CN106386865A - 3% gibberellin acid grease and preparation method thereof - Google Patents
3% gibberellin acid grease and preparation method thereof Download PDFInfo
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- CN106386865A CN106386865A CN201610791112.2A CN201610791112A CN106386865A CN 106386865 A CN106386865 A CN 106386865A CN 201610791112 A CN201610791112 A CN 201610791112A CN 106386865 A CN106386865 A CN 106386865A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/34—Shaped forms, e.g. sheets, not provided for in any other sub-group of this main group
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/02—Acyclic compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
- A01N41/10—Sulfones; Sulfoxides
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
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- Dentistry (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Environmental Sciences (AREA)
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Abstract
The invention provides 3% gibberellin acid grease, and relates to the technical field of pesticide agent processing formulas and technologies. The 3% gibberellin acid grease is prepared from gibberellin, wool grease, glycerin, beewax and dimethylsulfoxide, wherein the gibberellin accounts for 3% of the total component proportion and comprises gibberellin GA3 and GA[4+7]. According to the 3% gibberellin acid grease, GA3 and GA[4+7] are proportioned reasonably, the side effect is reduced when gibberellin is used in a single mode, and promotion to plant growth is better exerted.
Description
Technical field
The present invention relates to formulations of pesticide processing formula and Technology field, particularly to a kind of 3% gibberellins acid fat
And preparation method thereof.
Background technology
China is the agro-farming big country having thousand of years history, and in traditional planting industry, the yield of grain is to a great extent
Depending on weather conditions such as local sunshine, temperature, humidity.Using modern science and technology, break through the restriction of environmental area, be solution
The certainly important means of crisis in food.Research finds, plant cell, when accepting the ambient signals such as temperature light, can produce low concentration
The active substance of scalable plant physiology reaction, the division of impact cell, elongation, differentiation, these active substances are referred to as plant
Hormone.Gibberellins are one of six big phytohormone, have now been found that hundreds of gibberellins homologue, GA4+7And GA3Most use
It is worth and commercial value.Because GA3Hyperactivity, side effect is very big, GA4+7Agricultural neck at present is become with its unique advantage
The focus of domain research.Its content in plant body is very low, mainly passes through gibberella fermenting and producing, as one kind in industry
New and effective auxin, mainly has following features:1. destroy dormancy, plant is required for before flowering through low temperature
And the long-day, to promote GA4+7Synthesis, break the dormancy of plant, ectogenic interpolation GA4+7Plant seed can be made to send out in advance
Bud;2. increase setting, the florescence of plant uses GA4+7Cavity fruit can be prevented after sprinkling, increase percentage of fertile fruit, can prevent from using
The waste of the nutrition being brought during other growth hormone;3. cell division is stimulated to expand, GA4+7Cell wall can be suppressed
Peroxidase activity, increases the pliability of wall, and has more preferable extensibility, and growth is accelerated, and cell cycle can be made to shorten
30% about;4. induced parthenocarpy, such as in the growth early stage of the fruits such as Fructus Vitis viniferae, Fructus Fragariae Ananssae, Fructus Pruni, pears, Fructus Lycopersici esculenti, with necessarily dense
The GA of degree4+7Spray, can grow and obtain stenospermocarpy.
The Chinese invention of Application No. CN201110420530 discloses a kind of plant sprouting agent and preparation method thereof,
By 6- base gland is fast, kinetins, gibberellins, glycerol and lanoline form, each component proportion is 6- base to plant sprouting agent
The fast 0.04%-0.10% of gland, kinetins 0.01%-0.05%, gibberellins (GA4+7) 0.005%-0.02%, dimethyl sulfoxide
1.0%-3.0%, glycerol 1% and lanoline 94.93%-97.59%, have one to plant germination, plant stem-leaf elongation growth
Determine facilitation, but the unicity of the consumption due to gibberellins and use is so that its own activity is greatly affected, as plant
Thing hormone can not give play to its advantage function to plant growing well.
Content of the invention
It is an object of the invention to provide a kind of 3% gibberellins acid fat, rational proportion GA3And GA4+7, make gibberellins list
Side effect during one use reduces, and improves crop quality, promotes volume increase.
The above-mentioned purpose of the present invention technical scheme is that:A kind of 3% gibberellins acid fat, including
Gibberellins, lanoline, glycerol, also include Cera Flava, dimethyl sulfoxide, and wherein gibberellins account for the 3% of total component proportion, gibberellins bag
Include gibberellins GA3With gibberellins GA4+7.
By adopting technique scheme, gibberellins physiological effect the most prominent is to promote the elongation of stem and induction long day to plant
Thing bolting under the conditions of short day is bloomed, and gibberellins effect is absolutely to the effective percentage of crop, and effect is persistently, more efficient, more
Stable, safer, Seedling Stage starts to spray can make well developed root system, and pre- disease prevention, and it can be obviously promoted axis, Ye Sheng
Long, such as trophophase sprays, and also can make balanced in nutrition, contributes to crop growing state, Spraying in the flowering stage, can flower and fruit protecting, also can make fruit
Expand, more have U.S. fruit to act on;Gibberellins GA3Main Function is to promote plant to do and leaf growth, and gibberellins GA4 and GA7 then leads
If Accelerate bloom and stretching fruit, if containing more GA in plant growth regulator3If, fruit tree alabastrum can be led to be formed
Reduce, the gibberellins composition in existing 3% gibberellins acid fat is mainly gibberellins GA3, because gibberellins composition is single, live
Very high, therefore large side effects, the poor stability of property, and increase gibberellins GA4+7Afterwards, due to GA4+7There is energy active cell vigor, show
Write accelerate cell elongation growth effect, therefore can ensure 3% gibberellins acid fat highly active simultaneously, balance one-component
GA3The side effect bringing, the effect improving 3% gibberellins acid fat so as to more stable, strengthens the safety that fruit tree is used simultaneously
Property;Lanoline is attached to a kind of secretion oils and fatss on Pilus Caprae seu Oviss, and as the carrier of 3% gibberellins acid fat, chemical stability is high,
Adhesive force is good, is difficult to become sour, and the drug effect of 3% gibberellins acid fat can be made preferably to bring into play, make effective drug duration more longlasting;Grind
Study carefully discovery, the glycerol of suitable concentration can improve the yield of crops, improves the quality of crops;Triacontanol quilt in Cera Flava
As a kind of nonhazardouss, pollution-free, low cost, high efficiency broad spectrum activity plant growth regulator, it is also a kind of " environment friendly agricultural ",
It has multiple physiological regulation functions:Promote germination, improve germination percentage and germinating energy, promote the division of plant cell and stretch
Long, promote root, stem, the growth of leaf, stratification breaks up, increase number of blooming, improve setting percentage and mass of 1000 kernel, promote crop early
Ripe, improving quality, promote water absorption of plant tissues, promote the absorption of mineral element, increase chlorophyll content etc., therefore Cera Flava adds
Enter in 3% gibberellins acid fat and can strengthen its advantage function to plant further;Dimethyl sulfoxide is described as " alembroth ", tool
There are preferable dissolubility, stronger cell membrane penetration power, strong cell stability, and there is scavenging activated oxygen, improve and plant
The ability of thing metabolism, as the solvent of gibberellins, can be effectively improved each component quick penetration plant in 3% gibberellins acid fat and stop
Dormancy sprout cell film, it is directed into the ability of cell, so that drug effect is greatly improved, shorten action time, 3% gibberellins acid fat is more
Increase effect, stablize.
Preferably, GA in 3% gibberellins component3:GA4+7For 2: 1.
By adopting technique scheme, single use gibberellins GA3When due to its activity very high so that gibberellins acid fat
The stability of cream is poor, safety is low, also can bring the side effect such as plant alabastrum quantity of formation minimizing, therefore cannot play well
Go out the advantage function to plant growth regulating for the gibberellins, and allocate GA4+7Afterwards, GA4+7The activity of gibberellins can be balanced, reduce GA3
Side effect, both complementary actions, in plant, are more beneficial for rudiment and the late growing stage of plant.
Preferably, lanoline accounts for the 90%-95% of total component proportion.
By adopting technique scheme, the purposes of lanoline is the carrier as 3% gibberellins acid fat, and therefore it accounts for
The proportioning of total component is larger, as ointment base, can postpone each component in gibberellins acid fat and pass through plant cell so as to medicine
Effect is more longlasting.
Preferably, glycerol accounts for the 0.1%-0.5% of total component proportion.
By adopting technique scheme, the glycerol of suitable concentration can improve under the conditions of Chilling stress germination and
The growth of seedling, improves seed vitality, can also reduce nitrate content in plant body, improve content of soluble protein, can
Dissolubility sugared content, is favorably improved crop yield, improves crop quality;Additionally, glycerol and dimethyl sulfoxide synergism so that
The moistening effect of 3% gibberellins acid fat is more preferable.
Preferably, Cera Flava accounts for the 1%-2% of total component proportion.
By adopting technique scheme, in Cera Flava, plant growing is played regulatory role is mainly triacontanol, adds
A certain amount of Cera Flava can effectively improve the yield and quality of crop, although additionally, it is not fertilizer, can improve the profit of fertilizer
With rate, can be with the various plants nutritional mineral matter compounding use such as nitrogen, phosphorus, potassium, zinc, and action effect is more.
Preferably, dimethyl sulfoxide accounts for the 2%-3% of total component proportion.
By adopting technique scheme, as the solvent for dissolving gibberellins, content is with gibberellins for dimethyl sulfoxide
Depending on content;Simultaneously with glycerol synergism, there is the effect of the moisture-retaining capacity improving 3% gibberellins acid fat.
Another object of the present invention is to providing a kind of preparation method of above-mentioned 3% gibberellins acid fat.
The above-mentioned purpose of the present invention technical scheme is that:A kind of system of 3% gibberellins acid fat
Preparation Method, including 3% gibberellins acid fat described in above-mentioned any scheme, comprises the following steps:
A, by said components proportioning prepare 3% gibberellins acid fat raw material;
B, by the lanoline in above-mentioned raw materials, Cera Flava put into cutting kettle in mixed dissolution;
C, by the gibberellins GA in above-mentioned raw materials3, gibberellins GA4+7, glycerol, dimethyl sulfoxide mixed dissolution;
D, by gibberellins GA3, gibberellins GA4+7, glycerol, dimethyl sulfoxide mixed dissolution liquid put into cutting kettle in, mixing shearing
It is incubated discharging after 10 minutes;
E, cooling, subpackage obtain product.
By adopting technique scheme, first lanoline and Cera Flava are dissolved and mix, gibberellins and other components are used
Solvent dissolves, and finally two kinds of lysates is mixed to prepare 3% gibberellins acid fat.
Preferably, it is continuously agitated during mixed dissolution in step b, and the temperature in cutting kettle is maintained at 70 DEG C -75 DEG C
In the range of.
By adopting technique scheme, need when mixing lanoline and Cera Flava to be continuously agitated, cutting kettle temperature is protected
Hold 70 DEG C -75 DEG C be higher than lanoline and Cera Flava fusing points, to prevent lanoline or Cera Flava regelation becomes fritter so that 3%
The paste composition of gibberellins acid fat is uneven, affects the mixing of gibberellins and other plant growth regulating component below, finally
Have influence on the 3% gibberellins acid activity of fat and the adjustment effect to plant growing.
Preferably, put into mycin GA in step d3, gibberellins GA4+7, glycerol, the mixed dissolution liquid of dimethyl sulfoxide when,
Cutting kettle is maintained under the shearing condition of constant temperature.
By adopting technique scheme, so that cutting kettle is maintained under constant temperature, and maintain shearing condition, each group can be made
Point preferably, it is sufficiently mixed and dissolves, the 3% gibberellins acid fat obtaining each uniform component distribution is so as to can give play to
Best effect.
In sum, one kind 3% gibberellins acid fat that the present invention provides, activity is high, has stability, safety simultaneously again
Property, and there is moisture-keeping function, drug effect is more longlasting, can promote plant germination, accelerates axis, the elongation of leaf and growth, promotes fruit
Real cell growth is loose, improves yield, improves fruit quality, be a kind of excellent plant growth regulator.
Brief description
Fig. 1 is the preparation technology flow chart of 3% gibberellins acid fat.
Specific embodiment
Below in conjunction with accompanying drawing, the present invention is described in further detail.
Embodiment 1
A kind of 3% gibberellins acid fat, each component proportion is as follows:
As shown in figure 1, preparation method is as follows:
A, by said components proportioning prepare 3% gibberellins acid fat raw material:
B, by the lanoline in above-mentioned raw materials, Cera Flava put into cutting kettle in mixed dissolution, cutting kettle temperature constant is at 70 DEG C;
C, by the gibberellins GA in above-mentioned raw materials3, gibberellins GA4+7, glycerol, dimethyl sulfoxide mixed dissolution;
D, keep 70 DEG C, under shearing condition, by gibberellins GA3, gibberellins GA4+7, glycerol, the mixed dissolution liquid of dimethyl sulfoxide
Put in cutting kettle, mixing shearing was incubated discharging after 10 minutes;
E, cooling, subpackage obtain product.
Each component proportioning raw materials that the difference of embodiment 2~6 is in step a are different.
Table 1 is the component proportion of embodiment 2~6
Application examples:With pears for trial crops material, inquire into the regulating effect that 3% gibberellins acid fat grows to pears.
Soil property is experimental field selected to be sandy soil, pH value is 7.9, the content of organic matter 1.21%, better-than-average fertility, the pear tree age of tree
10a, seeding row spacing 3m × 4.5m, the test process time is fruit expanding period, fruit average transverse diameter 1cm~2cm.
Test medicine is 3% gibberellins acid fat of the embodiment of the present invention 1~6;Comparison medicament 1 is Zhejiang Qianjiang bioid
Learn the 3% gibberellin fat (GA that limited company produces3);Comparison medicament 2 is 3% gibberellins acid fat (GA4+7);Separately set
Blank is not dispenser.3% gibberellins acid fat (GA is set up in test separately3+GA4+7) it is A1~A6 trial zone, 3% gibberellin fat
Cream (GA3) it is B1 trial zone, 3% gibberellins acid fat (GA4+7) it is B2 trial zone, not dispenser is C trial zone.
Test first 5 days and spray 5% 5000 times of liquid of pyrrole Ah's cream, 7500 times of liquid of 40% lucky star cream and 70% Mancozeb
The pest and disease damages such as 800 times of liquid preventing and treating pear suckers, scabs, noiseless to this test.Test same day weather condition is good, to this test
Have no significant effect.It is stained with medicine uniform application pears young fruit fruit stem middle and upper part with float brush, close fruit side, coating length 2cm, from
Pears full blossom 1 month starts, daily when 9~14 when this period in dispenser once, and often really smear 20mg medicament.
After fruit reaches the ripe harvesting of finished product, respectively at winning at random from A trial zone, B trial zone, C trial zone on the same day
30 fruits, measurement fruit size and weight;Therefrom take out 5 fruits at random again, according to international standard《Fruit and vegetable vitamin
C content algoscopy》Measure its sugar content.
Increase fruit weight effect (%)=(treatment region mean fruit weight-check plot mean fruit weight)/check plot average fruit
Weight × 100
Increase output results (%)=(the average strain in treatment region average strain product-check plot product) the average strain in/check plot product × 100 to do sth. in advance
Ripe effect (d)=check plot average maturity area-treatment region average maturity area
Table 2 is embodiment 1~6, matched group, blank assay group test effect
During test, the fruit of each chemicals treatment has no poisoning phenomenon.The Maturation of Pear Fruits phase that dispenser is processed ratio in advance the 2 of not dispenser
~3 days.Each item data according further to table 2 understands, with 3% gibberellins acid fat (GA3+GA4+7) and 3% gibberellins fat
(GA3), 3% gibberellins fat (GA4+7), the contrast of the blank control group of not dispenser, the weightening of A1~A6 trial zone 8.8%~
Between 11.3%, A trial zone average weight gain 10.2%, the weightening of B1 trial zone is increased weight 5.6% in 2.7%, B2 trial zone.Use
3% gibberellins acid fat (GA3+GA4+7) units increased in production ratio be used alone 3% gibberellins fat (GA3) and 3% gibberellins fat
(GA4+7) total augment weight also big;Between 8.0%~13.0%, the average units increased in production in A trial zone is 10.5% to A1~A6 units increased in production,
In 1.3%, B2 trial zone units increased in production 3.1%, therefore A trial zone units increased in production adds B2 examination than B1 trial zone to B1 trial zone units increased in production
The total units increased in production testing area is bigger.
In sum, 3% gibberellins acid fat (GA3+GA4+7) to Pear Fruit growth adjustment effect ratio be used alone
3% gibberellins fat (GA3) or be used alone 3% gibberellins acid fat (GA3+GA4+7) effect is more notable, more prominent, fruit
Weightening and units increased in production improvement more preferably, and do not affect on the sugar content of fruit, sweet taste, and its reason is 3% gibberellins acid
Fat (GA3+GA4+7) in allocated gibberellins GA3And GA4+7, both remained GA3High activity, given play to GA again4+7Stablize
Property, safety, hence help to improve fruit quality, promote precocious and increase income.
This specific embodiment is only explanation of the invention, and it is not limitation of the present invention, people in the art
Member can make to the present embodiment after reading this specification as needed does not have the modification of creative contribution, but as long as at this
All protected by Patent Law in the right of invention.
Claims (9)
1. a kind of 3% gibberellins acid fat, including gibberellins, lanoline, glycerol it is characterised in that:Also include Cera Flava, diformazan
Sulfoxide, wherein gibberellins account for the 3% of total component proportion, and gibberellins include gibberellins GA3With gibberellins GA4+7.
2. according to claim 1 3% gibberellins acid fat it is characterised in that:GA in described 3% gibberellins component3∶
GA4+7For 2: 1.
3. according to claim 1 3% gibberellins acid fat it is characterised in that:Described lanoline accounts for total component proportion
90%-95%.
4. according to claim 3 3% gibberellins acid fat it is characterised in that:Described glycerol accounts for total component proportion
0.1%-0.5%.
5. according to claim 4 3% gibberellins acid fat it is characterised in that:Described Cera Flava accounts for total component proportion
1%-2%.
6. according to claim 5 3% gibberellins acid fat it is characterised in that:Described dimethyl sulfoxide accounts for total component proportion
2%-3%.
7. a kind of preparation method of 3% gibberellins acid fat, including 3% gibberellins described in any one in claim 1~6
Sour fat it is characterised in that:Comprise the following steps:
A, by said components proportioning prepare 3% gibberellins acid fat raw material;
B, by the lanoline in above-mentioned raw materials, Cera Flava put into cutting kettle in mixed dissolution;
C, by the gibberellins GA in above-mentioned raw materials3, gibberellins GA4+7, glycerol, dimethyl sulfoxide mixed dissolution;
D, by gibberellins GA3, gibberellins GA4+7, glycerol, dimethyl sulfoxide mixed dissolution liquid put into cutting kettle in, mixing shearing
It is incubated discharging after 10 minutes;
E, cooling, subpackage obtain product.
8. according to claim 7 3% gibberellins acid fat preparation method it is characterised in that:Mix in described step b
It is continuously agitated during dissolving, and the temperature in cutting kettle is maintained in the range of 70 DEG C -75 DEG C.
9. according to claim 8 3% gibberellins acid fat preparation method it is characterised in that:Throwing in described step d
Enter mycin GA3, gibberellins GA4+7, glycerol, the mixed dissolution liquid of dimethyl sulfoxide when, cutting kettle is maintained at the shearing condition of constant temperature
Under.
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CN113924884A (en) * | 2021-11-09 | 2022-01-14 | 广西壮族自治区农业科学院 | Fruit retention treatment method for improving storage and transportation resistance of sunshine rose |
CN114946858A (en) * | 2022-05-07 | 2022-08-30 | 渭南东旺农华生物科技有限公司 | Plant growth regulating composition containing triacontanol and gibberellin |
CN115644176A (en) * | 2022-05-07 | 2023-01-31 | 渭南东旺农华生物科技有限公司 | Plant growth regulating composition containing triacontanol and gibberellin A3 |
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CN113924884A (en) * | 2021-11-09 | 2022-01-14 | 广西壮族自治区农业科学院 | Fruit retention treatment method for improving storage and transportation resistance of sunshine rose |
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