CN106466291A - A kind of still cleaning products containing fermented grain thing and preparation method thereof - Google Patents
A kind of still cleaning products containing fermented grain thing and preparation method thereof Download PDFInfo
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Abstract
A kind of still cleaning products containing fermented grain thing and preparation method thereof, the present invention relates to a kind of fermented grain product and its application in still cleaning products.The method, first to grain culture medium heat sterilization, is followed by, into microorganism, fermenting, and sterilizing must comprise the fermented grain product of thalline, ferment filtrate and solid particle.Using described fermented grain product in cleaning products, in this cleaning products, do not contain foaming surfactant, such cleaning products has and good must remove skin surface oils and fatss, the effect of smooth skin after tested.Fermented grain product is prepared cleaning products and is had nutrition skin, gently removes skin keratin, low irritant, the gentle feature of safety.
Description
Technical field
The present invention relates to a kind of still Cleasing compositions, the particularly still skin cleansing compositions containing fermented grain product, more particularly do not contain foaming surfactant.
Background technology
In the cleaning products commonly used at present, no alveolitoid cleaning products contain appropriate oil content typically in formula, sometimes also contain a small amount of surfactant, it is characterized by foam is less, relatively gentleer, compared with the foam type cleansing milk containing exhibiting high surface activating agent, there is low irritant, do not result in excessive cleaning, the feature of suitable dry skin and sensitive skin use.But a disadvantage is that less to skin clean dynamics, do not possess removal epidermis unnecessary cutin function simultaneously.
Frosted type cleaning products are widely used in household chemicals field.Its main composition of frosted type cleaning products is：Abrasive particle, surfactant and other additives.Abrasive particle therein can be largely classified into organic abrasive particle and inorganic abrasive particle.Wherein organic abrasive particle includes natural shell granule, pit granule, conch meal, Margarita powder.Inorganic abrasive particle has bamboo charcoal, Kaolin, salt particle, quartz sand, Calcium Carbonate etc..Its main feature is in addition to outside the decontamination of abluent in formula, can also remove unnecessary cutin, dust and bag speckle etc. by abrasive particle mechanical friction effect.But if abrasive particle composition is really up to the mark or improper use can cause skin friction to damage, the excessively thin acceleration skin exfoliation of horny layer（Particularly dryness and neutral skin consumer）.
Nowadays, advocate natural Never Ending Fashion to have swept the globe, beauty and skin care circle also can not make an exception, started the upsurge that people pursue to natural safe skin care item, some natural, safe skin care item Effect raw materials pour in the visual field.Mixed grain rice play very favorable effect to the health of human body, contain rich in protein, carbohydrate, fat, mineral and multivitamin in grain rice, and these nutritions are quite helpful to skin nursing.Corn especially by fermentable is used in skin nursing having holding moisture content of skin, strengthens skin elasticity, strengthen skin barrier, promote subcutaneous collagen albumen to produce and certain anti-oxidation efficacy.
KR20130019192A discloses Fructus Pruni salicinae, Punica granatum L., mandarin orange, rice pulverizing, adds lactic acid bacteria culture, and centrifugation obtains filtrate, and for Exfoliating Scrub, but the cleaning product of the method preparation has no well report for the removal of skin oil and fat.
KR20090115844A discloses Chinese herbal medicine（The particularly Radix Angelicae Dahuricae）, Semen Phaseoli, Testa oryzae add lactic acid bacteria fermentation, the filtrate of filtration, for detergent or soap succedaneum clean vagina, there is the growth preventing vaginal mucosa harmful bacteria, go the effect eliminating the unusual smell.But the cleaning product of the method preparation is to have no skin surface oil stain removing is reported.
JP2001271096A discloses Testa oryzae as the application of cleaning agent, and described bran powder passes through to add lactic acid bacteria, 58 DEG C of cultivation and fermentation 6 hours, adds citric acid 5%, is dried, acquisition of sieving.The document compares ferment rice bran powder with azymic Testa oryzae powder cleaning skin effect, and result display ferment rice bran more can improve skin hydration degree.But this powder abluent using front need to mix with liquid or egg liquid in advance size mixing after smear skin, using cumbersome, and the nutrient substance in short time mixed-powder can not cmpletely discharge, and causes nutrition can not fully be absorbed by the skin.
CN103211749A discloses the method preparing shampoo by fermentable glutinous rice flour, but it selects strain fermentation for up to 15 days, can have impact on the granular sensation that glutinous rice flour script carries after fermentation.Weaken the effect of its frosted cleaning.
Therefore there is still a need for finding a kind of method being suitably used for still cleaning products.
Glutathione is contained in Semen Maydiss（GSH）, it is a kind of tripeptides being combined to form by glutamic acid, cysteine, glycine, wherein cysteine can suppress the activity of tryrosinase in melanin generating process, hinder melanin to be formed, play skin whitening efficacy.GSH is a kind of Natural antioxidant, the free radical that neutralization radiation produces, and plays delaying senility function.It is rich in the vitamin such as VB1, VB2, VB5, VB6, VE, VC and carotene in Semen Maydiss, skin metabolism, plump subcutaneous tissue can be strengthened, make skin high resilience and gloss.
At present, it is mainly used in field of food using fermentable bread basket both at home and abroad.CN101164428A discloses the method that the Semen Maydis powder of fermentation, bean cake etc. prepare biological feedstuff, the food of the viscous corn flour of CN103404779A lactic acid bacteria fermentation, " the research of lactic acid bacteria fermented grain food acid medicated porridge fermentation technology; processing of farm products; 2010.2; 27 ~ 30 " disclose and be cut as raw material with Oryza glutinosa, Semen setariae, rotten rice, Semen Maydiss, using the excellent lactic acid bacteria fermentation of character, record sample amino acid content and total amount showed increased after fermentation such as Wang Zhiwei." the Hypolipidemic effects of lactic acid bacteria fermented such as Immaculata
cereal in rats”. Banjoko et al.Lipids in Health and
Disease, 2012.11,170 disclose bacillus acidophilus, bacillus bifiduss and lactobacillus helveticuss mixed fermentation Semen Maydis powder, well-grown in Semen Maydis powder, and after fermentation, Semen Maydis powder reaches acceptable taste.And find this mixed fermentation food play the role of suppress fat absorption[2]." the Lactic acid such as Vittorio
bacteria producing B-group vitamins:a great potential for functional cereals
Products ", Appl Microbiol Biotechnol, 2012,96:1383-1394 discloses the screening that can pass through microorganism and the different contents improving VB race in fermented cereal of fermentation condition, and exploitation is in fermented grain product micro-organisms vitamin.Wu little Yan etc. " Agricultural University of the Inner Mongol, master's knowledge paper, 2013 " report and use lactic acid bacteria fermentation Semen Coiciss, polysaccharide in fermentation liquid, content of peptides do not ferment and increase 4 ~ 8 times, and fermentation liquid has good oxidation resistance.Fu Liang etc. " development of fermented type rice milk, food and machinery, 2006,5：103 ~ 105. " with rice as raw material, access a certain amount of lactic acid bacteria after the pretreatment such as gelatinizing and fermented, obtain sense organ and the good fermented type rice milk of structural state.Gong Yuansheng etc. " development of Semen setariae fermented beverage, Journal of Zhengzhou Grain College, 1999,3：41 ~ 43. " the good Semen setariae fermented beverage of taste is obtained using koji and yeast two-step fermentation.As can be seen here, microorganism while nutrient substance, itself produces some metabolites in using corn, makes the macromole in corn be decomposed into the material of molecular weight it is easier to absorb.Also the nutrient substance being difficult in corn discharge is discharged simultaneously.In addition distinctive material such as lactic acid, polysaccharide, antibiotics, antioxidant and bioconversion product can be produced through fermentable makes product have more high bioactivity it is easy to body absorption etc. acts on.But, the application that fermented grain product is used in still cleaning products have not been reported.
Inventor finds, fermented grain product is applied in Cleasing compositions, in particularly still skin cleansing compositions, because fermented grain product contains much starch and dextrin, there is good adsorption removal effect to skin oil and fat, secondly, fermented grain product is applied in cleaning products, remain the granular sensation of corn and gentle frosted sense, the abrasive action during cooperation cleaning can gently remove skin surface aging cutin.In addition nutrient substance such as thalline, lactic acid, polypeptide, aminoacid, polysaccharide, vitamin etc. in fermented grain product also impart cleaning product nourish skin, prevent from cleaning the scaly dry skin excessively brought, the sense of discomfort such as tight.
Therefore, the present invention relates to fermented grain product is applied in still skin cleansing compositions, described compositionss surfactant, it remains corn nutrition and granular sensation in the composition, skin surface aging cutin can gently be removed, remove surface grease, skin nutrition, releive skin irritation, there is low irritant, safety temperature simultaneously.
Content of the invention
The present invention relates to application in still skin cleansing compositions for the fermented grain product.Described fermented grain product passes through grain culture medium heat sterilization, is followed by, into microorganism, fermenting, and sterilizing must comprise the fermented grain product of thalline, ferment filtrate and solid particle.The product that described fermented grain product is obtained after fermentable by cereal-granules, it has 0.02mm ~ 1mm, preferably 0.05mm ~ 0.4mm, the more preferably particle diameter of 0.15mm ~ 0.25mm.
Further, the present invention relates to the still skin cleansing compositions containing corn fermentation product, described Cleasing compositions are essentially free of surfactant.
The corn fermentation product of the present invention, it is prepared by following step：
1st, culture medium heat sterilization
2nd, access the fermented bacterium having activated
3rd, ferment
4th, adjust pH
5th, sterilize
Wherein, culture medium is that corn particle is prepared with pure water.In its culture medium, grain content is 3% ~ 30 weight %, and its sterilising temp is 50 DEG C ~ 120 DEG C, and the time is 10min ~ 30min.
Microbial inoculant amount is 0.1% ~ 20% volume.
Fermentation temperature is 25 DEG C ~ 45 DEG C
Adjusting pH scope is 4.0 ~ 7.0.
The further pH scope that adjusts is 5.0 ~ 6.0.
Sterilising temp is 65 DEG C ~ 120 DEG C.Sterilization time is controlled to 15min ~ 60min.
Further, nutrient substance can be added in culture medium.Described nutrient substance is selected from glucose, Lactose, sucrose and/or maltose, preferably glucose.
Described microorganism, selected from beer yeast（Saccharomyces cerevisiae）, Candida utilis（Candida utilis）In yeast, or bacillus acidophilus（Lactobacillus acidophilus）, Lactobacillus paracasei（Lactobacillus paracasei）, lactobacillus rhamnosuss (Lactobacillus
Rhamnosus), Lactobacillus brevis（Lactobacillus brevis）, Lactobacillus bulgaricus (Lactobacillus bulgaricus), Lactobacillus reuteri (Lactobacillus
Reuteri), Lactobacillus salivarius (Lactobacillus salivarius), streptococcus thermophiluss (Streptococcus thermophilus), Leuconostoc mesenteroides (Leuconostoc mesenteroides), lactococcus lactis（Lactococcus
lactis）Deng lactic acid bacteria, or the mixture of one or more microorganisms of root enzyme bacterium or aspergillosiss.
The still skin cleansing compositions being suitable for the present invention can be the arbitrary forms such as cleanser, cleaning curry, and it can be applicable to facial cleansing and clean body.
In one particular embodiment, described still Emulsion Cleasing compositions contain：
Oily matter, typically refers to the whole oil components allowing in hydrophobic combination or oil-phase component, or cosmetics to use.It can be at least one oils and fatss in conventionally used vegetable oil, mineral oil, silicone oil and artificial oil, or various wax.
The silicone oil quasi-grease being applied to the present invention is, for example, polydimethylsiloxane and ring first silica oily matter 1% ~ 20 weight %, preferred content 2% ~ 15 weight %, particularly 3% ~ 10 weight %
Fermented grain product 10% ~ 80 weight %, preferred content 20% ~ 70 weight %, particularly 30% ~ 50 weight %.
Emulsifying agent 1% ~ 10 weight %, preferred content 2% ~ 8 weight %, particularly 3% ~ 5 weight %,
Viscosity modifier 0.01% ~ 5 weight %, preferably 0.05% ~ 3 weight %, particularly 0.1% ~ 1 weight %,
Pure water 10% ~ 80 weight %, preferred content 15% ~ 60 weight %, particularly 20% ~ 40 weight %.
In one particular embodiment, described still curry agent Cleasing compositions contain：
Fermented grain product 10% ~ 80 weight %, preferably 20% ~ 70 weight %, particularly 30% ~ 50 weight %
Gel 0.01% ~ 5 weight %, preferably 0.05% ~ 3 weight %, particularly 0.1% ~ 1 weight %.
Pure water 10% ~ 80 weight %, preferably 15% ~ 60 weight %, particularly 20% ~ 40 weight %.
Oily matter
Siloxanes, and also aryl-, the polymethyl siloxane of alkyl-or alkoxyl-replacement and ring first siloxanes.
It is applied to unitary and the binary esters of the straight chain that the oils and fatss of the present invention also include having 2-44 carbon atom and/or side chain unitary and/or dicarboxylic acids and the saturation with 1-22 carbon atom or undersaturated straight chain and/or branched-chain alcoho.Similarly, as the oils and fatss for the present invention, it is possible to use the ester of difunctional aliphatic's alcohol with 2-36 carbon atom and monofunctional aliphatic's carboxylic acid with 1-22 carbon atom.
As the oils and fatss for the present invention, the esters of the fatty acid with 12-22 carbon atom can also specifically be preferably used, as methyl ester and isopropyl ester, such as methyl laurate, methyl stearate, methyl oleate, methyl erucate, isopropyl palmitate, isopropyl myristate, isopropyl stearate and/or acid isopropyl.
In addition, as the oils and fatss for the present invention, the also specifically preferably just own ester of n-butyl stearate, lauric acid, Oleic acid ester of the positive last of the ten Heavenly stems, Ethylhexyl stearate, Palmic acid different nonyl ester, isononyl isononanoate, Palmic acid 2- ethyl hexyl ester, lauric acid 2- ethyl hexyl ester, stearic acid 2- hexyl decyl ester, Palmic acid 2- octyldodecyl, oleic oil alkene ester, erucic acid oil alkene ester and/or Oleic acid mustard ester.
As the oils and fatss for the present invention, also be particularly suitable is dicarboxylic acids esters, for example Di-n-butyl Adipate, n-butyl sebacate, adipic acid two (2- ethylhexyl) ester, succinic acid two (2- hexyl decyl) ester and/or Azelaic Acid two isotridecyl ester.As the oils and fatss for the present invention, be also particularly suitable is diol-lipid, the sad DOPCP of such as two oleic acid glycol esters, two different tridecanoic acid glycol esters, two (2 ethyl hexanoic acid) propylene glycol ester, two isostearic acid butanediol esters and/or two.
As the oils and fatss for the present invention, carbonic diester class can also be used, such as carbonic acid two (2- ethylhexyl) ester.
Equally applicable is the triglyceride of long-chain relatively, i.e. triple esters of glycerol and three acid molecules, and in these acid molecules, at least one is the acid molecule of a relative long-chain.Here by way of example it is mentioned that fatty acid triglycercide class, this includes the triglyceride of the mixture of caprylic/capric, the triglyceride of the triglyceride of industrial oleic acid, the triglyceride of isostearic acid and Petiolus Trachycarpi/oleic acid mixture synthesizing.Additionally straight or branched aliphatic alcohols, such as oleyl alcohol or octyldodecanol can be used, and also fatty alcohol ethers, such as dicaprylyl ether etc..
As the oils and fatss for the present invention, equally applicable is crude vegetal, such as olive oil, Oleum Helianthi, soybean oil, Oleum Arachidis hypogaeae semen, rapeseed oil, almond oil, Petiolus Trachycarpi oil and/or Jojoba oil, and also Oleum Cocois or palm shell oil liquid part, and also animal oil, such as the liquid part of sperm oil, neat's foot oil or Adeps Bovis seu Bubali.
As the oils and fatss for the present invention, squalene extracting, particularly liquid paraffin and isoparaffin can also be used.The example of the squalene extracting that can use is paraffin oil, white mineral oil, 2-Methylpentadecane, poly decene, petroleum jelly, light liquid paraffin and/or squalane.In addition, the esters of aryl carboxylic acid are also suitable, as benzoic esters, for example there is the benzoate that the saturation of 1-22 carbon atom or undersaturated straight or branched alcohol are formed with benzoic acid, such as benzoic acid iso stearyl ester and benzoic acid 2- octyldodecyl, preferably benzoic acid C12-15 Arrcostab.
According to the present invention, oily matter, based on the total amount of compositionss, its content is 1% ~ 20 weight %, preferably 2% ~ 15 weight %, more preferably 3% ~ 5 weight %.
In a preferred embodiment of the still skin cleansing compositions of the present invention, oily matter can be the combination of one or more of white oil, lauric acid, myristic acid, stearic acid, iso-octyl palmitate.
Emulsifying agent
In the still skin cleansing compositions of the present invention, further comprises emulsifying agent, it is nonionic emulsifier.The oil-in-water nonionic emulsifier being applied to the present invention is selected from having the hydrophilic non-ionic surfactant as hydrophilic group for the polyoxyethylene chain, polyglyceryl fatty acid ester, polyglycereol fatty alcohol ether, sucrose fatty acid ester.
According to the present invention, based on the total amount of compositionss, the consumption of emulsifying agent is 1% ~ 10 weight %, preferably 2% ~ 8 weight % more preferably 3% ~ 5 weight %.
In a preferred embodiment of the invention, described have polyoxyethylene chain and be selected from the group as the hydrophilic non-ionic surfactant of hydrophilic group：Polyoxyethylene fatty acid ester, polyoxyethylene aliphatic alcohol ether, polyoxyethylene glycerol mono fatty acid ester, polyoxyethylene hydrogenated Oleum Ricini and polyoxyethylene hydrogenated Oleum Ricini mono fatty acid ester.
As polyoxyethylene fatty acid ester, preferably polyoxyethylene caprylic ester, polyoxyethylene 2-ethylhexanoate, polyoxyethylene decanoin, polyoxyethylene laurate, polyoxyethylene myristinate, polyoxyethylene palmitate, polyoxyethylene isostearate, Myrj 45, polyoxyethylene oleate, polyoxyethylene behenic acid ester etc..
As polyoxyethylene aliphatic alcohol ether, preferably polyoxyethylene octyl ether, polyoxyethylene decyl ethers, polyoxyethylene lauryl ether, polyoxyethylene myristyl ether, polyoxyethylene palmityl ether, polyoxyethylene iso stearyl ether, polyoxyethylene stearyl base ether, polyoxyethylene oleyl ether, polyoxyethylene mountain base ether etc..
As polyoxyethylene glycerol mono fatty acid ester, preferably polyoxyethylene glycerol list caprylate, polyoxyethylene glycerol monkey cell, polyoxyethylene glycerol monolaurate, polyoxyethylene glycerol list myristinate, polyoxyethylene glycerol monopalmitate, polyoxyethylene glycerol list isostearate, polyoxyethylene glycerol monostearate, TMGO 5, polyoxyethylene glycerol list behenic acid ester etc..
As polyoxyethylene hydrogenated Oleum Ricini, polyoxyethylene structure division preferably wherein averagely comprises 20-80, those polyoxyethylene hydrogenated Oleum Ricini of preferred 30-60 ethylene oxide repeating units.
As polyoxyethylene hydrogenated Oleum Ricini mono fatty acid ester, preferably polyoxyethylene hydrogenated Oleum Ricini list caprylate, polyoxyethylene hydrogenated Oleum Ricini monkey cell, polyoxyethylene hydrogenated Oleum Ricini monolaurate, polyoxyethylene hydrogenated Oleum Ricini list myristinate, polyoxyethylene hydrogenated Oleum Ricini monopalmitate, polyoxyethylene hydrogenated Oleum Ricini list isostearate, polyoxyethylene hydrogenated Oleum Ricini monostearate, polyoxyethylene hydrogenated Oleum Ricini monoleate, polyoxyethylene hydrogenated Oleum Ricini list behenic acid ester etc..
As polyglyceryl fatty acid ester, the preferably list-of polyglycereol and many caprylates, the list of polyglycereol-and many 2-ethylhexanoate, the list of polyglycereol-and many decanoins, the list of polyglycereol-and many laurates (as Natrulon H-10 five laurate), the list of polyglycereol-and many myristinates, the list of polyglycereol-and many cetylates, the list of polyglycereol-and many isostearates, the list of polyglycereol-and many stearates (as polyglycereol -3 distearate), the list of polyglycereol-and many oleates (as polyglycereol -2 dioleate), the list of polyglycereol-and many behenic acids ester etc..
As above-mentioned polyglycereol fatty alcohol ether, the fatty alcohol forming this polyglycereol fatty alcohol ether preferably wherein is saturated or unsaturated and has 8-22 carbon atom and polyglycerol moiety averagely comprises the polyglycereol fatty alcohol ether of 2-60 glycerol repetitives.As the example, it can be mentioned：Polyglycereol Octyl Ether, polyglycereol decyl ethers, polyglycereol lauryl ether, polyglycereol myristyl ether, polyglycereol palmityl ether, polyglycereol iso stearyl ether, polyglycereol stearyl ether, polyglycereol oleyl ether, polyglycereol mountain base ether etc..The fatty alcohol particularly preferably wherein forming this polyglycereol fatty alcohol ether is saturated or unsaturated and has 8-18 carbon atom and polyglycerol moiety averagely comprises the polyglycereol fatty alcohol ether of 3-15 glycerol repetitives, the fatty alcohol especially wherein forming this polyglycereol fatty alcohol ether is saturated or unsaturated and has 10-14 carbon atom and polyglycerol moiety averagely comprises the polyglycereol fatty alcohol ether of 3-5 glycerol repetitives, such as polyglycereol -4 lauryl ether.
As sucrose fatty acid ester, the list-of preferably sucrose and many caprylates, the list-of sucrose and many 2-ethylhexanoate, the list-of sucrose and many decanoins, the list-of sucrose and many laurates (as sucrose dilaurate), the list-of sucrose and many myristinates, the list-of sucrose and many cetylates (as sucrose six cetylate), the list-of sucrose and many isostearates, the list-of sucrose and many stearates, the list-of sucrose and many oleates, the list-of sucrose and many behenic acids ester etc..
Viscosity-controlling agent and gel can be contained, it is hydroaropic substance, described aqueous substance is selected from water-soluble polymer in the compositionss of the present invention.
As water-soluble polymer, can be natural polysaccharide class, such as xanthan gum, arabic gum, guar gum, chitin derivativ（For example quaternized hydroxypropyl chitin）, hyaluronic acid, HANSHENGJIAO etc..
As water-soluble polymer, can also be semi synthetic polymer, such as modified cellulose class, it includes hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, quaternized cellulose etc..
According to the present invention, based on total composition, the content of water-soluble polymer is 0.01% ~ 5 weight %, preferably 0.05% ~ 3 weight %, 0.1% ~ 1 weight %
Further, the compositionss of the present invention can contain polyhydric alcohol, and the polyhydric alcohol that can be used for the present invention is the polyhydric alcohol with 1 to 6 carbon atom, including propylene glycol, hexanediol, glycerol and propylene glycol.According to the present invention, based on total composition, the content of polyhydric alcohol is 0.1% ~ 15%, preferably 1% ~ 10%, more preferably 3% ~ 5%.
Annexing ingredient
The plot compositionss of the present invention can comprise annexing ingredient, and these annexing ingredients can be selected according to the characteristic of required final products by technical staff, and these annexing ingredients are suitable to make said composition more attractive or make it have additional use beneficial effect.
The independent consumption of annexing ingredient is usually 0.001% to 10 weight %, preferably 0.01-5 weight % by weight of the composition.
Various other annexing ingredients can be formulated in the compositionss of the present invention.These components but be not limited to the compositions such as wetting agent, whitening agent, antioxidant, thickening agent, conditioner, preservative, pH adjusting agent, coloring agent, spice, chelating agen.
Foaming surfactant
The present composition is substantially free of foaming surfactant, and described foaming surfactant is selected from anionic lathering surfactant agent, nonionic lather surfactants, both sexes foaming surfactant and their mixture.
Anionic lathering surfactant agent non-limitative example includes sarcosinate, sulfate, isethionate, taurate, phosphate, lactate, glutamate, Glu and their mixture.
Nonionic foaming surfactant includes alkyl androstanediol, alkyl polyglucoside, polyhydroxy fatty acid amide, alkoxy fatty acid ester, foaming sucrose ester, amine oxide and their mixture.
" both sexes foaming surfactant " includes zwitterionic surfactant, known to the skilled formulator that it is this area as one group of amphoteric surfactant.Can be using quite extensive both sexes foaming surfactant in the present composition.The non-limitative example of both sexes or zwitterionic surfactant is selected from glycine betaine, sulfobetaines, hydroxyl sulfo betaine, alkyhminoacetates, iminodiacetic alkanoate, aminoalkanoates and their mixture.
Brief description
Fig. 1 is using the still Cleansing Foam of product containing corn fermentation with Testa oryzae fermentation cleaning powder face cleaning skin transdermal dehydration comparison diagram.
Fig. 2 is using the still Cleansing Foam of product containing corn fermentation with Testa oryzae fermentation cleaning powder face cleaning skin hydration degree water comparison diagram.
Fig. 3 is using the still cleansing milk of product containing corn fermentation with glutinous rice flour abluent face cleaning of fermenting, the non-smooth points amount situation of change of skin.
Fig. 4 is using the still Cleansing Foam of product containing corn fermentation with the still Cleansing Foam face cleaning of non-fermented maize, skin hydration degree comparison diagram.
Fig. 5 is using the still Cleansing Foam of product containing corn fermentation with the still Cleansing Foam face cleaning of non-fermented maize, skin transdermal dehydration comparison diagram.
Fig. 6 uses different-grain diameter fermented maize still Cleansing Foam face cleaning, the non-smooth comparison diagram of counting out of skin.
Fig. 7 uses different-grain diameter fermented maize still Cleansing Foam face cleaning, removes oils and fatss comparison diagram.
Fig. 8 corn fermentation product Cleansing Foam is with commercially available several cleansing milk zest comparison diagrams.
Fig. 9 difference fermented grain product still Cleansing Foam face cleaning removes oils and fatss comparison diagram.
Oils and fatss comparison diagram removed by the still facial milk cleanser of Figure 10 different strain fermented maize product.
Specific embodiment
For being best understood from present disclosure, it is embodied as example in conjunction with some and further illustrates.
Preparation example 1：Prepared by corn fermentation product
100g Semen Maydiss are taken to be cut（Particle diameter is：0.15mm ~ 0.25mm, 60 mesh ~ 80 mesh）In 900ml drinking water, heat sterilization, sterilising conditions are 105 DEG C, 15min, and cooling room temperature is followed by into lactobacillus casei, and inoculum concentration is 5% volume.37 DEG C of fermentation 24h ~ 48h.Adjust PH to 5.5 ~ 6.0, inactivate thalline, sterilising conditions are 105 DEG C, 15min.
Preparation example 2：Prepared by corn fermentation product
Identical with preparation example 1 method, difference is that Semen Maydiss are cut（Particle diameter is：0.25mm ~ 0.5mm, 40 mesh ~ 60 mesh）.
Preparation example 3：Prepared by corn fermentation product
Identical with preparation example 1 method, difference is that Semen Maydiss are cut（Particle diameter is 0.1mm ~ 0.15mm：80 mesh ~ 120 mesh）.
Contrast preparation example 1：Prepared by corn fermentation product
Identical with preparation example 1 method, difference is that Semen Maydiss are cut（Particle diameter is：＜ 0.1mm, more than 120 mesh）.
Contrast preparation example 2：Prepared by corn fermentation product
Identical with preparation example 1 method, difference is that Semen Maydiss are cut（Particle diameter is：＞ 0.5mm, below 40 mesh）.
Contrast preparation example 3：Testa oryzae ferment particulate with reference to JP2001271096A
Contrast preparation example 4：Glutinous rice flour tunning with reference to CN103211749A
Contrast preparation example 5：Preparation method is to be added without microorganism with preparation example 1, difference
Preparation example 1-3 and comparative example 1-5 still skin cleansing compositions sensory effects are evaluated
Select 5 expert opinion group members, carry out sensory evaluation in such a way
Respectively using embodiment 1-3 and the still skin cleansing compositions of comparative example 1-5, then using effect makes scoring.Granular sensation is with feeling to make evaluation.Cleaning effect carries out skin oil and fat assay by MPA580 skinanalysis apparatus, comprehensive marking is carried out to compositionss according to use feeling, standard is non-stimulated when using, easy to apply when using, using rear moisten, using rear salubrious, smoothed using rear skin and respectively account for 1 point, have one not meet and deduct 1 point.
[1] the corn fermentation product of preparation example 1
[2] the corn fermentation product of preparation example 2
[3] the corn fermentation product of preparation example 3
[4] contrast the corn fermentation product of preparation example 1
[5] contrast the corn fermentation product of preparation example 2
[6] with reference to the Testa oryzae ferment particulate of JP2001271096A
[7] with reference to the glutinous rice flour tunning of CN103211749A
[8] frosted granule is Semen Juglandiss frosted microgranule, and particle diameter is 0.15mm ~ 0.25mm, 60 mesh ~ 80 mesh.
Conclusion：
Embodiment 1 and the still composition effect evaluation of comparative example 3
20 volunteers are divided into two groups, are divided into Semen Maydiss still face breast group and ferment rice bran powder group, volunteer is twice daily using the still cleansing milk of Semen Maydiss and ferment rice bran powder face cleaning, routine use identical placebo cream skin protection.After 48 weeks, MPA580 tests skin hydration degree and transdermal dehydration.
Result shows that Semen Maydiss still cleansing milk group skin hydration degree is higher than ferment rice bran group using after 48 weeks, and transdermal percentage of water loss is less than ferment rice bran group.Illustrate in the still cleansing milk of corn fermentation product that nutrition more can fill part to be absorbed by the skin have enhancing skin barrier function more by force simultaneously.
Embodiment 1 and the still composition effect evaluation of comparative example 4
20 volunteers are divided into two groups, are divided into Semen Maydiss still Cleansing Foam group and fermentation glutinous rice flour abluent group, and volunteer uses the still Cleansing Foam of Semen Maydiss and fermentation glutinous rice flour abluent face cleaning, and after 5min, VISIA full face analysis instrument measures the non-smooth points amount of skin surface.
The result display non-smooth reduction rate of Semen Maydiss still Cleansing Foam group skin surface is significantly higher than fermentation glutinous rice flour abluent.Gentle frosted granule effect in the still Cleansing Foam of corn fermentation product is described, can be compared with removing by force unnecessary dirt around the unnecessary cutin of skin surface and pore.
Embodiment 1-3 and the contrast of comparative example 1-2 still Cleansing Foam
30 volunteers are divided into 6 groups, respectively using 5 kinds of different-grain diameter Cleansing Foam face cleanings and blank Cleansing Foam.Blank group is the still facial milk cleanser without fermented grain product.Face cleaning dries the facial smoothness of test and facial oil situation of change after 5min naturally.
Result showed 60 mesh ~ 80 mesh sieve fermented maize granule Cleansing Foam group best results in smoothness and oil stain removing rate.Granule is excessive cannot to be disperseed very well during face cleaning and rub, and granule is too small to lose frosted granule sensation and effect.
Embodiment 1 and the contrast still composition effect evaluation of preparation example 5
20 volunteers are divided into two groups, are divided into Semen Maydiss still Cleansing Foam group and non-fermented maize still Cleansing Foam group, and volunteer is twice daily using the still Cleansing Foam of fermented maize and non-fermented maize still Cleansing Foam face cleaning, routine use identical placebo cream skin protection.After 48 weeks, MPA580 tests skin hydration degree and transdermal dehydration.
Result shows that fermented maize still Cleansing Foam group skin hydration degree is higher than non-fermented maize group using after 48 weeks, and transdermal percentage of water loss is less than non-fermented maize group.Illustrate that the fermented rear metabolism of Semen Maydiss goes out more nutritions being easy to skin absorption, strengthen skin moisture-keeping and skin barrier function.
Embodiment 4
The still Cleansing Foam of corn fermentation product compares with commercially available several cleansing milk zests
| Sample number into spectrum | Cleaning composition |
| Embodiment 1 | Corn fermentation product |
| Sample 1 | Sodium lauryl tri(oxyethyl) sulfate, cocamido propyl betaine |
| Sample 2 | Glyceryl monostearate, sodium cocoyl glutamate |
| Sample 3 | Sodium lauryl sulfate, alkyl polyglucoside |
Take commercially available cleansing milk to be measured and corn fermentation product facial milk cleanser, be made into the solution that active substance fraction is 10%, add a certain amount of zein（zein）, stir 2h at 25 DEG C, then filter.Filtrate records the mass fraction of nitrogen with micro-Kjeldahl（A）.The mass fraction of nitrogen in the surfactant solution be not added with zein can be recorded with same method（B).
Zein value=A-B, in zein value solution, institute's nitrogen content mg (or g)/L represents, zein value bigger explanation surfactant zest is bigger.
Result shows that commercially available several cleansing milk Zein value is far above still corn fermentation Cleansing Foam, illustrates that several cleansing milk zests containing Common surface activating agent are far above still corn fermentation product facial milk cleanser.
Embodiment 5 prepares the still facial milk cleanser of different fermented grain granules
Identical with preparation example 1 method, difference be corn be rice, Semen setariae, fructus zizaniae caduciflorae, Sorghum vulgare Pers., Semen Coiciss（Particle diameter is：0.25mm ~ 0.5mm, 40 mesh ~ 60 mesh）One of.Blank control group is the still facial milk cleanser without fermented grain product.Its cleaning effect is shown in accompanying drawing 9：Result shows that several fermented grain product facial milk cleanser are removed oils and fatss effect and are much better than the blank group without fermented grain product.
Embodiment 6 prepares the still facial milk cleanser of different microorganisms fermented grain granule
Identical with embodiment 1 method, difference is using different microorganisms：Microorganism is respectively adopted saccharomyces cerevisiae（Saccharomyces
cerevisiae）, Rhizopus javanicus（Rhizopus）, aspergillus oryzae（ Aspergillus
oryzae ）One kind fermented.（Particle diameter is：0.25mm ~ 0.5mm, 40 mesh ~ 60 mesh）.Blank control group is the still facial milk cleanser without fermented grain product.Its cleaning effect is shown in Figure 10：Result shows that the still facial milk cleanser cleaning effect of several microbial fermentation product preparations is much better than the still facial milk cleanser without fermented grain thing.
Claims (10)
1. a kind of cleaning products compositionss, it contains fermented grain product 10% ~ 80 weight %, described fermented grain product is selected from one or more of rice, Semen setariae, Semen Maydiss, fructus zizaniae caduciflorae, Sorghum vulgare Pers., Semen Coicis, by pulverizing, the product obtaining after fermentable, it has 0.02mm ~ 1mm, preferably 0.05mm ~ 0.4mm, the more preferably particle diameter of 0.15mm ~ 0.25mm, described Cleasing compositions are substantially free of foaming surfactant.
2. compositionss as claimed in claim 1, it is Emulsion, contains:Oily matter 1% ~ 20 weight %, fermented grain product 10% ~ 80 weight %, emulsifying agent 1% ~ 10 weight %, viscosity modifier 0.01% ~ 5 weight %, pure water 10% ~ 80 weight %.
3. compositionss as claimed in claim 1, it is curry, and it contains：Fermented grain product 10% ~ 80 weight %, gel 0.01% ~ 1 weight %, pure water 10% ~ 80 weight %.
4. compositionss as claimed in claim 1, wherein said fermented grain product passes through the method preparation comprising the steps：
（1）Culture medium heat sterilization, foster base is cereal-granules,
（2）Access the fermented bacterium having activated, inoculum concentration is 0.1% ~ 20% volume,
（3）Fermentation, temperature is 25 DEG C ~ 45 DEG C,
（4）Adjust pH, scope is 4.0 ~ 7.0,
（5）Sterilizing, sterilising temp is 65 DEG C ~ 120 DEG C, and sterilization time is 15min ~ 60min.
5. compositionss as claimed in claim 2, wherein said microorganism, selected from the mixing of one or more of yeast, lactobacilluss, lactic acid bacteria, root enzyme bacterium, aspergillosiss.
6. compositionss as claimed in claim 2, in culture medium, add nutrient substance, described nutrient substance is selected from glucose, Lactose, sucrose and/or maltose, preferably glucose further.
7. compositionss as claimed in claim 2, wherein oily matter is selected from：One or more of vegetable oil, mineral oil, silicone oil and artificial oil combine.
8. compositionss as claimed in claim 2, wherein said emulsifying agent is selected from：One or more of polyglyceryl fatty acid ester, polyglycereol fatty alcohol ether, sucrose fatty acid ester combine.
9. the compositionss as described in claim 2,3, wherein said viscosity-controlling agent and gel are selected from：One or more of Carbomer, carrageenan, xanthan gum, hydroxymethyl cellulose combine.
10. application in preparing skin cleansing compositions for the fermented grain product as claimed in claim 1, is substantially free of foaming surfactant in described Cleasing compositions.
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| CN107233293A (en) * | 2017-07-04 | 2017-10-10 | 合肥仙之峰农业科技有限公司 | A kind of skin cleansing compositions |
| CN107536775A (en) * | 2017-08-30 | 2018-01-05 | 常州苏达欧包装材料有限公司 | A kind of preparation method of facial mask liquid |
| CN108685780A (en) * | 2017-04-11 | 2018-10-23 | 王慧贞 | A kind of composition and preparation method thereof for washing shield product |
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| CN108685780A (en) * | 2017-04-11 | 2018-10-23 | 王慧贞 | A kind of composition and preparation method thereof for washing shield product |
| CN107233293A (en) * | 2017-07-04 | 2017-10-10 | 合肥仙之峰农业科技有限公司 | A kind of skin cleansing compositions |
| CN107536775A (en) * | 2017-08-30 | 2018-01-05 | 常州苏达欧包装材料有限公司 | A kind of preparation method of facial mask liquid |
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