CN106378876A - Diamond wire slicing cooling liquid integrated treatment method for sapphire and silicon wafers - Google Patents

Diamond wire slicing cooling liquid integrated treatment method for sapphire and silicon wafers Download PDF

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Publication number
CN106378876A
CN106378876A CN201610845719.4A CN201610845719A CN106378876A CN 106378876 A CN106378876 A CN 106378876A CN 201610845719 A CN201610845719 A CN 201610845719A CN 106378876 A CN106378876 A CN 106378876A
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China
Prior art keywords
coolant
pipeline
tank
treatment method
sapphire
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Granted
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CN201610845719.4A
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Chinese (zh)
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CN106378876B (en
Inventor
陆继波
路景刚
王禄宝
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Jiangsu Meike Solar Technology Co Ltd
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Zhenjiang Huantai Silicon Technology Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28DWORKING STONE OR STONE-LIKE MATERIALS
    • B28D5/00Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor
    • B28D5/0058Accessories specially adapted for use with machines for fine working of gems, jewels, crystals, e.g. of semiconductor material
    • B28D5/0076Accessories specially adapted for use with machines for fine working of gems, jewels, crystals, e.g. of semiconductor material for removing dust, e.g. by spraying liquids; for lubricating, cooling or cleaning tool or work
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/001Processes for the treatment of water whereby the filtration technique is of importance
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/28Treatment of water, waste water, or sewage by sorption
    • C02F1/283Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/28Treatment of water, waste water, or sewage by sorption
    • C02F1/285Treatment of water, waste water, or sewage by sorption using synthetic organic sorbents
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00Controlling or monitoring parameters in water treatment
    • C02F2209/005Processes using a programmable logic controller [PLC]

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  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Processing Of Stones Or Stones Resemblance Materials (AREA)
  • Grinding-Machine Dressing And Accessory Apparatuses (AREA)

Abstract

The invention relates to a diamond wire slicing cooling liquid integrated treatment method for sapphire and silicon wafers. The treatment method comprises following steps that firstly, a first pipeline conveys waste cooling liquid drained by slicing machines to a storage tank; secondly, a plate frame pressure filter carries out pressure filtering to remove solid wastes in the cooling liquid; thirdly, a precise filter tank is used for carrying out precise filtering to remove fine particles and metal ions in the cooling liquid; fourthly, a fourth pipeline conveys the cooling liquid treated by the precise filter tank to a preparation tank, a PLC is controlled to enable a cooling liquid supplementing system to supplement cooling liquid to the preparation tank, and a finished product tank conveys the cooling liquid to a plurality of slicing machines through a fifth pipeline. The cooling liquid can be circularly used, the machining quality is improved, the equipment failure and switching time can be shortened, the product manufacturing cost is reduced, and the water treatment environment pollution is reduced.

Description

A kind of sapphire and silicon chip diamond wire section coolant integrated sewage treatment method
Technical field
A kind of coolant integrated sewage treatment method the present invention relates to sapphire and silicon chip diamond wire are cut into slices, belongs to photovoltaic material Material production technical field.
Background technology
The processing mode of traditional sapphire slices and the section of diamond wire silicon chip is as follows:
1st, the agitator of equipment self-carrying mixing, cooling water and the coolant of demand circulation is squeezed in cutting every time.Cut through Using interior circulation pattern it is desirable to the concentration of micropowder meets section demand in journey, after one or many cutting, carry out changing and give up Abandon;
2nd, due to the impact of micropowder, in cutting process, in the bearing clearance in micropowder part meeting access arrangement, form solidification heavy Form sediment, impact bearing running, cutting every time finishes and certain time need to be spent to be rinsed, and equipment needs to carry out every certain cutter time Thoroughly great purge;
3rd, the impact of micropowder can pollute the surface of processed finished products, and coolant, in the environment of processing high temperature, forms oxidation with micropowder Reaction, is attached to product surface, need to design long pre-flush time, chemical cleaning products surface time in next link.
Due to sapphire slices and the section of diamond wire silicon chip, belong to diamond wire section field, cutting process needs to cool down Water and coolant, during the sheet product being become by bulk material in cutting process,<50% material can become micropowder shape or granule Enter in cooling water, pollute cutting environment, cutting precipitation solidification, cause equipment fault, lead to cutting yield low, pollute simultaneously Water afterwards needs to be discharged, and enters sewage disposal, brings environmental protection pressure.
Content of the invention
The purpose of the present invention is the defect for prior art, provides a kind of sapphire and the section cooling of silicon chip diamond wire Liquid integrated sewage treatment method, improves processing quality quality, reduces equipment fault and switching time, reduces cost of goods manufactured, subtract The environmental pollution of few water process.
The present invention is achieved by the following technical solutions:
A kind of sapphire and silicon chip diamond wire section coolant integrated sewage treatment method, its processing method is as follows:
(1)Some microtomes are connected with holding vessel by the first pipeline, discarded cooling microtome discharged by the first pipeline Liquid is delivered to holding vessel;
(2)Holding vessel is connected with filter press with muddy water bypass line by the second pipeline, by the second pipeline by holding vessel Interior coolant is delivered in filter press, carry out filter pressing remove coolant in solid waste, when in pressure-filtering process not When clear water occurs, coolant is conveyed into holding vessel from muddy water bypass line;
(3)Filter press is connected with precise filtering tank by the 3rd pipeline, by the 3rd pipeline will be through filter press at Coolant after reason is delivered to precise filtering tank, carries out secondary filter and removes fine particle and metal ion in coolant;
(4)Precise filtering tank is connected with finished fluid management system by the 4th pipeline, described finished fluid management system includes adjusting Distribution tank, finished pot and PLC, described blend tank is connected with blend tank and PLC respectively, described blend tank and PLC It is provided with coolant replenishment system, some microtomes that described finished pot passes through in the 5th pipeline step (1) are connected between controller, The coolant processing through precise filtering tank is delivered to by blend tank by the 4th pipeline, control PLC controller makes coolant supplement system System supplements coolant to blend tank, subsequently coolant is delivered in some microtomes by the 5th pipeline by finished pot.
A kind of above-mentioned sapphire and silicon chip diamond wire section coolant integrated sewage treatment method, wherein, described sheet frame pressure The air inlet air pressure of filter>12kg, reversely charging air pressure force value 4 ~ 6kg.
A kind of above-mentioned sapphire and silicon chip diamond wire section coolant integrated sewage treatment method, wherein, described precision mistake It is provided with secondary filter cylinder in filter tank, in described secondary filter cylinder, is provided with the filter bag of aperture 200um, once filtered removal cold But the fine particle in liquid, is provided with adsorbent resin layer and activated carbon adsorption layer in described precise filtering tank, carry out secondary filter and go Except the metal ion in coolant.
A kind of above-mentioned sapphire and silicon chip diamond wire section coolant integrated sewage treatment method, wherein, described precision mistake Be provided with alkalinity acidity tester, conductivity measuring instrument, cod detector in filter tank, described alkalinity acidity tester, conductivity measuring instrument, Cod detector is all electrically connected with PLC.
A kind of above-mentioned sapphire and silicon chip diamond wire section coolant integrated sewage treatment method, wherein, described holding vessel Be equipped with agitating device in blend tank, to coolant stirring and evenly mixing.
A kind of above-mentioned sapphire and silicon chip diamond wire section coolant integrated sewage treatment method, wherein, described holding vessel, Precise filtering tank, blend tank and finished pot are provided with LOAD CELLS and liquid level display, and described LOAD CELLS and liquid level show Show that device is all electrically connected with PLC.
A kind of above-mentioned sapphire and silicon chip diamond wire section coolant integrated sewage treatment method, wherein, described first pipe It is equipped with electromagnetic valve and water pump on road, the second pipeline, muddy water bypass line, the 3rd pipeline, the 4th pipeline and the 5th pipeline, described Electromagnetic valve and water pump are all electrically connected with PLC.
A kind of above-mentioned sapphire and silicon chip diamond wire section coolant integrated sewage treatment method, wherein, described coolant Replenishment system includes coolant holding vessel, infusion pump and telltale, and described infusion pump is electrically connected with PLC, described warns Device is connected with liquid level sensor, and described liquid level sensor is arranged in coolant holding vessel.
Beneficial effects of the present invention are:
The coolant integrated form control method that the present invention provides, can be applicable in sapphire and the diamond wire slicing processes of silicon chip, And according to microtome production capacity matching unit quantity and storage weight, the dust that section machining process is produced is integrated with coolant Formula control and remove, do not pollute integral cutting environment, make cooling liquid energy formed recycle, reduces cost, during with PLC control Device processed controls operation, improves automatization and treatment effeciency, makes the coolant quality of every microtome be in same level, raising is cut Tablet stability, thus improving processing quality quality, reducing equipment fault and switching time, reduce cost of goods manufactured, reduces water The environmental pollution processing.
Brief description
Fig. 1 is schematic flow sheet of the present invention.
(in figure, microtome 1, the first pipeline 2, holding vessel 3, the second pipeline 4, muddy water bypass line 5, filter press 6, 3rd pipeline 7, the 4th pipeline 8, precise filtering tank 9, secondary filter cylinder 10, adsorbent resin layer 11, activated carbon adsorption layer 12, filters Bag 13, finished fluid management system 14, blend tank 15, finished pot 16, PLC 17, coolant replenishment system 18, the 5th pipeline 19, coolant holding vessel 20, infusion pump 21, agitating device 22, electromagnetic valve 23, water pump 24).
Specific embodiment
Below in conjunction with the accompanying drawings the specific embodiment of the present invention is described further.
A kind of sapphire and silicon chip diamond wire section coolant integrated sewage treatment method, its processing method is as follows:
According to microtome production capacity matching unit quantity and storage weight, some microtomes are passed through the first pipeline and holding vessel phase Even, holding vessel is connected with filter press with muddy water bypass line by the second pipeline, filter press is passed through the 3rd and manages Road is connected with precise filtering tank, and precise filtering tank is connected with finished fluid management system by the 4th pipeline, described secondary filter It is provided with secondary filter cylinder, adsorbent resin layer and activated carbon adsorption layer in tank, in described secondary filter cylinder, be provided with the mistake of aperture 200um Filter bag, is provided with alkalinity acidity tester, conductivity measuring instrument, cod detector in described precise filtering tank;
Described finished fluid management system includes blend tank, finished pot and PLC, described blend tank respectively with blend tank and PLC is connected, and is provided with coolant replenishment system between described blend tank and PLC, and described finished pot passes through the 5th Pipeline is connected with some microtomes;
Described coolant replenishment system includes coolant holding vessel, infusion pump and telltale, described infusion pump and PLC electricity Connect, described telltale is connected with liquid level sensor, and described liquid level sensor is arranged in coolant holding vessel;
Described holding vessel, precise filtering tank, blend tank and finished pot are provided with LOAD CELLS and liquid level display, described storage It is equipped with agitating device, described first pipeline, the second pipeline, muddy water bypass line, the 3rd pipeline, the 4th pipe in tank and blend tank It is equipped with water pump and electromagnetic valve on road and the 5th pipeline, described LOAD CELLS, liquid level display, alkalinity acidity tester, conductance Rate analyzer, cod detector, electromagnetic valve, water pump are all electrically connected with PLC.
(1)The discarded coolant that microtome is discharged is delivered to by holding vessel by the first pipeline, by agitating device to cooling Liquid is continuously stirred;
(2)Control electromagnetic valve to open by PLC, the coolant in holding vessel is delivered to by filter press by the second pipeline In machine, the air inlet air pressure controlling filter press is 15kg, and reversely charging air pressure force value 5kg carries out filter pressing and removes consolidating in coolant Body garbage, when clear water in pressure-filtering process, coolant is conveyed into holding vessel from muddy water bypass line;
(3)Electromagnetic valve is controlled to open by PLC, the coolant conveying after being processed through filter press by the 3rd pipeline To precise filtering tank, the fine particle removing in coolant is once filtered by filter bag, by adsorbent resin layer and activated carbon Adsorption layer carries out the metal ion that secondary filter removes in coolant, and passes through alkalinity acidity tester, conductivity measuring instrument, cod PH value in detector detection coolant, electrical conductivity and cod value;
(4)Control electromagnetic valve to open by PLC, by the 4th pipeline, the coolant processing through precise filtering tank is delivered to Blend tank, continuously stirred to coolant by agitating device, the liquid level according to pH value, electrical conductivity, cod value, LOAD CELLS shows Show device show value, control PLC controller makes coolant holding vessel supplement coolant to blend tank by infusion pump, works as level sensing When device transmitter liquid level is less than coolant storage tank volume 1/4, telltale is warned, and subsequently will be cooled down by the 5th pipeline by finished pot Liquid is delivered to step(1)In microtome.
The present invention can form coolant and recycle, during beneficial to improving processing quality quality, reducing equipment fault and switching Between, reduce cost of goods manufactured, reduce water process environmental pollution.
The above, the only present invention preferably specific embodiment, but protection scope of the present invention is not limited thereto, Any those familiar with the art the invention discloses technical scope in, the change or replacement that can readily occur in, All should cover within the scope of the present invention.Therefore, protection scope of the present invention should be with the protection domain of claims It is defined.

Claims (8)

1. a kind of sapphire and silicon chip diamond wire section coolant integrated sewage treatment method, it is characterized by, its processing method is such as Under:
(1)Some microtomes are connected with holding vessel by the first pipeline, discarded cooling microtome discharged by the first pipeline Liquid is delivered to holding vessel;
(2)Holding vessel is connected with filter press with muddy water bypass line by the second pipeline, by the second pipeline by holding vessel Interior coolant is delivered in filter press, carry out filter pressing remove coolant in solid waste, when in pressure-filtering process not When clear water occurs, coolant is conveyed into holding vessel from muddy water bypass line;
(3)Filter press is connected with precise filtering tank by the 3rd pipeline, by the 3rd pipeline will be through filter press at Coolant after reason is delivered to precise filtering tank, carries out secondary filter and removes fine particle and metal ion in coolant;
(4)Precise filtering tank is connected with finished fluid management system by the 4th pipeline, described finished fluid management system includes adjusting Distribution tank, finished pot and PLC, described blend tank is connected with blend tank and PLC respectively, described blend tank and PLC It is provided with coolant replenishment system, some microtomes that described finished pot passes through in the 5th pipeline step (1) are connected between controller, The coolant processing through precise filtering tank is delivered to by blend tank by the 4th pipeline, control PLC controller makes coolant supplement system System supplements coolant to blend tank, subsequently coolant is delivered in some microtomes by the 5th pipeline by finished pot.
2. a kind of sapphire and silicon chip diamond wire is cut into slices coolant integrated sewage treatment method as claimed in claim 1, and it is special Levy as the air inlet air pressure of described filter press>12kg, reversely charging air pressure force value 4 ~ 6kg.
3. a kind of sapphire and silicon chip diamond wire is cut into slices coolant integrated sewage treatment method as claimed in claim 1, and it is special Levy as being provided with secondary filter cylinder in described precise filtering tank, being provided with the filter bag of aperture 200um in described secondary filter cylinder, enter Row once filters the fine particle removing in coolant, is provided with adsorbent resin layer and activated carbon adsorption in described precise filtering tank Layer, carries out secondary filter and removes the metal ion in coolant.
4. a kind of sapphire and silicon chip diamond wire is cut into slices coolant integrated sewage treatment method as claimed in claim 1, and it is special Levy as being provided with alkalinity acidity tester, conductivity measuring instrument, cod detector, described acid-base value test in described precise filtering tank Instrument, conductivity measuring instrument, cod detector are all electrically connected with PLC.
5. a kind of sapphire and silicon chip diamond wire is cut into slices coolant integrated sewage treatment method as claimed in claim 1, and it is special Levy as being equipped with agitating device in described holding vessel and blend tank, to coolant stirring and evenly mixing.
6. a kind of sapphire and silicon chip diamond wire is cut into slices coolant integrated sewage treatment method as claimed in claim 1, and it is special Levy as described holding vessel, precise filtering tank, blend tank and finished pot are provided with LOAD CELLS and liquid level display, described title Retransmit sensor and liquid level display is all electrically connected with PLC.
7. a kind of sapphire and silicon chip diamond wire is cut into slices coolant integrated sewage treatment method as claimed in claim 1, and it is special Levy as being equipped with electricity on described first pipeline, the second pipeline, muddy water bypass line, the 3rd pipeline, the 4th pipeline and the 5th pipeline Magnet valve and water pump, described electromagnetic valve and water pump are all electrically connected with PLC.
8. a kind of sapphire and silicon chip diamond wire is cut into slices coolant integrated sewage treatment method as claimed in claim 1, and it is special Levy as described coolant replenishment system includes coolant holding vessel, infusion pump and telltale, described infusion pump and PLC Electrical connection, described telltale is connected with liquid level sensor, and described liquid level sensor is arranged in coolant holding vessel.
CN201610845719.4A 2016-09-23 2016-09-23 A kind of sapphire and silicon wafer are sliced coolant liquid integrated sewage treatment method with diamond wire Active CN106378876B (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108162215A (en) * 2017-12-28 2018-06-15 洛阳阿特斯光伏科技有限公司 A kind of diamond wire sliced crystal silicon production line and its water system
CN108164020A (en) * 2017-12-28 2018-06-15 洛阳阿特斯光伏科技有限公司 A kind of diamond wire sliced crystal silicon production line uses water method and water system
CN108162216A (en) * 2017-12-28 2018-06-15 洛阳阿特斯光伏科技有限公司 A kind of diamond wire sliced crystal silicon production line and its water system
CN108975533A (en) * 2018-07-20 2018-12-11 江苏吉星新材料有限公司 A kind of Sapphire Substrate intellectualization of factories sewage water treatment method
CN108972920A (en) * 2018-07-20 2018-12-11 江苏吉星新材料有限公司 A kind of central liquid supply system and its technique of intelligence sapphire slices system
CN109203265A (en) * 2017-06-29 2019-01-15 赛锡科技(镇江)有限公司 Buddha's warrior attendant wire cutting liquid online recycling and supply great circulation system
CN110919545A (en) * 2019-12-20 2020-03-27 宁波韵升磁体元件技术有限公司 Neodymium iron boron product grinds chamfer and concentrates solution feed system
CN111015988A (en) * 2019-12-25 2020-04-17 无锡荣能半导体材料有限公司 Method for recycling silicon wafer cutting cooling slurry
CN111195991A (en) * 2018-11-16 2020-05-26 胜高股份有限公司 Method for manufacturing wafer, method for evaluating quality of reusable slurry for wire saw, and method for evaluating quality of used slurry for wire saw
CN112624404A (en) * 2020-12-08 2021-04-09 句容协鑫光伏科技有限公司 Regeneration and utilization system of buddha's warrior attendant line coolant liquid

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CN202006519U (en) * 2011-01-17 2011-10-12 西安华晶电子技术股份有限公司 Mortar circulating and supplying system of multi-wire saw
CN102873774A (en) * 2012-04-10 2013-01-16 沈阳连城精密机器有限公司 Online mortar recovery method in silicon industry
CN203973784U (en) * 2014-06-13 2014-12-03 开封恒锐新金刚石制品有限公司 Resin diamond wire cutting machine cooling fluid reclaims filtration system
JP3197053U (en) * 2015-02-04 2015-04-16 株式会社クラレ Liquid replenishment device and coolant regeneration device provided with the same
CN204792698U (en) * 2015-07-08 2015-11-18 内蒙古中环光伏材料有限公司 Diamond wire cutting silicon chip coolant liquid recovery system

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CN202006519U (en) * 2011-01-17 2011-10-12 西安华晶电子技术股份有限公司 Mortar circulating and supplying system of multi-wire saw
CN102873774A (en) * 2012-04-10 2013-01-16 沈阳连城精密机器有限公司 Online mortar recovery method in silicon industry
CN203973784U (en) * 2014-06-13 2014-12-03 开封恒锐新金刚石制品有限公司 Resin diamond wire cutting machine cooling fluid reclaims filtration system
JP3197053U (en) * 2015-02-04 2015-04-16 株式会社クラレ Liquid replenishment device and coolant regeneration device provided with the same
CN204792698U (en) * 2015-07-08 2015-11-18 内蒙古中环光伏材料有限公司 Diamond wire cutting silicon chip coolant liquid recovery system

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109203265A (en) * 2017-06-29 2019-01-15 赛锡科技(镇江)有限公司 Buddha's warrior attendant wire cutting liquid online recycling and supply great circulation system
CN108162215A (en) * 2017-12-28 2018-06-15 洛阳阿特斯光伏科技有限公司 A kind of diamond wire sliced crystal silicon production line and its water system
CN108164020A (en) * 2017-12-28 2018-06-15 洛阳阿特斯光伏科技有限公司 A kind of diamond wire sliced crystal silicon production line uses water method and water system
CN108162216A (en) * 2017-12-28 2018-06-15 洛阳阿特斯光伏科技有限公司 A kind of diamond wire sliced crystal silicon production line and its water system
CN108975533A (en) * 2018-07-20 2018-12-11 江苏吉星新材料有限公司 A kind of Sapphire Substrate intellectualization of factories sewage water treatment method
CN108972920A (en) * 2018-07-20 2018-12-11 江苏吉星新材料有限公司 A kind of central liquid supply system and its technique of intelligence sapphire slices system
CN108975533B (en) * 2018-07-20 2021-09-03 江苏吉星新材料有限公司 Intelligent sewage treatment method for sapphire substrate factory
CN111195991A (en) * 2018-11-16 2020-05-26 胜高股份有限公司 Method for manufacturing wafer, method for evaluating quality of reusable slurry for wire saw, and method for evaluating quality of used slurry for wire saw
CN110919545A (en) * 2019-12-20 2020-03-27 宁波韵升磁体元件技术有限公司 Neodymium iron boron product grinds chamfer and concentrates solution feed system
CN111015988A (en) * 2019-12-25 2020-04-17 无锡荣能半导体材料有限公司 Method for recycling silicon wafer cutting cooling slurry
CN112624404A (en) * 2020-12-08 2021-04-09 句容协鑫光伏科技有限公司 Regeneration and utilization system of buddha's warrior attendant line coolant liquid

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Denomination of invention: Diamond wire slicing cooling liquid integrated treatment method for sapphire and silicon wafers

Effective date of registration: 20191113

Granted publication date: 20190205

Pledgee: China Everbright Bank Limited by Share Ltd. Nanjing branch

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