CN106474205A - A kind of processing method of selenium-rich fleece-flower root medicine materical crude slice - Google Patents
A kind of processing method of selenium-rich fleece-flower root medicine materical crude slice Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/704—Polygonum, e.g. knotweed
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/42—Cucurbitaceae (Cucumber family)
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/42—Cucurbitaceae (Cucumber family)
- A61K36/424—Gynostemma
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/888—Araceae (Arum family), e.g. caladium, calla lily or skunk cabbage
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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Abstract
The invention discloses a kind of processing method of selenium-rich fleece-flower root medicine materical crude slice, belongs to Chinese medicine processing technique field.The method that the processing method of the fleece-flower root medicine materical crude slice of the present invention is combined using physics and chemistry, not only increase the content of selenium element in fleece-flower root processed goods, and reduce the content of fleece-flower root Poisoning composition general anthraquinone, both the drug safety of the fleece-flower root had been ensure that, had enhanced the clearing heat and detoxicating effect of the fleece-flower root again.
Description
Technical field
The invention belongs to Chinese medicine processing technique field, specifically a kind of processing method of selenium-rich fleece-flower root medicine materical crude slice.
Background technology
The fleece-flower root, also known as ground smart, red interior disappear, the tuber of multiflower knotweed, what husband, iron sliding weight of steelyard, be the polygonaceae arsesmart fleece-flower root
The root tuber of (Polygonum multiflorumThunb.).Health product cures mainly defaecation, subduing inflammation, solution sore.
With understanding of the people to trace element, trace element and the relation of human health be increasingly subject to biologist and
The attention of medical worker.Known that now 14 kinds of trace elements are required for human body, i.e., iron, zinc, iodine, manganese, molybdenum, cobalt, selenium,
Chromium, nickel, tin, silicon, fluorine and vanadium.In the fleece-flower root rich in abundant iron, copper, zinc, manganese, potassium, calcium, magnesium, cobalt, chromium and several amino acids,
Polysaccharide isoreactivity composition, is one of conventional Chinese medicine,.
Research shows that selenium is relevant with biological antioxidant defense system, with removing interior free yl, anti-aging, enhancing people
Body immunity, antagonism heavy metal toxicity and the biological function such as anti-cancer, anticancer.It is prevention and treatment Keshan disease, Kaschin-Beck disease to mend selenium
The disease caused etc. many scarce selenium and the effective way of anti-cancer, anticancer, but in the fleece-flower root, selenium element content is considerably less, because
This, is the containing of the toxic component anthraquinone reduced in the fleece-flower root of pure at present in existing fleece-flower root medicine materical crude slice process technology
Amount, and do not have the report for both reducing that fleece-flower root Poisoning component content improves Se content.
Content of the invention
Present invention aims to the defect of prior art presence or deficiency, provide a kind of selenium-rich fleece-flower root medicine materical crude slice
Processing method.
In order to realize the purpose of the present invention, the present invention is realized by following technical method：
A kind of processing method of selenium-rich fleece-flower root medicine materical crude slice, specifically includes following steps：
(1) fleece-flower root raw medicinal herbs, is taken, is cut into slices after epidermis is cleaned, slice thickness is 10mm, fine day is selected, is exposed to the sun 2-4 days,
Microwave treatment 10-15min, microwave power are 300-500w, then the fleece-flower root thin slice of process are placed on irradiation 45- under infrared lamp
60min, after taking-up, room temperature transfers use of purchasing；
(2), process (1) middle for step in the fleece-flower root loading china container for completing, mother chrysanthemum water extract is poured into by the fleece-flower root
It is completely soaked, vessel port is sealed, and container is placed in 40 DEG C of environment, places 5-10 days, by the fleece-flower root after immersion together with leaching
The ultrasonically treated 3-5min of bubble liquid, filters, then concentrate the filtrate to stoste 1/6th；The fleece-flower root after ultrasound is dried naturally
Pour into after mixing with concentrate afterwards in transparent airtight container, vexed moisten to container in no liquid residual；Supersonic frequency 30kHz-
100kHz；
(3) the selenium-rich for, taking 2 times of fleece-flower root raw medicinal herbs weight strengthens liquid, is concentrated into 1/7th of stoste, then by step (2)
Prepare the fleece-flower root thin slice that completes to pour in the ceramic vessel equipped with concentrate, vexed moisten to container in no liquid residual, by vexed profit
Fleece-flower root thin slice afterwards, water proof are heated to alcohol-free taste, take out, dry naturally, obtain final product selenium-rich fleece-flower root medicine materical crude slice.
Described selenium-rich strengthen liquid be by fresh pumpkin skin, fresh Amorphophallus rivieri skin, fresh jerusalem artichoke petal, fresh gynostemma pentaphylla leaf according to weight ratio
1-4:3-7:1-5:After 2-8 mixing, add 25% ethanol solution of 1 times of its gross weight to extract 45min and obtain final product selenium-rich enhancing liquid.
The beneficial effects of the present invention is:The processing method of the fleece-flower root medicine materical crude slice of the present invention is combined using physics and chemistry
Method, not only increase the content of selenium element in fleece-flower root processed goods, and reduce fleece-flower root Poisoning composition general anthraquinone
Content, both ensure that the drug safety of the fleece-flower root, enhanced the clearing heat and detoxicating effect of the fleece-flower root again.
Specific embodiment
By the following examples further describing the present invention, it should be understood that these embodiments are only used for illustration
Purpose, is not limited to the present invention.
Embodiment 1
A kind of processing method of selenium-rich fleece-flower root medicine materical crude slice, specifically includes following steps：
(1) fleece-flower root raw medicinal herbs, is taken, is cut into slices after epidermis is cleaned, slice thickness is 10mm, fine day is selected, is exposed to the sun 2 days, micro-
Ripple processes 10min, and microwave power is 300w, after the fleece-flower root thin slice after process is placed under infrared lamp irradiation 45min, after taking-up
Room temperature transfers use of purchasing；
(2), will step (1) the middle fleece-flower root that completes of processing loads in china container, be subsequently poured into mother chrysanthemum water extract by what
The tuber of multiflower knotweed is completely soaked, and vessel port is sealed, and container is placed in 40 DEG C of environment, places 5 days, by the fleece-flower root after immersion together with leaching
The ultrasonically treated 3-5min of bubble liquid, filters, then concentrate the filtrate to stoste 1/6th；The fleece-flower root after ultrasound is dried naturally
Pour into after mixing with concentrate afterwards in transparent airtight container, vexed moisten to container in no liquid residual；Supersonic frequency 30kHz-
100kHz；
(3) the selenium-rich for, taking 2 times of fleece-flower root raw medicinal herbs weight strengthens liquid, is concentrated into 1/7th of stoste, then by step (2)
Prepare the fleece-flower root thin slice that completes to pour in the ceramic vessel equipped with concentrate, vexed moisten to container in no liquid residual, by vexed profit
Fleece-flower root thin slice afterwards, water proof are heated to alcohol-free taste, take out, dry naturally, obtain final product selenium-rich fleece-flower root medicine materical crude slice.
It is that fresh pumpkin skin, konjaku skin, jerusalem artichoke petal, gynostemma pentaphyllum leaf are compared 1 according to weight that described selenium-rich strengthens liquid:3:
1:After 2 mixing, add 1 times of 25% ethanol solution of its gross weight that 45min is decocted, obtain final product selenium-rich and strengthen liquid.
Embodiment 2
A kind of processing method of selenium-rich fleece-flower root medicine materical crude slice, specifically includes following steps：
(1) fleece-flower root raw medicinal herbs, is taken, is cut into slices after epidermis is cleaned, slice thickness is 10mm, fine day is selected, is exposed to the sun 3 days, micro-
Ripple processes 15min, and microwave power is 500w, then the fleece-flower root thin slice of process is placed on irradiation 60min under infrared lamp, after taking-up
Room temperature transfers use of purchasing；
(2), will step (1) the middle fleece-flower root that completes of processing loads in china container, be subsequently poured into mother chrysanthemum water extract by what
The tuber of multiflower knotweed is completely soaked, vessel port seal, container is placed in 40 DEG C of environment, place 10 days, by the fleece-flower root after immersion together with
The ultrasonically treated 3min of soak, filters, then concentrate the filtrate to stoste 1/6th；The fleece-flower root after ultrasound is dried naturally
Pour into after mixing with concentrate afterwards in transparent airtight container, vexed moisten to container in no liquid residual；Supersonic frequency 30kHz；
(3) the selenium-rich for, taking 2 times of fleece-flower root raw medicinal herbs weight strengthens liquid, is concentrated into 1/7th of stoste, then by step (2)
Prepare the fleece-flower root thin slice that completes to pour in the ceramic vessel equipped with concentrate, vexed moisten to container in no liquid residual, by vexed profit
Fleece-flower root thin slice afterwards, water proof are heated to alcohol-free taste, take out, dry naturally, obtain final product selenium-rich fleece-flower root medicine materical crude slice.
It is that fresh pumpkin skin, konjaku skin, jerusalem artichoke petal, gynostemma pentaphyllum leaf are compared 4 according to weight that described selenium-rich strengthens liquid:7:
5:After 8 mixing, add 1 times of 25% ethanol solution of its gross weight that 45min is decocted, obtain final product selenium-rich and strengthen liquid.
Embodiment 3
A kind of processing method of selenium-rich fleece-flower root medicine materical crude slice, specifically includes following steps：
(1) fleece-flower root raw medicinal herbs, is taken, is cut into slices after epidermis is cleaned, slice thickness is 10mm, fine day is selected, is exposed to the sun 4 days, micro-
Ripple processes 12min, and microwave power is 400w, after the fleece-flower root thin slice after process is placed under infrared lamp irradiation 50min, after taking-up
Room temperature transfers use of purchasing；
(2), will step (2) the middle fleece-flower root that completes of processing loads in china container, be subsequently poured into mother chrysanthemum water extract by what
The tuber of multiflower knotweed is completely soaked, and vessel port is sealed, and container is placed in 40 DEG C of environment, places 8 days, by the fleece-flower root after immersion together with leaching
The ultrasonically treated 3-5min of bubble liquid, filters, then concentrate the filtrate to stoste 1/6th；The fleece-flower root after ultrasound is dried naturally
Pour into after mixing with concentrate afterwards in transparent airtight container, vexed moisten to container in no liquid residual；Supersonic frequency 100kHz；
(3) the selenium-rich for, taking 2 times of fleece-flower root raw medicinal herbs weight strengthens liquid, is concentrated into 1/7th of stoste, then by step (2)
Prepare the fleece-flower root thin slice that completes to pour in the ceramic vessel equipped with concentrate, vexed moisten to container in no liquid residual, by vexed profit
Fleece-flower root thin slice afterwards, water proof are heated to alcohol-free taste, take out, dry naturally, obtain final product selenium-rich fleece-flower root medicine materical crude slice.
It is that fresh pumpkin skin, konjaku skin, jerusalem artichoke petal, gynostemma pentaphyllum leaf are compared 3 according to weight that described selenium-rich strengthens liquid:5:
4:After 5 mixing, add 1 times of 25% ethanol solution of its gross weight that 45min is decocted, obtain final product selenium-rich and strengthen liquid.
Test example
A kind of compliance test result of the processing method of the selenium-rich fleece-flower root medicine materical crude slice of the present invention
Fleece-flower root raw medicinal herbs 900g is taken, is cut into slices after epidermis is cleaned, slice thickness is 10mm, then 9 treatment groups is arranged,
Every group of fleece-flower root flake weight to be processed is 100g, respectively 3 test group, and numbering is 1-3, and 6 control group # are 4-9,
Concrete operations are：
Test group 1：Fleece-flower root thin slice is processed according to 1 processing method of embodiment.
Test group 2：Fleece-flower root thin slice is processed according to 2 processing method of embodiment.
Test group 3：Fleece-flower root thin slice is processed according to 3 processing method of embodiment.
Control group 4：Only (1) fleece-flower root thin slice is processed according to 3 step of embodiment.
Control group 5：Only (2) fleece-flower root thin slice is processed according to 3 step of embodiment.
Control group 6：Only (3) fleece-flower root thin slice is processed according to 3 step of embodiment.
Control group 7：(1) (2) fleece-flower root thin slice is processed with step according to 3 step of embodiment successively.
Control group 8：(2) (3) fleece-flower root thin slice is processed with step according to 3 step of embodiment successively.
Control group 9：(1) (3) fleece-flower root thin slice is processed with step according to 3 step of embodiment successively.
Assay method：The fleece-flower root that above-mentioned control group is taken per group before 10g processing and after processing respectively with test group carries out selenium
Content, the measure of total anthraquinones content, Assay of Total Anthraquinone method adopt ultraviolet spectrophotometry, selenium element content assaying method
The technology that should be known for those skilled in the art using fluorescence spectrophotometry, said determination method；Measurement result such as 1 institute of table
Show.
Table 1
Substantially learnt by table 1, the fleece-flower root that is processed using test group 1-3 of processing method of the present invention, with other
The method that control group 4-9 is adopted is compared, and the processing method of the fleece-flower root of the present invention can substantially improve selenium element in the fleece-flower root
Content, and through the method for the present invention, fleece-flower root Poisoning composition general anthraquinone class content is decreased obviously.
Claims (1)
1. a kind of processing method of selenium-rich fleece-flower root medicine materical crude slice, it is characterised in that specifically include following steps：
(1) fleece-flower root raw medicinal herbs, is taken, is cut into slices after epidermis is cleaned, slice thickness is 10mm, fine day is selected, is exposed to the sun 2-4 days, microwave
10-15min is processed, microwave power is 300-500w, then the fleece-flower root thin slice of process is placed on irradiation 45- under infrared lamp
60min, after taking-up, room temperature transfers use of purchasing；
(2), process (1) middle for step in the fleece-flower root loading china container for completing, pour mother chrysanthemum water extract into the fleece-flower root is complete
Soak, vessel port is sealed, and container is placed in 40 DEG C of environment, place 5-10 days, by the fleece-flower root after immersion together with soak
Ultrasonically treated 3-5min, filters, then concentrate the filtrate to stoste 1/6th；By the fleece-flower root after ultrasound dry naturally after with
Concentrate mixing after pour in transparent airtight container, vexed moisten to container in no liquid residual；Supersonic frequency 30kHz-
100kHz；
(3) the selenium-rich for, taking 2 times of fleece-flower root raw medicinal herbs weight strengthens liquid, is concentrated into 1/7th of stoste, then (2) step is prepared
The fleece-flower root thin slice for completing is poured in the ceramic vessel equipped with concentrate, vexed moisten to container in no liquid residual, by vexed profit after
Fleece-flower root thin slice, water proof are heated to alcohol-free taste, take out, dry naturally, obtain final product selenium-rich fleece-flower root medicine materical crude slice；Described selenium-rich strengthens
Liquid is that fresh pumpkin skin, fresh Amorphophallus rivieri skin, fresh jerusalem artichoke petal, fresh gynostemma pentaphylla leaf are compared 1-4 according to weight:3-7:1-5:After 2-8 mixing,
The 25% ethanol solution extraction 45min of 1 times of its gross weight is added to obtain final product selenium-rich enhancing liquid.
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| CN201611114158.7A CN106474205A (en) | 2016-12-07 | 2016-12-07 | A kind of processing method of selenium-rich fleece-flower root medicine materical crude slice |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113768003A (en) * | 2021-08-06 | 2021-12-10 | 辽宁省农业科学院 | Low-temperature dehydration technology-based jerusalem artichoke scented tea preparation technology |
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| CN113768003A (en) * | 2021-08-06 | 2021-12-10 | 辽宁省农业科学院 | Low-temperature dehydration technology-based jerusalem artichoke scented tea preparation technology |
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Application publication date: 20170308 |