、石榴皮15份、紫藤9份、八角莲23份、地胆草18份、败酱草11份、苦豆子12份、斑鸠菊26份、防葵9份、艾叶油7份、柑橘精油13份。
4.根据权利要求1-3所述的检验科用抑菌消毒液，其特征在于，所述晚香玉、苦豆子采用植物新鲜花瓣；八角莲、地胆草、斑鸠菊取新鲜植株。
5.一种如权利要求1-3任一所述的检验科用抑菌消毒液的制备方法，其特征在于，包括以下步骤：
1)将配方量的常青藤、紫藤、败酱草、防葵、石榴皮、花椒和大蒜捣碎后加入5-8倍重量的盐水中，武火煎开转文火煎煮20-30min，过滤得煎煮液冷却备用；
2)将配方量的晚香玉、苦豆子新鲜植物花瓣捣碎，加入8-10倍重量的乙醇溶液中浸泡20-24h，再用超声波处理1-2h，过滤取乙醇提取液备用；
3)将配方量的八角莲、地胆草和斑鸠菊捣碎与柑橘精油混合，置于反应釜中，加入5-8倍重量的去离子水，加热至80℃恒温浸泡1-2h，过滤得滤液备用；
4)将步骤1)中的煎煮液、步骤2)中的乙醇提取液、步骤3)中的滤液，加入搅拌罐中混合，在1200-1600r/min的转速下搅拌15-20min，再加入配方量的艾叶油，调整转速至600-800r/min搅拌10-15min，过滤并低温浓缩至原液体的15％，得到本发明的抑菌消毒液。
6.根据权利要求5所述的检验科用抑菌消毒液的制备方法，其特征在于，所述步骤1)中的盐水，以盐:水＝1∶25的质量比配置而成。
7.根据权利要求5所述的检验科用抑菌消毒液的制备方法，其特征在于，所述步骤2)中的乙醇溶液为体积分数80％-85％的乙醇水溶液。
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