CN106378845A - Preparation method of bamboo chip curing agent - Google Patents
Preparation method of bamboo chip curing agent Download PDFInfo
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- CN106378845A CN106378845A CN201610796497.1A CN201610796497A CN106378845A CN 106378845 A CN106378845 A CN 106378845A CN 201610796497 A CN201610796497 A CN 201610796497A CN 106378845 A CN106378845 A CN 106378845A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/002—Cane, bamboo
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention provides a preparation method of a bamboo chip curing agent. The bamboo chip curing agent comprises the following components: 30-50 parts of a strength modifier which comprises 30%-40% of ethylene glycol, 30%-40% of stearic acid and water in balancing amount; 3-5 parts of a form retaining agent which comprises 15%-25% of stearic acid, 30%-35% of pentaerythritol, 15%-20% of paraffin and water in balancing amount; 6-9 parts of an initiating agent which comprises 15%-25% of glyoxal, 20%-25% of methanol, 25%-30% of ethanolamine and water in balancing amount; 3-5 parts of an enhancer which comprises 10%-20% of talcum powder, 10%-15% of limestone powder, 20%-30% of calcium carbonate and water in balancing amount; and 100-120 parts of deionized water. The preparation method comprises the following steps: mixing the deionized water with the strength modifier, the form retaining agent, the initiating agent and the enhancer, which are prepared, keeping the mixture standing still for 1 h, removing impurities at the bottom, performing heating to 300-350 DEG C, and performing concentration to 30% to obtain the curing agent. The preparation method has the beneficial effects as follows: the curing agent prepared according to the method not only improves the strength of bamboo chips, but also highly improves the pressure resistance of the bamboo chips; and during a curing process, the bamboo chips can be soaked with herbal medicines to have a herbal smell, so that a handicraft made of the bamboo chips is better.
Description
Technical field：
The present invention relates to artware raw material firming agent field is and in particular to a kind of bamboo chip firming agent preparation method.
Background technology：
Existing artware is attractive in appearance and unique, and typically mostly wicker, bamboo weaving, rattan are prepared from, this artware
Outward appearance has stronger aesthetics, but inflammable afraid of water, in preparation process, due to raw material strength problem, folding often
Curved fracture, the phenomenons such as crackle in surface.
Content of the invention：
The technical problem to be solved is to overcome the defect of prior art, provides a kind of artware packaging fire insulation
Plate preparation method.
The technical problem to be solved employs the following technical solutions to realize.
A kind of bamboo chip firming agent preparation method it is characterised in that：Mainly include the following steps that：
Including 30-50 part intensity modifying agent：30%-40% ethylene glycol, 30-40% stearic acid, remaining is water；
3-5 part form retention agent：Stearic acid 15-25%, tetramethylolmethane 30-35%, paraffin 15%-20% part, remaining is
Water；
6-9 part initiator：Biformyl 15-25%, formaldehyde 20-25%, ethanolamine 25-30%, remaining is water；
3-5 part reinforcing agent：Pulvis Talci 10-20%, agstone 10-15%, Calcium Carbonate 20-30%, remaining is water；
Deionized water：100-120 part；
Described intensity modifying agent preparation method is：
Add the water of ethylene glycol and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition it is being full of the water adding stearic acid and half in the container of carbon dioxide, be warming up to 40～50
DEG C, stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, stir；
Described form retention agent preparation method is：
Add the water of stearic acid and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition being full of the water adding tetramethylolmethane and half in the container of carbon dioxide, it is warming up to 40～
50 DEG C, stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take Herba Ephedrae 15-18 part, 7 parts of the Radix Astragali-
14 parts, Semen Coiciss 6-12 part, Flos Lonicerae 9-16 part, Flos Chrysanthemi 15-20 part, it is wrapped in the string bag, the string bag is put in liquid, plus
Hot liquid, to liquid evaporation 30%-35%, takes out the string bag, paraffin is added, continue heating, be completely dissolved to paraffin；
Described initiator preparation method is：
Add the water of Biformyl and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition it is being full of the water adding formaldehyde and half in the container of carbon dioxide, be warming up to 40～50 DEG C,
Stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take Radix Rehmanniae 13-16 part, Caulis Akebiae 6-9 part,
Radix Astragali 5-8 part, Folium Mori 12-14 part, Rhizoma Polygonati Odorati 5-7 part, Radix Ophiopogonis 9-14 part, be wrapped in the string bag, the string bag put in liquid,
Heating liquid, to liquid evaporation 30%-35%, takes out the string bag, ethanolamine is added, continue heating, be completely dissolved to ethanolamine
?；
Described reinforcing agent preparation method is：
Add the water of Pulvis Talci and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition being full of the water adding agstone and half in the container of carbon dioxide, it is warming up to 40～
50 DEG C, stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take Radix Ginseng 13-16 part, Radix Ophiopogonis 6-9
Part, Fructus Schisandrae Chinensis 5-8 part, Rhizoma Polygonati Odorati 5-7 part, Rhizoma Arisaematiss 9-12 part, it is wrapped in the string bag, the string bag is put in liquid, heat liquid
Body, to liquid evaporation 30%-35%, takes out the string bag, Calcium Carbonate is added, continue heating, be completely dissolved to Calcium Carbonate；
By the intensity preparing modifying agent, form retention agent, initiator, reinforcing agent mixing deionized water, static 1 hour,
Take out bottom impurity, heat 300-350 DEG C, be concentrated into 30%, that is, obtain firming agent.
The present invention has the beneficial effects that：The firming agent prepared by this law, not only increases the intensity of bamboo, and makes
Bamboo crushing resistance obtains stronger lifting, and in solidification process, bamboo can also be made to soak, and medical material is fragrant, and the artware of preparation is more preferable.
Specific embodiment：
In order that technological means, creation characteristic, reached purpose and effect that the present invention realizes are easy to understand, tie below
Conjunction is embodied as, and specifically includes following steps：
Specific embodiment 1：A kind of bamboo chip firming agent preparation method, mainly includes the following steps that：
Including 30 parts of intensity modifying agents：30%-40% ethylene glycol, 30-40% stearic acid, remaining is water；
3 parts of form retention agents：Stearic acid 15-25%, tetramethylolmethane 30-35%, paraffin 15%-20% part, remaining is water；
6 parts of initiators：Biformyl 15-25%, formaldehyde 20-25%, ethanolamine 25-30%, remaining is water；
3 parts of reinforcing agents：Pulvis Talci 10-20%, agstone 10-15%, Calcium Carbonate 20-30%, remaining is water；
Deionized water：100 parts；
Described intensity modifying agent preparation method is：
Add the water of ethylene glycol and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition it is being full of the water adding stearic acid and half in the container of carbon dioxide, be warming up to 40～50
DEG C, stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, stir；
Described form retention agent preparation method is：
Add the water of stearic acid and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition being full of the water adding tetramethylolmethane and half in the container of carbon dioxide, it is warming up to 40～
50 DEG C, stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take 15 parts of Herba Ephedrae, 7 parts of parts of the Radix Astragali,
6 parts of Semen Coiciss, 9 parts of Flos Lonicerae, 15 parts of Flos Chrysanthemi, it is wrapped in the string bag, the string bag is put in liquid, heat liquid, to liquid
Evaporation 30%-35%, takes out the string bag, paraffin is added, and continues heating, is completely dissolved to paraffin；
Described initiator preparation method is：
Add the water of Biformyl and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition it is being full of the water adding formaldehyde and half in the container of carbon dioxide, be warming up to 40～50 DEG C,
Stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take 13 parts of Radix Rehmanniae, 6 parts of Caulis Akebiae, the Radix Astragali 5
Part, 12 parts of Folium Mori, 5 parts of Rhizoma Polygonati Odorati, 9 parts of Radix Ophiopogonis, it is wrapped in the string bag, the string bag is put in liquid, heat liquid, to liquid
Evaporation 30%-35%, takes out the string bag, ethanolamine is added, and continues heating, is completely dissolved to ethanolamine；
Described reinforcing agent preparation method is：
Add the water of Pulvis Talci and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition being full of the water adding agstone and half in the container of carbon dioxide, it is warming up to 40～
50 DEG C, stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take 13 parts of Radix Ginseng, 6 parts of Radix Ophiopogonis, five
5 parts of taste, 5 parts of Rhizoma Polygonati Odorati, 9 parts of Rhizoma Arisaematiss, it is wrapped in the string bag, the string bag is put in liquid, heat liquid, to liquid evaporation
30%-35%, takes out the string bag, Calcium Carbonate is added, and continues heating, is completely dissolved to Calcium Carbonate；
By the intensity preparing modifying agent, form retention agent, initiator, reinforcing agent mixing deionized water, static 1 hour,
Take out bottom impurity, heat 300-350 DEG C, be concentrated into 30%, that is, obtain firming agent.
Specific embodiment 2：A kind of bamboo chip firming agent preparation method, mainly includes the following steps that：
Including 50 parts of intensity modifying agents：30%-40% ethylene glycol, 30-40% stearic acid, remaining is water；
5 parts of form retention agents：Stearic acid 15-25%, tetramethylolmethane 30-35%, paraffin 15%-20% part, remaining is water；
9 parts of initiators：Biformyl 15-25%, formaldehyde 20-25%, ethanolamine 25-30%, remaining is water；
5 parts of reinforcing agents：Pulvis Talci 10-20%, agstone 10-15%, Calcium Carbonate 20-30%, remaining is water；
Deionized water：120 parts；
Described intensity modifying agent preparation method is：
Add the water of ethylene glycol and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition it is being full of the water adding stearic acid and half in the container of carbon dioxide, be warming up to 40～50
DEG C, stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, stir；
Described form retention agent preparation method is：
Add the water of stearic acid and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition being full of the water adding tetramethylolmethane and half in the container of carbon dioxide, it is warming up to 40～
50 DEG C, stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take 18 parts of Herba Ephedrae, 14 parts of the Radix Astragali, the heart of a lotus seed
12 parts of Semen Coicis, 16 parts of Flos Lonicerae, 20 parts of Flos Chrysanthemi, it is wrapped in the string bag, the string bag is put in liquid, heat liquid, to liquid
Evaporation 30%-35%, takes out the string bag, paraffin is added, and continues heating, is completely dissolved to paraffin；
Described initiator preparation method is：
Add the water of Biformyl and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition it is being full of the water adding formaldehyde and half in the container of carbon dioxide, be warming up to 40～50 DEG C,
Stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take 16 parts of Radix Rehmanniae, 9 parts of Caulis Akebiae, the Radix Astragali 8
Part, 14 parts of Folium Mori, 7 parts of Rhizoma Polygonati Odorati, 14 parts of Radix Ophiopogonis, it is wrapped in the string bag, the string bag is put in liquid, heat liquid, to liquid
Evaporation 30%-35%, takes out the string bag, ethanolamine is added, and continues heating, is completely dissolved to ethanolamine；
Described reinforcing agent preparation method is：
Add the water of Pulvis Talci and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to complete simultaneously
Dissolving, and it is incubated 1～2h；In addition being full of the water adding agstone and half in the container of carbon dioxide, it is warming up to 40～
50 DEG C, stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take 16 parts of Radix Ginseng, 9 parts of Radix Ophiopogonis, five
8 parts of taste, 7 parts of Rhizoma Polygonati Odorati, 12 parts of Rhizoma Arisaematiss, it is wrapped in the string bag, the string bag is put in liquid, heat liquid, steam to liquid
Send out 30%-35%, take out the string bag, Calcium Carbonate is added, continue heating, be completely dissolved to Calcium Carbonate；
By the intensity preparing modifying agent, form retention agent, initiator, reinforcing agent mixing deionized water, static 1 hour,
Take out bottom impurity, heat 300-350 DEG C, be concentrated into 30%, that is, obtain firming agent.
Ultimate principle, principal character and the advantages of the present invention of the present invention have been shown and described above.The technology of the industry
, it should be appreciated that the present invention is not restricted to the described embodiments, the simply explanation described in above-described embodiment and description is originally for personnel
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes
Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and its
Equivalent thereof.
Claims (1)
1. a kind of bamboo chip firming agent preparation method it is characterised in that：Mainly include the following steps that：
Including 30-50 part intensity modifying agent：30%-40% ethylene glycol, 30-40% stearic acid, remaining is water；
3-5 part form retention agent：Stearic acid 15-25%, tetramethylolmethane 30-35%, paraffin 15%-20% part, remaining is water；
6-9 part initiator：Biformyl 15-25%, formaldehyde 20-25%, ethanolamine 25-30%, remaining is water；
3-5 part reinforcing agent：Pulvis Talci 10-20%, agstone 10-15%, Calcium Carbonate 20-30%, remaining is water；
Deionized water：100-120 part；
Described intensity modifying agent preparation method is：
Add the water of ethylene glycol and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to being completely dissolved simultaneously,
And it is incubated 1～2h；In addition it is being full of the water adding stearic acid and half in the container of carbon dioxide, be warming up to 40～50 DEG C, stir
Mix to being completely dissolved；Again both are mixed, heat 90-110 DEG C, stir；
Described form retention agent preparation method is：
Add the water of stearic acid and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to being completely dissolved simultaneously,
And it is incubated 1～2h；In addition it is being full of the water adding tetramethylolmethane and half in the container of carbon dioxide, be warming up to 40～50 DEG C,
Stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take Herba Ephedrae 15-18 part, 7 parts -14 parts of the Radix Astragali,
Semen Coiciss 6-12 part, Flos Lonicerae 9-16 part, Flos Chrysanthemi 15-20 part, it is wrapped in the string bag, the string bag is put in liquid, heat liquid
Body, to liquid evaporation 30%-35%, takes out the string bag, paraffin is added, continue heating, be completely dissolved to paraffin；
Described initiator preparation method is：
Add the water of Biformyl and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to being completely dissolved simultaneously,
And it is incubated 1～2h；In addition it is being full of the water adding formaldehyde and half in the container of carbon dioxide, be warming up to 40～50 DEG C, stirring
To being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take Radix Rehmanniae 13-16 part, Caulis Akebiae 6-9 part, the Radix Astragali
5-8 part, Folium Mori 12-14 part, Rhizoma Polygonati Odorati 5-7 part, Radix Ophiopogonis 9-14 part, be wrapped in the string bag, the string bag put in liquid, heating
Liquid, to liquid evaporation 30%-35%, takes out the string bag, ethanolamine is added, continue heating, be completely dissolved to ethanolamine；
Described reinforcing agent preparation method is：
Add the water of Pulvis Talci and half in full of nitrogen reactor, be warming up to 50～60 DEG C, stir to being completely dissolved simultaneously,
And it is incubated 1～2h；In addition it is being full of the water adding agstone and half in the container of carbon dioxide, be warming up to 40～50 DEG C,
Stir to being completely dissolved；Again both are mixed, heat 90-110 DEG C, obtain liquid, take Radix Ginseng 13-16 part, Radix Ophiopogonis 6-9 part, five
Taste 5-8 part, Rhizoma Polygonati Odorati 5-7 part, Rhizoma Arisaematiss 9-12 part, it is wrapped in the string bag, the string bag is put in liquid, heat liquid, extremely
Liquid evaporation 30%-35%, takes out the string bag, Calcium Carbonate is added, and continues heating, is completely dissolved to Calcium Carbonate；
By the intensity preparing modifying agent, form retention agent, initiator, reinforcing agent mixing deionized water, static 1 hour, take out
Bottom impurity, heats 300-350 DEG C, is concentrated into 30%, that is, obtains firming agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610796497.1A CN106378845A (en) | 2016-08-31 | 2016-08-31 | Preparation method of bamboo chip curing agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610796497.1A CN106378845A (en) | 2016-08-31 | 2016-08-31 | Preparation method of bamboo chip curing agent |
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| CN106378845A true CN106378845A (en) | 2017-02-08 |
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| CN201610796497.1A Pending CN106378845A (en) | 2016-08-31 | 2016-08-31 | Preparation method of bamboo chip curing agent |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107325599A (en) * | 2017-07-05 | 2017-11-07 | 蚌埠市风驰滤清器有限公司 | Metal spray painting and preparation method thereof used in a kind of filter casing |
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|---|---|---|---|---|
| CN104493934A (en) * | 2014-12-10 | 2015-04-08 | 界首市祥雨竹编专业合作社 | Bamboo weaving softening agent and preparation technique thereof |
| CN104526808A (en) * | 2014-12-10 | 2015-04-22 | 界首市祥雨竹编专业合作社 | Bamboo strip softener and preparation process thereof |
| CN104589442A (en) * | 2014-12-19 | 2015-05-06 | 赵俊辉 | Bamboo cane softener and preparation method thereof |
| CN105058529A (en) * | 2015-07-20 | 2015-11-18 | 孙晨 | Environmentally friendly mildew preventives for willow rattans |
-
2016
- 2016-08-31 CN CN201610796497.1A patent/CN106378845A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104493934A (en) * | 2014-12-10 | 2015-04-08 | 界首市祥雨竹编专业合作社 | Bamboo weaving softening agent and preparation technique thereof |
| CN104526808A (en) * | 2014-12-10 | 2015-04-22 | 界首市祥雨竹编专业合作社 | Bamboo strip softener and preparation process thereof |
| CN104589442A (en) * | 2014-12-19 | 2015-05-06 | 赵俊辉 | Bamboo cane softener and preparation method thereof |
| CN105058529A (en) * | 2015-07-20 | 2015-11-18 | 孙晨 | Environmentally friendly mildew preventives for willow rattans |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107325599A (en) * | 2017-07-05 | 2017-11-07 | 蚌埠市风驰滤清器有限公司 | Metal spray painting and preparation method thereof used in a kind of filter casing |
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Application publication date: 20170208 |