CN106305776B - A kind of Radix Salviae Miltiorrhizae flower thinning composition, preparation method and application method - Google Patents

A kind of Radix Salviae Miltiorrhizae flower thinning composition, preparation method and application method Download PDF

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CN106305776B
CN106305776B CN201610711365.4A CN201610711365A CN106305776B CN 106305776 B CN106305776 B CN 106305776B CN 201610711365 A CN201610711365 A CN 201610711365A CN 106305776 B CN106305776 B CN 106305776B
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radix salviae
salviae miltiorrhizae
flower thinning
points
thinning composition
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CN106305776A (en
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李雨晴
李琦
俞磊明
朱光明
谈景福
张朋
王宏杰
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Huayu Medicine (linyi) Medicine Resources Ltd
Shanghai Huayu Pharmaceutical Co Ltd
SHANGHAI TRADITIONAL CHINESE MEDICINE CO Ltd
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Huayu Medicine (linyi) Medicine Resources Ltd
Shanghai Huayu Pharmaceutical Co Ltd
SHANGHAI TRADITIONAL CHINESE MEDICINE CO Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16Heavy metals; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system

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  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • Environmental Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)

Abstract

The invention discloses a kind of Radix Salviae Miltiorrhizae flower thinning composition, preparation method and application methods.The Radix Salviae Miltiorrhizae flower thinning composition includes the component of following mass percents: ferrous sulfate 55%~60%, calcium formate 17%~22%, naphthaleneacetamide 0.8%~3% and 6- benzyl aminoadenine 20%~25%.Radix Salviae Miltiorrhizae flower thinning composition of the invention can effectively avoid damage of the flower thinning component to Radix Salviae Miltiorrhizae plant leaf, can significantly improve medicinal material active constituent content while flower thinning;The composition significantly improves Radix Salviae Miltiorrhizae flower thinning operational security and working efficiency, and use is safe, and production cost is low, is suitble to industrialization promotion.

Description

A kind of Radix Salviae Miltiorrhizae flower thinning composition, preparation method and application method
Technical field
The present invention relates to plant planting field more particularly to a kind of Radix Salviae Miltiorrhizae flower thinning compositions, preparation method and application method.
Background technique
Radix Salviae Miltiorrhizae is Lamiaceae Salvia category herbaceos perennial, and rhizome is used as medicine, tool stasis-dispelling and pain-killing, blood circulation, clear The effect of heart relieving restlessness.Radix Salviae Miltiorrhizae is that indefinite inflorescence, florescence are long, starts bolting the general 4-5 month, blooms at the beginning of 5 months, continues to October, opens Spend 3 batches or so.
Radix Salviae Miltiorrhizae is as ratio of rhizome medicinal material, and reproductive growth occupies excessive nutrient and will lead under medical material quanlity and yield in growth period Drop.For this purpose, the prior art generally manually removes flower in mid or late May.But since Radix Salviae Miltiorrhizae is indefinite inflorescence plant, bud is planted after extracing Strain also will continue to sprout new one batch of bud, therefore, artificial except flower inefficiency.The artificial flower that removes is not only extremely time-consuming, and At this moment bud differentiation has been completed, and plant is started to extract inflorescence to reproductive growth transition and be actually difficult to avoid that from nutrient growth Waste part nutrition.
The prior art has the individually report using naphthaleneacetamide or 6- benzyl aminoadenine, but it is needed with stronger acidity Solution or alkaline solution dissolution, have the defects that operation risk is high;And exclusive use naphthaleneacetamide or 6- benzyl amino gland are fast When purine is as Flower thinning agent, Radix Salviae Miltiorrhizae flowering rate and percentage of fertile fruit decline degree be not high.
Summary of the invention
Technical problem to be solved by the present invention lies in overcome in the prior art individually using naphthaleneacetamide need with compared with Strong acid solution or alkaline solution dissolution, and Radix Salviae Miltiorrhizae flowering rate high there are operation risk and percentage of fertile fruit decline degree are not High disadvantage provides a kind of Radix Salviae Miltiorrhizae flower thinning composition, preparation method and application method.Radix Salviae Miltiorrhizae flower thinning composition of the invention exists While flower thinning, damage of the flower thinning component to Radix Salviae Miltiorrhizae plant leaf can be effectively avoided, medicinal material effective component can be significantly improved and contained Amount;The composition significantly improves Radix Salviae Miltiorrhizae flower thinning operational security and working efficiency, and use is safe, and production cost is low, is suitble to work Industryization is promoted.
The present invention is to solve above-mentioned technical problem by the following technical programs:
The present invention provides a kind of Radix Salviae Miltiorrhizae flower thinning compositions comprising the component of following mass percents: ferrous sulfate 55%~60%, calcium formate 17%~22%, naphthaleneacetamide 0.8%~3% and 6- benzyl aminoadenine 20%~25%.
In the present invention preferably, the Radix Salviae Miltiorrhizae flower thinning composition is grouped as by the group of following mass percents: sulfuric acid is sub- Iron 55%~60%, calcium formate 17%~22%, naphthaleneacetamide 0.8%~3% and 6- benzyl aminoadenine 20%~25%.
Wherein, the mass percent of the ferrous sulfate is preferably 56%.
Wherein, the mass percent of the calcium formate is preferably 20%.
Wherein, the mass percent of the naphthaleneacetamide is preferably 1%.
Wherein, the mass percent of the 6- benzyl aminoadenine is preferably 23%.
It can also include other conventional constituents of this field in Radix Salviae Miltiorrhizae flower thinning composition of the invention, as long as not significant shadow Ring the performance of the Radix Salviae Miltiorrhizae flower thinning composition.
The present invention also provides the preparation methods of above-mentioned Radix Salviae Miltiorrhizae flower thinning composition comprising following step: by the sulphur Sour ferrous iron, calcium formate, naphthaleneacetamide and 6- benzyl aminoadenine are uniformly mixed according to a ratio.
Wherein, the mixing preferably carries out in Multifunctional mixer;The mixed time is preferably 25 ~35min.
It is described after mixing, be preferably dispensed into black hermetic bag.
The present invention also provides the application methods of the Radix Salviae Miltiorrhizae flower thinning composition comprising following step: will be described After Radix Salviae Miltiorrhizae flower thinning composition is dissolved in water, it is sprayed on Radix Salviae Miltiorrhizae plant top in flowering stage, is added after 14~16 days primary.
Wherein, the mass ratio of the Radix Salviae Miltiorrhizae flower thinning composition and water is preferably 1:900~1100, is more preferably 1: 1000。
In the present invention, the flowering stage generally refers to the first tenday period of a month in May (1~10 day).
Wherein, the time sprayed preferably avoids 5 points~8 points of morning (dew is not dry), afternoon~14 at 11 points Point (high temperature) and (easily get damp) these three periods after 18 points at dusk, be more preferably at 9 points in the morning, at 10 points in the morning, at 4 points in afternoon or At 5 points in afternoon.
On the basis of common knowledge of the art, above-mentioned each optimum condition, can any combination to get each preferable reality of the present invention Example.
The reagents and materials used in the present invention are commercially available.
The positive effect of the present invention is that:
(1) flower thinning composition of the invention effectively avoids flower thinning component to the damage of Radix Salviae Miltiorrhizae plant leaf while flower thinning Evil;Up to 50% or more, percentage of fertile fruit declines up to 60% or more the decline of Radix Salviae Miltiorrhizae flowering rate;
(2) flower thinning composition of the invention significantly improves Radix Salviae Miltiorrhizae flower thinning operational security and working efficiency, and use is safe;
(3) flower thinning composition of the invention can significantly improve medicinal material active constituent content, and tanshinone content reaches in medicinal material 0.33% or more, content of danshinolic acid B is up to 4% or more;
(4) use cost is cheap, and Radix Salviae Miltiorrhizae flower thinning only needs 15-20 first per acre, is suitble to industrialization promotion.
Specific embodiment
The present invention is further illustrated below by the mode of embodiment, but does not therefore limit the present invention to the reality It applies among a range.In the following examples, the experimental methods for specific conditions are not specified, according to conventional methods and conditions, or according to quotient The selection of product specification.
In following embodiments, such as indicated without special, percentage each means mass percent.
Embodiment 1
In the present embodiment, flower thinning composition be include ferrous sulfate 56%, calcium formate 20%, naphthaleneacetamide 1%, 6- Benzyl aminoadenine 23%.Preparation step are as follows: by commercial sulfuric acid ferrous iron, calcium formate, naphthaleneacetamide, 6- benzyl aminoadenine, press Said ratio weighs, and is put into after mixing 30 minutes in Multifunctional mixer, is dispensed into 20g black hermetic bag.
Embodiment 2
In the present embodiment, flower thinning composition be include ferrous sulfate 55%, calcium formate 22%, naphthaleneacetamide 3%, 6- Benzyl aminoadenine 20%.Preparation step are as follows: by commercial sulfuric acid ferrous iron, calcium formate, naphthaleneacetamide, 6- benzyl aminoadenine, press Said ratio weighs, and is put into after mixing 25 minutes in Multifunctional mixer, is dispensed into 20g black hermetic bag.
Embodiment 3
In the present embodiment, flower thinning composition be include ferrous sulfate 60%, calcium formate 17%, naphthaleneacetamide 3%, 6- Benzyl aminoadenine 20%.Preparation step are as follows: by commercial sulfuric acid ferrous iron, calcium formate, naphthaleneacetamide, 6- benzyl aminoadenine, press Said ratio weighs, and is put into after mixing 35 minutes in Multifunctional mixer, is dispensed into 20g black hermetic bag.
Embodiment 4
In the present embodiment, flower thinning composition be include ferrous sulfate 55%, calcium formate 19.2%, naphthaleneacetamide 0.8%, 6- benzyl aminoadenine 25%.Preparation step are as follows: by commercial sulfuric acid ferrous iron, calcium formate, naphthaleneacetamide, 6- benzyl amino gland Purine is weighed by said ratio, is put into after mixing 35 minutes in Multifunctional mixer, is dispensed into 20g black hermetic bag.
The flower thinning effect of 5 flower thinning composition of embodiment
Using the flower thinning composition of embodiment 1, application method are as follows: now a small amount of clear water of flower thinning composition is dissolved, then Be diluted with water to 1000 times, then sufficiently shake up, in flowering stage, i.e. the first tenday period of a month in May, avoid 5 points~8 dew of morning it is not dry, in 18 points of 11 points~14 high temperature of noon and dusk get damp 3 stages later, and 9 points of the morning are sprayed on Radix Salviae Miltiorrhizae plant top.It is mended after 15 days It applies primary.
After the flower thinning composition, Radix Salviae Miltiorrhizae flowering rate and percentage of fertile fruit decline 72.2% and 82.4% respectively.Use the group After closing object, there is mottled wilting in only a few young leaflet tablet;It can restore normal growth after a period of time.By " Chinese Pharmacopoeia " Radix Salviae Miltiorrhizae Method under content determination item, measuring tanshinone content in institute's output red rooted salvia is 0.47%, content of danshinolic acid B 6.32%.
The flower thinning effect of 6 flower thinning composition of embodiment
Using the flower thinning composition of embodiment 2, application method are as follows: now a small amount of clear water of flower thinning composition is dissolved, then It is diluted with water to 900 times, then sufficiently shakes up, in flowering stage, i.e. the first tenday period of a month in May, avoid that 5 points~8 dew of morning are dry, noon 18 points of 11 points~14 high temperature and dusk get damp 3 stages later, and 10 points of the morning are sprayed on Radix Salviae Miltiorrhizae plant top.It is added after 14 days Once.
After the flower thinning composition, Radix Salviae Miltiorrhizae flowering rate and percentage of fertile fruit decline 59.8% and 66.7% respectively.Use the group After closing object, there is mottled wilting in only a few young leaflet tablet, and most wilting blades restore normal growth.By " Chinese Pharmacopoeia " Radix Salviae Miltiorrhizae Method under content determination item, measuring tanshinone content in institute's output red rooted salvia is 0.41%, content of danshinolic acid B 5.22%.
The flower thinning effect of 7 flower thinning composition of embodiment
Using the flower thinning composition of embodiment 3, application method are as follows: now a small amount of clear water of flower thinning composition is dissolved, then Be diluted with water to 1100 times, then sufficiently shake up, in flowering stage, i.e. the first tenday period of a month in May, avoid 5 points~8 dew of morning it is not dry, in 18 points of 11 points~14 high temperature of noon and dusk get damp 3 stages later, and at 4 points in afternoon is sprayed on Radix Salviae Miltiorrhizae plant top.It is mended after 16 days It applies primary.
After the flower thinning composition, Radix Salviae Miltiorrhizae flowering rate and percentage of fertile fruit decline 60.3% and 69.5% respectively.Use the medicine After agent, there is mottled wilting, yellow in a small number of young leaflet tablets;After a period of time, most wilting blades restore normal growth.It presses Method under " Chinese Pharmacopoeia " Radix Salviae Miltiorrhizae content determination item, measuring tanshinone content in institute's output red rooted salvia is 0.42%, tanshin polyphenolic acid B Content is 4.89%.
The flower thinning effect of 8 flower thinning composition of embodiment
Using the flower thinning composition of embodiment 4, application method are as follows: now a small amount of clear water of flower thinning composition is dissolved, then Be diluted with water to 1000 times, then sufficiently shake up, in flowering stage, i.e. the first tenday period of a month in May, avoid 5 points~8 dew of morning it is not dry, in 18 points of 11 points~14 high temperature of noon and dusk get damp 3 stages later, and at 5 points in afternoon is sprayed on Radix Salviae Miltiorrhizae plant top.It is mended after 15 days It applies primary.
After the flower thinning composition, Radix Salviae Miltiorrhizae flowering rate and percentage of fertile fruit decline 51.4% and 63.1% respectively.Use the medicine After agent, there is mottled wilting, yellow in a small number of young leaflet tablets;After a period of time, most wilting blades restore normal growth.It presses Method under " Chinese Pharmacopoeia " Radix Salviae Miltiorrhizae content determination item, measuring tanshinone content in institute's output red rooted salvia is 0.33%, tanshin polyphenolic acid B Content is 4.07%.
Comparative example 1
In the comparative example, flower thinning object is naphthaleneacetamide.Preparation step are as follows: by commercially available naphthaleneacetamide, it is black to be dispensed into 0.2g In color hermetic bag.
Its application method are as follows: now by a small amount of acid leach solution of flower thinning object, add water and be diluted to 100000 times, then fill Divide and shake up, in flowering stage, i.e. the first tenday period of a month in May, avoids not dry 5 points~8 dew of morning, 11 points~14 high temperature of noon and dusk 18 Point gets damp 3 stages later, and 9 points of the morning are sprayed on Radix Salviae Miltiorrhizae plant top.It is added after 15 days primary.
After the flower thinning object, Radix Salviae Miltiorrhizae flowering rate and percentage of fertile fruit decline 22.7% and 28.1% respectively.After the medicament, Leaf growth is vigorous, does not generate obvious yellow wilting phenomenon.By method under " Chinese Pharmacopoeia " Radix Salviae Miltiorrhizae content determination item, institute is measured Tanshinone content is 0.37% in output red rooted salvia, content of danshinolic acid B 4.26%.
Comparative example 2
In the comparative example, flower thinning object is 6- benzyl aminoadenine.Preparation step are as follows: by commercially available 6- benzyl aminoadenine, It is dispensed into 0.2g black hermetic bag.
Its application method are as follows: now by a small amount of acid leach solution of flower thinning object, add water and be diluted to 4300 times, then sufficiently It shakes up, in flowering stage, i.e. the first tenday period of a month in May, avoids 18 points of not dry 5 points~8 dew of morning, 11 points~14 high temperature of noon and dusk It gets damp 3 stages later, 9 points of the morning are sprayed on Radix Salviae Miltiorrhizae plant top.It is added after 15 days primary.
After the flower thinning object, Radix Salviae Miltiorrhizae flowering rate and percentage of fertile fruit decline 19.7% and 31.4% respectively.After the medicament, Leaf growth is vigorous, does not generate obvious yellow wilting phenomenon.By method under " Chinese Pharmacopoeia " Radix Salviae Miltiorrhizae content determination item, institute is measured Tanshinone content is 0.38% in output red rooted salvia, content of danshinolic acid B 4.09%.

Claims (11)

1. a kind of Radix Salviae Miltiorrhizae flower thinning composition comprising the component of following mass percents: ferrous sulfate 55%~60%, calcium formate 17%~22%, naphthaleneacetamide 0.8%~3% and 6- benzyl aminoadenine 20%~25%.
2. Radix Salviae Miltiorrhizae flower thinning composition as described in claim 1, which is characterized in that the Radix Salviae Miltiorrhizae flower thinning composition is by following matter The group of amount percentage is grouped as: ferrous sulfate 55%~60%, calcium formate 17%~22%, naphthaleneacetamide 0.8%~3% and 6- Benzyl aminoadenine 20%~25%.
3. Radix Salviae Miltiorrhizae flower thinning composition as described in claim 1, which is characterized in that the mass percent of the ferrous sulfate is 56%;
And/or the mass percent of the calcium formate is 20%;
And/or the mass percent of the naphthaleneacetamide is 1%;
And/or the mass percent of the 6- benzyl aminoadenine is 23%.
4. a kind of preparation method of Radix Salviae Miltiorrhizae flower thinning composition according to any one of claims 1 to 3 comprising Xia Shubu It is rapid: the ferrous sulfate, the calcium formate, the naphthaleneacetamide and the 6- benzyl aminoadenine are mixed according to the ratio It closes uniform.
5. preparation method as claimed in claim 4, which is characterized in that described being blended in Multifunctional mixer carries out.
6. preparation method as claimed in claim 4, which is characterized in that the mixed time is 25~35min.
7. a kind of application method of Radix Salviae Miltiorrhizae flower thinning composition according to any one of claims 1 to 3 comprising Xia Shubu It is rapid: after the Radix Salviae Miltiorrhizae flower thinning composition is dissolved in water, to be sprayed on Radix Salviae Miltiorrhizae plant top in flowering stage, added after 14~16 days Once.
8. application method as claimed in claim 7, which is characterized in that the mass ratio of the Radix Salviae Miltiorrhizae flower thinning composition and water is 1:900~1100.
9. application method as claimed in claim 8, which is characterized in that the mass ratio of the Radix Salviae Miltiorrhizae flower thinning composition and water is 1:1000。
10. application method as claimed in claim 7, which is characterized in that the time sprayed is to avoid morning~8 at 5 points Point, afternoon 11 points~14 points and at dusk 18 points these three later periods.
11. application method as claimed in claim 10, which is characterized in that the time sprayed is at 9 points in the morning, the morning 10 Point, at 4 points in afternoon or at 5 points in afternoon.
CN201610711365.4A 2016-08-23 2016-08-23 A kind of Radix Salviae Miltiorrhizae flower thinning composition, preparation method and application method Active CN106305776B (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102438450A (en) * 2009-04-07 2012-05-02 塔明克股份有限公司 Thinning agent
CN104725099A (en) * 2013-12-18 2015-06-24 天津市北方创业园林股份有限公司 Garden and park plant growth regulator and use method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102438450A (en) * 2009-04-07 2012-05-02 塔明克股份有限公司 Thinning agent
CN104725099A (en) * 2013-12-18 2015-06-24 天津市北方创业园林股份有限公司 Garden and park plant growth regulator and use method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
枇杷(Eriobotrya japonica Lindl.)花芽生理分化期6-BA处理对其生理生化的影响;董新龙;《福建农林大学硕士学位论文》;20010501;摘要,第32-32页

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