CN106281718A - The way of distillation extracts the method for Flos Rosae Rugosae quintessence oil from Cymbopogon martini - Google Patents

The way of distillation extracts the method for Flos Rosae Rugosae quintessence oil from Cymbopogon martini Download PDF

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Publication number
CN106281718A
CN106281718A CN201610924772.3A CN201610924772A CN106281718A CN 106281718 A CN106281718 A CN 106281718A CN 201610924772 A CN201610924772 A CN 201610924772A CN 106281718 A CN106281718 A CN 106281718A
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cymbopogon martini
quintessence oil
broken
cymbopogon
martini
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黄全
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses the method that the way of distillation extracts Flos Rosae Rugosae quintessence oil from Cymbopogon martini, medicines and health protection technical field, be to solve shortage and the purity problem of Flos Rosae Rugosae quintessence oil, mainly take below step to carry out: one, raw material used: Cymbopogon martini includes stem, leaf, flower;Two, instrument used: cut up with a hay cutter broken machine, distillation column, steam transmitting pipe, cooling tank, filling bottle;Three, the Cymbopogon martini cut off is cleaned up rear air dry to be dried;Four, with hand hay cutter broken machine, Cymbopogon martini hand hay cutter is broken into broken section of stalk length≤2cm;Five, put the Cymbopogon martini after broken for hand hay cutter into distillation column and carry out steam distillation, 120 DEG C >=vapo(u)rizing temperature >=100 DEG C;Six, the mixing gas distilled out is delivered directly to cooling tank ,-5 DEG C≤chilling temperature < 0 DEG C by steam transmitting pipe, and pressurized liquefied, in liquid, high precipitation ice cube, obtains Cymbopogon martini quintessence oil;Seven, filling bottle under Cymbopogon martini quintessence oil low temperature is sealed lid ,-5 DEG C≤filling bottle temperature < 0 DEG C.

Description

The way of distillation extracts the method for Flos Rosae Rugosae quintessence oil from Cymbopogon martini
Technical field
The method that the present invention relates to extract Flos Rosae Rugosae quintessence oil from Cymbopogon martini, belongs to pharmaceutical technology field.
Background technology
Cymbopogon martini another name Martin's perfume, India's Flos Pelargonii, Luo Sha, plant classification: grass family, Cymbopogon;Plant variety: Flos Rosae Rugosae Grass has two kinds: the Dalmatia that rubs (Motia) and Sophia (Sofia).Their growing environment all differs with latitude, Mo Diya Cymbopogon martini whether quintessence oil quality and abnormal smells from the patient all slightly better than Sophia.Main product ground: Madagascar, Brazil, India, print Degree Nicaea, Pakistan etc..Characteristic, abnormal smells from the patient: yellowish or yellow green, the sweet fragrance of a flower, slightly Radix Glycyrrhizae taste, and indistinctly give out Dense rose scent and gain the name.
Cymbopogon martini is close from type perennial herb for hanging down loosely shape.The plant of same genus with Radix Cymbopogonis Citrati, Herba Cymbopogonis Citrari, plant height up to 2m, shallow root system.Stem is sturdy, has lateral bud, and basal internode is short.Sheath surface is green or faint yellow;Blade bar shaped, long ribbon shape, it is about 100cm, wide about 3cm, tip is sharp-pointed, edge tool serration.Inflorescence is to form umbrella compound inflorescence by paired total shape flower, is born in stem Top;Raceme is made up of paired small ear;Small ear has handle or stockless, yellow;Grow small wooden raft, each 1 of lemma in flower tool, stamen 3, gynoecium 1 plumose stigma, 2 split.
Cymbopogon martini is by with extracting Flos Rosae Rugosae quintessence oil costly.The palmarosa oil of Sophia sometimes referred to as gingergrass oil, its The content of geraniol is relatively low.Once in a while, the palmarosa oil of Sophia also can be supported by the arm in the dike Asia palmarosa oil that preferably rubs, local Businessman can lean on clap the hands with bottle evaluate oil quality.If after rocking, it is the rapidest that the bubble in oil rises to surface Disappearing, this bottle of oil is exactly the oil of normal (without adulterated).The exporter in Bombay then evaluates oil with the test of simple solubility Quality.Cisse that also produces Cymbopogon martini, and its lighter odor is soft.The palmarosa oil that is produced from Java has then carried fruit fragrant.Most Flos Rosae Rugosae Grass oil export, to American-European and Japanese, in order to manufacture soap, cosmetics, perfume, is even added in Nicotiana tabacum L. to increase local flavor.
Cymbopogon martini effect: antibacterial, antiviral, sterilize, promote cell regeneration, brings down a fever;Soul curative effect: emotion is had peace Comfort effect, but also have the effect improved simultaneously.It is said that people's six roots of sensation can also be made quiet, fresh and new;Health curative effect: to body temperature mistake Height seems the most helpful, because Cymbopogon martini can play the effect of cooling.This function improves the effect of its antiviral, because carefully Bacterium the most relatively inactivity.
Cymbopogon martini is also the tonic of digestive system, has the function of suppression to the microorganism of enteral of living away from home or pathogen, is suffering from Can use when suffering from dysentery.It addition, it also can strengthen the muscle of coat of the stomach.The effect stimulating appetite contributes to nervous anorexia Patient, and the impact in front can be brought to emotion.According to " quintessence oil " book of Gu Ende (Guenther), it is understood that Rhizoma Zingiberis Recens is careless Oil can alleviate the stiff of joint, and its palmarosa oil in close relations should also have identical effect.Cymbopogon martini skin curative effect: Recover the state of moisturizing, stimulate the secretion of natural sebum, it can thus be appreciated that dry skin is necessarily very helpful by it.Can promote Reepithelialization, general problems with skin infections also can process with Cymbopogon martini.The little microgroove on skin and neck can also be smoothed Wrinkle on son.Owing to Cymbopogon martini quintessence oil has pleasant taste and special effect, therefore it is frequently added various cream product In.
Cymbopogon martini is by with extracting Flos Rosae Rugosae quintessence oil costly.Cymbopogon martini quintessence oil major part originates from Tropical Africa, motor adds this Add, Indonesia, the ground such as Brazil and Comoro Islands, whole world annual production about 50 ~ 60t.Palmarosa oil (Palmarosa Oil) obtained through water distillation by the stem and leaf of Cymbopogon martini motia kind, for light yellow to yellow-green liquid, have fragrant and sweet Flos Rosae Rugosae taste, The fragrance of a flower slightly lemon.The meaning of " Motia " is precious, is real Cymbopogon martini quintessence oil.It is dissolved in most of nonvolatile oil And propylene glycol.It is practically insoluble in glycerol.When holding in mineral oil, be generally creamy white muddiness.
Cymbopogon martini quintessence oil has strong fragrant and sweet, and the fragrance as Geranium Essential, is the most comprehensive a kind of sweet taste With the compound fragrance of Flos Rosae Rugosae, and slightly aftertaste as band point earth.Its soft and speciality does not has Flos Rosae Rugosae quintessence oil the most obvious, its taste Road, before the breath of Flos Rosae Rugosae quintessence oil and Geranium Essential, gives the effect rousing oneself and refreshing oneself.
Cymbopogon martini quintessence oil has sterilization and refreshing and other physiological function, can be as antidepressant, antibacterial, anticorrosion Agent, wound healing medicine, anthelmintic (internal), stimulate blood circulation, anti-anemia action agent, digestant, antirheumatic, antitoxin agent, Analeptic, cleanser, nourishing agent etc..
In Ayurvedic medicine, using the long history of Cymbopogon martini, its stem, leaf have the merits such as antibacterium, antifungal, anticorrosion Effect.Effective in treatment infectious disease and aspect of bringing down a fever especially.When body heat, it can help to reduce body temperature and bring down a fever, so Increase its antibacterial action.
It has stimulates and adjusts the effect along whole body system, is also strong fungicide and disinfectant.It kills as digestive system Microbial inoculum and reinforcing agent, have the strongest killing action to the pathogen in rimmer knife microorganism, can kill large intestine bar in 5 minutes Bacterium.
Cymbopogon martini quintessence oil is well suited for for maintenance skin, and it has moisturizing and the secretion naturally stimulating sebum, recovers water The function of balance-dividing, is highly profitable to drying property skin.Owing to Cymbopogon martini quintessence oil has pleasant taste and special effect, because of This often adds it in hand cream, moisturizing emulsion and other various skin care products.
Summary of the invention
In order to extract Cymbopogon martini quintessence oil with satisfied medicine, the healthcare field demand to Cymbopogon martini quintessence oil, my invention A kind of method extracting Herba Verbenae quintessence oil from Cymbopogon martini, this method is extracted simple, and processing is simple, and small investment brings notable results, carries Taking rate high, the Cymbopogon martini quintessence oil purity of extraction is high, the property of medicine is powerful efficiently.
The way of distillation is extracted the method solution problem of Flos Rosae Rugosae quintessence oil from Cymbopogon martini and is adopted the technical scheme that by following Step is carried out: one, raw material used: Cymbopogon martini includes stem, leaf, flower;Two, instrument used: cut up with a hay cutter broken machine, distillation column, steam transmitting pipe, Cooling tank, filling bottle;Three, the Cymbopogon martini cut off is cleaned up rear air dry to be dried;Four, with hand hay cutter broken machine, Cymbopogon martini hand hay cutter is broken into stalk Broken section of length≤2cm;Five, put the Cymbopogon martini after broken for hand hay cutter into distillation column and carry out steam distillation, 120 DEG C >=vapo(u)rizing temperature >= 100 DEG C, at the bottom of boiler, moisture to be kept, raw material can not touch the bottom of a pan, are charred in order to avoid producing, and vegetables pine is wanted in centre, it is simple to bottom airflow Rise;Six, the mixing gas distilled out is delivered directly to cooling tank ,-5 DEG C≤chilling temperature < 0 DEG C, pressurization by steam transmitting pipe Liquefaction, in liquid, high precipitation ice cube, obtains Cymbopogon martini quintessence oil;Seven, filling bottle under Cymbopogon martini quintessence oil low temperature is sealed lid ,-5 DEG C ≤ filling bottle temperature < 0 DEG C.
Processing Flos Rosae Rugosae quintessence oil: use water distillating method.During harvesting Cymbopogon martini, stem and leaf to be gathered all is dried and (about receives After cutting one week), the refined oil rate now extracted is the highest.During distillation, Cymbopogon martini stem and leaf can cut or without cut off, and puts into steamer In, during charging, the edge of pot is preferably tight, and middle part is the most loose.After often steaming 3 ~ 4 rice steamers, water should be changed 1 time.
Pick and process, the growth of Cymbopogon martini is similar to Radix Cymbopogonis Citrati, gathers in before usual florescence.The number of times of annual harvesting, Different because of its strain age and place of production weather difference.Typically can gather in every year 3 ~ 4 times.Gather in and appropriate to the occasion carry out after fine day dew is dry, cloudy It is low that rainy day gathers in its oil content.Harvesting position never should be opened at neat root and cut more than its sheath at 2 ~ 3cm;Cutter requires sharp, To alleviate the impact on root, in order to regeneration.
The way of distillation is extracted the method for Flos Rosae Rugosae quintessence oil from Cymbopogon martini and is provided the benefit that: the way of distillation extracts rose from Cymbopogon martini The method of rare quintessence oil is using Cymbopogon martini as extracting raw material, and dried by air dry, only work simply cuts up with a hay cutter broken processing and just can put steaming into Evaporate tower to carry out heating distillation extraction;The method extracting Flos Rosae Rugosae quintessence oil from Cymbopogon martini make use of Flos Rosae Rugosae quintessence oil composition contained by Herba Verbenae It is prone to the feature of volatilization, evaporates together with water vapour and be sent to cooling tank by steam transmitting pipe, liquefy after being cooled down by high pressure;Utilize again Flos Rosae Rugosae quintessence oil is different from water-cooled solidification temperature, is all separated out by the moisture in mixed vapour, obtain high-purity in cooling tower The Flos Rosae Rugosae quintessence oil of degree.
Detailed description of the invention
Embodiment.The way of distillation is extracted the method for Flos Rosae Rugosae quintessence oil from Cymbopogon martini and is carried out by below step: one, used Raw material: Cymbopogon martini includes stem, leaf, flower;Two, instrument used: cut up with a hay cutter broken machine, distillation column, steam transmitting pipe, cooling tank, filling bottle;Three, The Cymbopogon martini cut off cleans up rear air dry be extremely dried, preferably to cut during harvesting to root two leaf with upper bit, beneficially root Regeneration, is also beneficial to extract the quality of Flos Rosae Rugosae quintessence oil;Four, with hand hay cutter broken machine, Cymbopogon martini hand hay cutter is broken into broken section of stalk length≤2cm;Five, Cymbopogon martini after broken for hand hay cutter is put into distillation column carries out steam distillation, 120 DEG C >=vapo(u)rizing temperature >=100 DEG C, to protect at the bottom of boiler Water holding divides, raw material can not touch the bottom of a pan, is charred in order to avoid producing, and vegetables pine is wanted in centre, and surrounding can be compacted, it is simple to bottom airflow rises;Six, The mixing gas distilled out is delivered directly to cooling tank by steam transmitting pipe, and-5 DEG C≤chilling temperature < 0 DEG C is pressurized liquefied, liquid Middle high precipitation ice cube, obtains Cymbopogon martini quintessence oil;Seven, filling bottle under Cymbopogon martini quintessence oil low temperature is sealed lid ,-5 DEG C≤filling bottle Temperature < 0 DEG C.

Claims (1)

1. the method that the way of distillation extracts Flos Rosae Rugosae quintessence oil from Cymbopogon martini, is characterized in that carrying out by below step: one, used former Material: Cymbopogon martini includes stem, leaf, flower;Two, instrument used: cut up with a hay cutter broken machine, distillation column, steam transmitting pipe, cooling tank, filling bottle;Three, will The Cymbopogon martini cut off cleans up rear air dry and is dried;Four, with hand hay cutter broken machine, Cymbopogon martini hand hay cutter is broken into broken section of stalk length≤2cm;Five, Cymbopogon martini after broken for hand hay cutter is put into distillation column carries out steam distillation, 120 DEG C >=vapo(u)rizing temperature >=100 DEG C, to protect at the bottom of boiler Water holding divides, raw material can not touch the bottom of a pan, is charred in order to avoid producing, and vegetables pine is wanted in centre, it is simple to bottom airflow rises;Six, distill out is mixed Closing gas and be delivered directly to cooling tank ,-5 DEG C≤chilling temperature < 0 DEG C by steam transmitting pipe, pressurized liquefied, in liquid, height separates out ice Block, obtains Cymbopogon martini quintessence oil;Seven, filling bottle under Cymbopogon martini quintessence oil low temperature is sealed lid ,-5 DEG C≤filling bottle temperature < 0 DEG C.
CN201610924772.3A 2016-10-30 2016-10-30 The way of distillation extracts the method for Flos Rosae Rugosae quintessence oil from Cymbopogon martini Withdrawn CN106281718A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106675787A (en) * 2017-01-29 2017-05-17 毛华养 Method for extracting eucalyptus essential oil by distillation method

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CN103897807A (en) * 2014-04-24 2014-07-02 四川银谷玫瑰科技有限公司 Method for extracting rose essential oil
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CN101538510A (en) * 2009-05-04 2009-09-23 中国科学院植物研究所 Plant volatile oil extractor and application thereof
CN101619273A (en) * 2009-07-17 2010-01-06 张庆源 Method for extracting essential oil from natural essential oil residues
CN103897807A (en) * 2014-04-24 2014-07-02 四川银谷玫瑰科技有限公司 Method for extracting rose essential oil
CN105779131A (en) * 2016-05-06 2016-07-20 遵义医学院 Method for extracting essential oil from citrus peels

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106675787A (en) * 2017-01-29 2017-05-17 毛华养 Method for extracting eucalyptus essential oil by distillation method

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Application publication date: 20170104