CN106432925A - Color masterbatch formula and preparing process thereof - Google Patents
Color masterbatch formula and preparing process thereof Download PDFInfo
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- CN106432925A CN106432925A CN201610861877.9A CN201610861877A CN106432925A CN 106432925 A CN106432925 A CN 106432925A CN 201610861877 A CN201610861877 A CN 201610861877A CN 106432925 A CN106432925 A CN 106432925A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/16—Elastomeric ethene-propene or ethene-propene-diene copolymers, e.g. EPR and EPDM rubbers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/20—Compounding polymers with additives, e.g. colouring
- C08J3/22—Compounding polymers with additives, e.g. colouring using masterbatch techniques
- C08J3/226—Compounding polymers with additives, e.g. colouring using masterbatch techniques using a polymer as a carrier
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2323/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
- C08J2323/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
- C08J2323/16—Ethene-propene or ethene-propene-diene copolymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2423/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
- C08J2423/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
- C08J2423/04—Homopolymers or copolymers of ethene
- C08J2423/06—Polyethene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2310/00—Masterbatches
Abstract
The invention discloses a color masterbatch formula and a preparing process thereof. Color masterbatch is prepared from, by weight, 30-50 parts of ethylene propylene diene monomer rubber, 30-40 parts of halogen-free red toner, 3-6 parts of halogen-free PE wax, 4-8 parts of halogen-free dispersant, 15-25 parts of halogen-free orange toner, 3-6 parts of anti-yellowing agent, 5-15 parts of nanoscale ceramic powder, 3-8 parts of bamboo charcoal powder, 10-20 parts of nanoscale silica micro powder, 3-6 parts of negative ions, 4-8 parts of titanium dioxide and 1-2 parts of antiager RD. The color masterbatch is simple in preparing process, the preparing course is environmentally friendly and free of pollution, the prepared color masterbatch has the advantages of being resistant to abrasion and high temperature, not prone to deformation and suitable for manufacturing plastic products such as toys, electric appliances, shells and furniture.
Description
Technical field
The present invention relates to color masterbatch preparing technical field, specially a kind of color masterbatch formula and its manufacture craft.
Background technology
The full name of color masterbatch, Masterbatch, is also color kind, is a kind of novel high polymer material special coloring agent, also known as pigment system
Standby thing.Color masterbatch is used primarily on plastics.Color masterbatch is made up of pigment or dyestuff, carrier and three kinds of fundamentals of additive, is handle
The pigment of super quantity is uniformly attached to the aggregation being obtained among resin, can claim condensed pigment, so its tinting strength, tinting power is high
In pigment itself.Blended so that it may reach the pigmentary resin of design pigment concentration with a small amount of color masterbatch and non-pigmentary resin during processing
Or product.Existing color masterbatch complicated process of preparation, and be obtained color masterbatch low intensity, high temperature resistant, anti-wear performance is poor, ageing resistace
Difference is it is impossible to meet some different product needs.
Content of the invention
It is an object of the invention to provide a kind of color masterbatch formula and its manufacture craft, to solve to propose in above-mentioned background technology
Problem.
For achieving the above object, the present invention provides following technical scheme：A kind of color masterbatch formula, color masterbatch formula constituent is by weight
Number includes ethylene propylene diene rubber 30-50 part, Halogen redness toner 30-40 part, Halogen PE wax 3-6 part, Halogen dispersant 4-8
Part, Halogen orange toner 15-25 part, anti-yellowing agent 3-6 part, nanometer scale ceramicses powder 5-15 part, bamboo charcoal powder 3-8 part, nano silicone
Micro mist 10-20 part, anion part 3-6 part, titanium dioxide 4-8 part, anti-aging agent RD 1-2 part.
Preferably, described anti-yellowing agent adopts epoxy resin anti-yellowing agent.
Preferably, preferred composition proportion is：40 parts of ethylene propylene diene rubber, Halogen 35 parts of toner of redness, Halogen PE wax 4
Part, 6 parts of Halogen dispersant, 20 parts of the orange toner of Halogen, 5 parts of anti-yellowing agent, 10 parts of nanometer scale ceramicses powder, 5 parts of bamboo charcoal powder, receive
15 parts of meter level silicon powder, 4 parts of anion part, 6 parts of titanium dioxide, 2 parts of anti-aging agent RD.
Preferably, its preparation technology comprises the following steps：
A, by ethylene propylene diene rubber, Halogen redness toner, Halogen PE wax, Halogen dispersant, the orange toner of Halogen add kneading machine
Middle mixing, kneading machine rotating speed is 1000-1500 rev/min, 50 DEG C -60 DEG C of melting temperature, and mixing time is 30min-40min, obtains
To elastomeric compound A；
B, sequentially add in elastomeric compound A anti-yellowing agent, nanometer scale ceramicses powder, bamboo charcoal powder, nano silicone micro mist, anion part,
Titanium dioxide, anti-aging agent RD, pour stirring in mixer into, first carry out stirring at low speed, then carry out high-speed stirred after being sufficiently mixed,
Stirring at low speed speed is 300-600 rev/min, and mixing time is 5min；High-speed stirred speed is 3000-4000 rev/min, stirring speed
Rate is 10min, obtains epoxy glue B；
C, by epoxy glue B add double screw extruder in extruding pelletization, extrusion temperature be 180 DEG C -200 DEG C, that is, obtain color masterbatch
Grain.
Compared with prior art, the invention has the beneficial effects as follows：Manufacture craft of the present invention is simple, and manufacturing process environmental protection is no dirty
Dye, prepared color masterbatch has wear-resisting, high temperature resistant, on-deformable advantage, is suitable for making toy, electrical equipment, shell, furniture etc. and moulds
Glue product, the present invention is also added with nanometer scale ceramicses powder, bamboo charcoal powder, negative ion powder, its nonpoisonous and tasteless, stable chemical performance, and it is right
Human body is without any side effects, can prevent microorganism from growing in material.
Specific embodiment
Below the embodiment it is clear that described is clearly and completely described to the technical scheme in the embodiment of the present invention
It is only a part of embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of not making creative work, broadly falls into the model of present invention protection
Enclose.
The present invention provides a kind of technical scheme：A kind of color masterbatch formula, color masterbatch formula constituent includes ternary second by weight
Third rubber 30-50 part, Halogen redness toner 30-40 part, Halogen PE wax 3-6 part, Halogen dispersant 4-8 part, the orange toner of Halogen
15-25 part, anti-yellowing agent 3-6 part, nanometer scale ceramicses powder 5-15 part, bamboo charcoal powder 3-8 part, nano silicone micro mist 10-20 part, bear from
Sub- part 3-6 part, titanium dioxide 4-8 part, anti-aging agent RD 1-2 part.
Embodiment one：
Using composition proportion be：30 parts of ethylene propylene diene rubber, Halogen 30 parts of toner of redness, 3 parts of Halogen PE wax, Halogen dispersant
4 parts, 15 parts of the orange toner of Halogen, 3 parts of anti-yellowing agent, 5 parts of nanometer scale ceramicses powder, 3 parts of bamboo charcoal powder, 10 parts of nano silicone micro mist,
3 parts of anion part, 4 parts of titanium dioxide, 1 part of anti-aging agent RD.
In the present embodiment, anti-yellowing agent adopts epoxy resin anti-yellowing agent.
The preparation technology of the present embodiment comprises the following steps：
A, by ethylene propylene diene rubber, Halogen redness toner, Halogen PE wax, Halogen dispersant, the orange toner of Halogen add kneading machine
Middle mixing, kneading machine rotating speed is 1000 revs/min, 50 DEG C of melting temperature, and mixing time is 30min, obtains elastomeric compound A；
B, sequentially add in elastomeric compound A anti-yellowing agent, nanometer scale ceramicses powder, bamboo charcoal powder, nano silicone micro mist, anion part,
Titanium dioxide, anti-aging agent RD, pour stirring in mixer into, first carry out stirring at low speed, then carry out high-speed stirred after being sufficiently mixed,
Stirring at low speed speed is 300 revs/min, and mixing time is 5min；High-speed stirred speed is 3000 revs/min, and stir speed (S.S.) is
10min, obtains epoxy glue B；
C, by epoxy glue B add double screw extruder in extruding pelletization, extrusion temperature be 180 DEG C, that is, obtain color masterbatch particle.
In the present embodiment, in order to strengthen the fire resistance of color masterbatch, the present invention also added 7 parts of cumyl peroxide, carbon
Change 4 parts of calcium, 3 parts of bentonite, 5 parts of antimony oxide, add above composition, the crosslink density of sizing material can be improved, improve color masterbatch
Fire resistance.
Embodiment two：
Using composition proportion be：50 parts of ethylene propylene diene rubber, Halogen 40 parts of toner of redness, 6 parts of Halogen PE wax, Halogen dispersant
8 parts, 25 parts of the orange toner of Halogen, 6 parts of anti-yellowing agent, 15 parts of nanometer scale ceramicses powder, 8 parts of bamboo charcoal powder, nano silicone micro mist 20
Part, 6 parts of anion part, 8 parts of titanium dioxide, 2 parts of anti-aging agent RD.
In the present embodiment, anti-yellowing agent adopts epoxy resin anti-yellowing agent.
The preparation technology of the present embodiment comprises the following steps：
A, by ethylene propylene diene rubber, Halogen redness toner, Halogen PE wax, Halogen dispersant, the orange toner of Halogen add kneading machine
Middle mixing, kneading machine rotating speed is 1500 revs/min, 60 DEG C of melting temperature, and mixing time is 40min, obtains elastomeric compound A；
B, sequentially add in elastomeric compound A anti-yellowing agent, nanometer scale ceramicses powder, bamboo charcoal powder, nano silicone micro mist, anion part,
Titanium dioxide, anti-aging agent RD, pour stirring in mixer into, first carry out stirring at low speed, then carry out high-speed stirred after being sufficiently mixed,
Stirring at low speed speed is 600 revs/min, and mixing time is 5min；High-speed stirred speed is 4000 revs/min, and stir speed (S.S.) is
10min, obtains epoxy glue B；
C, by epoxy glue B add double screw extruder in extruding pelletization, extrusion temperature be 200 DEG C, that is, obtain color masterbatch particle.
In the present embodiment, in order to strengthen the fire resistance of color masterbatch, the present invention also added 8 parts of cumyl peroxide, carbon
Change 5 parts of calcium, 4 parts of bentonite, 6 parts of antimony oxide, add above composition, the crosslink density of sizing material can be improved, improve color masterbatch
Fire resistance.
Embodiment three：
Using composition proportion be：35 parts of ethylene propylene diene rubber, Halogen 32 parts of toner of redness, 4 parts of Halogen PE wax, Halogen dispersant
5 parts, 16 parts of the orange toner of Halogen, 4 parts of anti-yellowing agent, 8 parts of nanometer scale ceramicses powder, 4 parts of bamboo charcoal powder, 12 parts of nano silicone micro mist,
4 parts of anion part, 5 parts of titanium dioxide, 1 part of anti-aging agent RD.
In the present embodiment, anti-yellowing agent adopts epoxy resin anti-yellowing agent.
The preparation technology of the present embodiment comprises the following steps：
A, by ethylene propylene diene rubber, Halogen redness toner, Halogen PE wax, Halogen dispersant, the orange toner of Halogen add kneading machine
Middle mixing, kneading machine rotating speed is 1100 revs/min, 52 DEG C of melting temperature, and mixing time is 32min, obtains elastomeric compound A；
B, sequentially add in elastomeric compound A anti-yellowing agent, nanometer scale ceramicses powder, bamboo charcoal powder, nano silicone micro mist, anion part,
Titanium dioxide, anti-aging agent RD, pour stirring in mixer into, first carry out stirring at low speed, then carry out high-speed stirred after being sufficiently mixed,
Stirring at low speed speed is 400 revs/min, and mixing time is 5min；High-speed stirred speed is 3200 revs/min, and stir speed (S.S.) is
10min, obtains epoxy glue B；
C, by epoxy glue B add double screw extruder in extruding pelletization, extrusion temperature be 185 DEG C, that is, obtain color masterbatch particle.
In the present embodiment, in order to strengthen the fire resistance of color masterbatch, the present invention also added 9 parts of cumyl peroxide, carbon
Change 4 parts of calcium, 5 parts of bentonite, 5 parts of antimony oxide, add above composition, the crosslink density of sizing material can be improved, improve color masterbatch
Fire resistance.
Example IV：
Using composition proportion be：45 parts of ethylene propylene diene rubber, Halogen 38 parts of toner of redness, 5 parts of Halogen PE wax, Halogen dispersant
7 parts, 23 parts of the orange toner of Halogen, 5 parts of anti-yellowing agent, 13 parts of nanometer scale ceramicses powder, 7 parts of bamboo charcoal powder, nano silicone micro mist 18
Part, 5 parts of anion part, 7 parts of titanium dioxide, 1 part of anti-aging agent RD.
In the present embodiment, anti-yellowing agent adopts epoxy resin anti-yellowing agent.
The preparation technology of the present embodiment comprises the following steps：
A, by ethylene propylene diene rubber, Halogen redness toner, Halogen PE wax, Halogen dispersant, the orange toner of Halogen add kneading machine
Middle mixing, kneading machine rotating speed is 1400 revs/min, 58 DEG C of melting temperature, and mixing time is 38min, obtains elastomeric compound A；
B, sequentially add in elastomeric compound A anti-yellowing agent, nanometer scale ceramicses powder, bamboo charcoal powder, nano silicone micro mist, anion part,
Titanium dioxide, anti-aging agent RD, pour stirring in mixer into, first carry out stirring at low speed, then carry out high-speed stirred after being sufficiently mixed,
Stirring at low speed speed is 500 revs/min, and mixing time is 5min；High-speed stirred speed is 3800 revs/min, and stir speed (S.S.) is
10min, obtains epoxy glue B；
C, by epoxy glue B add double screw extruder in extruding pelletization, extrusion temperature be 195 DEG C, that is, obtain color masterbatch particle.
In the present embodiment, in order to strengthen the fire resistance of color masterbatch, the present invention also added 10 parts of cumyl peroxide, carbon
Change 5 parts of calcium, 6 parts of bentonite, 6 parts of antimony oxide, add above composition, the crosslink density of sizing material can be improved, improve color masterbatch
Fire resistance.
Embodiment five：
Using composition proportion be：40 parts of ethylene propylene diene rubber, Halogen 35 parts of toner of redness, 4 parts of Halogen PE wax, Halogen dispersant
6 parts, 20 parts of the orange toner of Halogen, 5 parts of anti-yellowing agent, 10 parts of nanometer scale ceramicses powder, 5 parts of bamboo charcoal powder, nano silicone micro mist 15
Part, 4 parts of anion part, 6 parts of titanium dioxide, 2 parts of anti-aging agent RD.
In the present embodiment, anti-yellowing agent adopts epoxy resin anti-yellowing agent.
The preparation technology of the present embodiment comprises the following steps：
A, by ethylene propylene diene rubber, Halogen redness toner, Halogen PE wax, Halogen dispersant, the orange toner of Halogen add kneading machine
Middle mixing, kneading machine rotating speed is 1250 revs/min, 55 DEG C of melting temperature, and mixing time is 35min, obtains elastomeric compound A；
B, sequentially add in elastomeric compound A anti-yellowing agent, nanometer scale ceramicses powder, bamboo charcoal powder, nano silicone micro mist, anion part,
Titanium dioxide, anti-aging agent RD, pour stirring in mixer into, first carry out stirring at low speed, then carry out high-speed stirred after being sufficiently mixed,
Stirring at low speed speed is 450 revs/min, and mixing time is 5min；High-speed stirred speed is 3500 revs/min, and stir speed (S.S.) is
10min, obtains epoxy glue B；
C, by epoxy glue B add double screw extruder in extruding pelletization, extrusion temperature be 190 DEG C, that is, obtain color masterbatch particle.
In the present embodiment, in order to strengthen the fire resistance of color masterbatch, the present invention also added 9 parts of cumyl peroxide, carbon
Change 5 parts of calcium, 6 parts of bentonite, 5 parts of antimony oxide, add above composition, the crosslink density of sizing material can be improved, improve color masterbatch
Fire resistance.
Experimental example：
The color masterbatch that common material is obtained is obtained color masterbatch with various embodiments of the present invention and carries out tensile strength and degradation, is counted
According to such as following table：
| Tensile strength（Mpa） | Aging coefficient | |
| Common material | 9.5 | 0.2 |
| Embodiment one | 16.1 | 0.7 |
| Embodiment two | 15.8 | 0.72 |
| Embodiment three | 15.9 | 0.68 |
| Example IV | 15.8 | 0.75 |
| Embodiment five | 16.5 | 0.82 |
From above table data, the color masterbatch that embodiment five is obtained can reach optimum efficiency.
Manufacture craft of the present invention is simple, and manufacturing process is environment friendly and pollution-free, prepared color masterbatch have wear-resisting, high temperature resistant, be difficult
The advantage of deformation, is suitable for making toy, electrical equipment, shell, the plasthetics such as furniture, the present invention be also added with nanometer scale ceramicses powder,
Bamboo charcoal powder, negative ion powder, its nonpoisonous and tasteless, stable chemical performance, it is without any side effects to human body, can prevent microorganism
Grow in material.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, permissible
Understand and can carry out multiple changes, modification, replacement to these embodiments without departing from the principles and spirit of the present invention
And modification, the scope of the present invention be defined by the appended.
Claims (4)
1. a kind of color masterbatch formula it is characterised in that：Color masterbatch formula constituent include by weight ethylene propylene diene rubber 30-50 part,
Halogen redness toner 30-40 part, Halogen PE wax 3-6 part, Halogen dispersant 4-8 part, Halogen orange toner 15-25 part, yellowing-resistant
Agent 3-6 part, nanometer scale ceramicses powder 5-15 part, bamboo charcoal powder 3-8 part, nano silicone micro mist 10-20 part, anion part 3-6 part, dioxy
Change titanium 4-8 part, anti-aging agent RD 1-2 part.
2. a kind of color masterbatch formula according to claim 1 it is characterised in that：Described anti-yellowing agent adopts epoxy resin anti-yellowing
Become agent.
3. a kind of color masterbatch formula according to claim 1 it is characterised in that：Preferably composition proportion is：Ethylene-propylene-diene monomer
40 parts of glue, Halogen 35 parts of toner of redness, 4 parts of Halogen PE wax, 6 parts of Halogen dispersant, 20 parts of the orange toner of Halogen, anti-yellowing agent 5
Part, 10 parts of nanometer scale ceramicses powder, 5 parts of bamboo charcoal powder, 15 parts of nano silicone micro mist, 4 parts of anion part, 6 parts of titanium dioxide, age resistor
2 parts of RD.
4. a kind of color masterbatch formula according to claim 1 it is characterised in that：Its preparation technology comprises the following steps：
A, by ethylene propylene diene rubber, Halogen redness toner, Halogen PE wax, Halogen dispersant, the orange toner of Halogen add kneading machine
Middle mixing, kneading machine rotating speed is 1000-1500 rev/min, 50 DEG C -60 DEG C of melting temperature, and mixing time is 30min-40min, obtains
To elastomeric compound A；
B, sequentially add in elastomeric compound A anti-yellowing agent, nanometer scale ceramicses powder, bamboo charcoal powder, nano silicone micro mist, anion part,
Titanium dioxide, anti-aging agent RD, pour stirring in mixer into, first carry out stirring at low speed, then carry out high-speed stirred after being sufficiently mixed,
Stirring at low speed speed is 300-600 rev/min, and mixing time is 5min；High-speed stirred speed is 3000-4000 rev/min, stirring speed
Rate is 10min, obtains epoxy glue B；
C, by epoxy glue B add double screw extruder in extruding pelletization, extrusion temperature be 180 DEG C -200 DEG C, that is, obtain color masterbatch
Grain.
Priority Applications (1)
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| CN201610861877.9A CN106432925A (en) | 2016-09-29 | 2016-09-29 | Color masterbatch formula and preparing process thereof |
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| CN201610861877.9A CN106432925A (en) | 2016-09-29 | 2016-09-29 | Color masterbatch formula and preparing process thereof |
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2016
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| JP2005023150A (en) * | 2003-06-30 | 2005-01-27 | Yokohama Rubber Co Ltd:The | Rubber composition |
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Application publication date: 20170222 |