CN106262919A - A kind of floral type peony seed oil toxin expelling microcapsule and preparation method thereof - Google Patents
A kind of floral type peony seed oil toxin expelling microcapsule and preparation method thereof Download PDFInfo
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- CN106262919A CN106262919A CN201610670870.9A CN201610670870A CN106262919A CN 106262919 A CN106262919 A CN 106262919A CN 201610670870 A CN201610670870 A CN 201610670870A CN 106262919 A CN106262919 A CN 106262919A
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- seed oil
- peony seed
- microcapsule
- toxin expelling
- enzyme
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- 235000015112 vegetable and seed oil Nutrition 0.000 title claims abstract description 44
- 241000736199 Paeonia Species 0.000 title claims abstract description 42
- 235000006484 Paeonia officinalis Nutrition 0.000 title claims abstract description 42
- 239000003094 microcapsule Substances 0.000 title claims abstract description 24
- 239000003053 toxin Substances 0.000 title claims abstract description 19
- 231100000765 toxin Toxicity 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims description 13
- 102000004190 Enzymes Human genes 0.000 claims abstract description 27
- 108090000790 Enzymes Proteins 0.000 claims abstract description 27
- 241000628997 Flos Species 0.000 claims abstract description 16
- 150000001875 compounds Chemical class 0.000 claims abstract description 12
- 210000000582 semen Anatomy 0.000 claims abstract description 12
- LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 claims abstract description 9
- 244000247812 Amorphophallus rivieri Species 0.000 claims abstract description 9
- 235000001206 Amorphophallus rivieri Nutrition 0.000 claims abstract description 9
- 229920002581 Glucomannan Polymers 0.000 claims abstract description 9
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 9
- 229920002752 Konjac Polymers 0.000 claims abstract description 9
- 108010073771 Soybean Proteins Proteins 0.000 claims abstract description 9
- 229940046240 glucomannan Drugs 0.000 claims abstract description 9
- 239000008103 glucose Substances 0.000 claims abstract description 9
- 239000000252 konjac Substances 0.000 claims abstract description 9
- 235000010485 konjac Nutrition 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims abstract description 9
- 235000019710 soybean protein Nutrition 0.000 claims abstract description 9
- 244000060011 Cocos nucifera Species 0.000 claims abstract description 7
- 235000013162 Cocos nucifera Nutrition 0.000 claims abstract description 7
- 235000002168 Tilia europaea Nutrition 0.000 claims abstract description 7
- 240000006909 Tilia x europaea Species 0.000 claims abstract description 7
- ZDXPYRJPNDTMRX-UHFFFAOYSA-N glutamine Natural products OC(=O)C(N)CCC(N)=O ZDXPYRJPNDTMRX-UHFFFAOYSA-N 0.000 claims abstract description 7
- 150000003904 phospholipids Chemical class 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 235000013372 meat Nutrition 0.000 claims abstract description 4
- 239000000243 solution Substances 0.000 claims description 21
- 239000000084 colloidal system Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 239000012460 protein solution Substances 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 7
- 238000000926 separation method Methods 0.000 claims description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 5
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 239000000839 emulsion Substances 0.000 claims description 4
- 238000004108 freeze drying Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 108090000145 Bacillolysin Proteins 0.000 claims description 3
- 102000035092 Neutral proteases Human genes 0.000 claims description 3
- 108091005507 Neutral proteases Proteins 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- 239000002304 perfume Substances 0.000 claims description 3
- 235000013599 spices Nutrition 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- 229910021529 ammonia Inorganic materials 0.000 claims description 2
- 235000014593 oils and fats Nutrition 0.000 abstract description 5
- 239000003921 oil Substances 0.000 abstract description 4
- 235000019198 oils Nutrition 0.000 abstract description 4
- 238000003860 storage Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 239000003205 fragrance Substances 0.000 abstract description 2
- 239000008187 granular material Substances 0.000 abstract description 2
- 230000000050 nutritive effect Effects 0.000 abstract description 2
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 4
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 4
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 description 3
- 102000002322 Egg Proteins Human genes 0.000 description 3
- 108010000912 Egg Proteins Proteins 0.000 description 3
- 235000014103 egg white Nutrition 0.000 description 3
- 210000000969 egg white Anatomy 0.000 description 3
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- 102000004316 Oxidoreductases Human genes 0.000 description 1
- 108090000854 Oxidoreductases Proteins 0.000 description 1
- 240000005001 Paeonia suffruticosa Species 0.000 description 1
- 235000003889 Paeonia suffruticosa Nutrition 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- 230000002052 anaphylactic effect Effects 0.000 description 1
- 238000010009 beating Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000007894 caplet Substances 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 206010008118 cerebral infarction Diseases 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 238000006911 enzymatic reaction Methods 0.000 description 1
- 238000001976 enzyme digestion Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 125000001165 hydrophobic group Chemical group 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 208000010125 myocardial infarction Diseases 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 235000015067 sauces Nutrition 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 230000008542 thermal sensitivity Effects 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/06—Preservation of finished products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/025—Pretreatment by enzymes or microorganisms, living or dead
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/106—Production of fats or fatty oils from raw materials by extracting using ultra-sounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of floral type peony seed oil toxin expelling microcapsule, be made up of the raw material of following weight parts: seed of Flos Moutan 100 150, niblet 10 15, Semen Granati 12 18, Semen sojae atricolor 8 12, Flos Moutan 24 36, coconut meat 69, Caulis et Folium Tritici aestivi 23, tilia europaea 46, Konjac glucomannan and proper amount of glucose, soybean protein isolate and phospholipid are appropriate, compound enzyme and glutamine transaminage appropriate；Add Semen Maydis, Semen Granati, Semen sojae atricolor etc. and there is the oil-containing raw material of the effects such as toxin expelling fat-reducing, more improve its healthy nutritive value in the mouthfeel and quality improving peony seed oil simultaneously, the embedding rate of finished product peony seed oil microcapsule reaches more than 75%, microcapsule subcircular, smooth surface, granule are little, flawless hole, the fragrance of flowers is strong persistently, shelf-life significantly extends, and powder oils and fats is more convenient when storage is transported and be edible.
Description
Technical field
The present invention relates to health-care vegetable oil technical field, particularly relate to a kind of floral type peony seed oil toxin expelling microcapsule and
Preparation method.
Background technology
Containing multiple unsaturated fatty acids such as oleic acid, linoleic acid, linolenic acid in peony seed oil, to improving intelligence, strengthening and exempt from
Epidemic disease power, protection vision, prevention myocardial infarction and cerebral infarction, prevention anaphylactic disease and slow down aging etc. all play an important role,
But the effective ingredient unsaturated fatty acid of peony seed oil in an oxidizing environment or is easily oxidized to trans fatty acid under high temperature,
Human body is harmful on the contrary, and the direct eating mouth feel of peony seed oil is more puckery, although and other oil allotments can change its mouthfeel, but by
In not heating, it is only used for cold and dressed with sauce, limits the use of peony seed oil, be unfavorable for peony seed oil industry development；The micro-glue of oils and fats
Encapsulated technology is for wall material, oils and fats to wrap up formation Caplet, capsule diameter size with the macromolecular compound being prone to film forming
For 5-200 μm, the product produced by this technology can not only be prevented peony seed oil from aoxidizing, and make liquid fat be converted into powder
Oils and fats, convenient storage is transported；Owing to peony seed oil has many merits, before peony seed oil product has wide market
Scape, so the present invention provides the peony seed oil microcapsule and production work thereof that a kind of oil yield is high, extraction efficiency is high, embedding rate is high
Skill.
Summary of the invention
The present invention is to make up the deficiencies in the prior art, it is provided that a kind of floral type peony seed oil toxin expelling microcapsule and system thereof
Preparation Method.
The present invention is achieved by the following technical solutions:
A kind of floral type peony seed oil toxin expelling microcapsule, is made up of the raw material of following weight parts:
Seed of Flos Moutan 100-150, niblet 10-15, Semen Granati 12-18, Semen sojae atricolor 8-12, Flos Moutan 24-36, coconut meat 6-9, Caulis et Folium Tritici aestivi
2-3, tilia europaea 4-6, Konjac glucomannan and proper amount of glucose, soybean protein isolate and phospholipid are appropriate, compound enzyme and glutamine turn ammonia
Enzyme is appropriate；
Described compound enzyme is maceraring enzyme and neutral protease obtains for 2:1 ratio mixed preparing in mass ratio.
A kind of described floral type peony seed oil toxin expelling microcapsule preparation method, comprises the following steps:
(1) filtering out the seed of Flos Moutan of high-quality, niblet, Semen Granati, Semen sojae atricolor, drain after cleaning, send into frying pan, little fire constantly stir-fries
To going out perfume (or spice), pulverize 30-40 minute under the conditions of-10 ± 2 DEG C with vibration type superfine comminution at low temperature machine after cooling, obtain ultra micro seed
Powder；
(2) fresh Flos Moutan and Caulis et Folium Tritici aestivi, tilia europaea roguing being cleaned, copra is cleaned, and all mixes, and adds 4-5 times clearly
Water is pulled an oar, and enzyme denaturing 4-5 second at 110-115 DEG C, more freeze-dried rear micronizing, obtains ultra micro pollen；
(3) above-mentioned ultra micro seed powder, ultra micro pollen are mixed homogeneously with 6-8 times of pure water, add the compound enzyme of gross weight 1-2%, add
Adding citric acid regulation pH to 5-5.5, sends in microwave ultrasonic wave combination type reactor, at temperature 40-50 DEG C, microwave power 400-
Under conditions of 500W, ultrasonic power 700-800W, enzymolysis 60-80 minute, obtains enzymolysis solution；
(4) will carry out solid-liquid separation process in above-mentioned enzymolysis solution feeding knockout drum, the separation liquid obtained is through enzyme denaturing, decolouring, remove impurity
Deng common process, obtain peony seed oil；
(5) Konjac glucomannan and glucose being pressed 1:1 mixing, is slowly even added in the pure water of both quality 28-30 times, stirring is all
Colloid solution is obtained after even；Soybean protein isolate and phospholipid are pressed 2:1 mixing, is slowly even added to both quality 8-10 times temperature
Spend in the warm water of 60-65 DEG C, after stirring, obtain protein solution；
(6) in above-mentioned protein solution, it is sequentially added into peony seed oil, colloid solution, maintains the temperature at 50-60 DEG C, after stirring
Obtain stable emulsion, with Fructus Citri Limoniae acid for adjusting pH to 6-6.5, add the glutamine transaminage of 250-300U/kg, at 40-50
Gel reaction 50-60 minute at DEG C, is warming up to 80-90 DEG C of enzyme denaturing 1-2 minute, in temperature-28 ± 2 DEG C, vacuum 15-17Pa
Under the conditions of vacuum lyophilization to constant weight, obtain finished product.
A kind of described floral type peony seed oil toxin expelling microcapsule preparation method, protein solution in described step (5): colloid
The volume ratio of solution is 6:1.
A kind of described floral type peony seed oil toxin expelling microcapsule preparation method, peony seed oil in described step (6): (egg
White solution+colloid solution) volume ratio be 1:4.
Compared with prior art, the invention have the advantage that
The present invention is blended in enzymolysis under microwave-ultrasonic after seed of Flos Moutan and Flos Moutan micronizing, and in utilizing microwave, heating is excellent
Gesture and supersonic cavity principle solve tradition aqueous enzymatic method enzymolysis time length and the problem of enzymatic isolation method breakdown of emulsion, reduce because of enzymolysis time
Length makes the problem that quality declines and productivity is low that in peony seed oil, unsaturated fatty acids acid oxidase causes；Use maceraring enzyme and neutral egg
White enzyme complex enzyme hydrolysis can make enzyme digestion reaction more abundant, and the peony seed oil extracted is more efficient and high yield；Use soybean separation protein
In vain, Konjac glucomannan, glucose as compound wall materials, soybean protein isolate exists hydrophilic group and hydrophobic group simultaneously, and Semen sojae atricolor separates
Albumen has good emulsibility and film property, and Konjac glucomannan, glucose can form protein-PS covalency with soybean protein isolate
Compound system, increases the mechanical strength of microcapsule wall and stability, reduces excessive in embedding process of peony seed oil simultaneously, carries
The stability of high microcapsule and embedding rate；Vacuum lyophilization have do not destroy peony seed oil thermal sensitivity unsaturated fatty acid and
The advantage that efficiency is high, adds Semen Maydis, Semen Granati, Semen sojae atricolor etc. and has the oil-containing raw material of the effects such as toxin expelling fat-reducing, improving Paeonia suffruticosa
Mouthfeel and the quality of seed oil more improve its healthy nutritive value simultaneously, and the embedding rate of finished product peony seed oil microcapsule reaches 75%
Above, microcapsule subcircular, smooth surface, granule are little, flawless hole, and the fragrance of flowers is strong persistently, and the shelf-life significantly extends, powder
Shape oils and fats is more convenient when storage is transported and be edible.
Detailed description of the invention
A kind of floral type peony seed oil toxin expelling microcapsule, is made up of the raw material of following weight (jin):
Seed of Flos Moutan 100, niblet 10, Semen Granati 12, Semen sojae atricolor 8, Flos Moutan 24, coconut meat 6, Caulis et Folium Tritici aestivi 2, tilia europaea 4, Konjac glucomannan and
Proper amount of glucose, soybean protein isolate and phospholipid are appropriate, compound enzyme and glutamine transaminage appropriate；
Described compound enzyme is maceraring enzyme and neutral protease obtains for 2:1 ratio mixed preparing in mass ratio.
A kind of described floral type peony seed oil toxin expelling microcapsule preparation method, comprises the following steps:
(1) filtering out the seed of Flos Moutan of high-quality, niblet, Semen Granati, Semen sojae atricolor, drain after cleaning, send into frying pan, little fire constantly stir-fries
To going out perfume (or spice), pulverize under the conditions of-10 DEG C 30 minutes with vibration type superfine comminution at low temperature machine after cooling, obtain ultra micro seed powder；
(2) fresh Flos Moutan and Caulis et Folium Tritici aestivi, tilia europaea roguing being cleaned, copra is cleaned, and all mixes, adds 4 times of clear water
Making beating, enzyme denaturing 4 seconds at 110 DEG C, more freeze-dried rear micronizing, obtain ultra micro pollen；
(3) by above-mentioned ultra micro seed powder, ultra micro pollen and 6 times of pure water mix homogeneously, add the compound enzyme of gross weight 1%, add lemon
Lemon acid for adjusting pH, to 5, is sent in microwave ultrasonic wave combination type reactor, at temperature 40 DEG C, microwave power 400W, ultrasonic power
Under conditions of 700W, enzymolysis 60 minutes, obtain enzymolysis solution；
(4) will carry out solid-liquid separation process in above-mentioned enzymolysis solution feeding knockout drum, the separation liquid obtained is through enzyme denaturing, decolouring, remove impurity
Deng common process, obtain peony seed oil；
(5) Konjac glucomannan and glucose are pressed 1:1 mixing, is slowly even added in the pure water of both quality 28 times, stirs
After obtain colloid solution；Soybean protein isolate and phospholipid are pressed 2:1 mixing, is slowly even added to 8 times of temperature 60 of both quality
DEG C warm water in, obtain protein solution after stirring；
(6) in above-mentioned protein solution, it is sequentially added into peony seed oil, colloid solution, maintains the temperature at 50 DEG C, after stirring
To stable emulsion, with Fructus Citri Limoniae acid for adjusting pH to 6, add the glutamine transaminage of 250U/kg, gel reaction 50 at 40 DEG C
Minute, it is warming up to 80 DEG C of enzyme denaturing 1 minute, under conditions of temperature-30 DEG C, vacuum 15Pa, vacuum lyophilization is to constant weight,
To finished product.
A kind of described floral type peony seed oil toxin expelling microcapsule preparation method, protein solution in described step (5): colloid
The volume ratio of solution is 6:1.
A kind of described floral type peony seed oil toxin expelling microcapsule preparation method, peony seed oil in described step (6): (egg
White solution+colloid solution) volume ratio be 1:4.
Claims (4)
1. a floral type peony seed oil toxin expelling microcapsule, it is characterised in that be made up of the raw material of following weight parts:
Seed of Flos Moutan 100-150, niblet 10-15, Semen Granati 12-18, Semen sojae atricolor 8-12, Flos Moutan 24-36, coconut meat 6-9, Caulis et Folium Tritici aestivi
2-3, tilia europaea 4-6, Konjac glucomannan and proper amount of glucose, soybean protein isolate and phospholipid are appropriate, compound enzyme and glutamine turn ammonia
Enzyme is appropriate；
Described compound enzyme is maceraring enzyme and neutral protease obtains for 2:1 ratio mixed preparing in mass ratio.
2. a floral type peony seed oil toxin expelling microcapsule preparation method as claimed in claim 1, it is characterised in that include with
Lower step:
(1) filtering out the seed of Flos Moutan of high-quality, niblet, Semen Granati, Semen sojae atricolor, drain after cleaning, send into frying pan, little fire constantly stir-fries
To going out perfume (or spice), pulverize 30-40 minute under the conditions of-10 ± 2 DEG C with vibration type superfine comminution at low temperature machine after cooling, obtain ultra micro seed
Powder；
(2) fresh Flos Moutan and Caulis et Folium Tritici aestivi, tilia europaea roguing being cleaned, copra is cleaned, and all mixes, and adds 4-5 times clearly
Water is pulled an oar, and enzyme denaturing 4-5 second at 110-115 DEG C, more freeze-dried rear micronizing, obtains ultra micro pollen；
(3) above-mentioned ultra micro seed powder, ultra micro pollen are mixed homogeneously with 6-8 times of pure water, add the compound enzyme of gross weight 1-2%, add
Adding citric acid regulation pH to 5-5.5, sends in microwave ultrasonic wave combination type reactor, at temperature 40-50 DEG C, microwave power 400-
Under conditions of 500W, ultrasonic power 700-800W, enzymolysis 60-80 minute, obtains enzymolysis solution；
(4) will carry out solid-liquid separation process in above-mentioned enzymolysis solution feeding knockout drum, the separation liquid obtained is through enzyme denaturing, decolouring, remove impurity
Deng common process, obtain peony seed oil；
(5) Konjac glucomannan and glucose being pressed 1:1 mixing, is slowly even added in the pure water of both quality 28-30 times, stirring is all
Colloid solution is obtained after even；Soybean protein isolate and phospholipid are pressed 2:1 mixing, is slowly even added to both quality 8-10 times temperature
Spend in the warm water of 60-65 DEG C, after stirring, obtain protein solution；
(6) in above-mentioned protein solution, it is sequentially added into peony seed oil, colloid solution, maintains the temperature at 50-60 DEG C, after stirring
Obtain stable emulsion, with Fructus Citri Limoniae acid for adjusting pH to 6-6.5, add the glutamine transaminage of 250-300U/kg, at 40-50
Gel reaction 50-60 minute at DEG C, is warming up to 80-90 DEG C of enzyme denaturing 1-2 minute, in temperature-28 ± 2 DEG C, vacuum 15-17Pa
Under the conditions of vacuum lyophilization to constant weight, obtain finished product.
3. a floral type peony seed oil toxin expelling microcapsule preparation method as claimed in claim 2, it is characterised in that described step
Suddenly protein solution in (5): the volume ratio of colloid solution is 6:1.
4. a floral type peony seed oil toxin expelling microcapsule preparation method as claimed in claim 2, it is characterised in that described step
Suddenly peony seed oil in (6): the volume ratio of (protein solution+colloid solution) is 1:4.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112535291A (en) * | 2020-12-03 | 2021-03-23 | 山西省农业科学院农产品加工研究所 | Peony seed oil microcapsule and preparation method thereof |
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| CN103947957A (en) * | 2014-03-25 | 2014-07-30 | 刘阿君 | Toxin expelling and face nourishing rice cake and preparation method thereof |
| CN105482890A (en) * | 2016-01-22 | 2016-04-13 | 西安科技大学 | Microwave ultrasonic-assisted aqueous enzymatic method for extracting linseed oil |
| CN105613792A (en) * | 2015-12-31 | 2016-06-01 | 成都市农林科学院 | Microcapsule preparation technology beneficial for quality control |
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2016
- 2016-08-16 CN CN201610670870.9A patent/CN106262919A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103947957A (en) * | 2014-03-25 | 2014-07-30 | 刘阿君 | Toxin expelling and face nourishing rice cake and preparation method thereof |
| CN105613792A (en) * | 2015-12-31 | 2016-06-01 | 成都市农林科学院 | Microcapsule preparation technology beneficial for quality control |
| CN105482890A (en) * | 2016-01-22 | 2016-04-13 | 西安科技大学 | Microwave ultrasonic-assisted aqueous enzymatic method for extracting linseed oil |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112535291A (en) * | 2020-12-03 | 2021-03-23 | 山西省农业科学院农产品加工研究所 | Peony seed oil microcapsule and preparation method thereof |
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Application publication date: 20170104 |