CN106397029A - High-activity seaweed compound fertilizer and preparation method thereof - Google Patents

High-activity seaweed compound fertilizer and preparation method thereof Download PDF

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Publication number
CN106397029A
CN106397029A CN201610779278.2A CN201610779278A CN106397029A CN 106397029 A CN106397029 A CN 106397029A CN 201610779278 A CN201610779278 A CN 201610779278A CN 106397029 A CN106397029 A CN 106397029A
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China
Prior art keywords
sargassum
extract
compound fertilizer
urea
carbamide
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CN201610779278.2A
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Inventor
汤洁
王连启
裴建滨
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Shandong Leili Green Fertilizer Co Ltd
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Shandong Leili Green Fertilizer Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/20Mixtures of one or more fertilisers with additives not having a specially fertilising activity for preventing the fertilisers being reduced to powder; Anti-dusting additives
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners

Abstract

The present invention discloses a high-activity seaweed compound fertilizer and a preparation method thereof and belongs to the technical field of compound fertilizer production. According to the technical scheme of the invention, the high-activity seaweed compound fertilizer is prepared by the following raw materials: urea, monoammonium phosphate, calcium magnesium phosphate, potassium sulfate, borax, ferrous sulfate, zinc sulfate, seaweed extract and seaweed powder. Compared with the prior art, the production device technology for existing urea-melt spray granulation compound fertilizers is fully utilized, wherein the uniformly mixed mixture of urea and seaweed extract is heated and melted in a urea melting tank. In this way, the carboxyl group and the hydroxyl group of the seaweed extract, and the carbonyl group of the urea, are subjected to sufficient condensation reaction to form a ureide-based alginate urea condensation product alginate ureide of a molecular network structure. Based on the sufficient combination reaction of the seaweed extract and urea molecules, the effect of the seaweed extract is improved and the slow-release effect of alginic acid to urea is also enhanced. Since the molecular weight is increased, the leaching of urea is reduced. The fertilizer efficiency is prolonged and the utilization rate of the fertilizer is improved.

Description

A kind of high activity seaweed compound fertilizer and preparation method thereof
Technical field
The invention belongs to Chemical Mixed Fertilizer technical field is and in particular to a kind of high activity seaweed compound fertilizer and preparation method thereof.
Background technology
Complex fertilizer is the general designation of compound fertilizer and mixed fertilizer, is processed by chemical method and physical method.Produce Complex fertilizer can improve fertilizer efficiency with materialization fertilizer practice, reduces fertilizer application frequency, saves fertilising cost.China's crop variation, soil Earth also from overcoming so-called " the correction fertilising " of single nutrient deficiency to proceed to multiple nutritional components in the past, " apply by balance Fertile ".According to China's agricultural development present situation, repair improved soil, reduce the usage amount of fertilizer, improve utilization rate of fertilizer, reduce agriculture Industry environmental pollution, has had become as the development trend of modern agriculture.
Currently, the high activity marine alga fertilizer adding Sargassum extract making is increasingly paid close attention to both at home and abroad, is primarily due to In Sargassum extract in addition to containing organic nutrition and mineral nutrition composition, it is rich in the plant endogenous hormones of enhancing development again And active substance.The high activity alga fertilizer that interpolation Sargassum extract obtains can effectively facilitate plant growth;Alginic acid is in soil Heavy metal have a passivation, stop the absorption of crop heavy metal ion, also there is stronger water conservation, function of fertilizer retention, for Carbamide has certain slow release effect, can reduce the volatilization of nitrogen, increases the persistency of available nutrient;Increase Soil ventilation and gather Group's ability;Reduce the surface tension of water, increase the active area of crop leaf or root system, strengthen and absorb.In addition, after enzyme fermentation Sargassum powder in, the content of organic matter is more than 60%, easily decomposes after being manured into soil, can play improved soil physical behavior, The effect of complexation nutrient near root system of plant, and then promote plant growing, improve fruit quality, but at present containing Sargassum Fertilizer, has effective ingredient and is easy to run off, utilization rate of fertilizer is not high, the shortcomings of indifferent to soil improvement.
Content of the invention
For solving above-mentioned technical problem, the invention provides a kind of high activity seaweed compound fertilizer and preparation method thereof, by sea Fully it is condensed formation alginic acid urea condensate between the carbonyl that carboxyl, hydroxyl and the carbamide that algae extract contains contains, Form molecular network, there is prolongation fertilizer efficiency, improve utilization rate of fertilizer, nutrient comprehensively, stimulate plant growing and degeneration-resistant Property, improve soil physical property and other effects.
The complete technical scheme of the present invention includes:
A kind of high activity seaweed compound fertilizer, the component that this high activity seaweed compound fertilizer is comprised and its weight percent are such as Under:Carbamide 25%-42.5%, MAP 7.5%-22.5%, calcium magnesium phosphate 2%-10%, potassium sulfate 20%-41%, Borax 0.5%-3%kg, ferrous sulfate 0.1%-1%kg, zinc sulfate 0.1%-1kg, Sargassum extract 0.1%-5%, Sargassum powder 3%-15%;Described Sargassum extract content is in terms of butt.
Preferably, the component that described high activity seaweed compound fertilizer comprises and its percentage by weight are as follows:Carbamide 28.5%, MAP 19%, calcium magnesium phosphate 10%, potassium sulfate 30%, Borax 1.5%, ferrous sulfate 1%, zinc sulfate 1%, Sargassum is extracted Thing 1%, Sargassum powder 8%.
Preferably, in Sargassum extract, also include the liquid of 4 times of butt weight.
A kind of preparation method of high activity seaweed compound fertilizer it is characterised in that:Using urea smelting and spraying cylinder pelletize work Skill, its concrete production stage is as follows:
(1) first by technical recipe list requirement, carbamide and Sargassum extract are proportionally added in urea molten tank, With steam, carbamide and Sargassum extract mixture are heated to 130~140 DEG C under stirring condition to be melted and kept 1.5-2.5 Hour, make between the carbonyl that carboxyl, hydroxyl and carbamide that Sargassum extract comprises contains, to be fully condensed formation Sargassum aciduria Plain condensation substance, to form molecular network, improves the slow release effect to carbamide for the alginic acid, carbamide and Sargassum extract mixing are molten Melt liquid and pipelined is passed through to comminutor through metering by urine pump;
(2) after the preliminary premixing of amount calculating Borax, ferrous sulfate, zinc sulfate according to proportioning, with the phosphoric acid after metering One ammonium, calcium magnesium phosphate, potassium sulfate, Sargassum powder, together put into agitated kettle, are thoroughly mixed in agitated kettle;
(3) after above-mentioned material mix homogeneously, comminutor is conveyed into belt, comminutor front arranges two shower nozzles, wherein One sprays the carbamide calculating according to proportioning and Sargassum extract mixed melting liquid, another shower nozzle spraying steam, so that material is tentatively become Ball pelletize, prilling temperature controls at 40 DEG C -50 DEG C;
(4) material of preliminary balling-up sequentially enters the first drying roller and the second drying roller, the first Drying outlet material Temperature control system is at 60 DEG C -70 DEG C;Second drying roller outlet material temperature controls at 50 DEG C -60 DEG C;
(5) after the second drying roller discharging, material is sieved, the big grain sifting out is thrown again with granule after crushed Enter comminutor and carry out pelletize;
(6) compound fertilizer granules having sieved are carried out with the anti-cakings such as bag oil, face powder process, finally measure, pack.
Described Sargassum extract is prepared by following steps:
(1) light dry Sargassum and water are according to 1:After 6 mass ratio is soaked in water 2 hours, takes out and rub;
(2) prepare the ethanol water of 30% percentage by weight;
(3) the size-reduced Sargassum obtaining step (1), according to 1:30% ethanol that 10 ratio and step (2) obtain Solution forms mixture, extracts 3 hours at stirring and 55 DEG C;
(4) make the mixture that step (3) obtains be cooled to room temperature, be centrifuged 30 minutes under 3500r/min rotating speed, filter Sargassum to after extracting solution and extraction;
(5) extracting solution is evaporated under reduced pressure, reclaims ethanol, the solid obtaining after evaporation is containing plant growing promotion effect Sargassum extract.
Described Sargassum powder is prepared by following steps:
(1) pulverized having extracted the Sargassum that Sargassum extract obtains with equal pulp grinder;
(2) 2 kilograms of alginate lyase and 3 kilograms of cellulase are added in 995 kg of water;
(3) 1000 kilograms of the composite enzyme solution that step (2) obtains is added to be formed to 100 kilograms of the Sargassum that step (1) obtains Mixture;
(4) under agitation with 55 DEG C, it is little that the Sargassum in the mixture that step (3) is obtained declines solution 3 in compound enzyme effect When, add the Sargassum extract containing plant growing promotion effect obtaining, stir, be cooled to room temperature.
(5) 2 hours are stood, filter centrifugation carries out solid-liquid separation, gained liquid concentration extremely >=20% solid content after separating, Obtain for liquid seaweed extract;After separating, solid is dried to moisture≤30%, as Sargassum activity powder.
In addition to Sargassum extract and Sargassum powder, other raw materials are commercially available prod, wherein:
Described carbamide is graininess, specification 46.0-0-0;
Described MAP is white powder, specification 11-44-0;
Described calcium magnesium phosphate is white powder, and phosphorus pentoxide content is 18%, and calcium oxide content is 45%, and magnesium oxide contains Measure as 12%, silica content is 20%;
Described potassium sulfate is white powder, specification 0-0-50;
Described Borax is industrial sodium tetraborate decahydrate, pure boron >=10%;
Described ferrous sulfate is ferrous sulfate heptahydrate, iron content >=20%;
Described zinc sulfate is zinc sulphate heptahydrate, Zn content >=22%.
The present invention with respect to the advantage of prior art is:
High activity seaweed compound fertilizer provided by the present invention, belongs to compound fertilizer field, and it with wild or is manually supported Grow that Sargassum is treated to use its effective ingredient, carbamide reaction partial cross-linked with the common mixed melting of Sargassum extract forms urea melting After liquid, then with after metering together put into agitated kettle, the MAP being thoroughly mixed in agitated kettle, calcium magnesium phosphate, sulfur The common mixture pelletize of sour potassium, Sargassum powder, Borax, ferrous sulfate, zinc sulfate forms.Beneficial effect is specific as follows:
1 and urea reaction, strengthen Sargassum effect
Fully it is condensed formation Sargassum aciduria between the carbonyl that carboxyl, hydroxyl and the carbamide that Sargassum extract contains contains Plain condensation substance, forms molecular network, extends fertilizer efficiency, improves utilization rate of fertilizer, strengthens Sargassum effect.
2nd, nutrient is comprehensive
The present invention preparation high activity seaweed compound fertilizer in addition to containing plant growing necessary a great number of elements nitrogen, phosphorus, potassium, Also contain plant growing necessary moderate-element calcium, magnesium, sulfur, micronutrient boron, ferrum, zinc etc., plant growing can be effectively facilitated, carry The activity of high enzyme, strengthens vegetation growth of plant and reproductive growth ability, and then improves crop yield.
3rd, stimulate plant growing
The Sargassum extract adding in the present invention contains the natural plants endogenous hormones extracting from Sargassum, such as gibberellins, Heteroauxing, cytokinin etc., can effectively improve plant photosynthesis Product formation speed, delay nutrition organs old and feeble, make crop Robust plant, stimulates plant growth.
4th, strengthen crop anti-adversity
In the present invention add Sargassum extract contain abscisic acid, glycine betaine, salicylic acid isoreactivity composition, strengthen crop Opposing funguses, antibacterial, virus infection, the ability of opposing pest damage;Strengthen crop tolerance to salt, drought-enduring, resistance to frost etc. and resist non-life The ability of thing stress.
5th, improve soil physical property
The Sargassum powder added in the high activity seaweed compound fertilizer of present invention preparation, containing abundant organic matter, alginic acid, can Promote the formation of soil aggregate, coordinate the soil water, fertilizer, vaporous condition.
Specific embodiment
With reference to embodiment, the present invention is described in further detail, but embodiments of the present invention not limited to this.
Embodiment 1
Proportioning raw materials:Carbamide 285kg, MAP 190kg, calcium magnesium phosphate 100kg, potassium sulfate 300kg, Borax 15kg, Ferrous sulfate 10kg, zinc sulfate 10kg, Sargassum extract 10kg (liquid 50kg, i.e. butt 10kg), Sargassum powder 80kg.
Concrete production technology is as follows:
1st, carbamide and Sargassum extract are proportionally added in urea molten tank, under agitation with steam by carbamide It is heated to 130~140 DEG C with Sargassum extract mixture to be melted, and keep 130~140 DEG C of melting 1.5-2.5 hours;
2nd, after the preliminary premixing of amount calculating Borax, ferrous sulfate, zinc sulfate according to proportioning, with the phosphoric acid one after metering Ammonium, calcium magnesium phosphate, potassium sulfate, Sargassum powder, together put into agitated kettle, are thoroughly mixed in agitated kettle;
3rd, after above-mentioned solid material mix homogeneously, comminutor is conveyed into belt, comminutor front arranges two shower nozzles, One atomizer spray carbamide and Sargassum extract mixture fused solution, an atomizer water spray steam, so that material balling-up is made Grain, prilling temperature controls at 40 DEG C -50 DEG C;
4th, the material of preliminary balling-up sequentially enters the first drying roller and the second drying roller, the first Drying outlet material temperature Control at 60 DEG C -70 DEG C;Second drying roller, outlet material temperature controls at 50 DEG C -60 DEG C.
5th, after the second drying roller discharging, material is once sieved, the big grain sifting out puts into after crushed again Comminutor carries out pelletize;
6th, the semi-finished product sieving enter cooling cylinder cooling, carry out second screening to material, that sifts out is little after material cooling Granule again puts into comminutor and carries out pelletize.
7th, the compound fertilizer granules having sieved are carried out with the anti-cakings such as bag oil, face powder process, finally measure, pack.
The product specification obtaining is 15-10-15.
Embodiment 2
Proportioning raw materials:Carbamide 285kg, MAP 190kg, calcium magnesium phosphate 100kg, potassium sulfate 300kg, Borax 15kg, Ferrous sulfate 10kg, zinc sulfate 10kg, Sargassum extract 10kg (remarks:Liquid 50kg, i.e. butt 10kg), Sargassum powder 80kg.
Concrete production technology in addition to step 1,3, with embodiment 1:
Step 1 is:With steam, Urea is melted to 120~130 DEG C under agitation;
Step 3 is:After above-mentioned solid material mix homogeneously, comminutor is conveyed into belt, comminutor front arranges two Shower nozzle, a certain amount of urea melting liquid that an atomizer spray calculates according to proportioning;One atomizer sprays according to proportioning meter A certain amount of seaweed extracted liquor calculated, makes material balling-up pelletize, prilling temperature controls at 40 DEG C -50 DEG C;
The product specification obtaining is 15-10-15.
Embodiment 3
Proportioning raw materials:Carbamide 285kg, MAP 190kg, calcium magnesium phosphate 100kg, potassium sulfate 300kg, Borax 15kg, Ferrous sulfate 10kg, zinc sulfate 10kg, chalk powder 90kg.
Concrete production technology is as follows:
1st, after the preliminary premixing of amount that Borax, ferrous sulfate, zinc sulfate are calculated according to proportioning, with metering after carbamide, MAP, calcium magnesium phosphate, potassium sulfate, chalk powder, together put into agitated kettle, are thoroughly mixed in agitated kettle;
2nd, after above-mentioned solid material mix homogeneously, comminutor is conveyed into belt, comminutor front arranges an atomization spray Head spray into saturation with steam, make material balling-up pelletize, prilling temperature controls at 40 DEG C -50 DEG C;
3rd, the material of preliminary balling-up sequentially enters the first drying roller and the second drying roller, the first Drying outlet material temperature Control at 60 DEG C -70 DEG C;Second drying roller, outlet material temperature controls at 50 DEG C -60 DEG C.
4th, after the second drying roller discharging, material is once sieved, the big grain sifting out puts into after crushed again Comminutor carries out pelletize;
5th, the semi-finished product sieving enter cooling cylinder cooling, carry out second screening to material, that sifts out is little after material cooling Granule again puts into comminutor and carries out pelletize.
6th, the compound fertilizer granules having sieved are carried out with the anti-cakings such as bag oil, face powder process, finally measure, pack.
The product specification obtaining is 15-10-15.
The compliance test result of high activity seaweed compound fertilizer of the present invention
With Fructus Cucumidis sativi as trial crops, demonstrate the effect of fertilizer of high activity seaweed compound fertilizer of the present invention.
1st, EXPERIMENTAL DESIGN and mensure
Soil ingenious fertility content is:Organic 21.12g/kg, full nitrogen 1.06%, alkali-hydrolyzable nitrogen 98.7mg/kg, available phosphoruss (P2O5) 115mg/kg, available potassium (K2O)125mg/kg.
For studying species it is:Fructus Cucumidis sativi, excellent No. 17 of Tianjin.
This experiment sets 4 process altogether, often processes and is repeated 2 times, random district's groups arrangement, and experimental plot area is 66.7m2,10m × 6.7m rectangle.
Fructus Cucumidis sativi was sowed on April 20th, 2015, average row away from 80cm, spacing in the rows 18cm, 49000 plants/acre of planting density, 2015 The field planting of on May 10, in, 5 days~July 16 June in 2015 harvests.
All process doses are 80 kgs/acre, and every cell dose is 8kg, and base is applied, and dose and fertilization mode are shown in Table 1, the field management measure such as remaining weeding, laxative, irrigation is identical.
Table 1 Fructus Cucumidis sativi fertilizer treatment
2nd, test results and analysis
Fructus Cucumidis sativi list melon weight, Fructus Cucumidis sativi melon length, 3 aspects of cucumber yield are compared, wherein assay method is:
Fructus Cucumidis sativi list melon weight, the long assay method of Fructus Cucumidis sativi melon:Multidraw, avoids side row, using diagonal sampling method, chooses Representative sampling point 5, each sampling point takes 10 Fructus Cucumidiss sativi, measures respectively, calculates meansigma methodss.
Cucumber yield assay method:Test plot individually harvests, individually counts and produce, and is converted into a hectare yield.
The impact to Fructus Cucumidis sativi list melon weight, Fructus Cucumidis sativi melon length for the different disposal is shown in Table 2.
The Fructus Cucumidis sativi list melon weight of table 2 different disposal, melon are long
From the above understand, process 1, process 2, process 3 with process 4 compared with, Fructus Cucumidis sativi list melon again respectively increase by 9.8 grams, 6.4g and 2.4 gram, increment rate is respectively 10.3%, 6.4% and 2.4%;Fructus Cucumidis sativi melon length increase respectively 1.6cm, 1.1cm and 2.0cm, increment rate is respectively 6.17%, 4.25% and 1.16%.
The impact to cucumber yield for the different disposal is shown in Table 3.
The cucumber yield of table 3 different disposal
Process Yield (kg/ mu) Volume increase (kg/ mu) Rate of growth (%)
Process one 6357.36 539.66 10.3
Process two 6092.23 328.53 5.7
Process three 5896.26 132.56 2.3
Process four 5763.7
Understand from the above, process 1 (Sargassum extract and the co-melting molten complex fertilizer of carbamide), process 2 (containing alginic acid again Complex fertilizer material), process 3 (conventional complex fertilizers) compared with processing 3 (conventional fertilizer applications), cucumber yield increases respectively 539.66kg/ Mu, 328.53kg/ mu and 132.56kg/ mu, rate of growth is respectively 10.3%, 5.7% and 2.3%.
The above, be only presently preferred embodiments of the present invention, and not the present invention is done with any pro forma restriction, every according to Any simple modification above example made according to the technical spirit of the present invention, equivalent variations, each fall within the protection of the present invention Within the scope of.

Claims (7)

1. a kind of high activity seaweed compound fertilizer is it is characterised in that the component that comprised of this high activity seaweed compound fertilizer and its weight Percentage ratio is as follows:Carbamide 25%-42.5%, MAP 7.5%-22.5%, calcium magnesium phosphate 2%-10%, potassium sulfate 20%- 41%, Borax 0.5%-3%kg, ferrous sulfate 0.1%-1%kg, zinc sulfate 0.1%-1kg, Sargassum extract 0.1%-5%, Sargassum powder 3%-15%;Described Sargassum extract content is in terms of butt.
2. the high activity seaweed compound fertilizer described in claim 1 is it is characterised in that what described high activity seaweed compound fertilizer comprised Component and its percentage by weight are as follows:Carbamide 28.5%, MAP 19%, calcium magnesium phosphate 10%, potassium sulfate 30%, Borax 1.5%, ferrous sulfate 1%, zinc sulfate 1%, Sargassum extract 1%, Sargassum powder 8%, described Sargassum extract content is with dry Base meter.
3. the high activity seaweed compound fertilizer described in claim 2 is it is characterised in that in described Sargassum extract, also include 4 times The liquid of butt weight.
4. high activity seaweed compound fertilizer described in any one of claim 1-3 preparation method it is characterised in that:Using urea melting Whitewashing cylinder prilling, its concrete production stage is as follows:
(1) first by technical recipe list requirement, carbamide and Sargassum extract are proportionally added in urea molten tank, in stirring Under the conditions of with steam, carbamide and Sargassum extract mixture are heated to 130~140 DEG C and are melted and kept 1.5-2.5 little When, make between the carbonyl that carboxyl, hydroxyl and carbamide that Sargassum extract comprises contains, to be fully condensed formation alginic acid carbamide Condensation substance, to form molecular network, improves the slow release effect to carbamide for the alginic acid, carbamide and Sargassum extract mixed melting Liquid passes through pipelined to comminutor by urine pump through metering;
(2) after the preliminary premixing of amount that Borax, ferrous sulfate, zinc sulfate are calculated according to proportioning, with metering after MAP, Calcium magnesium phosphate, potassium sulfate, Sargassum powder, together put into agitated kettle, are thoroughly mixed in agitated kettle;
(3) after above-mentioned material mix homogeneously, comminutor is conveyed into belt, comminutor front arranges two shower nozzles, one of Spray the carbamide calculating according to proportioning and Sargassum extract mixed melting liquid, another shower nozzle spraying steam, so that the preliminary balling-up of material is made Grain, prilling temperature controls at 40 DEG C -50 DEG C;
(4) material of preliminary balling-up sequentially enters the first drying roller and the second drying roller, the first Drying outlet material temperature control System is at 60 DEG C -70 DEG C;Second drying roller outlet material temperature controls at 50 DEG C -60 DEG C;
(5) after the second drying roller discharging, material is sieved, the big grain sifting out puts into again with granule after crushed to be made Grain machine carries out pelletize;
(6) compound fertilizer granules having sieved are carried out with the anti-cakings such as bag oil, face powder process, finally measure, pack.
5. high activity seaweed compound fertilizer described in claim 4 preparation method it is characterised in that described Sargassum extract pass through with Lower step preparation:
(1) light dry Sargassum and water are according to 1:After 6 mass ratio is soaked in water 2 hours, takes out and rub;
(2) prepare the ethanol water of 30% percentage by weight;
(3) the size-reduced Sargassum obtaining step (1), according to 1:30% ethanol solution that 10 ratio and step (2) obtain Form mixture, extract 3 hours at stirring and 55 DEG C;
(4) make the mixture that step (3) obtains be cooled to room temperature, be centrifuged 30 minutes under 3500r/min rotating speed, be filtrated to get and carry Sargassum after taking liquid and extracting;
(5) extracting solution is evaporated under reduced pressure, reclaims ethanol, the solid obtaining after evaporation is the Sargassum containing plant growing promotion effect Extract.
6. the preparation method of high activity seaweed compound fertilizer described in claim 5 is it is characterised in that described Sargassum powder is by following step Rapid preparation:
(1) pulverized having extracted the Sargassum that Sargassum extract obtains with equal pulp grinder;
(2) alginate lyase 2 weight portion and cellulase 3 weight portion are added in 995 weight portion water;
(3) Sargassum powder 100 weight portion obtaining step (1), adds in the composite enzyme solution that 1000 weight portion steps (2) obtain Form mixture;
(4) under agitation with 55 DEG C, the Sargassum in the mixture that step (3) is obtained declines solution 3 hours in compound enzyme effect, plus Enter the Sargassum extract containing plant growing promotion effect of acquisition, stir, be cooled to room temperature;
(5) 2 hours are stood, filter centrifugation carries out solid-liquid separation, after separating, gained liquid concentration, to >=20% solid content, obtains For liquid seaweed extract;After separating, solid is dried to moisture≤30%, as Sargassum activity powder.
7. high activity seaweed compound fertilizer described in any one of claim 4-6 preparation method it is characterised in that
Described carbamide is graininess, specification 46.0-0-0;
Described MAP is white powder, specification 11-44-0;
Described calcium magnesium phosphate is white powder, and phosphorus pentoxide content is 18%, and calcium oxide content is 45%, and content of magnesia is 12%, silica content is 20%;
Described potassium sulfate is white powder, specification 0-0-50;
Described Borax is industrial sodium tetraborate decahydrate, pure boron >=10%;
Described ferrous sulfate is ferrous sulfate heptahydrate, iron content >=20%;
Described zinc sulfate is zinc sulphate heptahydrate, Zn content >=22%.
CN201610779278.2A 2016-08-31 2016-08-31 High-activity seaweed compound fertilizer and preparation method thereof Pending CN106397029A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108409496A (en) * 2018-05-04 2018-08-17 李小婷 A kind of composite fertilizer and preparation method thereof preparing improvement soil using dead leaf
CN108586129A (en) * 2018-05-04 2018-09-28 李小婷 A kind of biological compound fertilizer and preparation method thereof of improvement soil
CN109369251A (en) * 2018-11-09 2019-02-22 中国农业科学院农业资源与农业区划研究所 A kind of granular urea preparation method containing alginic acid synergistic carrier suitable for acid soil
CN111205130A (en) * 2020-01-13 2020-05-29 广州市阔途生物科技有限公司 Biomass compound fertilizer for increasing yield of amomum villosum

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101486619A (en) * 2009-03-02 2009-07-22 中国海洋大学生物工程开发有限公司 Process for preparing seaweed urea
CN102765999A (en) * 2012-07-25 2012-11-07 北京雷力农用化学有限公司 Algal polysaccharide modified urea and preparation method thereof
CN102775235A (en) * 2012-08-16 2012-11-14 北京雷力农用化学有限公司 Algin high-tower compound fertilizer and preparation method thereof
CN102898245A (en) * 2012-11-09 2013-01-30 中国农业科学院农业资源与农业区划研究所 Seaweed synergia compound fertilizer and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101486619A (en) * 2009-03-02 2009-07-22 中国海洋大学生物工程开发有限公司 Process for preparing seaweed urea
CN102765999A (en) * 2012-07-25 2012-11-07 北京雷力农用化学有限公司 Algal polysaccharide modified urea and preparation method thereof
CN102775235A (en) * 2012-08-16 2012-11-14 北京雷力农用化学有限公司 Algin high-tower compound fertilizer and preparation method thereof
CN102898245A (en) * 2012-11-09 2013-01-30 中国农业科学院农业资源与农业区划研究所 Seaweed synergia compound fertilizer and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108409496A (en) * 2018-05-04 2018-08-17 李小婷 A kind of composite fertilizer and preparation method thereof preparing improvement soil using dead leaf
CN108586129A (en) * 2018-05-04 2018-09-28 李小婷 A kind of biological compound fertilizer and preparation method thereof of improvement soil
CN109369251A (en) * 2018-11-09 2019-02-22 中国农业科学院农业资源与农业区划研究所 A kind of granular urea preparation method containing alginic acid synergistic carrier suitable for acid soil
CN111205130A (en) * 2020-01-13 2020-05-29 广州市阔途生物科技有限公司 Biomass compound fertilizer for increasing yield of amomum villosum

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Application publication date: 20170215