CN106243873A - A kind of aqueous tape measure dip-coating baking vanish and preparation method thereof - Google Patents
A kind of aqueous tape measure dip-coating baking vanish and preparation method thereof Download PDFInfo
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- CN106243873A CN106243873A CN201610772528.XA CN201610772528A CN106243873A CN 106243873 A CN106243873 A CN 106243873A CN 201610772528 A CN201610772528 A CN 201610772528A CN 106243873 A CN106243873 A CN 106243873A
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- Prior art keywords
- tape measure
- baking vanish
- coating baking
- agent
- aqueous tape
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of aqueous tape measure dip-coating baking vanish and preparation method thereof, a kind of aqueous tape measure dip-coating baking vanish of the present invention, described aqueous tape measure dip-coating baking vanish is by base material, auxiliary agent, color stuffing and levelling agent composition, described base material is the most composed of the following components: water-borne acrylic resin 30 50 parts, 48 parts of amino resins, described auxiliary agent is the most composed of the following components: environmentally friendly solvent 2 16 parts, nertralizer 0.5 3 parts, 10 25 parts of water, wetting dispersing agent 0.1 2 parts, defoamer 0.1 0.5 parts, deaeration agent 0.1 0.5 parts, bentonite 0.3 3 parts, levelling agent 0.29 0.35 parts, pigment 25 35 parts.It is fabulous that the present invention has adhesive force, and edge is opacifying property good, low-carbon environment-friendly, the short feature of baking time.
Description
Technical field
The present invention relates to industrial coating field, particularly relate to a kind of aqueous tape measure dip-coating baking vanish and preparation method thereof.
Background technology
Along with improving constantly of people's environmental consciousness, water paint has obtained and has increasingly been widely applied, traditional oil
Painting, during producing and using, health and the environment of people is had significant damage, the popularization of sealing wax can reduce the row of VOC
Put, the generation of refuse, reduce workman's contact to poisonous releaser.Current haze is administered and also has certain facilitation.
It is reported, " 13 " period, the control to VOC (VOC) total amount will be strengthened, to nitrogen oxides and VOC in the whole nation
Carry out collaborative reduction of discharging.
Tape measure dip-coating water-based stoving paint coating is mainly used in the necks such as tape measure, coiled material, aluminium, zinc-plated tubing, machine components
Territory, the Water-borne modification level of current domestic industry coating also exists the biggest gap with technology compared with industrially developed country.Aqueous is soaked
It is coated with baking vanish to there is poor adhesive force, easily go out the shortcomings such as cut, opacifying property difference, baking time length.Therefore develop a high adhesion force,
Hardness is high, opacifying property by force, baking time is short, the high-grade aqueous tape measure dip-coating baking vanish of low VOC, thus greatly reduces the discharge of VOC
Amount, reduces environmental pollution, energy-saving and emission-reduction, low-carbon environment-friendly is had very important realistic meaning.
Summary of the invention
For solving the problems referred to above, it is an object of the invention to provide the shortcoming being i.e. to overcome prior art, it is provided that a kind ofAttached Put forth effort fabulousAqueous tape measure dip-coating baking vanish and preparation method thereof.
For realizing above-mentioned technical purpose, the technical solution used in the present invention is as follows: a kind of aqueous tape measure dip-coating of the present invention
Baking vanish, described aqueous tape measure dip-coating baking vanish is made up of base material, auxiliary agent, color stuffing and levelling agent, described base material by weight by with
Lower component forms:
Water-borne acrylic resin 30-50 part,
Amino resins 4-8 part,
Described auxiliary agent is the most composed of the following components:
Further, described color stuffing is titanium dioxide, and described bentonite is organobentonite, and described water is deionized water,
Described base material is the most composed of the following components:
Water-borne acrylic resin 40 parts,
5.2 parts of amino resins,
Described auxiliary agent is the most composed of the following components:
Further, described amino resins is high imino-type methyl-etherified amino resins, and described defoamer is polyethers silicon
Oxygen alkane co-polymer emulsion.
Further, described environmentally friendly solvent is one or both the combination in ethylene glycol monobutyl ether, ethanol.
Further, described wetting dispersing agent is the high molecular weight block copolymer aqueous solution containing high pigment affinity groups
Type dispersant.
Further, described levelling agent be the one in acrylate levelling agent, fluorine-carbon modified acrylic acid levelling agent or
The combination of two kinds
Further, described defoamer is one or both the combination in organic silicon defoamer, aqueous deaeration agent.
Further, described bentonite is organobentonite.
The preparation method of aqueous tape measure dip-coating baking vanish of the present invention, comprises the steps:
(1) said components described in claim 1 is weighed, the water-borne acrylic resin by described 25%, the environmental protection of 25%
Solvent, the nertralizer of 25% are added sequentially to first and get the raw materials ready in pot, are slowly stirred, and stir 5-under 200-500r/min speed
15min;Wherein, the 25% of described environmentally friendly solvent is butyl glycol ether,
(2) adjust mixing speed, successively wetting dispersing agent, defoamer, water, pigment, organobentonite are added slowly to
First gets the raw materials ready in pot, heightens mixing speed, stirs more than 20 minutes;
(3) described uniform mill base is ground, is ground to fineness less than or equal to 20 microns;
(4) make later stage resin liquid by 75% water-borne acrylic resin, the environmentally friendly solvent of 75%, amino resins, 75%
Nertralizer, levelling agent, defoamer join second and get the raw materials ready and stir in pot;
(5) by grind qualified mill base and later stage resin liquid press the quality of 1.325:1 than mixing and stirring after, wrap
Dress, prepares aqueous tape measure dip-coating baking vanish.
Further, in step (2), adjust mixing speed, successively will profit under the mixing speed of 300-800r/min
Hygroscopic water powder, defoamer, water, pigment, organobentonite are added slowly to first and get the raw materials ready in pot, heighten mixing speed, at 600-
Stir more than 20 minutes under the mixing speed of 1500r/min;
In step (4), described environmentally friendly solvent is the compositions of ethylene glycol monobutyl ether and ethanol, described environmentally friendly solvent
Middle butyl glycol ether is 1:2 with the mass ratio of ethanol;Described defoamer is organic silicon defoamer, and described levelling agent is propylene
Acid esters levelling agent and fluorine-carbon modified acrylic acid levelling agent.
Beneficial effect: the present invention has high adhesion force, edge is opacifying property good, and low-carbon environment-friendly, baking time is short.It is applicable to attached
Putting forth effort fabulous, edge is opacifying property good, and baking time is short.
Compared with prior art, present invention have the advantage that
(1) aqueous tape measure dip-coating baking vanish of the present invention uses water-borne acrylic resin and water-compatible amino resin solidification crosslinking conduct
Film forming matter, 180 DEG C of baking 30s i.e. cross-linkable solidifying film forming, it is greatly improved production efficiency, paint film has a high rigidity simultaneously, 3H,
High adhesion force is opacifying property good for sharp edge.Do not fire the performances such as the most quick-fried, low-carbon environment-friendly.Adhesive force is good, adhesive force on tape measure
> 1 grade, and be difficult at designated port wipe off.
(2) formula adds high boiling point environmentally friendly solvent, makes this invention product not contain the poisonous and harmful substance such as benzene, dimethylbenzene,
VOC content is low, and the healthy impact on environment and workmen is less.
Detailed description of the invention
Further illustrate the present invention by the following examples.It should be understood that these embodiments are the explainations of the present invention
And citing, limit the scope of the present invention the most in any form.
Embodiment 1
A kind of aqueous tape measure dip-coating baking vanish of the present invention of the present invention, described aqueous tape measure dip-coating baking vanish by base material, auxiliary agent,
Color stuffing and levelling agent composition, described base material is the most composed of the following components:
Water-borne acrylic resin 30 parts,
6 parts of amino resins,
Described auxiliary agent is the most composed of the following components:
Described environmentally friendly solvent is ethylene glycol monobutyl ether.
Described wetting dispersing agent is the high molecular weight block copolymer aqueous solution type dispersant containing high pigment affinity groups.
Described levelling agent is acrylate levelling agent.
Described defoamer is organic silicon defoamer.
Described bentonite is organobentonite.
The preparation method of aqueous tape measure dip-coating baking vanish of the present invention, comprises the steps:
(1) said components is weighed, the water-borne acrylic resin by described 25%, the environmentally friendly solvent of 25%, the neutralization of 25%
Agent is added sequentially to first and gets the raw materials ready in pot, is slowly stirred, and stirs 5min under 500r/min speed;Wherein, described environmental protection is molten
The 25% of agent is butyl glycol ether,
(2) adjust mixing speed, under the mixing speed of 500 600r/min successively by wetting dispersing agent, defoamer,
Water, pigment, organobentonite are added slowly to first and get the raw materials ready in pot, heighten mixing speed, in the stirring speed of 800 900r/min
The lower stirring of degree more than 20 minutes;
(3) described uniform mill base is ground, is ground to fineness less than or equal to 20 microns;
(4) make later stage resin liquid by 75% water-borne acrylic resin, the environmentally friendly solvent of 75%, amino resins, 75%
Nertralizer, levelling agent, defoamer join second and get the raw materials ready and stir in pot;Described environmentally friendly solvent is ethylene glycol monobutyl ether
With the compositions of ethanol, in described environmentally friendly solvent, butyl glycol ether is 1:2 with the mass ratio of ethanol.
(5) by grind qualified mill base and later stage resin liquid press the quality of 1.325:1 than mixing and stirring after, wrap
Dress, prepares aqueous tape measure dip-coating baking vanish.
Embodiment 2
Embodiment 2 is with the difference of embodiment 1: a kind of aqueous tape measure dip-coating baking vanish of the present invention of the present invention, described
Aqueous tape measure dip-coating baking vanish is made up of base material, auxiliary agent, color stuffing and levelling agent, and described base material is by weight by following components group
Become:
Water-borne acrylic resin 40 parts,
4 parts of high imino-type methyl-etherified amino resins,
Described auxiliary agent is the most composed of the following components:
Described wetting dispersing agent is the high molecular weight block copolymer aqueous solution type dispersant containing high pigment affinity groups.
Described environmentally friendly solvent is the combination of two kinds in ethylene glycol monobutyl ether, ethanol.Described defoamer is that organosilicon disappears
The combination of two kinds in infusion, aqueous deaeration agent.
Described levelling agent is the combination of two kinds in acrylate levelling agent, fluorine-carbon modified acrylic acid levelling agent.
Described bentonite is organobentonite.
The preparation method of aqueous tape measure dip-coating baking vanish of the present invention, comprises the steps:
(1) said components is weighed, the water-borne acrylic resin by described 25%, the environmentally friendly solvent of 25%, the neutralization of 25%
Agent is added sequentially to first and gets the raw materials ready in pot, is slowly stirred, and stirs 10 15min under 200 300r/min speed;Wherein, institute
The 25% of the environmentally friendly solvent stated is butyl glycol ether,
(2) adjust mixing speed, under the mixing speed of 600 800r/min successively by wetting dispersing agent, defoamer,
Water, pigment, organobentonite are added slowly to first and get the raw materials ready in pot, heighten mixing speed, in the stirring of 600 1000r/min
Stir more than 15 minutes under speed;
Embodiment 3
Embodiment 3 is with the difference of embodiment 1: a kind of aqueous tape measure dip-coating baking vanish of the present invention of the present invention, described
Aqueous tape measure dip-coating baking vanish is made up of base material, auxiliary agent, color stuffing and levelling agent, and described base material is by weight by following components group
Become:
Water-borne acrylic resin 50 parts,
8 parts of amino resins,
Described auxiliary agent is the most composed of the following components:
Described levelling agent is fluorine-carbon modified acrylic acid levelling agent.Described environmentally friendly solvent is ethanol.
Described defoamer is aqueous deaeration agent.
The preparation method of aqueous tape measure dip-coating baking vanish of the present invention, comprises the steps:
(1) said components is weighed, the water-borne acrylic resin by described 25%, the environmentally friendly solvent of 25%, the neutralization of 25%
Agent is added sequentially to first and gets the raw materials ready in pot, is slowly stirred, and stirs 15min under 300r/min speed;Wherein, described environmental protection is molten
The 25% of agent is butyl glycol ether,
(2) adjust mixing speed, under the mixing speed of 300 600r/min successively by wetting dispersing agent, defoamer,
Water, pigment, organobentonite are added slowly to first and get the raw materials ready in pot, heighten mixing speed, in the stirring of 1000 1500r/min
Stir more than 20 30 minutes under speed;
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.The technology of the industry
Personnel, it should be appreciated that the present invention is not restricted to the described embodiments, simply illustrating this described in above-described embodiment and description
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, the present invention
Claimed scope is defined by appending claims, description and equivalent thereof.
Claims (10)
1. an aqueous tape measure dip-coating baking vanish, it is characterised in that: described aqueous tape measure dip-coating baking vanish is by base material, auxiliary agent, color stuffing
Forming with levelling agent, described base material is the most composed of the following components:
Water-borne acrylic resin 30-50 part,
Amino resins 4-8 part,
Described auxiliary agent is the most composed of the following components:
Aqueous tape measure dip-coating baking vanish the most according to claim 1, it is characterised in that: described color stuffing is titanium dioxide, described
Bentonite is organobentonite, and described water is deionized water,
Described base material is the most composed of the following components:
Water-borne acrylic resin 40 parts,
5.2 parts of amino resins,
Described auxiliary agent is the most composed of the following components:
Aqueous tape measure dip-coating baking vanish the most according to claim 1, it is characterised in that: described amino resins is high imino-type
Methyl-etherified amino resins, described defoamer is polyethers oxosilane co-polymer emulsion.
Aqueous tape measure dip-coating baking vanish the most according to claim 1, it is characterised in that: described environmentally friendly solvent is ethylene glycol list
One or both combination in butyl ether, ethanol.
Aqueous tape measure dip-coating baking vanish the most according to claim 1, it is characterised in that: described wetting dispersing agent is containing Gao Yan
The high molecular weight block copolymer aqueous solution type dispersant of material affinity groups.
Aqueous tape measure dip-coating baking vanish the most according to claim 1, it is characterised in that: described levelling agent is acrylate stream
One or both combination in flat agent, fluorine-carbon modified acrylic acid levelling agent.
Aqueous tape measure dip-coating baking vanish the most according to claim 1, it is characterised in that: described defoamer is organosilicon froth breaking
One or both combination in agent, aqueous deaeration agent.
Aqueous tape measure dip-coating baking vanish the most according to claim 1, it is characterised in that: described bentonite is organic swelling
Soil.
9. the preparation method of the aqueous tape measure dip-coating baking vanish described in any one of claim 1 to 8, it is characterised in that include as follows
Step:
(1) weigh the said components described in claim 1, water-borne acrylic resin by described 25%, the environmentally friendly solvent of 25%,
The nertralizer of 25% is added sequentially to first and gets the raw materials ready in pot, is slowly stirred, and stirs 5-15min under 200-500r/min speed;
Wherein, the 25% of described environmentally friendly solvent is butyl glycol ether,
(2) adjust mixing speed, successively wetting dispersing agent, defoamer, water, pigment, organobentonite are added slowly to first
Get the raw materials ready in pot, heighten mixing speed, stir more than 20 minutes;
(3) described uniform mill base is ground, is ground to fineness less than or equal to 20 microns;
(4) make later stage resin liquid by 75% water-borne acrylic resin, the environmentally friendly solvent of 75%, amino resins, in 75%
Mediating recipe, levelling agent, defoamer join second and get the raw materials ready and stir in pot;
(5) by grind qualified mill base and later stage resin liquid press the quality of 1.325:1 than mixing and stirring after, pack,
Prepare aqueous tape measure dip-coating baking vanish.
The preparation method of described aqueous tape measure dip-coating baking vanish the most according to claim 9, it is characterised in that: in step
(2) in, adjust mixing speed, under the mixing speed of 300-800r/min successively by wetting dispersing agent, defoamer, water, pigment,
Organobentonite is added slowly to first and gets the raw materials ready in pot, heightens mixing speed, stirs under the mixing speed of 600-1500r/min
More than 20 minutes;
In step (4), described environmentally friendly solvent is the compositions of ethylene glycol monobutyl ether and ethanol, second in described environmentally friendly solvent
Glycol butyl ether is 1:2 with the mass ratio of ethanol;Described defoamer is organic silicon defoamer, and described levelling agent is acrylate
Levelling agent and fluorine-carbon modified acrylic acid levelling agent.
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106893423A (en) * | 2017-02-16 | 2017-06-27 | 河北晨阳工贸集团有限公司 | Agricultural machinery aqueous amino-stoving varnish and preparation method thereof |
CN108300036A (en) * | 2017-08-29 | 2018-07-20 | 河北晨阳工贸集团有限公司 | A kind of farm implement aqueous dip-coating baking vanish and preparation method thereof |
CN108342134A (en) * | 2018-01-09 | 2018-07-31 | 河北晨阳工贸集团有限公司 | Aqueous ceramic paint and preparation method thereof and ceramics and preparation method thereof |
CN108456469A (en) * | 2018-01-15 | 2018-08-28 | 河北晨阳工贸集团有限公司 | Agricultural machinery sealing wax and preparation method thereof |
CN108948905A (en) * | 2018-04-03 | 2018-12-07 | 河北晨阳工贸集团有限公司 | A kind of aqueous bicycle special emulsion type Lacquer finish polishes and preparation method thereof |
CN109294410A (en) * | 2018-08-30 | 2019-02-01 | 山东七维新材料有限公司 | A kind of aqueous tape measure baking vanish and preparation method thereof |
CN109836927A (en) * | 2017-09-08 | 2019-06-04 | 河北晨阳工贸集团有限公司 | One kind thick can apply environment-friendly water-based woodcare paint and preparation method thereof |
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CN102888163A (en) * | 2012-10-25 | 2013-01-23 | 南京长江涂料有限公司 | Water-based paint for Christmas glass ornaments, and preparation method and application thereof |
CN104164145A (en) * | 2014-07-15 | 2014-11-26 | 合肥科润节能建材有限公司 | Water-based baked industrial paint |
CN104927526A (en) * | 2015-07-08 | 2015-09-23 | 安庆联泰电子科技有限公司 | Water-borne acrylic amino baking varnish special for intelligent ashtray metal shell |
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CN102888163A (en) * | 2012-10-25 | 2013-01-23 | 南京长江涂料有限公司 | Water-based paint for Christmas glass ornaments, and preparation method and application thereof |
CN104164145A (en) * | 2014-07-15 | 2014-11-26 | 合肥科润节能建材有限公司 | Water-based baked industrial paint |
CN104927526A (en) * | 2015-07-08 | 2015-09-23 | 安庆联泰电子科技有限公司 | Water-borne acrylic amino baking varnish special for intelligent ashtray metal shell |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106893423A (en) * | 2017-02-16 | 2017-06-27 | 河北晨阳工贸集团有限公司 | Agricultural machinery aqueous amino-stoving varnish and preparation method thereof |
CN108300036A (en) * | 2017-08-29 | 2018-07-20 | 河北晨阳工贸集团有限公司 | A kind of farm implement aqueous dip-coating baking vanish and preparation method thereof |
CN109836927A (en) * | 2017-09-08 | 2019-06-04 | 河北晨阳工贸集团有限公司 | One kind thick can apply environment-friendly water-based woodcare paint and preparation method thereof |
CN109836927B (en) * | 2017-09-08 | 2024-01-05 | 河北晨阳工贸集团有限公司 | Environment-friendly water-based wood paint capable of being thickly coated and preparation method thereof |
CN108342134A (en) * | 2018-01-09 | 2018-07-31 | 河北晨阳工贸集团有限公司 | Aqueous ceramic paint and preparation method thereof and ceramics and preparation method thereof |
CN108456469A (en) * | 2018-01-15 | 2018-08-28 | 河北晨阳工贸集团有限公司 | Agricultural machinery sealing wax and preparation method thereof |
CN108456469B (en) * | 2018-01-15 | 2024-02-09 | 河北晨阳工贸集团有限公司 | Water paint for agricultural machinery and preparation method thereof |
CN108948905A (en) * | 2018-04-03 | 2018-12-07 | 河北晨阳工贸集团有限公司 | A kind of aqueous bicycle special emulsion type Lacquer finish polishes and preparation method thereof |
CN109294410A (en) * | 2018-08-30 | 2019-02-01 | 山东七维新材料有限公司 | A kind of aqueous tape measure baking vanish and preparation method thereof |
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