CN106265431B - A kind of skin care item and preparation method thereof with oil-control - Google Patents

Abstract

The present invention provides a kind of skin care item and preparation method thereof with oil-control, the skin care item include each component of following mass parts: 0.2-12 parts of oil-control composition, 2.0~8.0 parts of C12-15 alcohol benzoic ether, 20.6~52.6 parts of ring five dimethyl silicone polymer, 0.1~0.5 part of tocopherol acetate, 0.2~0.8 part of distearyl dimethylammonium hectorite, 1.0~5.0 parts of octyl polymethyl siloxane, 5.0~20.0 parts of diphenyl dimethicone；Wherein, the oil-control composition includes each component that shared mass parts are following in skin care item: 0.2~1.0 part of the royal jelly oil-control factor, silica 1 .0~5.0 part, 1.0~3.0 parts of methyl methacrylate, 1.0~3.0 parts of octyl butanedioic acid aluminium starch.Skin care item provided by the invention have the characteristics that oil-control effect it is good, using feel all right, be not in use process rub with the hands mud phenomenon.

Description

A kind of skin care item and preparation method thereof with oil-control

Technical field

The invention belongs to cosmetic technical fields, in particular to a kind of to have effects that the skin care item of oil-control and its preparation side Method.

Background technique

The secreting function of the people of Oily, sebaceous glands are more vigorous, and Oily was precisely due to skin oil and fat was secreted Caused by more, facial perception is greasy, not easy to clean, and have an impact the glossy of beauty, and be easy to cause clogging of pores, pore thick Greatly, the skin problems such as long acne.The fuel-displaced, composition of change sebaceous glands of excessive secretion, reduction etc. for controlling sebaceous glands is this kind of skin It keeps fit, beautiful key.

In order to control or regulate sebum secretion, product in the market reaches somewhat by addition various plants extract etc. The purpose of oil-control, but its oil-control effect is often unobvious, or need to be used for a long time and could embody, and need to add into formula system Entering Determination of Preservatives can be only achieved preferable anti-corrosion effect, guarantee the stability of product quality, due to the introducing of preservative etc., often Product is caused to there are the ill-effects such as stimulation to skin.In addition, there are also products to pass through addition silica, nylon in the market Powder, boron nitride powder, talcum, polymethyl methacrylate etc. reach oil-control purpose, but reach ideal oil-control effect, Additive amount needed for these components is often bigger, and is easy to appear rubs mud phenomenon with the hands in use, and use feeling is bad, And influence beautiful and oil-control effect performance.

In addition, current oil-control product, often has a single function, the more polynary skin care needs of consumer are unable to satisfy, and It is very easy to permeability, layering, thinning equistability problem occur.In the prior art, cosmetic art engineer allows to reach Product is while having Controlling oil effect, moreover it is possible to have other skin-care effects, formula system be often difficult to hold, effect, Product stability, product irritation etc. are difficult to take into account.

Summary of the invention

The present invention is to make up the deficiencies in the prior art, and it is good to provide a kind of oil-control effect, using feeling all right, in use process not It will appear the skin care item for rubbing mud phenomenon with the hands.

The present invention be reach its purpose, the technical solution adopted is as follows:

It is a kind of to have effects that the skin care item of oil-control, each component including following mass parts: 0.2-12 parts of oil-control composition, 2.0~8.0 parts of C12-15 alcohol benzoic ether, 20.6~52.6 parts of ring five dimethyl silicone polymer, tocopherol acetate 0.1~ 1.0 parts, 0.2~0.8 part of distearyl dimethylammonium hectorite, 1.0~5.0 parts of octyl polymethyl siloxane, the poly- diformazan of diphenyl 5.0~20.0 parts of radical siloxane；

Wherein, the oil-control composition includes each component that shared mass parts are following in skin care item: royal jelly oil-control because 0.2~1.0 part of sub (Acnacidol), silica 1 .0~5.0 part, 1.0~3.0 parts of methyl methacrylate, octyl amber 1.0~3.0 parts of sour aluminium starch.

In formula system of the invention, pass through the royal jelly oil-control factor, silica, methyl methacrylate, octyl amber Amber acid aluminium four kinds of component combination collocations of starch assign the extraordinary oil-control effect of product, can adsorb on skin to a greater extent The excess oil and sweat of secretion, bellding light, the colour of skin be not natural for another skin；Although and make in product added with grease at Point, but greasy feeling will not be generated when use, with rear dry and comfortable；Due to the ingenious collocation of these components, organically combined physics and Chemical oil-control assigns product instant and long-acting oil-control effect.

It preferably, further include each component of following mass parts: 1.0~5.0 parts of ethylhexyl methoxy cinnamate, nanoscale 0.5~5.0 part of titanium dioxide dispersion pulp, using the preferred embodiment, physical sunscreen and chemical sunscreen are organically combined, can allow product With preferable sun-proof isolation effect.

It preferably, further include 1.0~3.0 mass parts of apple seed extract, dimethyl silicone polymer/vinylpolydimethyl 5.0~20.0 mass parts of Dimethicone Crosspolymer, 5.0~35.0 mass parts of Dimethicone Crosspolymer, this is excellent Scheme is selected, so that product is in use, not only wrinkle can be filled with physics, but also the generation of wrinkle can be inhibited, reach Instant and long-acting crease-resistant tightening effect.

More preferably, the skin care item by following mass parts each component: ethylhexyl methoxy cinnamate 1.0~ 5.0 parts, 2.0~8.0 parts of C12-15 alcohol benzoic ether, 20.6~52.6 parts of ring five dimethyl silicone polymer, tocopherol acetate 0.1~1.0 part, 0.2~1.0 part of the royal jelly oil-control factor (Acnacidol), 1.0~3.0 parts of apple seed extract, distearyl 0.2~0.8 part of dimethylammonium hectorite, silica 1 .0~5.0 part, 1.0~3.0 parts of methyl methacrylate, octyl amber 1.0~3.0 parts of sour aluminium starch, 0.5~5.0 part of Nano titanium dioxide dispersion pulp, 1.0~5.0 parts of octyl polymethyl siloxane, 5.0~20.0 parts of diphenyl dimethicone, Dimethicone/Vinyl Dimethicone cross-linked polymer 5.0~20.0 parts, 5.0~35.0 parts of Dimethicone Crosspolymer.The optimization formula, to be entirely free of the non-of moisture Water prescription system, product is not necessarily to add moisture completely, and without adding any preservative, stable product quality is good, safety Property is high, non-stimulated to skin, has no toxic side effect, is applicable to sensitive people and the elderly.The product not only has very well Oil-control effect, and sun-proof, crease-resistant tightening effect is good, is a kind of multiple-effect unification product, good using rear skin sense, non-greasy is in Existing dry and comfortable natural beige.In use, the product use feeling is very good, without any stranding mud phenomenon, and does not seep Oil, layering and it is thinning phenomena such as.

Second aspect of the present invention provides a kind of preparation method with the skin care item of oil-control, which is characterized in that including Following steps:

1) each component is weighed according to formula, the formula includes each component of following mass parts: methoxy cinnamic acid ethyl 1.0~5.0 parts of own ester, 2.0~8.0 parts of C12-15 alcohol benzoic ether, 20.6~52.6 parts of ring five dimethyl silicone polymer, fertility 0.1~1.0 part of phenol acetic acid esters, 0.2~1.0 part of the royal jelly oil-control factor, 1.0~3.0 parts of apple seed extract, distearyl diformazan 0.2~0.8 part of ammonium hectorite, silica 1 .0~5.0 part, 1.0~3.0 parts of methyl methacrylate, octyl butanedioic acid aluminium 1.0~3.0 parts of starch, 0.5~5.0 part of Nano titanium dioxide dispersion pulp, 1.0~5.0 parts of octyl polymethyl siloxane, hexichol 5.0~20.0 parts of base dimethyl silicone polymer, Dimethicone/Vinyl Dimethicone cross-linked polymer 5.0 ~20.0 parts, 5.0~35.0 parts of Dimethicone Crosspolymer；

2) ethylhexyl methoxy cinnamate, C12-15 alcohol benzoic ether, ring five dimethyl silicone polymer are sequentially added In emulsion pot, stirring is opened, until substantially uniformity；

3) tocopherol acetate, the royal jelly oil-control factor, apple seed extract, distearyl dimethylammonium hectorite are mixed Uniformly, it is then added in emulsion pot, stirs evenly；

4) silica, methyl methacrylate, octyl butanedioic acid aluminium starch are added in emulsion pot, stirring, homogeneous；

5) Nano titanium dioxide dispersion pulp is added in emulsion pot, stirring, homogeneous；

6) remaining ingredient is sequentially added in emulsion pot, stirring, homogeneous are uniformly dispersed.

Technical solution provided by the invention has the following beneficial effects:

The a large amount of greases and sweat of skin generation can be absorbed in product of the present invention, provide instant and persistently dry and comfortable for skin Skin sense；Product made from preferred embodiment can also effectively fill pore and microgroove, the skins such as moment smooth out wrinkles, pore, blackhead Flaw allows face skin to show natural gloss and soft sense.In addition, product of the invention also has in another preferred embodiment There is good sun-proof isolating function, effectively avoids skin by the injury of ultraviolet light.

Formula system of the invention, can accomplish moisture-free, also not need to add any preservative, a large amount of knots on probation Fruit shows that the safety of product is high, and good stability.

Product of the present invention be free of a variety of ingredients that may cause skin sensitivity, not spirituosity, without dioxanes, be free of first Aldehyde, without talcum powder, essence etc., the safety of product is good.

It can carry out the sliding sense of touch of silk after product of the present invention use for skin tape, it and foundation cream class product use, and can make adornment It is lasting to hold nature, bottoming is used before may be used as adornment.

Preparation method of the invention matches production technology using cold, can save a large amount of energy consumption, while the effect produced Rate is also high.

Detailed description of the invention

Fig. 1: skin-tightening efficacy test result

Specific embodiment

Technical scheme is described further in the following with reference to the drawings and specific embodiments, each component in embodiment It can be bought and be obtained by commercial channel.

Embodiment 1-3

Embodiment 1-3 is that the present invention has effects that the skin care item embodiment of oil-control, is formulated referring to table 1.

The skin care item of embodiment 1-3 are prepared in accordance with the following steps:

1) each component is weighed by the formula of table 1, the numerical value in table 1 is the mass parts of each component in formula；

2) A phase component is sequentially added in emulsion pot, opens stirring, until substantially uniformity；

3) B phase component is uniformly mixed, is then added in emulsion pot, open stirring, until substantially uniformity；

4) C phase component is slowly added into emulsion pot, high-speed stirred 5 minutes.Homogeneous 2000RPM is kept for 3 minutes；

5) D phase component is added in emulsion pot, high-speed stirred 5 minutes, homogeneous 2000RPM, is kept for 3 minutes；

6) E phase component is sequentially added in emulsion pot, is stirred 30 minutes, homogeneous 1000RPM, kept for 5 minutes, be uniformly dispersed After discharge；

7) it is qualified to examine, and discharges filling.

Table 1

Reference examples 1-3

Shown in the formula table such as the following table 2 (numerical value in table 1 is the mass parts of each component in formula) of reference examples 1-3.It is right The product of 1-4 is prepared according to embodiment 1-3 essentially identical method as usual, is repeated no more.

Table 2

Products of the present invention is tested for the property, detailed description are as follows:

One, 10 hours oil-control effect experiments

The volunteer of 90 oiliness or combination is chosen, the age was 18~35 one full year of life, was divided into 3 groups, every group of 30 people will The invention patent product (embodiment 1,2,3) and the product of reference examples 1 are applied to the forehead left and right sides of experimenter respectively, then stay In temperature at 20~25 degree, humidity is in 50%~70% interior, by 10 hours, the oil-control and use of comparative analysis product Skin sense.Wherein, the case where effect is glossy, the dry and comfortable degree of face, comfort level, statistical result see the table below shown in 3-5:

Table 3

Table 4

Table 5

Experimental result:

Find that the product of 1-3 of the embodiment of the present invention has the energy of reduction sebum secretion of 10 hours continuous and effectives after tested Power, this effect is through entire test process.Each product of embodiment 1-3 is bright to facial glossy, dry and comfortable degree, the improvement degree of comfort level It is aobvious to be higher than reference examples 1.Present inventor has also carried out survey identical with reference examples 1 to the product of reference examples 2-3 in an experiment Examination finds that the experimental result of reference examples 2-3 and reference examples 1 are essentially identical, the improvement journey of glossy to face, dry and comfortable degree, comfort level Degree is not so good as each product of embodiment 1-3.Moreover, during the test, inventor also found, the product of reference examples 1-3 has stranding mud Phenomenon occurs, and embodiment 1-3 absolutely not phenomenon.

Present inventor also tests the Product Safety of the cosmetic composition of above-described embodiment 1,2,3, and Using commercially available oil-control essence cream as control, test crowd is 90 people.During on probation, the product of 1-3 of the embodiment of the present invention is equal Irritation and allergic phenomena are not found, and reference product discovery there are 3 volunteers the case where allergy occur, it is seen then that product of the present invention It is a kind of product of safety in utilization with higher.

Two, instant anti-wrinkle effect test

60 female volunteers are chosen, the age was 35~50 one full year of life, was divided into 3 groups, and every group of 20 people produce 0.2 gram of present invention Product (embodiment 1-3) and 0.2 gram of commercially available reference examples (famous brand name anti-wrinkle eye cream) are applied to the left and right canthus of experimenter respectively At crow's feet, the wrinkle situation of change at crow's feet is then observed.Statistical result see the table below:

	Do not have effect completely	There are some effects	It is effective	It is very effective	It is very effective
						Embodiment 1	0	1	1	5	13
Reference examples	5	6	5	2	2

It is drawn a conclusion according to test result analysis, in 20 experimenters, there are 13 to think that the wrinkle of filling and leading up of embodiment 1 is imitated Fruit clearly, has 5 to think that effect is obvious；The embodiment of the present invention 1 compared with commercially available reference examples, embodiment 1 It is more preferable to fill and lead up wrinkle effect.

	Do not have effect completely	There are some effects	It is effective	It is very effective	It is very effective
						Embodiment 2	0	0	2	6	12
Reference examples	6	5	4	3	2

It is drawn a conclusion according to test result analysis, in 20 experimenters, there are 12 to think that the wrinkle of filling and leading up of embodiment 2 is imitated Fruit clearly, has 6 to think that effect is obvious；The embodiment of the present invention 2 compared with commercially available reference examples, embodiment 2 It is more preferable to fill and lead up wrinkle effect.

	Do not have effect completely	There are some effects	It is effective	It is very effective	It is very effective
						Embodiment 3	0	1	1	3	15
Reference examples	8	7	2	1	2

It is drawn a conclusion according to test result analysis, in 20 experimenters, there are 15 to think that the wrinkle of filling and leading up of embodiment 3 is imitated Fruit clearly, has 3 to think that effect is obvious；The embodiment of the present invention 3 compared with commercially available reference examples, embodiment 3 It is more preferable to fill and lead up wrinkle effect.

Three, skin-tightening efficacy test

Its test method and result are as follows:

Test sample: embodiment 1

Subject: the age 40~50 years old, women, 20 people

Test position: canthus

Application method: uniformly it is applied to specified region

Service life: 4 weeks

Frequency of use: once a day

Test parameter: 1, skin elasticity analyzer Cutometer MPA 580 is for detecting skin elasticity index:

Conceptual design: the 0th day

Research starts the last week, and target area stops using any a compact or aging product

Target area is simultaneously exposed in the environment of constant temperature constant temperature by cleaning target area, is rested 20 minutes

Carries out the parametric measurement of skin elasticity index to target area

Takes pictures

Distributes sample

14th day

Target area is exposed in the environment of constant temperature and humidity by, is rested 20 minutes

Carries out the parameter testing of skin elasticity index to target area

Takes pictures

28th day

Target area is exposed in the environment of constant temperature and humidity by, is rested 20 minutes

Carries out the parameter testing of skin elasticity index to target area

Takes pictures

Data statistics: data are counted using SPSS 13.0for Windows software package, difference before and after the test It is compared using pairing T detection, significance is P < 0.05.

Test result: referring to Fig. 1.

Experiment conclusion: after product 2 weeks and 4 weeks of embodiment 1, the skin elasticity of basic value, the skin at canthus are compared Elasticity has conspicuousness promotion during the test.The product of embodiment 2,3 is also carried out and the identical test of embodiment 1, Experimental result is similar, repeats no more.

Four, preservative efficacy test report

Preservative efficacy test: EU criteria USP51, BP2002XVI C EFFICAIY test basis and analysis method: are pressed OF ANTIMICROBIAL PRESERVATION measures the ability execution that cosmetics resist microbial contamination.

Preservative efficacy test

Sample ID: embodiment 1

Conclusion judgment criteria:

Experimental result: for the protective system of the product (embodiment 1) by challenge test, the protective system is reasonable to microorganism Effect is killed in the suppression thought, product production, storage and using when be less susceptible to pollution by microorganism.Production to embodiment 2,3 Product have also carried out this test, and result and embodiment 1 are essentially identical, are no longer described in detail.

The above described is only a preferred embodiment of the present invention, limitation in any form not is done to the present invention, therefore All contents without departing from technical solution of the present invention, it is made to the above embodiment according to the technical essence of the invention any simply to repair Change, equivalent variations and modification, all of which are still within the scope of the technical scheme of the invention.

Claims (2)

1. a kind of have effects that the skin care item of oil-control, which is characterized in that the skin care item are grouped by each group of following mass parts At:

1.0~5.0 parts of ethylhexyl methoxy cinnamate, 2.0~8.0 parts of C12-15 alcohol benzoic ether, five poly dimethyl silicon of ring 20.6~52.6 parts of oxygen alkane, 0.1~1.0 part of tocopherol acetate, 0.2~1.0 part of the royal jelly oil-control factor, apple seed extract 1.0~3.0 parts, 0.2~0.8 part of distearyl dimethylammonium hectorite, silica 1 .0~5.0 part, polymethyl methacrylate 1.0~3.0 parts, 1.0~3.0 parts of octenoic acid butanedioic acid aluminium starch, 0.5~5.0 part of Nano titanium dioxide dispersion pulp, octyl it is poly- 1.0~5.0 parts of methylsiloxane, 5.0~20.0 parts of diphenyl dimethicone, dimethyl silicone polymer/vinyl are poly- 5.0~20.0 parts of dimethicone crosspolymers, 5.0~35.0 parts of Dimethicone Crosspolymer.

2. the preparation method with the skin care item of oil-control described in claim 1, which comprises the steps of:

1) each component is weighed according to formula, the formula includes each component of following mass parts: ethylhexyl methoxy cinnamate 1.0~5.0 parts, 2.0~8.0 parts of C12-15 alcohol benzoic ether, 20.6~52.6 parts of ring five dimethyl silicone polymer, tocopherol second 0.1~1.0 part of acid esters, 0.2~1.0 part of the royal jelly oil-control factor, 1.0~3.0 parts of apple seed extract, distearyl dimethylammonium lithium 0.2~0.8 part of montmorillonite, silica 1 .0~5.0 part, 1.0~3.0 parts of polymethyl methacrylate, octenoic acid butanedioic acid aluminium 1.0~3.0 parts of starch, 0.5~5.0 part of Nano titanium dioxide dispersion pulp, 1.0~5.0 parts of octyl polymethyl siloxane, hexichol 5.0~20.0 parts of base dimethyl silicone polymer, Dimethicone/Vinyl Dimethicone cross-linked polymer 5.0 ~20.0 parts, 5.0~35.0 parts of Dimethicone Crosspolymer；

2) ethylhexyl methoxy cinnamate, C12-15 alcohol benzoic ether, ring five dimethyl silicone polymer are sequentially added into emulsification In pot, stirring is opened, until substantially uniformity；

3) tocopherol acetate, the royal jelly oil-control factor, apple seed extract, distearyl dimethylammonium hectorite are mixed equal It is even, it is then added in emulsion pot, stirs evenly；

4) silica, polymethyl methacrylate, octenoic acid butanedioic acid aluminium starch are added in emulsion pot, stirring, homogeneous；

5) Nano titanium dioxide dispersion pulp is added in emulsion pot, stirring, homogeneous；

6) remaining ingredient is sequentially added in emulsion pot, stirring, homogeneous are uniformly dispersed.