CN106390048A - Extraction method for Xiaochaihu decoction and radix bupleuri-dragon's bone-oyster decoction - Google Patents
Extraction method for Xiaochaihu decoction and radix bupleuri-dragon's bone-oyster decoction Download PDFInfo
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Abstract
The present invention relates to an extraction method for a Xiaochaihu decoction and a radix bupleuri-dragon's bone-oyster decoction. The extraction method comprises: (a) respectively carrying out steam distillation on cassia twig and ginger in the prescription for 1-3 h with a mixture comprising 85-90 wt% of ethanol and 10-15 wt% of water; (b) respectively extracting radix bupleuri, ginseng and licorice root in the prescription for 1-3 h with a mixture comprising 10-30 wt% of ethanol and 70-90 wt% of water; (c) extracting pinellia ternata in the prescription for 1-3 h with a mixture comprising 70-90 wt% of ethanol and 10-30 wt% of water; (d) boiling dragon's bone and oyster in the prescription for 3-6 h with water; (e) respectively extracting herbs excluded in the steps (a)-(d) for 1-3 h with water twice; and (f) merging the extracts in the steps (a)-(e).
Description
Technical field
The present disclosure generally relates to a kind of extracting process of prescription, particularly one kind add Os Draconis with regard to Herba Sidae Rhombifoliae soup and Radix Bupleuri
The extracting process of oyster soup.
Background technology
The history of the existing thousands of years of Chinese medicine development, in Chinese medicine, contained chemical composition is sufficiently complex, has both contained multiple
Effective ingredient, also contains invalid components it is also possible to comprise toxic component.Extract its effective ingredient and add further
With separation, purification, obtain the important content that effective monomer is in Chinese medicine research field.Chinese medicine extraction is exactly
Extract wherein effective ingredient using some technology to greatest extent so that the inherent quality of Chinese medicine preparation and clinical treatment
Effect improves, and so that the effect of Chinese medicine is played to greatest extent, the extraction of Chinese medicine is the important ring of production process
Section, its process, the selection of technological process and device configuration all will be directly connected to quality and the clinic of Chinese medicine
Effect.
According to《Typhoid fever acute disease is discussed》, the usage of general Herba Sidae Rhombifoliae soup is with 2.4 liters of water, boils and takes 1.2 liters, goes dregs,
Take 600 milliliters again, 200 milliliters of decoction being taken warmly.Taking medicine three times daily；The usage of general Cyclic nucleotide is with water eight
Rise (1600cc), boil and take four liters (800cc), interior Radix Et Rhizoma Rhei, cut such as chess piece, more boil one, two boilings, go dregs, temperature
Take one liter (200cc).
Content of the invention
It is an object of the invention to, the extracting process of a kind of Herba Sidae Rhombifoliae soup and Cyclic nucleotide is provided, with
Solve prior art and carry out its own shortcomings that Chinese medicine extraction has：Loss of effective components in Chinese medicine, especially its
In non-water-soluble composition；Non-active ingredients can not be to remove to greatest extent, and enrichment factor is not high enough；Extracting solution
In in addition to effective ingredient, often impurity is more, still has a small amount of water solublity paste property composition, is often unfavorable for refining；And
Excessively high-temperature operation can cause a large amount of decomposition of thermal sensitivity effective ingredient.
For solving the above problems, the present inventor surprisingly invents the extraction of a kind of Herba Sidae Rhombifoliae soup and Cyclic nucleotide
Take method, it comprises the steps of：(a) by the Ramulus Cinnamomi in prescription and Rhizoma Zingiberis Recenss, respectively with 85～90wt% ethanol and
The mixture steam distillation of 10～15wt% water 1～3 hour；B (), by the Radix Bupleuri in prescription, Radix Ginseng and Radix Glycyrrhizae, divides
Do not extracted 1～3 hour with the mixture of 10～30wt% ethanol and 70～90wt% water；(c) by the Rhizoma Pinelliae in prescription,
Extracted 1～3 hour with the mixture of 70～90wt% ethanol and 10～30wt% water；(d) by the Os Draconis in prescription and
Concha Ostreae, with decocting in water 3～6 hours；(e) by the medical material beyond above-mentioned steps (a)～(d), respectively with water extraction 1～
3 hours, it is repeated twice；F above-mentioned steps (a)～(e) extract is merged by ().
In a preferred embodiment, wherein the prescription system Radix Bupleuri of this Herba Sidae Rhombifoliae soup, Radix Scutellariae, Radix Ginseng, Radix Glycyrrhizae, half
Summer, Rhizoma Zingiberis Recenss, Fructus Jujubae.
In another preferred embodiment, wherein the prescription system Radix Bupleuri of this Cyclic nucleotide, Radix Scutellariae, Radix Ginseng,
The Rhizoma Pinelliae, Ramulus Cinnamomi, Rhizoma Zingiberis Recenss, Os Draconis, Concha Ostreae, Poria, Fructus Jujubae.
In another preferred embodiment, wherein this step (a) is with the mixture steam of 90wt% ethanol and 10wt% water
Distillation 1 hour.
In another preferred embodiment, wherein this step (b) extracts 1 with the mixture of 30wt% ethanol and 70wt% water
Hour.
In another preferred embodiment, wherein this step (c) extracts 1 with the mixture of 70wt% ethanol and 30wt% water
Hour.
In another preferred embodiment, wherein this step (d) was with decocting in water 3 hours.
In another preferred embodiment, it filters after being contained in each (a)～(d) step further.
In another preferred embodiment, it comprises step (f) further by mixture pelleting.
Inventor finds, using the extracting process institute of above-mentioned Herba Sidae Rhombifoliae soup and Cyclic nucleotide prescription
The extract obtaining, has the effective ingredient of high level.
Specific embodiment
The terms " one " or " a kind of " when being used in conjunction in claim or description with "comprising",
May represent has one, but also complies with " one or more " or " at least one ".
The present invention provides the extracting process of a kind of Herba Sidae Rhombifoliae soup and Cyclic nucleotide, and it comprises following step
Suddenly：(a) by the Ramulus Cinnamomi in prescription and Rhizoma Zingiberis Recenss, respectively with the mixture of 85～90wt% ethanol and 10～15wt% water
Steam distillation 1～3 hour；(b) by the Radix Bupleuri in prescription, Radix Ginseng and Radix Glycyrrhizae, respectively with 10～30wt% ethanol and
The mixture of 70～90wt% water extracts 1～3 hour；(c) by the Rhizoma Pinelliae in prescription, with 70～90wt% ethanol
And the mixture of 10～30wt% water extracts 1～3 hour；(d) by the Os Draconis in prescription and Concha Ostreae, with decocting in water 3～6
Hour；E () by the medical material beyond above-mentioned steps (a)～(d), respectively with water extraction 1～3 hour, is repeated twice；
F above-mentioned steps (a)～(e) extract is merged by ().
From the foregoing, the method for the present invention can be applicable to Herba Sidae Rhombifoliae soup and Cyclic nucleotide prescription, side
Whether the enforcement of each step in method, depending on the medical material having in each prescription.
For example, it is an aspect of the invention to providing a kind of extracting process of Herba Sidae Rhombifoliae soup prescription, wherein this prescription
Including but not limited to Radix Bupleuri, Radix Scutellariae, Radix Ginseng, Radix Glycyrrhizae, the Rhizoma Pinelliae, Rhizoma Zingiberis Recenss, Fructus Jujubae.
Additionally, when extracting Herba Sidae Rhombifoliae soup prescription, above-mentioned steps (e) more can be separately added into down according to following symptom
Row prescription, if restlessness in the chest and do not vomit, remove the Rhizoma Pinelliae, Radix Ginseng, plus real 1 piece of Chinese juniper beach wormwood；If thirsty, remove the Rhizoma Pinelliae, Radix Ginseng
Add to 9 grams, 12 grams of RADIX TRICHOSANTHIS；If abdominal pain person, remove Radix Scutellariae, plus 9 grams of Radix Paeoniae；If fullness and rigidity in the hypochondrium, remove Fructus Jujubae,
Plus 12 grams of Concha Ostreae；If palpitation, dysuria person, remove Radix Scutellariae, plus 12 grams of Poria；If not thirsty, slight exterior fever
Person, removes Radix Ginseng, plus 6 grams of Ramulus Cinnamomi, and warm mild perspiration induced by covering the patient is healed；If the person of coughing, remove Radix Ginseng, Fructus Jujubae, Rhizoma Zingiberis Recenss, plus the five tastes
Sub 5 grams, 5 grams of Rhizoma Zingiberiss.
It is another aspect of the invention to provide a kind of extracting process of Cyclic nucleotide prescription, wherein should
Prescription including but not limited to Radix Bupleuri, Radix Scutellariae, Radix Ginseng, the Rhizoma Pinelliae, Ramulus Cinnamomi, Rhizoma Zingiberis Recenss, Os Draconis, Concha Ostreae, Poria,
Fructus Jujubae.
Additionally, when extracting Cyclic nucleotide prescription, above-mentioned steps (e) more can be divided according to following symptom
Not adding following prescription, if defecating no secret person, Radix Et Rhizoma Rhei can be removed；Shock palpitation not sleep, slight Hypertension person：Plus Ramulus Uncariae Cum Uncis,
The Cortex Eucommiae；Uncomfortable in chest, ambition is not smooth：Perfuming is attached, Radix Curcumae, Bulbus Allii Macrostemonis；Epilepsy：Plus Rhizoma Acori Graminei, Radix Curcumae, Radix Polygalae；
Demented：Plus Scorpio, Rhizoma Gastrodiae；Dizzy：Plus Ramulus Uncariae Cum Uncis, Folium Mori；Insomnia：Adduction drink skin, Caulis Polygoni Multiflori；Scrofula：
Plus Bombyx Batryticatus, Thallus Laminariae (Thallus Eckloniae), Sargassum, Spica Prunellae.
In above-mentioned extracting process, filter after preferably being further contained in each (a)～(d) step.
In above-mentioned extracting process, preferably can further comprise step (f) by mixture pelleting.
Above-mentioned term " extraction " is to extract wherein effective ingredient to greatest extent so that Chinese medicine using some technology
The inherent quality of preparation and clinical therapeutic efficacy improve, and so that the effect of Chinese medicine is played to greatest extent.Chinese medicine
Extraction be Chinese Traditional Medicine important unit operation, its process, the selection of technological process and equipment are joined
Put and all will be directly connected to quality and the clinical effectiveness of Chinese medicine.
In the present invention, Chinese medicine containing volatile oil, such as Radix Angelicae Sinensis, Ramulus Cinnamomi, Rhizoma Zingiberis Recenss, Rhizoma Chuanxiong, Cortex Cinnamomi, Roast Rhizoma Zingiberis Recens
Deng, wherein this volatile oil also known as quintessence oil, it is one to there are volatility, the oily liquids that can go out with vapor distillation,
There is fragrance, and this volatile oil is the polytype such as aliphatic compound, aromatic compound note class compound
The mixture of compound, inventors be surprised to learn that this volatile oil Chinese medicine preferably system is extracted to have volatile solution
Take, more preferably but the mixture that is not limited to mix with the ratio of 90wt% ethanol and 10wt% water with ethanol and water
Steam extraction.
In the present invention, containing tcm with glycosides, such as Radix Et Rhizoma Rhei, Cortex Moutan, Radix Glycyrrhizae, Semen Armeniacae Amarum, Radix Ginseng, Radix Astragali, bavin
Recklessly, SHANGZI, Semen Persicae, Radix Paeoniae, the Radix Paeoniae Alba, Radix Paeoniae Rubra, Radix Platycodoniss, Radix Clematidis etc., mostly have colourless, odorless,
Tool bitterness, minority is coloured, minority has the feature of sweet taste, and most in neutral or acid, minority is in alkalescence, big
Most of soluble in water and ethanol, easily generated sugar and aglycon by diluted acid or enzyme hydrolysiss, typically has certain optics and lives
Property, inventors be surprised to learn that the above-mentioned preferably system containing tcm with glycosides is extracted with the mixture of ethanol and water, its ratio is relatively
Good system is with the water of the ethanol mixing 70wt% of 30wt%.
In the present invention, Chinese medicine containing alkaloidss, such as Radix Aconiti Lateralis Preparata, Rhizoma Coptidis, Cortex Phellodendri, Herba Ephedrae, the Rhizoma Pinelliae etc., mostly
Number alkaloids are crystal material, colourless and have optical activity, inventors be surprised to learn that above-mentioned containing in alkaloidss
Medicine preferably system is extracted with the mixture of ethanol and water, and its ratio is preferably with the water of the ethanol of 70wt% and 30wt%.
In the present invention, Olibanum, Myrrha, Sanguis Draxonis etc., preferably system are extracted 30 minutes with ethanol.
In the present invention, the Chinese medicine such as Os Draconis, Concha Ostreae, preferable system extracts by the way of boiling, the time preferably 3～6
Hour, most preferably 3 hours.
In the present invention, Colla cornus cervi, Colla Corii Asini, Testudiniss angle glue, Borneolum Syntheticum etc., preferably system, without extraction, direct plunge into height
In warm solution, the mixture of the extract of prescription that this pyrosol can extract for other.
In the present invention, Herba Menthae, Herba Asari etc., preferably system, with water extraction 5～15 minutes, are more preferably with water extraction 10
Minute.
Medical material in addition to above-mentioned enumerating in the present invention, preferably system, with water extraction 1 hour, merge after being repeated twice.
If Chinese medicine washes with water before extracting, these powder or particle can be made washed away, adjuvant and effective ingredient
Can be dissolved in water and be washed off so as to curative effect reduces, therefore before Chinese medicine extraction, handy water does not rinse, can only be with cold
Water soaks.The prepared slices of Chinese crude drugs after cold water soak, organizational structure can loose expansion, make effective ingredient easily fried,
Make effective ingredient easily fried.If using hot-water soak at the very start, in medical material, contained protein component will be very
Fast dissolution and freezing film, are wrapped in medical material surface, make moisture be not easy to penetrate in medical material histiocyte,
Effective ingredient also is difficult to decompose out, affects the fried of composition.
Traditional Chinese medicine extraction method includes decocting cooking method, infusion process, percolation, Gelatin improving method, circumfluence method, solvent
Extraction method, steam distillation and sublimed method etc..Solvent extraction method is most widely used method, and it is basis
The property of various effective ingredient dissolubility in Chinese herbal medicine, from molten to other compositions greatly to needing ingredient solubility
The little solvent of Xie Du, a kind of extracting method that required active component is dissolved out in medical material tissue.
Embodiment
Embodiment 1- utilizes the method for the present invention to extract Herba Sidae Rhombifoliae soup
By taking 8 grams of Radix Bupleuri, 3 grams of Radix Scutellariae, 3 grams of Radix Ginseng, 3 grams of Radix Glycyrrhizae, 5 grams of the Rhizoma Pinelliae, Rhizoma Zingiberis Recenss 3 in prescription respectively
Gram, 2 grams of Fructus Jujubae, and according to the method for the present invention extraction, after extraction with weighing method measurement extracted have
Effect composition is 5 grams.
Comparative example 1- utilizes prior art method to extract Herba Sidae Rhombifoliae soup
By taking 8 grams of Radix Bupleuri, 3 grams of Radix Scutellariae, 3 grams of Radix Ginseng, 3 grams of Radix Glycyrrhizae, 5 grams of the Rhizoma Pinelliae, Rhizoma Zingiberis Recenss 3 in prescription respectively
Gram, 2 grams of Fructus Jujubae according to known decocting method extraction, will all medical materials in water extraction 2 hours, after extraction with
The extracted effective ingredient of weighing method measurement is 3 grams.
Embodiment 2- utilizes the method for the present invention to extract Cyclic nucleotide
By taking 5 grams of Radix Bupleuri, 2 grams of Radix Scutellariae, 2 grams of Radix Ginseng, 3 grams of the Rhizoma Pinelliae, 2 grams of Ramulus Cinnamomi, Rhizoma Zingiberis Recenss 2 in prescription respectively
Gram, 2 grams of Os Draconis, 2 grams of Concha Ostreae, 2 grams of Poria, 2 grams of Fructus Jujubae, and according to the method for the present invention extraction, after extraction
With the extracted effective ingredient of weighing method measurement for 4.5 grams.
Comparative example 2- utilizes prior art method to extract Cyclic nucleotide
By taking by taking 5 grams of Radix Bupleuri, 2 grams of Radix Scutellariae, 2 grams of Radix Ginseng, 3 grams of the Rhizoma Pinelliae, osmanthus in prescription respectively in prescription respectively
2 grams of branch, 2 grams of Rhizoma Zingiberis Recenss, 2 grams of Os Draconis, 2 grams of Concha Ostreae, 2 grams of Poria, 2 grams of Fructus Jujubae, and according to known decocting method
Extraction, will all medical materials in water extraction 2 hours, the effective one-tenth being extracted with the measurement of weighing method after extraction
It is divided into 3 grams.
Claims (9)
1. the extracting process of a kind of Herba Sidae Rhombifoliae soup and Cyclic nucleotide, it comprises the steps of：
A (), by the Ramulus Cinnamomi in prescription and Rhizoma Zingiberis Recenss, is steamed with the mixture of 85～90wt% ethanol and 10～15wt% water respectively
Steam distillation 1～3 hour；
B () is by the Radix Bupleuri in prescription, Radix Ginseng and Radix Glycyrrhizae, mixed with 10～30wt% ethanol and 70～90wt% water respectively
Compound extracts 1～3 hour；
C (), by the Rhizoma Pinelliae in prescription, extracts 1～3 with the mixture of 70～90wt% ethanol and 10～30wt% water little
When；
(d) by the Os Draconis in prescription and Concha Ostreae, with decocting in water 3～6 hours；
E () by the medical material beyond above-mentioned steps (a)～(d), respectively with water extraction 1～3 hour, is repeated twice；
F above-mentioned steps (a)～(e) extract is merged by ().
2. extracting process as claimed in claim 1 it is characterised in that this Herba Sidae Rhombifoliae soup prescription be Radix Bupleuri, Radix Scutellariae,
Radix Ginseng, Radix Glycyrrhizae, the Rhizoma Pinelliae, Rhizoma Zingiberis Recenss and Fructus Jujubae.
3. extracting process as claimed in claim 1 it is characterised in that this Cyclic nucleotide prescription be Radix Bupleuri,
Radix Scutellariae, Radix Ginseng, the Rhizoma Pinelliae, Ramulus Cinnamomi, Rhizoma Zingiberis Recenss, Os Draconis, Concha Ostreae, Poria and Fructus Jujubae.
4. extracting process as claimed in claim 1 is it is characterised in that this step (a) is with 90wt% ethanol and 10wt% water
Mixture steam distillation 1 hour.
5. extracting process as claimed in claim 1 is it is characterised in that this step (b) is with 30wt% ethanol and 70wt% water
Mixture extract 1 hour.
6. extracting process as claimed in claim 1 is it is characterised in that this step (c) is with 70wt% ethanol and 30wt% water
Mixture extract 1 hour.
7. extracting process as claimed in claim 1 is it is characterised in that this step (d) was with decocting in water 3 hours.
8. extracting process as claimed in claim 1 is it is characterised in that be contained in mistake after each (a)～(d) step further
Filter.
9. extracting process as claimed in claim 1 is it is characterised in that comprise step (f) further by mixture pelleting.
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Cited By (5)
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| CN108042756A (en) * | 2017-12-01 | 2018-05-18 | 广西玉林市和兴农业科技有限公司 | Treat the Chinese medicine composition of hypertension |
| CN108355113A (en) * | 2018-03-26 | 2018-08-03 | 陈俊梅 | A kind of Chinese medicine composition and preparation method thereof for treating cough and asthma flu |
| CN114470146A (en) * | 2022-01-26 | 2022-05-13 | 河南中医药大学 | Traditional Chinese medicine composition for treating phlegm-heat internal disturbance type insomnia and preparation method thereof |
| CN116392540A (en) * | 2023-03-14 | 2023-07-07 | 广西国际壮医医院 | Jinxiangxueyu vine drink for relieving stroke depression and preparation method thereof |
| CN116808162A (en) * | 2023-05-22 | 2023-09-29 | 上海中医药大学附属岳阳中西医结合医院 | Traditional Chinese medicine composition for preventing and treating ventricular premature contraction due to stagnation of gallbladder and phlegm and application thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108042756A (en) * | 2017-12-01 | 2018-05-18 | 广西玉林市和兴农业科技有限公司 | Treat the Chinese medicine composition of hypertension |
| CN108355113A (en) * | 2018-03-26 | 2018-08-03 | 陈俊梅 | A kind of Chinese medicine composition and preparation method thereof for treating cough and asthma flu |
| CN114470146A (en) * | 2022-01-26 | 2022-05-13 | 河南中医药大学 | Traditional Chinese medicine composition for treating phlegm-heat internal disturbance type insomnia and preparation method thereof |
| CN116392540A (en) * | 2023-03-14 | 2023-07-07 | 广西国际壮医医院 | Jinxiangxueyu vine drink for relieving stroke depression and preparation method thereof |
| CN116392540B (en) * | 2023-03-14 | 2024-01-30 | 广西国际壮医医院 | Jinxiangxueyu vine drink for relieving stroke depression and preparation method thereof |
| CN116808162A (en) * | 2023-05-22 | 2023-09-29 | 上海中医药大学附属岳阳中西医结合医院 | Traditional Chinese medicine composition for preventing and treating ventricular premature contraction due to stagnation of gallbladder and phlegm and application thereof |
| CN116808162B (en) * | 2023-05-22 | 2024-04-12 | 上海中医药大学附属岳阳中西医结合医院 | Traditional Chinese medicine composition for preventing and treating ventricular premature contraction due to stagnation of gallbladder and phlegm and application thereof |
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