CN106235389B - A kind of electronic cigarette tobacco tar with the sharp sound function that hawks - Google Patents

A kind of electronic cigarette tobacco tar with the sharp sound function that hawks Download PDF

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CN106235389B
CN106235389B CN201610853882.5A CN201610853882A CN106235389B CN 106235389 B CN106235389 B CN 106235389B CN 201610853882 A CN201610853882 A CN 201610853882A CN 106235389 B CN106235389 B CN 106235389B
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parts
electronic cigarette
tobacco tar
hawks
cigarette tobacco
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CN106235389A (en
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蹇顺华
齐富友
吕品
孙炜炜
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/81Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/19Acanthaceae (Acanthus family)
    • A61K36/195Strobilanthes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/31Brassicaceae or Cruciferae (Mustard family), e.g. broccoli, cabbage or kohlrabi
    • A61K36/315Isatis, e.g. Dyer's woad
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/70Polygonaceae (Buckwheat family), e.g. spineflower or dock
    • A61K36/704Polygonum, e.g. knotweed
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/85Verbenaceae (Verbena family)
    • A61K36/855Clerodendrum, e.g. glorybower
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/87Vitaceae or Ampelidaceae (Vine or Grape family), e.g. wine grapes, muscadine or peppervine
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/899Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Medical Informatics (AREA)
  • Medicinal Chemistry (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

A kind of electronic cigarette tobacco tar with the sharp sound function that hawks that the present invention is provided.It is described it is a kind of there is the sharp sound function that hawks electronic cigarette tobacco tar be by Chinese medicine oleoresin propylene glycol solution and glycerine it is well mixed after stand and obtain, wherein the preparation of the Chinese medicine oil resin propylene glycol solution:20 100 mesh are crushed to after wintercherry fruit or calyx, ardisia japonica, lophatherum gracile, folium isatidis, purslane, Japanese Cayratia Herb, FRUCTUS TERMINALIAE IMMATURUS are mixed, then addition ethanol solution refluxing extraction under the conditions of normal pressure, 60 90 DEG C is concentrated under reduced pressure for 16 hours removes the oleoresin that solvent obtains Traditional Chinese drug mixture;Then dissolved in and stirred in propane diols 0.5 2 hours, obtained after then standing filtering.The electronic cigarette tobacco tar that the present invention is provided is free of tobacco component and flavouring essence for tobacco, small to health hazard, adds the oleoresin constituents of Chinese medicine so that fragrance is more rich when electronic cigarette is aspirated, and mouthfeel is more plentiful, and with the function such as antibacterial, anti-oxidant.

Description

A kind of electronic cigarette tobacco tar with the sharp sound function that hawks
Technical field
The invention belongs to electronic cigarette field, and in particular to have treatment hoarse voice to one kind, improve chronic pharyngitis symptom Electronic cigarette tobacco tar preparation method.
Background technology
In recent years, electronic cigarette rapid popular, consumption in society is hot, and consumption figure is all increasing every year.In the public to strong In the environment of health growing interest, such a " less harmful ", the product of " can help to give up smoking " have undoubtedly complied with social Tobacco Control, smoking cessation The healthy megatrend with pursuit, and the active response in market has been won rapidly.Publicized by the smoking cessation of decades, many smokers Electronic cigarette has been turned to meet psychological need.With the increasing of world control traditional cigarette dynamics, the market scale of electronic cigarette can Can meeting rapid growth.
Current electronic cigarette tobacco tar is mainly tobacco extract and propane diols, glycerine and flavouring essence for tobacco etc. according to a certain ratio Mix, to reach the purpose of the fragrance of simulation traditional cigarette, fragrance and mouthfeel to the full extent, carried due to adding tobacco Thing or flavouring essence for tobacco are taken, therefore there is also a certain degree of harm to health.The electronic cigarette of natural extract is added on the market Tobacco tar, there is also state it is muddy, easily precipitate the problems such as, cause physics and chemistry state labile.Due to electronic cigarette tobacco tar unlike Traditional cigarette equally participates in burning, therefore can add a certain amount of traditional Chinese medicine ingredients wherein, by all kinds of Chinese medicines according to the traditional Chinese medical science " monarch " pure science compatibility, and by nebulae inhalation principle medically, makes it have certain treatment and health care is made With.
The content of the invention
There is the sharp sound effect that hawks it is an object of the invention to provide one kind, treat hoarse voice, improve chronic pharyngitis symptom, And the preparation method of the electronic cigarette tobacco tar without tobacco component, while solving the tobacco tar physics and chemistry shape after natural extract is added The problem of state is unstable, to solve weak point of the prior art.
The present invention is achieved by the following technical solutions:A kind of electronic cigarette tobacco tar with the sharp sound function that hawks, It is characterized in that being prepared from according to following steps:
(1) Traditional Chinese drug mixture is prepared according to the material of following parts by weight:10-30 parts of wintercherry fruit or calyx, 10-30 parts of ardisia japonica, 10-30 parts of lophatherum gracile, 5-15 parts of folium isatidis, 5-15 parts of purslane, 5-15 parts of Japanese Cayratia Herb, 5-15 parts of FRUCTUS TERMINALIAE IMMATURUS;Above-mentioned substance Gross weight number is 100 parts;
(2) Traditional Chinese drug mixture prepared in step (1) is crushed to 20-100 mesh, and be well mixed;
(3) it is 60-95% ethanol solutions in normal pressure, temperature the Chinese medicine mixed-powder in step (2) to be added into 3-10 times of concentration Spend for refluxing extraction 1-6 hours under the conditions of 60-90 DEG C, extract the removing solvent that is concentrated under reduced pressure after terminating and (extract is concentrated under reduced pressure Untill solvent-free distillate) obtain the oleoresin of Traditional Chinese drug mixture;
(4) by the Traditional Chinese drug mixture oleoresin extracted in step (3) according to mass ratio 1:10-100 ratio dissolves in the third two In alcohol, then stirred 0.5-2 hours with 200-2000 revs/min of speed, then 24-48 hours are stood, in being obtained after filtering Medicine oil resin propylene glycol solution;
(5) 40-90 parts of Chinese medicine oleoresin propylene glycol solution is taken, 10-50 parts of glycerine stands 24- after being mixed evenly 48 hours, produce the electronic cigarette tobacco tar with the sharp sound function that hawks.
Electric mixer is used after being mixed in step (5) with quiet after being stirred 0.5-2 hours under 200-2000 revs/min of speed Put.
Using electric mixer stirring in step (4).
The advantage of the invention is that:
1st, the wintercherry fruit or calyx in the present invention has effects that clearing heat and detoxicating, relieving sore-throat resolving sputum, inducing diuresis for treating strangurtia;Ardisia japonica has heat-clearing Resolving sputum, effect of smooth throat to stop cough;It is mute that the eficac Clinical that there is lophatherum gracile clearing heat-fire, relieving restlessness to quench the thirst is commonly used to treatment lung heat sound; Folium isatidis, purslane, Japanese Cayratia Herb have effects that clearing heat and detoxicating cool blood, and clinic is usually used in the hoarseness caused by larynx numbness;It is western blue or green Fruit has effects that clearing heat and promoting fluid, and clinic is usually used in the hoarseness caused by Lung-Yin deficiency.All there is all Chinese medicines treatment sound to neigh It is mute, improve effect of chronic pharyngitis symptom, be clinically usually used in the dry discomfort such as itch for the treatment of hoarseness, bottleneck throat.Each Chinese medicine according to Matched according to the traditional Chinese medical science " monarch " pure science, and by the nebulae inhalation principle of modern medicine, consumer is swallowing clouds and blowing out fog Simultaneously, moreover it is possible to treat hoarseness, chronic pharyngitis symptom is improved.
2nd, electronic cigarette tobacco tar provided by the present invention is free of tobacco component and flavouring essence for tobacco, small to health hazard, but also With good health care and therapeutic action.
3rd, the present invention is directly extracted in the solvent of oleoresin constituents involvement electronic cigarette tobacco tar of Traditional Chinese drug mixture, is solved The problems such as natural extract adds easy muddy easily precipitation common in electronic cigarette, therefore the physics and chemistry state of electronic cigarette tobacco tar is more steady It is fixed.
4th, electronic cigarette tobacco tar provided by the present invention adds the oleoresin constituents of Chinese medicine so that fragrant when electronic cigarette is aspirated Gas is more rich, and mouthfeel is more plentiful, and with the function such as antibacterial, anti-oxidant.
5th, the electronic cigarette tobacco tar preparation method that the present invention is provided is simple, is adapted to industrialization production.
Embodiment:
In order to preferably explain the present invention, below in conjunction with the specific embodiment particular content that the present invention is furture elucidated, but Present disclosure is not limited solely to following examples.
Embodiment 1, a kind of electronic cigarette tobacco tar with the sharp sound function that hawks, it is characterised in that prepared according to following steps Form:
(1) according to mass ratio by 30 parts of wintercherry fruit or calyxs, 20 parts of ardisia japonicas, 20 parts of lophatherum graciles, 10 parts of folium isatidis, 10 parts of dents Amaranth, 5 parts of Japanese Cayratia Herbs, 5 parts of FRUCTUS TERMINALIAE IMMATURUSs are well mixed;
(2) Traditional Chinese drug mixture matched is crushed to 20 mesh, and be well mixed;
(3) Traditional Chinese drug mixture after crushing is taken, 8 times of 75% ethanol solution is added, refluxing extraction 5 is small at a temperature of 65 DEG C When, the removing solvent that is concentrated under reduced pressure after terminating is extracted, the oleoresin of Traditional Chinese drug mixture is obtained;
(4) by the oleoresin of Traditional Chinese drug mixture according to mass ratio 1:10 ratio is incorporated in propane diols, uses electric mixer To be stirred 2 hours under 500 revs/min of speed, stirring stands 24 hours after terminating, and Traditional Chinese drug mixture oleoresin is obtained after filtering Propylene glycol solution.
(5) 60 parts of the propylene glycol solution of Chinese medicine oleoresin is taken, 40 parts of glycerine is stood after being sufficiently mixed with electric mixer 24 hours, produce required electronic cigarette tobacco tar.
Embodiment 2, a kind of electronic cigarette tobacco tar with the sharp sound function that hawks, it is characterised in that prepared according to following steps Form:
(1) according to mass ratio by 20 parts of wintercherry fruit or calyxs, 20 parts of ardisia japonicas, 20 parts of lophatherum graciles, 10 parts of folium isatidis, 10 parts of dents Amaranth, 10 parts of Japanese Cayratia Herbs, 10 parts of FRUCTUS TERMINALIAE IMMATURUSs are well mixed;
(2) Traditional Chinese drug mixture matched is crushed to 100 mesh, and be well mixed;
(3) Traditional Chinese drug mixture after crushing is taken, 5 times of 85% ethanol solution is added, refluxing extraction 4 is small at a temperature of 75 DEG C When, the removing solvent that is concentrated under reduced pressure after terminating is extracted, the oleoresin of Traditional Chinese drug mixture is obtained;
(4) by the oleoresin of Traditional Chinese drug mixture according to mass ratio 7:100 ratio is incorporated in propane diols, uses electric mixer To be stirred 0.5 hour under 2000 revs/min of speed, stirring stands 24 hours after terminating, and Traditional Chinese drug mixture oil tree is obtained after filtering The propylene glycol solution of fat;
(5) 75 parts of the propylene glycol solution of Chinese medicine oleoresin is taken, 25 parts of glycerine is stood after being sufficiently mixed with electric mixer 24 hours, produce required electronic cigarette tobacco tar.
Embodiment 3, a kind of electronic cigarette tobacco tar with the sharp sound function that hawks, it is characterised in that prepared according to following steps Form:
(1) according to mass ratio by 30 parts of lophatherum gracile, 20 parts of wintercherry fruit or calyx, 10 parts of ardisia japonica, 15 parts of folium isatidis, purslane 10 Part, 10 parts of Japanese Cayratia Herb, 5 parts of FRUCTUS TERMINALIAE IMMATURUS are well mixed;
(2) Traditional Chinese drug mixture matched is crushed to 80 mesh, and be well mixed;
(3) Traditional Chinese drug mixture after crushing is taken, 3 times of 95% ethanol solution is added, refluxing extraction 2 is small at a temperature of 85 DEG C When, the removing solvent that is concentrated under reduced pressure after terminating is extracted, the oleoresin of Traditional Chinese drug mixture is obtained;
(4) by the oleoresin of Traditional Chinese drug mixture according to mass ratio 3:100 ratio is incorporated in propane diols, uses electric mixer To be stirred 1 hour under 1000 revs/min of speed, stirring stands 24 hours after terminating, and Traditional Chinese drug mixture oleoresin is obtained after filtering Propylene glycol solution;
(5) 90 parts of the propylene glycol solution of Chinese medicine oleoresin is taken, 10 parts of glycerine is stood after being sufficiently mixed with electric mixer 24 hours, produce required electronic cigarette tobacco tar;
The present invention can also be according to the actual requirement of tobacco tar, further proportioning, the extraction process of adjustment Chinese medical extract, with And Chinese medicine oleoresin propylene glycol solution and glycerine mass fraction proportioning, make prepared electronic cigarette tobacco tar it is thicker, diluter, Cracked effect is treated to become apparent from.

Claims (3)

1. a kind of electronic cigarette tobacco tar with the sharp sound function that hawks, it is characterised in that be prepared from according to following steps:
(1) Traditional Chinese drug mixture is prepared according to the material of following parts by weight:10-30 parts of wintercherry fruit or calyx, 10-30 parts of ardisia japonica, henon bamboo 10-30 parts of leaf, 5-15 parts of folium isatidis, 5-15 parts of purslane, 5-15 parts of Japanese Cayratia Herb, 5-15 parts of FRUCTUS TERMINALIAE IMMATURUS;
(2) Traditional Chinese drug mixture prepared in step (1) is crushed to 20-100 mesh, and be well mixed;
(3) it is that 60-95% ethanol solutions are in normal pressure, temperature the Chinese medicine mixed-powder in step (2) to be added into 3-10 times of concentration Refluxing extraction 1-6 hours under the conditions of 60-90 DEG C, the removing solvent that is concentrated under reduced pressure after terminating is extracted, the oil tree of Traditional Chinese drug mixture is obtained Fat;
(4) by the Traditional Chinese drug mixture oleoresin extracted in step (3) according to mass ratio 1:10-100 ratio is dissolved in propane diols, Then stirred 0.5-2 hours with 200-2000 revs/min of speed, then stand 24-48 hours, Chinese medicine oil tree is obtained after filtering Fat propylene glycol solution;
(5) 40-90 parts of Chinese medicine oleoresin propylene glycol solution is taken, 10-50 parts of glycerine stands 24-48 small after being mixed evenly When, produce the electronic cigarette tobacco tar with the sharp sound function that hawks.
2. a kind of electronic cigarette tobacco tar with the sharp sound function that hawks according to claim 1, it is characterised in that:Step (5) Electric mixer is used after middle mixing to stand after stirring 0.5-2 hours under 200-2000 revs/min of speed.
3. a kind of electronic cigarette tobacco tar with the sharp sound function that hawks according to claim 1, it is characterised in that:Step (4) Middle use electric mixer stirring.
CN201610853882.5A 2016-09-27 2016-09-27 A kind of electronic cigarette tobacco tar with the sharp sound function that hawks Active CN106235389B (en)

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Publication number Priority date Publication date Assignee Title
CN109619656A (en) * 2019-01-18 2019-04-16 薪火高科(深圳)有限公司 It is a kind of to have effects that the tobacco juice for electronic smoke of antiphlogistic antibacterial

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CN102266125B (en) * 2011-07-28 2013-01-09 易侧位 Health care type traditional Chinese medicine electronic cigarette for quitting smoking
CN104605484A (en) * 2015-03-03 2015-05-13 华健 Organic tobacco tar capable of relieving cough and reducing sputum and preparation method for organic tobacco tar
CN105341995A (en) * 2015-10-27 2016-02-24 深圳瀚星翔科技有限公司 Electronic cigarette liquid and preparation method thereof

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